Document wqgEkVzLQq1kq9Q9r31kVGze6

TToo:: DDaallee LL.. BBaaccoonn!EETT--EETT&&SS//3MAM/UUSS ccRcci::chardJJEaa.mmePessurDDd..yEJJooThh-nnEssoTon&n!SEE/TT3--EMET/T&U&SSS/3AMM/UUSS RTIicMhaAr.d EK.OPEuNrIdGy[/EATL-LEITN&1S/U3SM26!U66S30] @ HOSTMAIL TRIOMGEAR. GKOPEENRIKGI[NASL[LV1MNO11..UUSS21616263380]8]@@HOHSOTSMTMAAILIL RSSuuObbjGejecEtc:tR: G HHPFEFEER--K77I11N00S00 [HHVyyMddrr0ool1lyy.sUsiiSss 1SS1tt2uu3dd8yy8] @ HOSTMAIL oDsallee,, hIItitaamllkkteehddatttioon RRtohogegeeMrraPPeyrekr1ki5inndssatfthhtiissthmmaotorrRnniicinhn,gg aJaibbmoo.uuttattnhhdee| HHruuenntvtiiinngegdwdooennwdeh,hyydodrbrooslleyyrssivissedssttmuudadyynyoonnerHHrFoFrEEs--7a71n10d000de((fTTi--c66i33e33n4c4)i.)e.s|I ttooldd ranging him that ranging from the approach selected and is in the May 15 draft that Rich, Jim, from the approach selected and its execution, 1 the reporting and interpretation of results. and I reviewed, we observed many errors and deficiencies execution, to the reporting and interpretation of results. RDRioovgigeseirrossnaaciidodnhhceeerwwnoso.uullddHesseejnnuddsmmreeecaaeiccvooeppdyythooiffsHHrueunpnlotirinntggrddeocoennn''tsslyJJ.uullyyS22o55mereeppsopoorrtt iicnnhwwehchikiccshhdHHoununenttidinngguddoonnrohuhiaarddpnhrreoesgnsppeoonnddeedd ttoo `cDcoiovnnivvseeiorrnssaatctiiooonnnc,,essrhnhoso.wweeHddetthjhuaastttthhrieisscenniveeewwdrreethppioosrrttreddprraoafrfttt srsetticlllehhnaatlssy.ssiiSggnnoiimffiicecaansntpt oeertrrrcoorhrsse..cks done during our phone WKWioitethhniJJgiimmfoarannSddCRRDiiccrhhe'v'ssiehhwee.llpp,,Th|Iewwni,lilll wppuiutthctogDgeitevhithesreornwrwaiprtiptttreeonvnalcc,oommwmmeeenwnitltslssooennnttdhiiossurJJuuclloyym22m55enrrteepspo,orrtttaharnnoddugssehennRddogiiet rfto,o TTbiiammck to Huntingdon and Koenig for SCD Huntingdon and ask them to tosolve the manyproblemswith this study. review. Then, with Division approval, we will send our comments, ask them to resolve the many problems with this study. through Roger, back to To EiEricEric A ReinerET-ETSSIMUS FTDFraroooc: mm::: 0ED9D/rAAi1cNN2A/AA9. 6SRSCC0eiH8Hn3NeN1OrO/BEABRTRMI-EICCTHH&I[ASAL/3LLMLII!NNUI1S.UUSS223399995511]] @ Hostal @Hostmail Date: 09/12/96 08:31 AM SSuubbiiceectt: FFlloouurroocchheemmiiccaall WWaasstteess oCCnuutrrthreeenndtlilsyypyoysooauulaaarenediinnhttahhneedlppirrnoogccoeesfsss looffporpuererppaoarrciinnhggeaamwddiarracasfftattslpp.rrooccYeeeddsuutrreeerday oiidnninsapthommseeaeedleotitsiifpnnfogglsao~wlwi'irttahhoncdCChoeohmttatianacggdaeellinGGwgraroosovvifeesf.lSSoMuMDruDDorciphpneegomeptilchoeeawlwpce~eowvulwaerssreteeeerseo. fddYiitssheccisusutssessriidnnaggy dmnpeeiseerperfotioisnnuaggrlitotshhfoeefbyyluoiriunnyrddloiiecccnhaaeetteemmddaicttyhhaaalbttweaaatfscetellese.vovaaDttaeesuddrr1teiendmmgepmceptohremerapatactouuoseruiesrtsls.i,eoonfptrhoidsuct. and that they material s considered perflouroisobublene may be formed and that they material is considered extremely oxic. as a decomposition extremely toxic. product, EcEerrriitcca,,iInT'lmmy snnoeotetmsssuurrteehiafityfytoohuiusaarwroefufaladrmibileliaawrriwtwihtiihtnhttthhheiissssicsuospeue,e,obbfututhiteitt issues chearttaiynoluy-wsoeuelmdsadthdartosthias w.opualdrboefwthiethidnistphoesaslcpoopleicoyf the issues thai you would address as a part of the disposal policy. cJcO: HN PITTLhhNooEmYma[asAGsGLL. IAANssIhheenUnmSm2aa1c4hce8hr0e/7Er)T/-@EETT-H&EoSsT/m3RaISVi/lfMfUUSS