Document x5a6BQVOMBjMkkbQOJm2eNvB0

ITA-LG 00164 lElHllElIirailiil Page Dr- Robert K. Schaffner In Table II I have compered Dr Lewin s results for tremolite wi th amples at FDA (by means of optical those obtained for . pome fche poffizetrheMisanmeerasls, Pigments, aannad mMeetals Divasion microscopy) a-if Fraction). This comparison, which was undertaken (by means - j B S in order tHot a t i v e agreement among the three laboratories. srWhajteovefr -quantitative g _amounts of tremolite found can be quantici;;_ (a) preferred orien understood readily on the basis the packing of the X-Ray diffraction tation Of plates and fibers l u inhomogeneities in sample composition, caused for example sample, and (b) within the container when it Is shaken. by air lutriation I have compared Dr. Uewin's results for chrysotie In Table III, of the same samples by four other la o m tor xes study are Columbia differential thermal analysis) and the Health Stone apparatus for dirterencii ional Health and Welfare of TPir*-ot-eDcr.ti-x-ionTn Branch of the Department The agreement. o.f- _re,,s,,ullt-<s> ffrroTMm ddiiff the Canadian government in Ottawamuch leas satisfactory for chrysotile than that ferent laboracorres ls discussed above for tremolite For samples 89 and 163 were res pectively found by Dr Lewin to contain 5% and 10/Q of these samples by the other laboratories. but chrysotile was .t _ ,, not found: in these sam finding of chrysotile in a sample of Johnson and Also, Johnson Shower to bSnhoowweetr o ^ . b several different techniques which claimed that their own l y s e s ^ nation or these fail to show the presence of hrys otile attributable largely to ur Lewin s inclusion in the term from "chrysotile'':l"ofminera1 species which show significant ^differences eiscal dhrysotile, as discussed in paragraph 3 above. 6. The difficulties iinnvvooilvveead i n apalyzing. talc ^by J^an^y iSnve*sti*gat*ors small amounnttss oorf aassDbeeasLtuos have been pcxnt-e.afofu,,crenuty laboratories disagree surprising that the results u drHereut la lueru- it is not sometimes in the presence of transitional or with tegard to. the two varieties of asbestos logical species of concern here, Moreover ' it is unfortunate that t-he o--ne which is a clear mhala- poses an intrinsically more, dif- tion hasard to man, namely which has not yet fiStltanalyticl problem than the -tha^tremolitei.s dus in part to tine less prominent X-ray diffraction peaks een in the optical microscope. the fibers are often too small to be ' . S T S i? metic talcum powders we r w * test for asbestos which must be b tbe satisrieabasciys cuofe pviOnWf^do_er_rm_sa=t,>ii,1fo*nthaevyaialrabelneot to be considrted adulterate - ^ . following procedure* The aatt pprreesseeunt-,, I1 r--e-c-o-mm-end c o n s i d ebr a tyi_orna^y difffraaccttiioonn,, wwnhriecnh hnaass * sensx- powders shall be-examined . 