Document xzRj6BqY4Z4kLx8pdrLGk882m
STL Burlington Colchester, Vermont
Extended Data Package
SDG: 117507
Case Narrative Chain of Custody................................................................................................ Sample Report Summary - Geotechnical......................................................... Supportive Documentation - Geotechnical...................................................... Sample Handling................................................................................................. Last Page of this Document...............................................................................
1 2 8 30 38 42
Case Narrative
i
STLS E V E R N
TRENT
November 30, 2006
Mr. Charlie Young Weston Solutions 1400 Weston Way West Chester, PA 19380
STL Burlington 208 South Park Drive, Suite 1 Colchester, VT 05446
Tel: 802 655 1203 Fax: 802 655 1248 www.stl-inc.com
Re: Laboratory Project No. 26000 Case: 26000: SPG: 117507
Dear Mr. Young:
Enclosed are the analytical results for the samples that were received by STL Burlington on October 18th, 2006. Laboratory identification numbers were assigned, and designated as follows:
Lab ID
Client Sample ID
Sample Date
Sample Matrix
Received: 10/18/06 ETR No: 117507
691397 691398 691399 691400 691401 691402 691403 691404 691405 691405DP 691406 691407 691408 691409 691410 691411 691412 691413 691414 691415 691416
DL3F01IPF0010041021 DL3F01IPF0020041021 DMCF01IPF0010041021 DMCF01IPF0020041021 DMCF01IPW0010041021 DMCF01IPW0020041021 DMCF01MSW0010041021 DMCF01MSW0020041021 DL2F01IPF0010041021 DL2F01IPF0010REP DL2F01IPF0020041021 DL2F01IPF0030041021 DL2F01IPF0040041021 DL2F01IPF0050041021 DL2F01IPW0010041021 DL2F01MSF0010041021 DL2F01MSF0020041021 DL2F01MSF0030041021 DL2F01MSF0040041021
DL1F01IPF0010041021 DL3F01IPF0030041021
10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/22/04 10/22/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04
TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE
Documentation of the condition of the samples at the time of their receipt and any exception to the laboratory's Sample Acceptance Policy is documented in the Sample Handling section of this submittal.
Leaders in Environmental Testing
1.1
Severn Trent Laboratories, Inc.
STL
November 30, 2006 Mr. Charlie Young Page 2 of 2
In order to accommodate field length limitations in processing the data summary forms, the laboratory did, in certain instances, abbreviate the sample identifiers. Dashes have been removed from the client identifiers in this delivery group. The electronically formatted data provides the full sample identifier.
Lipids: No exceptions to the method prescribed quality control criteria were observed during the analyses of the samples in this delivery group.
The analytical results associated with the samples presented in this test report were generated under a quality system that adheres to requirements specified in the NELAC standard. Release of the data in this test report and any associated electronic deliverables is authorized by the Laboratory Director's designee as verified by the following signature.
If there are any questions regarding this submittal, please contact me at 802 655-1203.
Sincerely,
Ron Pentkowski Project Manager
Enclosure
1.2
Chain of Custody
2
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-B032
F: 814-231-1580
3117 Research Drive
' State College, PA 16B01
PAGE _1_ of _4
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari email: i.kesari@westonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
Charles Young
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
Client Sample Identification
DL3 F01 IPF001 0 041021
DL3 F01 IPF002
041021
DMC F01 IPF001
041021
DMC F01 IPF002
041021
DMC F01 IPW001
041021
DMC F01 IPW002
041021
DMC F01 MSW001 041021
DMC F01 MSW002 041021
DL2 F01 IPF001
041021
DL2 F01 IPF002 0 041021
Collection
Date
21-Oct-04 21 -Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 22-Oct-04 22-Oct-04 21-Oct-04 21-Oct-04
Collection
Time
20:30 20:40 20:50 21:00 21:10 21:15 0:20 0:20 21:35 21:40
c o. c
zo oo
Sample
Matrix
Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue
CHAIN OF CUSTODY
Relinquish?*! J?y:
Date 10/22/04
Cooler ID No.: f(cam-
CoolerTem p. ( C):
Time
Received By:
Date Time
12:00
Fed Ex
10/22/04 12:00
-- -------- ,i A lA f i Q, __ Kombi cPiio
Comments
PROJECT REQUIREMENTS C'O Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3117 Research Drive
State College. PA 16801
PAGE 2 of 4