MJWMOAAAHRYRNDNDIPEIIJJLANANCECEOUOYBMBS[AAESNNEL|NNLUII[SNUAS1LSP.SLUOPI1S0.N21U1L.SU4U28SS40228745]98325@118111H]])o@@st@mHHaHooioslssttmtmaaaliil l W W W"iDAliAlllYViiaENammTEKEKNR..EMRRUOeeNaMagTgeAIneNUfnESNETS[T-APE-OLTELL&UTINSSR/O1S3.DMAUTMS!SUU272SS39]281@] @ Hostmail HOSTMALL DAVE TERMONT[USSP01.US0975731 @ HOSTMAIL Exhibit 1467 MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppePecacttliiomonenraavnn.dd3CCMo,oppyNyoii.nnggC2aa.ss0CC4o-on6nf3ifid0de9enntitiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000011 I3MMAAO011441100773333 Robert D. HowclVET-ETESSMUS Robert D. HowelFET-ET&S/3MAJS TToor: rEiricc AA. RReeiinneerr/FETT-EETT&ASS/3MMU/USS FDFarrtooemm::: 0DD9AA/NN13AA96SSCC1HH0:NN4O1OBABRRMIICCHH|[AALLLLIINNI1.UUSS223399995511]] @ @ HOSTMAIL HOSTMAIL Date: 09/13/96 10:41 AIM SSuubbjejecct:t: RRee:: FFolouuroroschhenenmiiccaall WWaasstteess EErriicc,, IrLommtiidssecacolom0mmmumununicicahctaewdtimtemhydythcceoonenmccieesrrnsiiionnnsmmydyumrmieenmmgoot htteoo iyynoocuu.i.neMrMaytyicocnoonnoccfeerrnn did did fnfoloooiutucrdrcooeoccahhlmmmpsiooiccumaanllus,dc,shaadsswuiiritttihddniitdgdhewwmiaeittnmhhuifttshahsceeiotffunoorsrrimmdnangatrtiaiiononngndototfhfhePPeiFrFnIIcpBBirneooesrrreaonottctihhoeeenirrt owfaste tmdmoaexatsetisecrirricapalotlsmso..npsoM Musoonussdctshoodfaofusour"uirfnrlgwwoawmarssotatseenhuessfnttarnrecieactaumamlripnperrgroofaftiinll"edesstohhhanaevvtierhegeppgerreneonsefeerinralacleleaint dwaste dnbpeoeotstihchnriicninplggtuidleoelsnsd.se.isnuIItcffhthethhdaeeesrrse"claalrroreeiuprttoootcxxiihioccseonmmmaitatchteaaertlriiiwaanlleessrtcppsarr"neessoweenenntatthrttehhteephyyreonnfceileeeddattnood baaacpepcppiorrnroocdpplirurniidgaaelttydee protective equipment in the description so protective equipment andthat and inform we can inform ovisde partis wear the outside parties accordingly. Ie'mctnmioonttgssuluarrset itwfhetehiiksscissoamannmeisnssstue.ed. tOOhnntetehooeffytthhheeaeennndglgieinnemeeaernrssyiinnRooouuurrrochemical wmwwaaaesssetttteeissndgaaessslciaifrsftithtphwteeiyeyoenkhhsaaccddoehmrhiaimggnhhelcnyctooedndoncntehtcnaltrreeatfhtlnieeocynttshohraoifnfsacdcalatreHrccmieiinnatooonhggyeneennfnsslso..urTTohhceheemical wmi`nmaedesinntvtteiiioddonuneaeeslddcrissinpooctmmiuoeernwwsloaocbrre.kkrtaooTinnnhliPPysFIdIaDBogantti'hthnaartaet fphhlpeaaecddat rbbteheedieesnn.toddHopooennteetnhbbteyyinaaalRRyuusbssseiiaann iccTnaaadssneeidvoioifrdfsual.aabblooTirnhraaeottroureryrymlaiianbnyfsfo.ohrrmaTmvahaettiisibooeannegnnnaooinnttobbtaeehpiiipnnnegggarccneoodnntvvthoeeeyypceeooddtme0tnmoteittanhhle.elyawbsOaeisrtcaee more hing foryou 0consdier. handlers. There may have thing for you to consdier. been nothing in the comment. One more 3M Internal Comespondence. 3M Internal Correspondence TDTooA.:VE SPPCAAHTTULSSZHHEEEILLHLLPEEDRREI[SHHKPPDDUEESSSOKK01.UU3SS5O0]332266H99o11s]]t@@maiHHloossitmmaaiill DRMRAAAARYYVDEDDIAASVJCVIAHISCSU[O[HHLBPSZPDEEDENIEHS|SKUPK.SD.USUESPSSUOK0717.1.1U1U1S3S805230]41153@5a516HH11]oo@ss@ttmHaaHoliosltsmuamiil l MARDI JACOBSEN[USSP01.US248511] @ Hostmail cc: SSeeee BBoellooww FDFarrtooemm::: DD10AA/NN18AA96SSCC02HH:NN5O3OBPBRMRIICCHH|IAALLLLIINNI1.UUSS2233999955111] @ @ Hostal Hostmail Date: 10/18/96 02:53 PM Subect: Flourochemical Waste Disposal Update Subject: Flourochemical Waste Disposal Update TfTlhhoiiussrwwoeseheeekkmiaacmamleeewettiiinsngge