7 somewhat greater sensitivity tivity Of the order of 17 for chrysotile and ITA-LG 00165 ITA-LG 00166 FINAL REfOST w\ ' '-'^ySr X=HA posras BPPRAtSKO AHALYSSS OF 0MMERG1AE C0SM5TIC fOWEBHS ?hlcgoSample Tale Ohlorite pite' 1 7 0 # 3# 2 nodo 3 99# n de 4 loo# ndo 3 95# 2# #6 80 2# 7 86# 7# 8 95# 2# 9 7# 10 93# 3# 11 90# 2# 12 100# nodo 13 60# n o d , 14 31# 50# 15 1 0 0 # nodo 16 7# ndo 1# nodo 3# 5# 2# 3# 2# 2# 2# nodo t)do m nd nodo n*4o iodo nodo nodo nde 3# no do 2# 2# 4# Udda n* da 10# nodo D o le -We nodo nodo n .d . nodo n.do no do a# Qed t e do no do 2# no do nodo 7# n<,do C a lelte llte n , do n.do nodo ho do n.do no do n .d D ndo no do nodo n.do nodo nodo nodo nodo n .d . Ti. do nad nodo: n.d* nodo n.do n.do nodo nodo nodo nido nodo n ?do nod n.do n.do nodo n.do Hodo nodo ? nod. nodo n.do n do n.do Ho de nodo nod. 17 6o# 30 # 18 90# 4# 19 9 7 # i # 20 3 5 # 5 to# 21 67 # 25# 22 5 9 # 3 5 # 3 42# 50# 24 94# 1# 25 95# 2# 26 9 5 # 1# 27 7 8 # n .d o 20# 1# 4# 2# 2# 1# 2# i# 2# 2# 3# 4# 2# n.do nod. 2# ndo 4# 3# n.do 3# 3# nod. nod n.do Hedo 6# 2# n,,do n.do 3# 5# 3# n .d . n.d n .d . 20# ndo nodo Be do n .d . n.do Had. nodo nod. nod. nodo n .d nod. 10# nod. n .d s Hedo nodo n.dg ndo Hado nado nodo nado Be d e ntdo dado n.do n.d . n.do n 0do n<>do ? n<.do 1 ? n.do nodo 94# ' n.do 30 97# 1 # 31 4 7 # 5 0 # 32 0# 7# 2# 2# 2# 3# nodo Hado 3# 2# 2# n.d 8# 8# n.do n .d . Bp do nodo od, n.d n ,d 0 mda n.d . n.d Be d n.do Ofcher apeales Cahdecyl ZnUndeayI Kaoln Staroh Kaoln; Mica K aoln ITA-LG 00167 -7 if #9 100 50 9 5 # 51 100# 52 53 90^ 54 ca,, 87# 55 80# 56 57 58 9$# 59 60 o a .60# 61 62 63 8 7 # 64 oa< 65 cao78# 66 67 78# 68 80# 69 97# 3o # 40# nodo 4# .Rodo 5# n&do m 4# 3# 15# 7# 15# n. do Q d do 30# 40# 2# 2# 5# 15# 5# 15# 15# 1# Fhiog&= a= Itolo Quarti' miiiag fld0 3# 3# n<>do 5# ndo Xloda 2# 2# 3 # nod. 3# 2$ nodo 3# 5# 5# 3# nodo nodo n.d. 4# Rodo nodo 2# 50 70 nodo od 20 4 # n,do. A o d o n,da ziod. n c da nodo nodo ndo nodo 2# 3# 2 # 20 nodo 2$ 4# Aodo 4# nodo 50 ndo nodo S'e d et" n Qdo 30 n do 4# Rodo 50 nodo liodo .30 Hada Rodo Rodo 70 Rodo 4# 18# Zldo 3# n.do 2# 4 # nodo 30 2 # 30 ndo nodo 4# 30 - 3 # 30 Ad# Qad nodo nodo nada nado 50 50 ndo n,,d ndo nodo nodo ndo nodo nodo 2# nodo nodo Roda 20 Rod nodo ndo Roda Rodo Rod. Aodo nodo Aodo Aodo nado Aodo ' 20 Aodo 10# Hddo Hdn nda toCo Aa<It> Aodo- 20 TreJB= O h r y e e ifcer n ,d e liodo n .d e nd, nd n Qd nodo nodo A* d n.do nodo nodo n.do nodo Aoda nodo nodo Rod. n,do A*do nitd Rodo n.do A do Asdo Hade Rod*. Rdo Aodo Hada Rdo Ro do Rdtf R do 50 Rodo Rodo Rod 20 Rod. Rod. n.do Rodo Rodo nodo Rodo Aodo Aodo Aod. Rod .? Aodo Aodo Aodo . n.do Rodo Rodo Aodo Ra do Ado Ao da Aodo A 20 Aodo Ado n.d Mca ZnO,Kaoln Stmv&h ZAStearo ZnStearu ZnStaro ITA-LG 00168 691-00 DTV1I j[Bs4ga2 bs>T6S "poti op>U fk p pou p*n P't* *p*u Al 0t ppiti pu pop pu pop pop ptl' A 0 A 0% A A A A "pop 0 A "pop opW A Op"U opou 0 A A A 0 A A A* opo A 6 i?0 0 6 o` 0 9 SO' 0 9 IO- 0e 00' Air' 66 faycBa ppu - A* Al .. 