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Analytical Report
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3M Environmental Technology and Safety Services
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Analysis of Perfluorooctanesulfonate in Mallard and Quall Egg Yolk
Exygen Report No. 023-070
Testing Laboratory
-
30E5x8ygReenseRaersceharDcihve
`State College, PA 16801
.
Requester
Wiliam K. Reagen, PhD.
3M Environmental`BPTuiOelcdBhinongoxl23o-33g06y3-a10n9d Safety Services
St.Paul, MN 55133-3331
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REESE Ren, use
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AE 105
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629330
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TTReR A -- SEEma
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`conducted in accordancewiththe analyticalphase protocol given inAttachment E.
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ampleRoe R ER R IER CS R EM i) SYED SEY
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`Twelv makardaggyoksamplesand woio qual69gYo sampieswerorocahedonOBD12.
-
ThesampleswereshippedfrozenondryiceviaFederalExpress(FedEx).The twelvemallard
`SFyououlekrsammaqplulaaerlsdywoaekbrsueacmmpoolmnebsi.anneTddhsaehnsadalhmopmmlooegsmenwaionzreedssoirnateomofnsoez.seaanmnpdflfreoom.uTrmhqoeusoafalmraeekcwu0apmtseudnnodnaaennfdoasrehtsheel
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mpermbiroannassampleswerd io ecoiedonOS01/2.Thesesampaswere notsnayzed 5part
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Raredandana byLOMSNS lckospay.
3.12 PFOSContent inYokFrecions
=
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canigotube.Thosamplewecaniugeda 200000 ga 4 for 24 hours.Thesample
wGaasntshenrs acteon p (HOaPi)nrtoa2st egmeentds: theverylowdensitykpoprotein(VLDL)andthehigh
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Tho HOF was schedin asobion coniaing 045 MMGSO. 1 mM PSF, and 2 uhh
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32 SampleAnalbyyLOsMSiMsS
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PalsERCCTER JR ERAOR E AB
41 Calibration 1aA.n0ai,pi2oc0ia,nts2cenadqlbur5ea0ntncogenicfmourLrP_vReTOwhSa.esTanhsneracuzambeerdnaat1to6nt8h9po0ob1na0gsiwVieonrrsgeu,psrtohrpeoaCrouengcdehno,trraaPntFidoOanStawt1ahes0.e1p,nl0do2ot,fdt0f.ho5e. `oalcorhmpioniantto.nUsi7n)gwrneecaoraorgmriensieodn.wAiChab1rxawteoignhciunge,&heSscooopp, -nterc5ept0.a4n9d0c.osficentof FnorothrearwesduasarnepAorttaedchehrmeeCcn.alratoncreawereme. Thecalbcuvresaartoinocunded
42 `SSuumrorgaotgeastiessarenotacomponentofteanayicalmethod.
43 LaboratoryControlSpikes Loafbotrhaetaonryaceonstro1lscponiteosling1gyaonkasyamapllesst. Lrabooprraotpoarrycodonbyraodldsipnigkeskanroewunscaodncteonatsrsaeosns hMeetchodaaiccsurtrejaeccyat.edT.heFoarborhesrireyscuonstroelpospriekdesnmruo,stshohospwirkeecosvwereireos bwietthwineetnh7oa0c-c1e3p0l%aboire range.
44 MMaattirxisxpiSkepsiwkoerso otinchdedwh 4stc. 45 SOuapmipcalteeinRjeecltiaotnsewdeCreopmemroernmtedsforallsampleanbysas.
5 Data Summary,
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