wwdaiassspheoelslidd fptocoravecavtialslauestatewehppirrcoohggrraeerssebss eooinnnccghhcaaannuggseeessdiinbny bfttahlhoceeukaargoddrocoophputetinimoodnnicioaonflfftowthhraeemsatRRteiCCdoRRnisAAfpooSStsuauhblbeppparacrarotctptCCyicCCeissrrtuwuflseho.si.clhlPPoarrrwooevvebibidyddeaeeipnddrgbboeecgllaroouewwssesiid.ss by background iufommtion for the copy list followed by a progress MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000022 I3MMAAO011441100773344 rreeppoorrtt oonn ppaasstt aaccttiioonn ies items. BACKGROUND. B ACKGROUND UUunsnddteeprrroSSvuubibpdpaearrtvtaCCpoCCr., TTcSiSDsDiffoaacnciillciitotineetssrwwolhhsiicci hhh sesitaabbViilOliizCzeecwwoanascstteeensstriiantttiaaonnnkksss exncmesal dpro0v0ideppvma.poFraecimliistsiieosnwhciocnhlrdools nioftIhceurVreOntClycohnacveenvlraaploiorns eeelxmmeiciasesiesnodioni5nm0cpc0olonepnimptrremoonllt.ssacFctaaiannocniccliooptnilnetatsiinnnwbuuyeheitt(coh0heeedxexoclceeenpcpotttit5>vce50u0rd0r0aenepptpploymmf htwwahaveasestievssaipfffohtrheeyy frDuioelllec(ee(aDDmnebecicemeermpmbolbefemer1r9e696n.7,t.a11t99i9o96n6).)p. laAAnllllbyffaatcchiielliitetiefefssemcmtuiusvstet be in compliance date of the be in compliance by by December of 1997. Ta"Tnhhdee ESSuPubbAppaahrrattsCChCCdrrotuloleeissshhsuaaevveesebbveeereeannlvveiixggtooerrnoosuuissollnyysccwoohnnittleeessttceeeddrtbbayyiniinniddsuusssutterrsyy awnerdeEbPeAinhgans ehagd oto.issue several extensions while certain issues were being negotiated. MLMoaosnsttdoofetfdthheea1fftlluhvoeorrLooaccihhederlmmaiiwcc/aalUlSssPoolCliiIdd LaaonnnddelliiMqquuoiinddwiwansat,steessOkrarleeahnnooowmwabbefeiainncggi.li lTSTa1hhn5eed0f/cciodolslrsetutdnra.aanntggtAehebsesofLfurrtaooimdomnlaS$ew11h33/U00a-S-2o2P8fl8C0t/I/fhddLerruouwmnmaeswwMtiitohihuttnhhhateaeziaaanrvv,deeoOrruaaksggl.eaebhbeHoeiamiznnaaggrfaaadcrrooiouliuusbnnTdd. waw$a1nas5sdtt0lee/.mdmruuusmLstto.bbneeeAMssbotaoauubbtinilloitzniieezdneh(ddiaonilacfnasotafanntnhokke)h) wappvrareiisoovtrera1tipos0ophprlalaazeccameerimdmsoeseunintsot.niincHnottanhhzteeraorldsous laaDanenncdddedfdmioobllcee.ssr,Lnnooo1tn9eii9nn7Mtt.eenonFdudonoortnnahiiniinnsssdttoraaeellsallisinnnogogntvvthaahapepvyooerrweviemlamilpsionssrsoiieoolmnnoiccsoosnnintobtrgnreoolclebobblnyryetrotlos accspt 500ppm on the lfctive December, 1997. For this reason accept >500 ppm on the effective datethey date ofthe rl. will no longer of the rule. be able to IcInenrMtMiafayiyc.,a1t1i99o9n966tLhLaotonniee MMwoaousuntmetasaitinnreaaassmkkseeddwe33rMeMuDDneeccceaarttuu$rr00ttoopppormro.ovvidiBedaaseaed cocorenngrtoaoinuufiirrccakkstniwnoownooltwehdablgtueeeioptdosfrlfewtgsthheaeednsette.pprrsoobtscrueeetassmvssewwsrieewfiddeciriadedtiunnonontdteeeesxrxtpp5iee0ncc0gtt pthuhpasamittn.vvgooBMllaeaatttsiiellheedod o2M255rg0Du,a,nowwicaarssswoccooouncnlddduhucbactetmseepddeirbbeysycterQQnauatu,amanlbsntute.terrvTrreaaroiLLfoiaacbfbasstihoooennntDDteehcestceaiantstguu,rir'susrsttihchnrrgaweeeeeMmhhresaaetzzhaaorrdddoouuss fahalbbiuoosovvrleeoicm50hi0t0e0mgpepinpcpeam.rl.awteTTadshhteeethuusetnnfreeeoxxalpmpleeosccw.titeenTddgwflaacoutiliourofrneetoheoeffmtttshhhr:eeesseeesssttrtrereaeamammssswt1o0ermmeeeeett this limit generated the following action items: (1) (1) IIMndceiemnnietfrifaiitcciaaotini.oonnooff AtermatveDisposal Alternative Disposal Sites Sites including including Incineration. @(2)) coAAnntaemlnytasiisnoyocffossnseeylliueecnctctseetddonflloowuuirtroohccahhenemmeivicacalalulawwtaiasostnteeossffoMorertVVhOOodCC 25D by the Enmironmental Lab. content in conjunction with by the Environmental Lab. an evaluation of Method 25D ((33)) MMMoeuetnthhioaodid,2255D aannaallyyssiissoofsfesleelecctteedd wwaassttee ssttreraemasmaasit LLaonnee Mountain. 