0 'm A -, A ; 0 sui 0 ...; 0 x ,- A .A (,pu pu ap 6u pu P"U ptt JT2^gUZ peu Dpu p pu Eq|o =ae^titig pPU Al A A A A pop 0 A A *p*u p *u A opop "pop pop "pop opU P"U A A ap*u pfn A op*p pDii pu p*tr pti pop pop opop cpp opsp Op*p PDTI "pop pp A 0 A pop pop pu pop A pop 8opop "pop "pop A 0 pop $3 pop "pop *Tt ^PI^0 "Shsp.J; $9 0t 0% A 0 05 03 0 3 0% 0Z Al A A 0 A 0 A op"U A 0 PCU Ai 0i 0 0 p p "PU A iec[ "p A A A A A A "pop A 'A A A A "pop p flp*w A A A p 6p A A A "pop ptl A A A A A A A pop A A peu "pop A A "pop p*o A "P "U "poti 0 A A op"U A A A A Dpu *pm p"U A opou optt *pu po "PU A A poti A poti A opou A A' 0 A $9 Al A Afr A A "pop "PXI 0 op"XI Al A Ai A3 A ir"e jC? A? A3 Atr 09 86 16 96 se 0 6 A9 A S &sa AS A9 jSJ9 A A8 A g'eo A6* 8e s %6 06 68 88 8 98 Sfi irS 8 38 8 * " 18 A S " 03 A 3 6L CO 03 06 li 0 1 91 0 1 Si 06 As* A3 A8 A3 U u zi u Ql s^sengr & 4 fJX > ft|0 tB J, ^3@Xtl5 g si paga 4 ?hlg= *= Trm~ Chrya Other i s S ale Ghlar&te isifec Quarts mit C a lslt e i l t e t i l e Speeles 05 92# .06 91# .07 87# .08 8# m 74# 10 99# i i 42# .12 ca60# 3# 3# 5# 10# 15# nodo 40# nodo .13 75# 14 53# 15 53# 16 53# .17 42# 18 53# 19 49# 20 46# 21 87# 2i2 56# 23 51# 24 54# 25 55# 26 75# 27 85# 28 60# 29 97# 30 a,,88# 31 a.92 -32 ; 33 .34 95# 94# 93# 35 93# 36 89# 37 91# .38 85# 3 9 c&o85# 15# 4q# 40# 4o# 35# 40# 40# 40# 8# 35# 4q# 4o# 40# lo# Hado iiodo nodo 7# 3# 3# 2# 3# 2# 4# 4# 7# Zlad'o 1# 1# 2# 2# 3# 1# 2# n.do Hado n*dc ndo iodo n<,do Zlvda lid d Qde 2# xiodo li do Hod.fr ndo 3# n do ad Un nodo 3# 2# 4# 2# 3# 3# npd 3# fiodo 2# 3# 11*do 2# 3# lio do ziodo 4# 3# 3# 3# 3# 15# 3# 6# e# lindo 5# 3# 3# 2# 4# 4# fio do nodo 2# fiode iodo n.d* Soda Rodo 2# 3# 2# 2# 2# s# 6# 3# 3# fio do 15# fio do 7# 4# 4# 4# 4# 4# 5# 4# 3# 4# 4# 3# 3# 8# n Bdo nodo 3# 3# 2# nodo lio d0 2# 2# 2# 2# 3# fie do ndo fiedn n 0do n ado nodo n 9do n edo 10# ndo n,do nod 2# 2# ziad 1# md nodo n.d nodo nodo 2# fiode nodo fioda nod n<>d nodo nodo fiada fiada n 0jdd n ado fiado odi: n edo nd nd0 nda nodo nodo n.d nodo fie do nd nodo ziodo nod ndo nd a n*d0 nod ndo &.o nodo nudo n.do nod fiada n*do rudo trae* trae nodo nodo fiada nodo nde nod0 n.do .. nodo nodo n.d fio d n od 0 t Kaoln nod nod nodo S a lla y lic A,,Borle n 0d 0 nod n 0do nod r nedo fiada ? n ado ? ? ? 5 liada nodo nodo Borle Ael SaCndacyl. Hado trac -x ' fie dq nod0 n<do fie do nodo nodo nodo nodo nado ,40 ea 085# n 0do node 2# 1# fioda fiad* nedo ZiiStearo Mg2 ITA-LG 00170 il Talc 'ChXritfe s i t a 141 30$ HoCto Dodg 142 79$ 143 55$ 144 oa*70$ 7$ 2$ 10$ 5$ had* il do 14$ eao70$ 3$ Hada 146 ea.85$ 147 ca.85$ 140 sa ,4 s$ 149 ea50$ 150 00$ 51 63$ 152 oa70$ 153 eso8o$ 154 cao7Q$ 155 cab84$ 156 79$ 157 63$ I5 78$ 159 Sa 74$ 160 60$ 161 59$ 162 58$ 163 55$ 164 92$ 165 92$ 166 ca .5 0 $ 167 7$ 168 -- L69 -- 170 52$ m 70$ 172 43$ 173 oa99$ 174 ca 60$ Had R-0d 40$ 10$ 2$ 25$ 2$ 2$ 10$ 10$ 10$ 2$ 7$ 10$ 25$ 25$ 25$ 2$ 3$ 5$ 40$ 10$ eoe. 9 do 10$ 50$ Aodc 1$ ha-da ludo Undo n.da nd9 Redo Rodo hdo 4$ Ha da Had* Ilado Roda 2$ nodo ndo Xlodg nod. 2$ Rodo nod Rodo -- nwd nod. nd. Hodo 2$ pag 5 Dolete Tram Chioso Other Quarts mita C alcite e l i t e til Species 2$ ' 4$ 3$ 6$ Hada 4$ Uda Rado 10$ 5$ 2$ nodo Hado 4$ 4$ 6$ 3$ 3$ iUde nodo 2$ 2$ 3$ Roda Rado 2$ Redo -- 5$ 5$ nod nda 15$ 1$ nod 5$ 25$ Rode nod n.do nodo 3$ nod. Rade n .d . 