Document x1ZmOEYO2Kyjm608QwKEg4QxE
* SVV.
:*W=SSf 2
*'v' 1 DATE, PRINTED: D*V* 363, 315, 3! 7, ^32 "2J, ^2^)
3/61/82
Cu 40
CODE RT-539-D PKG
JJil.2_8.-ig-. .
G2H26
(.DATE )
(LOT NUMBER)
PROCESSES ( )RT-539-D (N)
APPROVED BY JJG 3/18/81 EWK 12/2/81
TYPED BY:JMM JOB= 40RT539DMN
EQUIP HENT
sEMI-BLEEDIHG
NAME: NAPHTHANIL RED DARK
USE ! N-CQDE | ACCT
LBS I
I LBS
NOTE: N24C (4NITR0-2 AMINOANISGLE HYDRO- !
CHLORIDE) IS AN EXPERIMENTAL CARCINOGEN* i
ALTHOUGH MONITORING VERIFIES WE ARE WELL !
BELOW THE RECOMMENDED EXPOSURE LEVEL, IT IS)
ESSENTIAL THAT YOU ADHERE STRICTLY TO THE ]
SAFETY RULES WHEN HANDLING N24C* THIS IN- 1
CLUDES RUBBER-GLOVES, LONG SLEEVES, SAFETY i
MASSES, RESPIRATOR AND WASH UP AFTERWARDS*i
SEE YOUR SUPERVISOR IF YOU'HAVE QUESTIONS* |
,OBTAIN 4-NITR0-2-AMIN0ANIS0LE HYDROCHLORIDE I
'STEP 6
\
"AIN METANITRQANILIDE OF B-HYDROXY
\
NAPHTHOIC ACID FOR STEP 31*
.4-
CLEAN, DRESS, CLOSE 24" CLARIF""PRESS
T
15 FRAMES
''
i
l
24-C,D 151 -C
T" (398 G> WATER INTO V-_.,, JS3zS=s> IN HYDROCHLORIC ACID FROM V-324
' M___/____ DUMP IN FROM
4-NITRO-2AMINOANISOLE HXDROCHLGRIDE
I
:
28-D [ 66
MIN TO WET LOT_______
(71OG) AT 28`-32 DEG- F
16X330 I 57-A i JAM 9
SODIUM NITRIJE: in 4-d^Mji* M__
Ul z J
1 725-A 1
69
ST5R 5 MIN 6 RECORD: i
, + > K
( -h ) i
t
1
NOTE: <i) 3F CR--, KI- ADD> 20* "AS IS' IN- 1
4
i
3RIC iCID ASSUME 32%
11 28-D 1_____
RECORD : CR______ ( + ) KI _____ ( +) <2) IF CR+,KI~, ADD 1.6* * AS IS' INCREMENTS
JUS 301982!I
SODIUM NITRITE ASSUME 33%
I 725-A i
RECORD: CR(4) KX( + >
II
2 DEG F MAINTAINING +CR 1 i
RECORD TIME START_____
i ... 1
SLURRY IN 40 GAL WATER IN DRUM & T'RECOAT YCLARIF PRESS WITH .
! 777-A i !I
nniMnu iiu i r\wu i -- UHl) DM i un ,UIU
EQUIP' 1 -i ' KENT i [ RAGE 2 OF 3 CG 4* CODE RT-539-D <N>
' 4 \lSl RECORD" PH/_*aL(6.S-7.5>
CONT. i [
ACETIC ACID
1 | ADJ- TO PH 6.5-7.5 RECORD
T [ >
SODIUM HYDROXIDE
& IF NECESSARY
ASSUME 70% PHj&ifi^.