4) (4) aM fMfocontniitotoonrr NEEoPPuAArio/ncindhudesumtsitecryaylnndeeiggseoptotsiiaatltii.oonnss to to determing determine ultimate ultimate affcct on flourochcmical disposal. (5) Desclopmment ofa Nowrochnnical disposal policy (5) Development of a flourochendcal disposal policy. Ie1t0emsme((59i) iistasahesseemppoaasrrtaattaeeppbbruuottprrreeillaaattteeedddisisspsuouesealwwhmheeertreehiionnd.wweeic.wwiilll aatttteemmpptt tiiionsncbcsiapinseneecerdiarftyoaiontthniieotosnmrcllhoaaesnntmddifaficpilalpllliirnnocggph.,arriffaaooctrreteecdraaiiccssthhpiocflsslooa,ulurrmooccehthheeommdii,ccaia.lel.sitraeamm wwhhiicchh is based on its chemical characteristics. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000033 I3MMAAO011441100773355 CCUURRRREENNTTSSTTAATTUUSS. )(1) AAlltteerrnmaattiivvee DDiissppoossaall SStiteess TTShuhrbrpeeaeertssiiltCeessCwwceoernrteeroiilddsee:nntliEiffQiieUeddetIthrhaaot!tww)i,illllCahhaevvmee-MIhheeet(rreDeqeq~tufioirriee)dd, and LSCLW huWbeDDpma-(r(MtKKeeCetnnCtfhuucaccovkkneyyt))rp..orTlosTov:oinEndQeAAd(Dssqheehutnroomeitta)nc,ahmCetohraferrimaeecprpo-oooMhrnurttneeiesdtdd(teDht$hea8ratt0rtoaEEitnQ)Qd, aaa$nnn2ddd00 ppCterehrarnedsdmrprouu-rMmmta,,ettirroeehnssa.ppveeecctTtiphivvreeoelvylEy.id.QeTTdnhhuqeemulbolaaettattrtteeiriorsnnnasuubmmoobufbteaerrr0ioniu%ncnclodluufd$de8ehs0seand $200 rectcraduarurntrcseeepnntotdrccitoaovttsi.itso,inoiir.nroodnTniiihcscepaaollEls.yaQ,lhtchneoetsmtnslssbeebeoyroffiusttphhaiib0ssolfu$~ata2cc25ili50iD,l%r00ccoo0ofunptllhedder yNsrceeoadalrur.u.cmeeTTsdooim1vm0iswdwiieoiltlnlledbbrmeeisipiinnonecwcsllahuuleddctiionhnsggetstrthhbweyenpuoocpnnathnhoaanz$zaa2err2gdd5aoo,0uut0sse0wwaapaslestorteever ovovEoevQrleubarmalyllleDcscoeotsosctt..deemWWtebeeremcc,riaannme1ee9wxx9pph.eeeccttht et1or0bwbeee shipoupriwasntegs fo can negotiate a lower shipping our wastes to EQ by December 6, 1996. @) EnvironmentalLaband Loan Mountain Analysis (2) Environmental Lab and Loan Mountain Analysis "TMTehhteehaaonndaally2ys5siiDssoomffstthhteeoEEfntnvhvieirrofolnnommuerenontctahalelnLLiaacbbalhhawasascsciooennsffisirrimrmseeaddmstt.hhaatt cwM cohoneinttcthaahoiinndrvve2oo5lalDaabttioimllveeeoSoosr0trggo0aafnnptiiphccemmm.falaottTueehrrroeiaicylahsaleaarmstteiccccoooannnlctcweiennantustrrtiaeantstgiiosohtnnresseraems awapnrnheaasillceyynhssti.iassreanLnodadbno:aavrreeMe oii5ddu0ee0nnntttpiifapfymyiiinn.ngg'Thtshhe)eeyss2ppa5eerDcceiiffaciinoccanlootyirrmsggiaafsnniniaiccgsssthbeereen Spstiiermlesnitsliielananrgr.t.. Dave Lone Dave Clifton wil instruc LM to discontinue Mountain's(LM) 25D analysis has been Clifton will instruct LM to discontinue testing. ) (3) EEPPAAI/Inndduussrtryy NNeeggootitiaattiioonnss OOSunnbeepannreetwwCitCteemmistathhaa"tctohhnaasstsbibteeuceenntaadsdpddeeceiddfittooc ctthohreerelaacttteeissottnv"eerwrshsiiioocnnhooff pSruobvpiadretsCorCth is a d"lciomnisntaittuieonntosrpceocnifciecnctorarrteicotnioand"juwshtmicehnt of non-regulated VOC's. provides for the elimination of non-regulated