5$ 5$ n.do oda Rodo 10$ "" t 2$ ndo ndo 8$ 12$ Rada 10$ Hoda 5$ 5$ ziodo nodo 5$ Ziodo Hodg n.do n.do 2$ 8$ n 0d. Re do Re da Re de ? Rod ? n.do nodo n.do n ad0 Hi dg n,,do Red-o 2$ nd. 2$ 2$ nd. Ridu 3$ h . d 2$ 18$ n ,d . .6$ 2$ 10$ nod. 4$ 10$ nodo 4$ 10$ nod. 4$ 10$ 5$ 10$ 20$ no da Rodo Aedo 10$ 2$ n.d. nodo 2$ n.d n .d . 8$ nodo n.do 12$ Bada . 2$ ir =<= ca . 80$ 25$ 15$ 5$ nod n,do Rode nod nod. ndo nodo Rqdf Ile dg 2$ nodo Rode nodo t nod. 8$ ^ n .d . ? trace n.do Rodo 10$ * 1$ ? ? Re do rr a. 8$ n^d node 7 n .d . ZnStear, ifeSOj ZnStcar. Kaolin ZnStear K aolin , ZnO ZnStear, Kaolin ZnStear. Kaolin Kaolin ^yrcpbyll it Zn0aB o r ic Acid ZnO Gypsum K aolin , Mica ITA-LG 00171 sus s Ph.lege= fls~ Dol=- Tres= hrys= Ofchar Samle Talc C h lorite o it e Quart m ite C a leite t i l e ' Sttecloa 175 ca 086# 176 ea,a79# m 84# 173 ca50# 179 97# ISO 88# 181 cao70# 182 ca40# 183 ca76# 184 93#. 185 CftoSO# 186 a50# 1ST ea85# 183 70# 189 72# ISO C&0Q2# 191 96# 192 100# 193 ea*93# 194 ea.94# 195 97# 3# 3# 10# 20# lla-CU nd ndo 25# 10# 2# 8# 5# 5# 15# 12# 12# 2# nd. 2# 2# ndo Utoa 2# 4# 2# n.d Q Hado 15# Hd nod {lado Hod. hed 2# nodo 2# a do Hada Dad. Hada Hada 10# 15# 2# 5# 3# node Hada liada riodo 2# Rode n.d 2# 3# 3# Hado U4do nada 2# n^do Rodo Hada nado Roda 4# Rodo 12# iwd nd. 2# nad* Rodo n.da nado 4# 2# 3# 2# nda 2# 3# 3# Hada nada nado Hada nd Rudo 10# lindo lo# Rodo 25# 25# 5# 5# 5# n.d nada Roda hada 3# nada ndo Roda nd,, Rada Ra4* Rade Rada Rad 1# 3# Rada nada 2# 1# i# Rad* Rodo Rada Rad nd^ Rs do ? ? Rodo ? Rodo Rodo nado -i 7 Rad, Rodo 7 Rad 7 nado 7 Roda Roda 7 7 Rodo Kaolin Kaolin Zn Zn Zn ZnStear, ITA-LG 00172 New York U niversity Department of Chemistry 4 Washington Place, Room 410 New York, N .Y . 10003 Telephone: (212) 598-3427 1TT^/-iTrMTTVfr TO TABLE I Memorandum to Dr' George Thomps on . S5d ana Etile.Administration Fr" n: Cheralstw^Department, New York University , betemination or Asbestos Contents or b e r c i a i a 4 . will -- to the P O - - o f - " i f T..W 10 1973 With respect to the tactoxs on this date of July fu, - talc the status in the detection and est3^ ^ t h e ^ l y s e s of commercially availof the tabulation of s u i t s of the affiuys aWe has been engaged^in nflLing r w ^ r in T b ir T ir " --- ^ problass: - A, Tabulate x .ray diffraction data for talc and all . . added in the course of r" . r . - r -- r" --- locations and relative _n of ehrysotile. ^ planes responsible for phy of the e ec X. diffraction peaks to the crystal and interpretation, in terms of crystallogr, ^ d e n t a t i o n , and sample preparation, chemical properties of ehrysotile, C' ^ T l o r i t e ! tremolite, and tale; specifically, measurement ,,- n arid ion replacement reactions, or the rates of Z th ^ electron, of ehrysotile and of D Microscopy, both optical ____ r minerals, including ehrysotile talcs containing various accessory and tremolite. enrichment, due to air elutria- tion'f = t