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari email: i.kesariiSwestonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
Charles Young
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
Client Sample Identification
DL2 F01 IPF003
041021
DL2 F01 IPF004
041021
DL2 F01 IPF005
041021
DL2 F01 IPW001
041021
DL2 F01 MSF001
041021
DL2 F01 MSF002
041021
DL2 F01 MSF003
041021
DL2 F01 MSF004
041021
DL1 F01 IPF001
041021
DL3 F01 IPF001
041021
Collection
Date
21 -Oct-04 21 -Oct-04 21-Oct-04 21-Oct-04 21 -Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 21-Oct-04
Collection
Time
21:50 22:00 22:10 22:15 22:25 22:30 22:35 22:40 22:45 22:50
zo
o
o
Sample
Matrix
Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue
CHAIN OF CUSTODY
_Rngut?heBy:
Date 10/22/04
Cooler ID No.: <r//*->i
Time
Received By:
Cooler Temp. (C): Date Time
12:00
Fed Ex
10/22/04 12:00
_--------------------------- -
______ ltfio
Comments
PROJECT REQUIREMENTS 0.0 Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
I
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3117 Research Drive
State College, PA 16801
PAGE 3 of
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Ja! Kesari email: i.kesarl@westonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
m r a t ad :!=<'
Sampler:
Charles Young
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
Client Sample IdentificationT
DL3 F01 IPF002
041021
DL3 F01 IPF003
041021
DBC F01 IPF001
041021
DBC F01 IPF002
041021
DBC F01 IPF003
041021
DBC F01 IPW001
041021
DBC F01 IPW002
041021
DBC F01 IPW003
041021
DOU F01 IPF001
041021
DOU F01 IPF002
041021
Collection
Date
21-Oct-04 21-Oct-04 21-Oct-04 21-Oct-04 2 1 -Oct-04 2 1 -Oct-04 21 -Oct-04 21-Oct-04 21-Oct-04 21-Oct-04
Collection
Time
23:00 23:10 23:25 22:30 23:30 22:35 22:35 22:40 23:00 23:20
CHAIN OF CUSTODY
RelingiilstjJBd&>
Date
3 y?
10/22/04
Cooler ID No.:
f
Time 12:00
Received By:
Fed Ex
__ _
oo ZO
Sample Matrix
Tissue
Tissue
Tissue
Tissue
Tissue
Tissue
Tissue
Tissue
Tissue
Tissue
Cooler Temp. (C)
Date Time 10/22/04 12:00
/ / A / h
\b h' 4 k' >
J X i-
r fiW
Comments
PROJECT REQUIREMENTS
- Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summa^ Add Calibration Summary Add Raw Data Other:
Login
Sample ID L0003679-0001
Container C0048126
Matrix SOLID
Fraction Fish
Samples
Sample DL3-F01-IPF001-0-041021
L0003679-0002
C0048127
SOLID
Fish DL3-F01-IPF002-0-041021
L0003679-0003
C0048128
SOLID
Fish DMC-F01-IPF001-0-041021
L0003679-0004
C0048129
SOLID
Fish DMC-F01 -IPF002-0-041021
L0003679-0005
C0048130
SOLID
Fish DMC-F01-IPW001 -0-041021
L0003679-0006
C0048131
SOLID
Fish DMC-F01-IPW002-0-041021
L0003679-0007
C0048132
SOLID
Fish DMC-F01-MSW001 -0-041021
L0003679-0008
C0048133
SOLID
Fish DMC-F01-MSW002-0-041021
L0003679-0009
C0048134
SOLID
Fish DL2-F01-IPF001-0-041021
L0003679-0010
C0048135
SOLID
Fish DL2-F01-IPF002-0-041021
L0003679-0011
SOLID
C0048136
OOS Investigation #: OOS-04-071
L0003679-0012
C0048137
SOLID
Fish DL2-F01-IPF003-0-041021 Fish DL2-F01-IPF004-0-041021
L0003679-0013
C0048138
SOLID
Fish DL2-F01-IPF005-0-041021
L0003679-0014
C0048139
SOLID
Fish DL2-F01-IPW001-0-41021
L0003679-0015
C0048140
SOLID
Fish DL2-F01-MSF001 -0-041021
L0003679-0016
C0048141
SOLID
Fish DL2-F01-MSF002-0-041021
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Page 3 of 5
6
Date SamDled 10/21/2004
Date Due
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/22/2004
10/25/2004
10/22/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
Instance:
R0291646
R0291646
L0003679-0017
C0048142
SOLID
L0003679-0018
C0048143
SOLID
L0003679-0019
CO048144
SOLID
L0003679-0020
C0048145
SOLID
L0003679-0021
CO048146
SOLID
L0003679-0022
C0048147
SOLID
L0003679-0023
C0048148
SOLID
L0003679-0024
C0048149
SOLID
L0003679-0025
C0048150
SOLID
L0003679-0026
C0048151
SOLID
L0003679-0027
C0048152
SOLID
L0003679-0028
C0048153
SOLID
L0003679-0029
C0048154
SOLID
L0003679-0030
C0048155
SOLID
L0003679-0031
C0048156
SOLID
L0003679-0032
C0048157
SOLID
L0003679-0033
C0048158
SOLID
L0003679-0034 10/17/2006
SOLID
Login
Fish DL2-F01-MSF003-0-041021 Fish DL2-F01-MSF004-0-041021 Fish DL1-F01-IPF001-0-041021 Fish DL3-F01-IPF003-0-041021 Fish DL3-F01-IPF004-0-041021 Fish DL3-F01-IPF005-0-041021 Fish DBC-F01-IPF001-0-041021 Fish DBC-F01-IPF002-0-041021 Fish DBC-F01-IPF003-0-041021 Fish DBC-F01-IPW001-0-041021 Fish DBC-F01 -IPW002-0-041021 Fish DBC-F01-IPW003-0-041021 Fish DOU-F01-IPF001-0-041021 Fish DOU-F01-IPF002-0-041021 Fish DOU-F01-IPF003-0-041021 Fish DOU-F01-IPF004-0-041021 Fish DOU-F01-IPF005-0-041021 Fish DOU-F01-IPW001 -0-041021