VOC's. or concentration adjustment 4) Flourochemical Disposal Policy (4) Flourochemical Disposal Policy pEEorrliiicccyR.ReeEiinnneecrr wiissilwwloorbrkekipinnrggovwwiiidttihhnDDgaaivvstees TToeefrsrmpmeoocnnittf i0toc develop develop his this cdpchuhoerleimimcinyicg.caatlElhsserioocErrcnwhcvhieilremlmoibnceimcaepalnrlssotvagglirrdLooiauunbppg'sssltithshataansttaolwwfyiissllilplsebb.ceeiGfttuiaacirrgdgeaettneecdde wil bbsdeeeufnrfcioonargltrhltcyhtoeamhEgirnnecvgeiodoroonntdmnhimdatsiisseppononostmasaglalolLofoaffbst'spshpeeaecncilfiaofiliayccrssisctstcr.reehaaGemmmusisi..adlaIInttwcwwaesaawtsseisll generally agreed that some of the flourochemical wastes ithnatthaerfsutcuurrer,ently being landfled will be incinerated that are currently being landfilled will be incinerated in the future. AeAvnneaalddokdpiimtiieoonnntaallofaaccattiimooonnriietedeemfintthihtaaittvehaassubboerenoncahadeddneiedcattloo coNuuarrslliissttt iirssahthnee dlsgitees.ntv.eerlW Wiocpeem0bbeeanlilitleoovewfeattuhmhsaaotormmeiaandnnkeyyfoitnohfifetittavhhpeeeprfWWlouSpSorPPrioappctrrheooefdfmiiillseiepcssoasaalarswleiamslsteitlltelhst0ootrdeawmith the waste. generic to the waste. | wilallow I will beatempiing 0do tis in my new capacity us to link the appropriate disposal method with be attempting to do this in my new capacity. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppePecacttliiomonenraavnn.dd3CCMo,oppyNyoii.nnggC2aa.ss0CC4o-on6nf3ifid0de9enntitiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000044 I3MMAAO011441100773366 PHILIP WIREVRPDESK.US2ISS7S] @ Hosnail cJJTOcOS:EEELLTTHHLEEEPRRH[UUAILNMLTULP[SUISWNSPISIORPLU0ESU1Y0.SU9[OH7S930P999D619E]15S58@8K)]UH@@oSs2tHH1mo8oas5sitt7lnm8aa]iill@ Hostmail ITTBIlRhlSoEoEmNmTaTTasGLsGBE.Y. [SAAATssLhRkLeOaInNMnm[1aa.AccUhLhSeLe0rI/9rEN7ET3IT-9E-6UT]SE&2T@0SR1/IS35IMo2S0sMFt]mUtJ@SaSil Hosmail BDJDORAAHERRNNYYTLLHUBHHNYUUTGSGEGTRGERIETOATTMLTIL[[AAAILNLLLILLIIINNNULS11UO..USIUG?SS612219416184]580206@06]]]H@@@ostHHHmooaosisstlttmmmaaaiiilll JTTCOaAamHMnNrIiaLHaSL..USYSNAaoTarEBresRRs/Y[EEAATTLN-ELTEITITNA&&1LS.SUL/A3ISMM0N1I/UU6S6US1S63]21@66H3]ost@maHilostal DJJCOOOAUHHMGNNILLPPALIILYLSNNAEJEBOYY[HR[AANYLSLALOLNININNTII[A1A.LUULLSSLI22IN11NL4418U8.0S0U77OS]]I39@@21066HF64oo3s]s]tmma@HiaiolHlsotsmtmaialil DRDROAOOVNNUIGKKDLEEACIICLSCIHHJFOLLTEEHORRNNI[ISHIAOPPLNDDL[EEIASNSLKLKLU.UIUSNSS201057.79U999S33%1012717]]9]0@ @a64]HHHoo@osssttHntmaaoailsilltmail DKWKEAEANNVYINGGDRERACANNLNETIFTIUT[AMAOLALLNNLIN[AININLLA1ULL.USILNISI910N.79UL73US3SS251512)9]299@@8228H]H1oo@)ssttmH@aaolislHtmosatimlail W JEJIInMAMcYGGANEERESSeEENn[[cEAArULL/MLLEITAIN-NN1EI.NUT[&SUASS22L2M26L68I8UN44441S]].U@@S2HH2oo9ss2tt8mma1ai]ill@ Hostmail EJarimcesA.D.ReJionhenr/sEoTn-EETT-&EST/3&MS!SUMSUS James D. JohnsoIffET-ET&S/3M/US 33MM IInntteerrnnaall CCoorrrreessppoonnddeennccee TTDooA:VE TESSccRooMttttOBN.TSISUtIrSanESdPT/OEELTU-TESTRI&DSTSAS/37MM3U]/USS@ HOSTMALL DRoAbeVrEt DT.EHRoMweOlNlTE[TU-SESTP0&1S.USSM0U9S7573] @ HOSTMAIL Robert D. HowelFET-ET&S/3M/US cDcA: NA M.JJaamSmeCseHDDsN..OJBJooRhhInnCssooHnn[!EAELTTL--EIETNT&1&SUS/3S/M 2M3/9UU9SS51] @ HOSTMAIL DANA M. SCHNOBRICH[ALLIN1.US239951] @ HOSTMAIL FFDraroocmm::: EE1rr0iicc25AA.9.R6Reie1ni1ne:er2r5/EEATTM--EETT&&SS/3MMU!USS Date: 10/25/96 11:25 AM SSuubbljeetc:t: MMoorree1Iddeeaass oonn DDrraafft FFuluoorrooschheemmiiccaall W Waassttee DDiissppoossaall