t t i g h t L t fractions of the dust * - -- ITA-LG 00173 a2 Development of a method based on the combination of *-ray F. diffraction, chemical reactivity, and microscopy for of the chrysttile and tremolite contenta of c o n c u r product^ (theae two being the only asbestiform minerals encountered In all the products examined so far, with only one and application of the method to the analysis o a oil store-purchased specimens. O. Investigation of alternative analytical methods, vis-,, dir erential thermal analysis and density gradient centmtugation, as alternative or supportive techniques- Our results to date support the following conclusions: 1 The chrysotile that is found in commercial talcs is generally, different In significant respects from the dbqmrttt. massive fibrous growths in veins in serpentine rochs. Tht is, the r men has diffraction peaks that may differ from the latter by as umic as 0 2 A (at 7.3 a ); it is more reactive toward dilute acids, it Shows a different appearance under the miorosoopej and its O T e n j > therms and exotherm are shifted relative to those of the laoter (an " tlyTM S : f ; f chrysotile as a minor restituent in talc may be established with reasonable certainty on the basis of ( a ) ^ e presence of x-ray diffraction peaks in the vicinity !nd 3 59 to 3 .6 5 A, fb> pronopneed weakening or complete disappea unce o f these peaks upon t r e a t m e n t - a p e s ^ m a ^ e n t . of the specimen tth 1 M HC1 at 80C for 1 hour, (c) the presence of fiber bundles visible size under 250X or higher magnification In the optical micro- ^e h s" a refractive index of about 1.5* (these fiber bundles short and straight, and may be coated with a h u ^ y encrustation of M-cto or may he embedded in talc or other particles), and (d) the V ' o f fibers under the e l e c t r o microscope which yield an electror diffraction pattern that corresponds in d-values to those oun in ^ x-ra^diffraction pattern (these fibers typically do not have a hollow ~ nit r s S i T r ; * * - - , be peak * ^ ITA-LG 00174 - 3- is calcium oxalate mon.ohydra.te (peak, at 5*83 A ) The quantitative results are conditioned by the fact that segregation effects in talc powders are considerable; the analytical method gives a reproducibility of 2 to 3 $ average deviation in replicate determinations on the same sample, but different samples from the same bulk container are found to vary by as: much as 200$. 5. The quantitative results are further complicated by the fact^f that antigorite gives an x-ray pattern, that is indistinguishable from that of chrysotile. The HG1 treatment specified above does hot affect: ground antigorite, but it is not yet known whether antigorite, if it occurs in talc, has the same chemical reactivity as the ground material from massive antigorite, or whether (like chrysotile) its properties may be variable depending upon the rock matrix in wlilefc it is found. 