Report Version: Oct 12 2006 9:14AM Page 4 of 5
7
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/22/2004
10/25/2004
10/22/2004
10/25/2004
Instance:
R0291646
R0291646
Sample Report Summary - Geotechnical
8
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691397 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
0.5
Qual.
Printed on: 11/20/06 08:01 AM
9
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPF0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691398 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
0.7
Quai.
Printed on: 11/20/06 08:01 AM
10
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCF01IPF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691399 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
2.6
Qual.
Printed on: 11/20/06 08:01 AM
11
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCF01IPF0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691400 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/16/06
% 1 0.1 1.0
Printed on: 11/20/06 08:01 AM
12
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCF01IPW0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691401 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
0.5
Printed on: 11/20/06 08:01 AM
13
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCF01IPW0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691402 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
1.0
Quai.
Printed on: 11/20/06 08:01 AM
14
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCF01MSW0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691403 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Quai.
1 0.1
0.5
Printed on: 11/20/06 08:01 AM
15
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCF01MSW0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691404 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
0.8
Quai.
Printed on: 11/20/06 08:01 AM
16
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691405 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units
0/o/
DF RL
1 0.1
Cone.
5.9
Quai.
Printed on: 11/20/06 08:01 AM
17
GEOTECHNICAL / GENERAL CHEMISTRY
Duplicate Sample Report Summary
Client Sample No. DL2F01IPF0010REP
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691405DP Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llplds Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
Sample Result Cone. Qual.
5.9
Duplicate Sample Result
Cone. Qual.
5.5
RPD*
7
* Control Limit for RPD is + /- 20%, unless otherwise specified.
Printed on: 11/20/06 08:01 AM
18
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPF0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691406 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
1.8
Printed on: 11/20/06 08:01 AM
19
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPF0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691407 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
4.6
Printed on: 11/20/06 08:01 AM
20
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPF0040041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691408 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
1.8
Printed on: 11/20/06 08:01 AM
21
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPF0050041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691409 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
7.8
Qual.
Printed on: 11/20/06 08:01 AM
22
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPW0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691410 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
10.9
Printed on: 11/20/06 08:01 AM
23
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691411 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Quai.
1 0.1
0.4
Printed on: 11/20/06 08:01 AM
24
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSF0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691412 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
0.6
Qual.
Printed on: 11/20/06 08:01 AM
25
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSF0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691413 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
0.5
Qual.
Printed on: 11/20/06 08:01 AM
26
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSF0040041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691414 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
0.5
Printed on: 11/20/06 08:01 AM
27
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691415 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL Cone. Qual.