GGuuiiddaannccee. Scott, Dave, Robert, Scott, Dave, Robert, Tu"Tohhreefofocolhloleowmwiiincnagglaawrraeesisseoosmm.ee 1aaddwddoiiuttliioodnnaaalplpririessckifafatccettooyrorssurnnooittdemmaesennottniioownnheeeddthiinnermmwyyepprsreehvvoiiuooduu,ss ommreehmmooow aawbbeoonuctocduiidss,ppoocssaallluccdreiiteercisaeffoorfractors in ffMallcuuutoooorrrrooosccchhhheeeammmtiiicaccaaaflll cwwwaaamsssttoeeevsdd.eiimssIeppwonostsoaaulollfdggufuaiuipddrpaaornncecccheeieaccmtreriiicttyeeaoriliauas.r. iidnCCeataannhssyyoeoonuuwwattshhteienhtshkeooiorfrfwoonofettthhhkseehreroirurilisddkke,gfforacractdhtooaorrtwssiowwwneeepssrchhooooduuuullcdlddt, siccnooicnnnslsiuiidddaeeeirrr,t,ho<eer1.sg.ge.r,foauooctntthohdereusrra in te . factors that affect movement of fluorochemicals in these wastes or of their degradation products into air or groundwater. 11.. PPrrooppeennssiittyyooffwwaassttee ttoo ffoorrmm dduusst.t. TThhiiss ccoouullddbbeeaaddddrreesssesdebbdyy pprreettrreeaattmmeenntt 1to aagggglloommeerraattee dduussttyy mmataetreiraialsls.. 2. Sizeofthe Muorochemical molecules. 2. Size of the fluorochemical molecules. 3. Suscepubitey 10 andratesof hydrolysis. or ther degradation mechanisms. This is particulaly reevant for fSM3l.uguonoSrirofuoccscchaheenepntmtmicbiicoiclanialctlsye.nttththoraatatatnaairrdoeenrs1tao0looe0fslaamonrofggrheee1yt0dmoborobbeileyleosto,isxx,imicooroorrer tmmhbeiooorbblidoligeeigcniranaldlssoyaoialli.ilc.otniCCvmooeuuMellciddhoarfTlnlouoicosohmrreoosmcc.hiheceTaamnhliiisccs"aaillsss pinnatrtthhiceeuwwlaaarslsytterddeeleeggvrraaanddteeft0oor ffoorrmm: significant concentrations of more mobile, more biologically active fluorochemicals? 44p.e. rsMMiosoddeienssobolffoobidcioaascscuummulualattiioonn ootthheer tthhaan ppaarrtiitiioonniinngg iinntoo fafatty ttiissssuueess,, .&.e.g., tthhoosse ccaauussiinngg fflluuocrroocshheemmiiccaall ssuurrffaaccttaanntt t(o0 persist in blood. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000055 I3MMAAO011441100773377 5o5..vDDeeelflafacyyteesdd.ttooxxSiicociitmtyye.. MuSShohororortcthtteeerrrmmniattoolxxiiiccniisttyyctssitctuiudddieeiss smmhaaoyyw nnsootct hsshhdoowwlttooaxicicititotyxyicwwihthyeenn sslloowwllyy ffoorrmmeedd mmeettaabboolliicc pprroodduuccttss ccaauussee toxic effects. Some fluorochemical insecticides show such delayed toxicity. 6s6.i.teSSssuuosslcceupebtpiiltbiibizlieliiotttyyhtteoorwssooillsuuebbiiillniizszaoalttiiuoobnnlebbyyuootrthohecerhremmmaatietcerariilaalslss?.. CCoouulldd ssaallttssoorraohtherr oorrggaanniiccss,, 5e.g. ssuurrffaaccttaannttss,, iin llaanndd ddiissppoossaall sites solubilize other~visc insoluble fluorochemicals? Eric Eric IM Internal Corsspondence 3M Internal Correspondence TTRooob:ert D.SSccHoootutwtBBl. SSEtITraM-ndEE/TTE&T--SEESTTM&EUSSS/3AMM/UUSS RDoAbVeErt DT.ERHMoOwNeTlFIEUTS-SEPTO&LSU/3SMIDATJSST3] @ HOSTMAL DAVE TERMONT[USSP01.US097573] @ HOSTMAIL cTGcca::mesD. DDJAAohNNnAsAoMn.MSE. CTSHC-NHEOTNB&ORSBIMCRHIUCIHSA[LALLILNILNU1S.U2S32939995511]] @ @ HOSTMAIL HOSTMAIL James D. JohnsoIffET-ET&S/3M/US FDFrraoocmm:: EE1rr0iicc2AA4..R9Rei0en5in:ee1rr6/EEPTTM--EETT&&SS/3MMU!USS Dale: 10/24/96 05:16 PM SSuuibcjcetc:t: DDrraafftt FFlluvoorroocchheemmiicaall W Waassttee DDiissppoossaall GGruiiddaannecse