6. Subject to the qualifications inherent in the above, we have obtained quantitative estimates of the chrysotile contents of about 200 commercial talcum powder specimens. We have also de termine a the contents of the other minerals in these products, including tremolite, quartz, chlorite, dolomite, and others. There is no ambiguity in the identification of these latter species, ht.th quantitative results for these are also affected by the segregation problem, which is most serious for those constituents present in the smallest amounts. 7. Most: of the commercial talcs tested are free of any detectable amount if any of the asbestiform minerals, according to the criteria enumerated above. Thus, there appears to be an adequate supply of talc for which there is no ambiguity about the absence of chrysotile or tremolite. In about 10$ of the samples tested, there appear to be definitely detectable amounts of either chrysotile or tremolite present. ITA-LG 00175 = ITA-LG 00176 ITA-LG 00177 SAMPLE NO. 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 N-Y. t n t - HAY DIFFRACTION) n. d. n>d. XL.d. n.d. XL.d. n. d. n. d. n. d. n.d. n. d. n.d. n.d. IU d. n, d. 57. n. d. n.d. n. d. 2% n.d. n. d. n. d. 3% n. d. n.d. n. d. RESULTS______ ' FDA copttcal microscopy) PFIZER fX-RAY DIFFRACTION) n. d. tu d. n-d n. d, n.d ITA-LG 00178 ITA-LG 00179 iS liil ITA-LG 00180 SAMPLE TO. 127 128 129 130 131 132 133 134 135 136 137 ,138 139 140 141 142 143 144 145 146 147 148 149 '150 151 152 a. d, n.d. n.d. trace trace n. d. n.d. tud. n.d. fi.d. n.d. a. d . n.d. a. d. n.d. a. d. 57, 57 a. d. n.d. n.d. 27. 87. a. d. a. d. n.d- small amount present n.d. ITA-LG 00181 (S i ITA-LG 00182 ITA-LG 00183 f-Z 1 2 n. d. 3 ru d . 4 ti.d. 5 a. d. 6 tu . 77 8 n.d. 9 n. d. 10 n. d. 11 n.d. 12 a. d. 13 n. d. 14 n.d. 15 n. d. 16 17 n.d. 18 n.d. 19 n.d. 20 n.d. 21 n. d. 22 n.d. S ITA-LG 00184 ITA-LG 00185 ITA-LG 00186 ITA-LG 00187 n, d. possible, in talc grains much , antigorite? n. d. n. d. n- d. ITA-LG 00188 AMPLE NO, 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 .145 146 147 148 RAY DIFF n. d. Trace tu d. a. a. i,d. n. d. a. d. n. di a,d. n.d. n. d. n. d. a. d. n. d. 10% 1 2% n. d. n. d. n. d- FDA (OPT MICE. RESULTS PFIZER' & RAY DIFF n. d. COLUMBIA SCIENTIFIC HPBC ITA-LG 00189 ITA-LG 00190 ITA-LG 00191 F'C 2 TABLE 17 KEY TO SAMPLE NUMBERS OF COSMETIC TALCUM-TYPE POWDERS AMPLE HO. PRODUCT NAME 1 Ammens Powder, Medicated 2 Anolin Deodorant Powder 3. Aquamarine Cooling Spray Bath Powder 4 Bagatelle Amber Dusting Powder 5 Bourjois Bath Powder 6 caldesene Medicated Powder 7 Cashmere Bouquet Body Powder S Chanel No. 5 Bath Powder 9 Countess Rocheau Cate Dus ting powder 10 Crepe Die Chine Disting Powder, Millot 11 Crepe De Chine Poudre Mist, Millot 12 Cuticura Talcum Powder 13 Des enex 14 Desitin Bahy Powder 15 Desitin Baby Powder 16 Diaparene Baby Powder 17 Dorothy Gray "Secret Of The Sea" Dusting Powder 18 Bmeraude Talcum Powder 19 English Leather 20 Faberge "Music" Dusting- Powder 21 Friendship Garden Dusting Powder 22 Friendship Garden Dusting Powder 23 Friendship Garden Dusting Powder- FURTHER IDENTIFICATION Bristol-Myers (No. F25) Norwich Revlon (143) Corand (DCH) Pennwa.lt (5274) Colgate-Palmolive Jergens \ V\ \ Douse of Fragrance (L1132) . House of Fragrance Purex (07170) N T S -Pharmacraft Pfjeer (1139Z) (3/29/72) Pfizer (115A) (5/10/72) Breon (E1030) s Coty (355-4010) Mem (2891) Shulton (3/27/72) Shulton (5/9/72) Shulton (7/13/72) ITA-LG 00192 PLF PRODUCT SAME 0. 