1 0.1
2.6
Printed on: 11/20/06 08:01 AM
28
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPF0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117507 Lab Sample ID: 691416 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/16/06
Units %
DF RL
1 0.1
Cone.
0.4
Qual.
Printed on: 11/20/06 08:01 AM
29
Supportive Documentation - Geotechnical
30
STLS E V E R N
TRENT
PERCENT LIPIDS
31
Percent Lipids Calculations
Date: Time:
11/16/2006 2330
Analyst: ETR(s):
Client:
JFF 117507 WESTN2
Sample ID
MB111606C 691397 691398 691399 691400 691401 691402 691403 691405 691406 691407 691408 691409 691410 691411 691412 691413 691414 691415 691416
691405DP
Sample Weight
(g ) 10.00 10.03 9.99 10.04 10.00 9.99 10.04 10.04 10.03 10.03 10.03 10.04 10.04 10.04 10.04 10.01 10.02 10.04 10.04 10.03 10.02
Dish ( Dish/Residue
g) 1.0095 1.0678 1.0383 1.0683 1.0667 1.0220 1.0561 1.0185 1.0205 1.0206 1.0017 0.9953 1.0096 1.0076 1.0290 1.0179 1.0272 1.0257 1.0143 1.0203 0.9889
(g ) 1.0089 1.0732 1.0450 1.0943 1.0767 1.0270 1.0658 1.0235 1.0795 1.0391 1.0479 1.0129 1.0880 1.1171 1.0329 1.0238 1.0321 1.0311 1.0404 1.0245 1.0438
Extract Final Volume (mLs)
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
Aliquot Used in Determination
( mLs )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% Lipids
<0.1 0.5 0.7 2.6 1.0 0.5 1.0 0.5 5.9 1.8 4.6 1.8 7.8 10.9 0.4 0.6 0.5 0.5 2.6 0.4 5.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117507MBLK111606C
32
11/17/2006
Percent Lipids Calculations
Date: Time:
11/17/2006 2200
Analyst: ETR(s):
Client:
TPB 117507,117522
WESTN2
Sample ID
MB111706E 691404 691475 691476 691477 691478 691479 691480 691481 691482 691483 691484 691485 691486 691487 691488 691489 691490 691491 691492 691493 691494
691481DP
Sample Weight
(g ) 10.00 3.00 10.02 10.02 10.00 10.04 10.02 10.03 10.04 10.04 10.01 10.03 10.00 10.01 10.03 10.03 10.01 10.02 10.02 9.97 10.01 10.00 10.01
Dish ( Dish/Residue
g) 1.0121 1.0083 0.9996 0.9966 0.9765 1.0164 1.0377 1.0373 1.0452 1.0456 1.0187 1.0432 1.0209 1.0010 1.0106 1.0343
(g ) 1.0118 1.0160 1.0592 1.0454 1.0454 1.1122 1.0788 1.0737 1.0490 1.0640 1.0569 1.0986 1.0239 1.0204 1.0203 1.0480
1.0435 1.0170 0.9804 0.9957 1.0384 1.0332 1.0447
1.0567 1.0206 0.9930 1.0007 1.0501 1.0463 1.0492
Extract Final Volume (mLs)
10 3 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
Aliquot Used in Determination
( mLs )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% Lipids
<0.1 0.8 5.9 4.9 6.9 9.5 4.1 3.6 0.4 1.8 3.8 5.5 0.3 1.9 1.0 1.4 1.3 0.4 1.3 0.5 1.2 1.3 0.4 #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117507117522MB111706E
33
11/20/2006
Percent Lipids Calculations
Date: / i l i C / C 6 Time: 7 . ^ Z c )
Analyst: ETR(s):
Client:
\J lA lf~ ~ '
// 7 $D 7
V
Sample
Extract Final
(Weight Dish
Dish/Residue
Volume
Sample ID ( g )
g)
(g)
ov vn G9l 9>99 0?( m
</<?/
fd .0 0
Ad. O l iO .