DDaavvee,, SSocott,t, RRoobbeerrt., T"oTrhheeottrhhorieceehoeoffmyyioocuualhhaacvvoeentaaaggirrneeieenddgtooprhhoeceleppssUmwleeasddteeesvv.eellooBppeggluuoiiwddeeillsiiannegfssirttshthaartyccooatuuldddebbsselouupssieeddngt0ossusecehlcectgtuiaadppappnrrcooep.prriiaa1tlweeodduiilsdpsoplsialklepporruooccreeddiuunrprueetss for fluorochemical containing process wastes. Below is a first try at developing such guidance. I would like your input 0onborawinshtiosrmconofbuerutihmeprlcrroivtdeerdiaorexpanded. Let me know if southink it wobuevalluabdle 0fo the ooufusr10 meet on how this could be improved or expanded. Let me know ifyou think it would be valuable to for the four of us to meet to brainstorm on further criteria. T"wThheeibooebbjrjeleeccdttuiivvcleeedooffbttyhhiissselFFeulcuotorironocgchdheiemsnmpioicscaaalll oW WpaaissottneesDDtiishspptoosmsaaillniGGmuuiiizddeaannhccueemiiassnt0oorrreeeddnuuiccreeorinimsskeksntt0oalppeeeoxopplpoesuaarnneddtttohheefleeunnovvriiorrcoohnnemmmeinectna.tl.s.RRiisskkss wFailal rbedoresduucoerdobcyhesmeileccatlingtrdainsspfoosramlatoipotniopnrsodthucatts,miannidmi0zoethhuemr ahn aordenvircoonmmpoennetanltsexpfotshuerewtaosftleuosrtorcehaemmicWaels,witlol ry thp1o0earzmmsaaoarkndkseoendttsihhsiifsspluoggsouuiriinoddgcaahonnefccmteehiccceooanwnlsastisirssatttneeesnnwfttiolwwrlmiitrtahehttiaccoiuunnrrrrpreerennotstdprruoeecnggtsusuli,labaatitnoolrd~ytoorrreeoqqrtuhueigieruerrlmmhaetaenoznrtatyssrdcbbooutumtpsltthchiaoaattnmciipess.onnnooettnttthhseeoppfuutrhrppeoowsseeaosoftfettshhteereggauumii.ddaaW nncceee..wiTTllhhtoorsysee persons disposing of the waste will retain responsibility for regulalory compliance. DDRRAAFFTT FFlluoorroocchheemmicicaall WWaassttee DDiissppoosasl GGuuiiddaannccee.. IIrnnevooirreddweoerrft1o0thuuesseeattshhetsseegeggunuieidrdeaeltliiinnneegss.,prtthhoeeceuussseearrnmmduusisttst cffiihrrssettmcchshararriaacsctteearrniidzzeemttahhyee fMbleuuoosrruoopccphhleeemmmieicncatalledwwaasbstytee.c.heTTmhihicissaliissaddnooannleessbbiyyofattthhhoeorrowouausggthh. IrIsFefavnwweiaeaswtsthteeaotssftttcrhheeaearmmwanaccgsootememopgfpoepsoonissteitsiriaiootbnnilniiegsscpllioirkmokelpclyyoessttosiobtabineeodvnvaiartirsiiaacubbhnldleeeem,,rsiccsthhtoereoimmdei.siccaaanlIltdaamnnmaaaylalybyysseibissensseshhcuoeposupuslldadermiyinec0nnlutecsddaeembaapylssceuuhffafefiinmccdiiieecannanttlannlauyunzmmaelbbyewsearirsosotfofesfsstaahfmermpowmlpeacsslat0tecoe.hbbsee ptpsuhrrosroecsuetseshsssarlcc0oothnntestrrliricbabnuuttgtiiaennpggporftooopportthsihseaeitbwwelaeatsscrtteoemsmstteprreoneaassmmit.oi.ordniUUssnnpidsdoeesurrasnsltdtaaeonnrpsddtiiioonnonggdst.t.hheeIctcomommpayopsboiestitniieoocnneososffawwrayassttoteesssattmreepaalmmessanaanndddantthaheleyiirzevvaawrriaaisbatieblisltyyf,rowwmiillleaaallcllhooww the user to select appropriate treatment or disposal options. TdTihhspeeosccarrlii.tteerrtiihaaeaaspppepllryyst(ho0owwualasdsttceehssaaarssachttheeeyryizaaerreethfleinpayrlelytrddeaiistspeodpsooersdesootfdfa..biTlTihhzuesds,,wiiafsftae.wwaasstteethssetreencaatmauriiess ossftttaahbbiielliizwzeaeddsotorrappcrrteuetarrlealaytteedddisppprroiisooerrdo(to0f is dKnisopwons.al, the user should characterize the pretreated or stabilized waste, so the nature of the waste actually disposed of is known. DDiissppoossaall ctr criteria: MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000066 I3MMAAO011441100773388 FFMiuirrscstr,t,occchooemmmppillcyyalwwiaittshhiRRcCCsRRAA aanndd otthheerr aapppplliiccaabbllee