4 Haven Sent Aerosol Bath Powder Mist 5 Heaven Sent Bath Powder FURTHER IDENTIFICATION Rubinstein Rubinstein !6 Helen Prssi ''Little Lady" 7 Importa, Spain Mens'1 Talc 28 Isis Floral Talcum Powder 29 Johnson's Baby Powder 30 Johnson and Johnson Medicated Powder (028Q) (3612) 31 Koscot Beauty Dust-- Oil of Mink 32 Lanvin Arpege Dusting Powder (1288) 33 Lanvin Arpege Powdered Mist 34 Lanvin Arpege Talc 35 Lewis Baby Powder 36 Loves Fresh Lemon Glossy Powder Manley & James 37 Mcy'S Scented Borated Talcum 38 Many's. Talcum, Apple 39 Marcelle Dusting Powder, Hypo-Allergenic 40 Mary Chess Perfumed Dusting Powder 41 Mermen Baby Magic Powder 42 Mermen Quinsana Poot Powder (11202) Merck Talc, Product Ho- 6460, Lot Kp, 6460) 43 (8039301) 44 Mexsana 2387-D Medicated Powder Plough Shulton 45 Old Spice Body Talcum 46 Persian Lilac Deluxe Dusting Powder April Showers (LFN) April Showers (B200B) 47 Persian Lilac Spray Bath Powder (115B) Pond's Perfumed Talc Body Deodorant Dream Flower 48 Prince Matchabelli Beloved Spray Powder 49 ITA-LG 00193 cipLE STO- PRODUCT NAHE Quest odorant Powder Replique Spray Bath Powder Riviana Foods Italran S t e a r m Talc September Morn By Pond Seven Winds After Bath Tal Talc Vaseline Intens Lve Care Baby powder Laurent Rive Gauche Spray Tal Baby Powder Zeasorb Super Absorbent Medicated Powder Ambush Dana Dusting Powder April Showers Avon Unforgettable Perfumed Talc Beloved perfumed Dusting Powder Prince Matchabelli Coty Face Powder Rachel Desert Flower Spray Bath Powder Emeraude Dusting Powder Emeraude Spray Dusting Powder Faberge Flambeau Deodorant Spray Powder Jean Nate Spray Bath- Powder 70 J e n s Talc Flesh Jolie Madame Dustin Powder Balmain Lady Es ther Face Powder Rachel Max Factor Face Powder Rachelle Medicated Comfort powder OH de London Talc FURTHER IPECTlFICATKjR Parfums (004) For Rice (19B) DuBarry (021085) (I 209) (F121) Stiefel (9884) Shu1ton (F 1 BKI) Coty Coty (1 ARY) (37 WBF) (1 N 247) ITA-LG 00194 MrLE NO P RODUCT NAME To Know Me Is To Love Me - Tinkerbell Touch And Glow Face Powder, Creamy Peach Toujours Moi Bath Powder Tardley April Violets Chantilly Dusting Powder Cashmere Bouquet Jean Nte Talc Kennen Shave Talc Shower To Shower Body Powder Pure Baby Powder, Dart Drug Pond's Dream Flower perfumed Talc Almay Hypo-Allergenic Face Powder Constance Carroll, Bouquet Talc Djer-Kiss Talcum Flamingo Dusting Powder, Tussy T.antipr Lilacs And Roses Talc Mavis Talcum Mavis Body Powder 94 Tangee ZBT Baby Powder Blanchard's Dusting Powder B o m Wild Dusting Powder Lander Gardenia And Sweet Pea Talc Lander Lilacs And Roses Deodorant Body Talc 100 Miss Dior Dusting Powder Tai Winds Spray Talc prmTWFT; IDENTIFICATION