Cf C}j
/0 0 9 $ Add 39
/Ob-K ; . d i 3 v / 0 39? A V 3 ^6
/ d&Y3> 0
5
A /)0 0 1 / 0 7<fc7
AOZZ f . b Z 7 d
90 L I d . 0 3 /.0S>G\ A 0 &
b 9 t 0 3 / > .D l AO 9 3 A O Z ^ S '
3 09i s 6 # i 0G
&<fi <rf07
A liA dQ
td-0% t\D2dS~ / , o w s t - t b /. QZOb / 0 -& U
/O -6 l . c o i l A 0 3 1 3 /d .d 3 (? 9 9 *5 A 1 2 1
0 9 / <>9 `/ . 3 / . 0 0 9 b i, A 3 9 0
09 < *9(0 f . 0 3 A 0 6 7 0 / . 1 1 1 1
v C,9( 91) id , o c\ A V9 / O b Z I
09 f </n, tO .O l 1 - 0 / 1 9 A 0 2 1 , 3
&9t y l^ id .0 0 !,0 1 1 V / - G i v i
U9M(<A id).do) / , 0 1 ^ 1 A 0 Z ) 1
0 9 / 9 / < lO.O<1 A d M 3 0 3 0 3
0 9 /3 /0 <0. d 3 A O Z b /. & Z ViT
6>f/0T& iO AoV 0 .9 3 9 9 A o t f i r
----------
----------- ?
-r J A t I f if e --' cFv* H t T1 1
-
(mLs)
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
Aliquot Used in
Determination
(mLs) 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% Lipids
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
v" K>
00
LEPIDCAL_UPLO A D 1
34
ll7r5/86~~,
Percent Lipids Calculations
Date: Time:
11/16/06 2330
Analyst: ETR(s):
Client:
JFF 117507 WESTN2
Sample ID
MB111606C 691397 691398 691399 691400 691401 691402 691403 691405 691406 691407 691408 691409 691410 691411 691412 691413 691414 691415 691416
691405DP
Sample Weight
(g ) 10.00 10.03 9.99 10.04 10.00 9.99 10.04 10.04 10.03 10.03 10.03 10.04 10.04 10.04 10.04 10.01 10.02 10.04 10.04 10.03 10.02
Dish (
g) 1.0095 1.0678 1.0383 1.0683 1.0667 1.0220 1.0561 1.0185 1.0205 1.0206 1.0017 0.9953 1.0096 1.0076 1.0290 1.0179 1.0272 1.0257 1.0143 1.0203 0.9889
Dish/Residue
(g ) 1.0089 1.0732 1.0450 1.0943 1.0767 1.0270 1.0658 1.0235 1.0795 1.0391 1.0479 1.0129 1.0880 1.1171 1.0329 1.0238 1.0321 1.0311 1.0404 1.0245 1.0438
Extract Final Volume (mLs)
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
Aliquot Used in Determination
( mLs )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% Lipids
<0.1 0.5 0.7 2.6 1.0 0.5 1.0 0.5 5.9 1.8 4.6 1.8 7.8 10.9 0.4 0.6 0.5 0.5 2.6 0.4 5.5 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117507MB LK111606C
35
11/17/06
STL BURLINGTON
9Z
4-
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0
O O ,,O L
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Bottle ID
ci t$; d ^ ' S . JS
<i.-i O-
-- < * S ' C nmjV
b o -c ^i c$Weigah 10gam sample into a-250ml wide
^ - ^ C l ' A ^ m n n th Inr
^ r / I
Add 10gm Na2S04
V s v5' ^
X xJ -N io . ^
V\ (# ^vO ^
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i^Add 60mls CH2CL2 U
*;3> Tissuemize 3 min.
_i3 Decant thru a Na2S04 funnel into a K-D set"pup \
^Repeat 2(X)
Cone, extract to 10ml
^ ; FFiilter extract thru a 0.45um filter
''~ 9 iPull 1.0ml for % Lipids. See % Lipids ` Calculations sheet..
H% W ^> z2^ m ^ -<
co m oo CO 7 0 H
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) Bottle ID
-^ P p jiO ^ ^ O o lb o o J O
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Smouthj : ^ ^ a ^
Weigh 10gm sample into a 250ml wide Jar
O O> m >>O Eml HHDm z
m 73 CD m --i
--- -J i *. r(CfP-t og -l
" -I t -j'~ H rJ-"*-. o-n <J f*
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L^.
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r
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^ D e c a n t thru a Na2S04 funnel into a K-D set'3 up
^ R e p e a t 2(X)
c>4W^-
o 3 iConc. extract to 10ml J>-- ^ ................................... ' ^Filter extract thru a 0.45um filter
__ iSjPull 1.0ml for % Lipids. See % Lipids ^ "Calculations sheet.
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Sample Handling
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From: Origin ID: (814)231-8032 MarkAmmeiman EXYGEN RESEARCH 3058 RESEARCH DRIVE
STATE COLLEGE, PA 16801
Fedlsz.