ASSUME.50%
. 1 USE i LBS
i
1 1 1
1 N-CODE 1 ACCT 1 1 LBS
1 as* 1 1 30-D | JU 11 I 7-D I ""X
DV MZ-H^IJHEN.Sli STIR COMPLETE, TEST jDV & RECORD: 1
I
1
5
1 t CR.._4n<+) KI_jb_._( + ) TEMP __Jj___ 28-32*F 1 -- I
57-A | --
j tOTE: <15 IF CR-, KI -, ADD 2* "AS IS" J.NCRE-1
1
i
1 [ "MENTS
HYDROCHLORIC ACID
ASSUME 32% 1
I ' 28-D i
I t RECORD; CR
< + ) KI.............. ('+)
11
1
I | (2) IF CR+, KI-, ADD 104 "AS IS' INCREMENTS! i , !
SODIUM NITRITE I (RECORD' cR,,_4rrrn
ASSUME 33%
i 725-A
!
1 \#T\ WEIGH SULFAMIC i IM&SH INTO DV
ACID
ifl
RUBBER .
BUCKET"-ANDN \
i I 395-D
I IJi-rSTIR -5 MIN & RECORD: KI_,,2LL_(-'>
Li___ I
| 2>*&ir~ NECESSARY, ADJ TO -KX & RECORD
i 395-D
ver-^mr in a c t iv a t e d c a r b o n
V i 25 I i13-B
b ic a u ;t e f il t e r AID IN & STIR 15 MINA [ 10 i 777-A
i -JL
! 25 [ 16
ON AGITATOR ADD ICE, THEN OFF AGITATOR
i 2X33 1
-57-A ! As p
DV THRU CLARIF PRESS INTO DV USED IN MAINTAINING, TEW* AT 28-32*F. RECORD:
lf I^
I START,,_1__I1 ,,TOTAL MIN _,,J_
I-Ml wWhHeEN S23 CLAR*Fa8MPfc-TE, WASH DV <S4) . i LINES, PUMPTPRESS FOR 20 MIN OR TO A
i
1
i
I -CR TEST ON A SMfL OF TOTAL PRESS EFFLUENT,!
I
i WHICHEVER~CC?Mg^iRSTr''CaLLECT WASHINGS INI
..... 1
(523)
1. I
STIR 5 MIN &' RECORD: TEMP,,J?V_.< 28-32 F)
1
!
IF NECESSARY ADJ TO 28-32 DEG F AND
i____ .__! 57-A I.
RECORD
.. ______ DEG F
II
RECORD: wrJtkL" AND HOLD'FOR S45
I' !
INSTALL V-^fTEMP CHART h SET AGITATOR AT i
6 RPM RUN IN 20" <i938G) WATER
i I
3*5
)2^TnjHA- 23' (457 G) WATER INTO
I %'
IN 20G WATER AND POUR IN TRISULPHOIL]
I **><?CAP D
[13
|3fT 1 DUMP- IN META NITROANILIDE OF B-HYDROXY
|
I j NAPHTHOIC ACID FROM S2 I AND STIR 40 MIN. TO WET
I FOR S38.
LOT I ,, ___ 7A&-L_____l__TM_
\j j t ,,
I
I
39-A 151-C
i
!
i i
\
! I
13 3G8
MI SC 8
IJBrl WEIGH SODIUM HYBiMMgP' BU&GIE 6 HOLD
1i TaJr i
FOR S35
,`
" ASSUME 50%
WEIGH ACETIC ACI%IN RlBBERLINED DRUM .AND
r ^MOLD FOR S39
_____ ,
f NOTE: (1)1)0 NOT PROCEED WITH BATCH <S'S 35 ) THRU 50) UNTIL S26 CLARIFICATION COMPLETE i (2) WHEN S26 COMPLETE PROCEED WITH BALANCE i OF'BATCH WITH NO DELAYS TO PREVENT N-151-C I SOL'N HYDROLYSIS RESULTING IN BLUE TINE.
I (3) StjPV.R WILL PROVIDE RELIEF IF NECESSAR Yi
156 |
a0\j !]
*m~ i i i
7-D 1 78
30-D i 58 essm [ ~SSk
!
