Document wqzv04aonRDgyLjQMqrwM7yzo

Ethanolamines/Glycol Ethers Tier 3 Procedure Section Number: Issue Number: Original Date: Revision Date: Title: References: 616 1.3 12-17-91 Author: 12-29-95 Percent Water Determination Of T-230 Bottoms Glossary Of Equipment Identification (Text #114) 616. Percent Water Determination Of T-230 Bottoms 1.0 Objective: 1.1 To provide instruction for the measurement of water in a sample from the distillation column t-230. 2.0 Procedure: 2.1 Draw up 0.1 cc of sample using a I.Occ disposable plastic syringe. 2.2 Put this sample on the analytical balance. 2.3 Tare or zero the scale by pressing the red bar at the bottom of the display panel. 2.4 Press the start button on the amines water instrument to begin drying the solution. 2.5 When the solution is dry (red light comes on), zero the karl fisher counter. 2.6 Inject the sample, press start to begin titration. 2.7 Put the syringe back on the scale to get the weight of the sample. 2.8 When the titration is complete (red light comes on), calculate the percent water as follows: 2.8.1 % water = ml karl fisher x factor posted on the board/weight. 3.0 Revisions: Revision No. 1 07-20-93 Yearly Review Revision No. 2 12-21-94 Yearly Review Revision No. 3 12-29-95 Yearly Review Daate Printed: April 18, 1998 Page 1 Of 1 Paper Copies Of This Document Are Uncontrolled & Not Subject To Update. The Controlled Document Resides In File: T230h20.doc DO A 060044 CONFIDENTIAL