ShipDale: 17OCT06 AdWgl: 36 LB System#: 5675287/INET2500 Account: S****,,,**
Dry Ice: 11 KGS
REF:-
7208 SOUTH PARK DRIVE SUITE 1
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SHIPTO: (802)655-1203
BILL SENDER
KirkYoung .
Severn-Trent Lab-Burlington
208 South Park Drive Suite 1
Delivery Address Bar Code
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C.V;.V{ii'-?'y'
Colchester, VT 05446
PRIORITY OVERNIGHT
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From: Origin ID: (814)231-6032 MarkAmmerman EXYGEN RESEARCH 3056 RESEARCH DRIVE
STATE COLLEGE, PA 16801
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Ship Data: 17OCT06 AdWgl: 31 LB System#: 5675287/INET2500 Account#: S *********
Dry Ice: 11KGS
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REF:
7208 SOUTH PARK DRIVE SUITE 1
cLSMma/ii/2i
SHIPTO: {802)655-1203
BILL SENDER
KirkYoung
Severn-Trent Lab-Burlington
208 South Park*Drive Suite 1
Delivery Address Bar Code
' p' .
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Colchester, VT 05446
PRIORITY OVERNIGHT
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STL BURLINGTON
SAMPL E RECEIPT & LOG IN CHECKLIST
Client: \ S S X / J 3 .
ETR: SDG:
1l 7 b ~7 11-7 S o ~7
Project:
Date Received: / O - f 'i< -C<V>
Log In Date: \ \ / \ / / a &
' Time Received: CjQ rsC l
By: A
Received By:
Ji
Signature:
- L X J ^ d --J
# Coolers Received: 2
PM Signature:
Samples Delivered By: ^Shipping Service a Courier a Hand a Other (specify) [List Air bill Numbers) of Attach a photocopy of the Air Bill
2:_____ X / f h jl L _________
COOLER SCREEN
,
, YES :i NO - vNA -
COMMENTS : \
There is no evidence to indicate tampering
X
Custody seals are present and intact
7v
Custody seal numbers are present
If yes, list custody seal numbers:
`
Thermal Preservation Type: Wet Ice Blue Ice a None pother (specify) Px f a t r ,L
IR Gun ID: ( ,, 2 .
Correction Factor (CF) = C>
"C
i~>
i
Cooler 1: ' 2S.C> "C Cooler 6 ' .
*C Cooler 11
"C Cooler 16
C
Cooler 2: - l U . U C Cooler 7
C Cooler 12
*C Cooler 17
C
Cooler 3:
"C Cooler 8
C Cooler 13
"C Cooler 18
: *C
Cooler 4:
C Cooler 9
C Cooler 14
"C Cooler 19 '
C
Cooler 5
"C Cooler 10
C Cooler 15
"C Cooler 20 .
C
Unless otherwise documented, the recorded temperature readings are adjusted readings to account for the CF of the IR Gun
ERA Criteria: 0-6C, except for air and geo samples which should be at ambient temperature and tissue samples, which may be frozen.
Some clients require thermal preservation criteria of 2-4C or other such criteria. The PM must notify SM when alternate criteria is specified.
iYES: ;Nr? LNA ^ ^ i ^ i e M i ^ N T S S i S S ^
Sample containers were received intact Legible sample labels are affixed to each container C H ftif^ ie u irq ^
.
X
m mX
y e s : >NO |
COC is present and includes the following information for each container: Sample ID / Sample Description Date of Sample Collection Time of Sample Collection Identification of the Sampler ,
X X X X
t
1
Preservation Type
Requested Tests Method(s)
Necessary Signatures
Internal Chain of Custody (ICOC) Required
If yes to above, ICOC Record initiated for every Worksheet
/SAMPLE INTEGRITY U S A B IL IT Y ^ '
i `5 4 T 4 ,4"
The sample container matches the COC
Appropriate sample containers were received for the tests requested
Samples were received within holding time
Sufficient amount of sample is provided for requested analyses
XK
X X
IX <JgYES/i a s s N
ST XX X
VOA vials do not have headspace or a bubble >6mm (1/4" diameter) Appropriate preservatives were used for the tests requested
X
X
pH of inorganic samples checked and is within method specification If no, attach Inorganic Sample pH Adjustment Form
X
AJa
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*
FSM 002:10.26.05:2 S T L B urlington
41
Last Page of this Document
42