lom Fields, Ltd Revlon Corday (4908) Houhigant (ILF) (on 345) (B 81) Johnson Johnson (5507BG) (K 11C) (0 13 D) Kerkoff (L1047) Vivaudou Vivaudou Luft-Tangee (B0Q48) Del Labs (Avon (DCC 1272 2-14-72, ITA-LG 00195 111 Old Spice Body Talc 112 Dr. Scholl's Foot Powder 113 Faberge Xanadu Luxury Bath Powder Spray 114 Faberge Zizanie de Fragonard .115 Fab ergo. Tigress, Bath Powder 116 paberge VJoodhue for Men 117 Faberge Brut for Men Shower Buff All-Over Body Powder 118 119 120 121 122 123 124 Faberge:Talc Faberge Aphrodesia Bath Powder Faberge Straw Hat Bath Powder Faberge Aphrodesia for Men Shower Buff Faberge Xanadu de Luxe Bath Powder Faberge Woodhue Bath Powder Faberge Music Dusting Powder FURTHER i d e n t i f i c a t i o n (lJJ) (01A) (1M) (IDE) (2D0) (241) Lanvin - Charles of the Sitz (2137) Lanvin - Charles of the Ritz (2103) Saulton, Inc. (MFO) (20517) au (2132) Ref. 61159-019 Ref. 2052-003 Ref. 5027 (0252) Ref. 5400 (raw material: from France) Ref. 2052 (2172) Ref. 5027 Ref. 1244-028 (2342) Ref. 2052-002 Ref- 0714-018 (3121) ITA-LG 00196 IMPLE MO126 127 128 129 130 131 132 133 134 135 135 137 138 139 140 141 142 143 PRODUCT mame VtTRTBER TTNTIFICATION Mannen Baby Magie Walgreen's Crib Age Caldasene Medicated Powder Desiten Vaseline Intensive Care Johnson and Johnson Medicated Powder Johnson Baby Powder Johnson's Baby Powder Johnson's Baby Powder Johnson and Johnson Medicated Powder Johnson and Johnson Shower to Shower Body Powder Johnson and Johnson Shower to Shower Body Powder Johnson and Johnson Shower to Shower Body Powder Avon Brocade Spray Avon Bird of Paradise Spray Avon Tax Minds Spray Talc Mennen Bath Talc Pin-Zow (108T) (109T) (0452K) (C 5122) (0709X1) (0872K) (31602) (B1652) (4065) (A308) Perfection Beauty Products, Inc., Pearl River, N.Y- 144 145 146 147 148 149 150 Overton's "Sigh-Brown" Pace Powder Softee Face Powder Westport Pace Powder Hazel.Bishop Pressed Powder Lady Wayne Face Powder Solitaire Cake Makeup Breamglo Pressed Powder ITA-LG 00197 ITA-LG 00198 AMPLE MO. 175 176 177 178 179 180 PRODUCT SAKS Lander Baby Powder Lander Lilac & Roses Body Talc Beloved Perfamed Dusting Powder Jean Natd' Talc No. 60 jean Natd' Spray Bath Powder Tinkerbell Body Talc 181 182 183 184 185 186 187 188 189 :190 191 192 193 194 195 Yardley Sigh Shadow Brush-On Eye Shadow Max Factor Face Powder, Rachelle Tweed Bath Powder, Leatherie Yardley Next to Nature Sheer Pressed Powder Yardley April Violets Dusting Powder Yardley Red Roses Dusting Powder Yardley Springflowers Talc Yardley White Lavender Talc Yardley Red Roses Talc April Showers Deodorant Talc Chantilly Houhigant Dusting Powder Tinkerbell testing Powder Tinkerbell Powder Mitt Tinkerbell Dusting Powder Tinkerbell Body Talc v m m ra n IDENTIFICATION Prince Matchabel (235A) (2264) (2101) (Tm Fields, Ltd., d v . of m e m ) Ref. No. 721 (Supplied by Mfgr.) (Yardley)(44) (A2) (162) (165) (260) (271) (21A) Ref. No. 9882 (2JBB) (Tom Fields, Ltd. ) (Tom Fields, Ltd.) (Tom Fields, Ltd.) (Tom Fields, Ltd.) ITA-LG 00199