DUP050463616
EQUIP MEN't
PAGE 3 OF 3 CG 40 CODE RT-539-D <N>
USE LBS
IJjT \a WHEN S26 COMPLETE, POUR IN N-7-D FROM S32 I
? 3><^HEAT TO 155-162*F AFAP RECORD: MIN_JT___ i
f$r\ STIR 5 MIN TO DISSOLVE FOR S38. RECW^D:
i
SOLUTION COLOR
DARK BROUN)
i CLARITY__iVLAeL______ (MUST BE CLEAR) .
1 |
i | NOTE-: IF SOLUTION NOT DARK BROWN & CLEAR, I
I i HEAT TO 185-192F AFAP AND RECORD:
1
1 1 COLOR_________________(DARK BROWN)'
-i
1 I CLARITY(MUST BE CLEAR) .j-------,-------------------------------------------------------- -g.--------------------------------
1 i-
M -13^1 WHEN S37 COMPLETE WITH V-#$? AGITATOR OFF, |
1 ! J> IMMEDIATELY RUN N-330 INTO V-26 AFAP
J`
J^r I IMMEDIATELY TURN ON V-26 AGITATOR 6 SIPHON|
! L> IN N-30-D FROM S33 IN 5-8 MIN *
!
ISTIR 5 MIN ONLY & RECORD PH_|J_iC-( 11.0-12.0)1
f4i ( IF NECESSARY, ADJ TO PH 11.0-12.
I
f|
SODIUM HYDROXIDE ASSUME 5% 1_
! L.RECORD &?C______ ACETIC ACID ASSUME 7% |..
\J^n RUN IN V-5Q2 OR V-314.1TR0H Si A'
I
iJ^T HEAT TO 148-152*F IN 15-2 MIN AND RECORD: I
! > HT 1X0 *P AND REC_iJC?LF
f
WHEN S44 COMPLETE, IMMEDIATELY `COUPLE DV 1
7 I UNDERSURFACE IN 65-7 MIN. MAINTAIN CV AT [
I U148-152*F. RECORD STARTjCiffifTOTAL MIN_<fcfe_l
[4>n STIR 5 MIN 6 RECORD: DIAZO V|+,,<- OR + ) |
- ' " >SE_Tfcl__MUST BE + PH__jA.<4.5-5.0)
!
*r 1 STIR 15 MIN & DISCQNNEXJLTRANS-FER LIN&^WP T
SV RECORD: START
*
!
1 WHEN S47 STIR COMPLETE, TEST CV AND .I
"I ' I RECORD: DIAZO__!TIL__MUST BE
` ' I
i i BASE_^.,,_(MUST BE +) FOR BOTH HEALTH AND J
[ ! SAFETY REASONS, IF RT-539-D FINISHES WITH AI
I [ + DIAZO, WHEN IT DRIED, IT CAN PRESENT A
1
I j THREAT OF FIRE OR EXPLOSION ON GRINDING IN !
I i FINISHING AREA. SEE YOUR SUPERVISOR IF
I
[ | THERE ARE ANY QUESTIONS.
1
i49 1 IF S48 DIAZO IS + AND BASE IS ALSO + SIFT i
1 j IN 20$ N-3-A, SODIUM CARBONATE, 6 STIR TO !
I | - DIAZO. WATCH FOAM.
I.
1 I RECORD: DIAZOMUST BE -
I
I .i
BASE__MUST .BE +
1
||
PH(4.8-5.2)
I
I I,TOTAL MIN SINCE S43________________________
15^1 FLOOD TO 32" (8126 G) AND STOP AGITATOR
i
I | VAT ' I [S4 (398G) i . jS8 (?1G) II.
ii
V-303 16" 29"
V-315 12" 21"
V-317 .V-322 12* 12* 21" 21"
3%- m-
V-3231 12*I 21*I I
i
I I --JfeZMZ
1
I!
oa&L&ye^ |
: 1 M
W
W
K
/ 1 r
2/26/82 N-CODE | ACCT
LBS
7-D 30-D
- %*
3-A 1
DUP050463617
N32567.01
DUP05046361 8