rreegguullaattoorryy rreqeuqireumienrtseofmorressttnoorrtiinnsgg., rtraetaitningg., ccllaassssiiffyyiinngg,, aanndddidsisppoossiinngg ooff fluorochemical wastes. T"Thheenn,, eaiitthheerr ppeerrffoorrmm a rriisskk aasssseessssmmenetn,t,oorrccoommppllyy wwiitthh tthhee nnuummbbeerreedd ccrriitteerriiaa lliisstteedd bbeellooww. ItIfhpepeesrrtffooorrrammgeeedd,r,aatrimissekkntaa,ssssaeesnssdmmedenintslpssohosouaulollfdd ddeeftlleerlrmmicinhnaeertaIhhceetepprrrioozbbeaadbbifliliuitloyyrooofcfahadedvmvieecrrasslee ewefafffseectcteslsstI0orehhaeemaallilnh asapnnedcdiftIihhecereecnnavvtiimrroeonnnmtm,eenSntloffrrooamm, or tddphiriessoppcsooetsssoasarlelasgffaeaac,cniitdlroilteiifaestsf.l.nuteTunTrhht,eiissaenafafdssesscdestsisssspmmooecesncnatutlrsosihhfnooaguulflouddcvlloceynosnctiihsmdiaeder.erarcbtboTeotrhthiehzettidhhseefklppuorrofoorbboaacbubihrlieliemit.tyyifcooalffleeewsfcfadetsectestpsesddntruuderrsaiinmnoggnissnttthooserrpaapeggoceeti.,efintcttrrietearaleatmaiotmmerennetw,n, ataa,nnssddtotddriraissgappenoo,s,saoalrl pccdioroosmmpcpopeossoansnleeesnantpatpnaardnnoddoacfddhfeeuggotrrruaarfddeaaaettcfiiiofoelnncitppfsrrtooohddceucucuctrtrissrsi0ktnogismmodovoeveveeremtffiermrdooemmu. mttahhTceeheddeciipsrsaippsbooklssa.aollf facility nto the environment. future effects depends on the facility into the environment. Select an alfermative potential for waste stream Select an alternative disposal approach or facili_ty if the risk is deemed unacceptable. DDoo nnoott andr landfill: N11.o.teW W:aasstTtheeisssww$ii0tthh0 vvmooallakttileecuoolrrgogaanniwiccas((VVsOOel))ecccotonencdcebeneinrctraaatutisiooennsus,n,diiennrccll4uu0ddiiCnnFggRvv,oolPlaattrietle2f6Ml5un,oorrSoouccbhhpeeammriticcClacsl,,s,tggrerraeatamtteeenrtt,thhaisnntoS5ra00g00e,mmorgg/dksigs.posal Nf"caTochiteielrei:etiseiTswhswhiosihmc5iehc0h0qussmettasagbbt/iiiklloiginzzeecwuwhwtaeoastsfthtfeeewssraiistnnhsetteaaOlnneckkctsstoebmdmeurbus,esttc1app9urr9oso6evviiuuddneepdvveadarppo4oro0rf CemSmiuFsbRisps,iasoirPontanrCtcceoo2nn6it5trnr,oocllSlssuiufibftdpthelahreslet vVVCoOcOl,acttocirnoelcneaetcfmneutneortnrartoat,tciishootennosmsriaxecgxaeecl,esodernddt5$ihs00pe00o"ppsapVplmO.TM. TcceoxohncneclcreueendnteitsrsraastttohiimoeosnneebbqVeeuOcceaaCsuu-tsiseoeexnEEewPmPhApAelleehlxxeueerommtrphpotetcssshOesoocnmtmioecbeaevlvroso,lla1aft9trii9ollee6mtuutluhpaeodrradoleoecfihconeifhmtSeiioucnnbapilosaffcrtVrttaoOoCms,mc ittnthhhceeilsuddecdefrefiiisnntieaitrtliiilooovnnnooaolfyafslV"iltVeOhOCfaltC.uo.""3roMEEcvhwvieeelmnnl iiincffeaEEvlePsPrAiAtnheaathlllsseeooss"VO" tercroexenacactltueaandltlellrsafMlttouhiroeoosrnoecochVhefeOmmiCwcia-casealtxlessemsmmtepreaetaasfsmuluu.rroeerddocbbhyyeM Mmeietcthahloosddfr22o55mDD orthe or which have vapor definition of VO, which have vapor pressures > 0.1 Tor, a this criterion says that pressures > 0.1 Torr, as contributing 10 the VO. 3M will nevertheless contributing to the VO concentration of a waste stream. 2h2..aW WnaaststhteeesslottwhheaastttiinnltithhaeeblTTeCCLLLCPtSlOeesols,foottrrhae,anlueeoqqruuoiicvvhaalelemenintctallleeaacchhiinnggNttoeetste,t:, lleeTaahccihhsaLssCppSeec0ciiffiiisccafurlbouirotorroacrchyheembmuitcicanaltl ia0t0a ccinoocnnoccneesnnitstrrtaaettniitoonnwiggtrrheeaatteerr t(sshoUoaTmmSnee9t)hTT.eCCLlL1oPPwwoellueesvvlteedlrlses.ll.iiakIbe| laateommLacCcduuo5rprr0rteenocntrftliltyytheerssieefaaalurtrcochhhrtoiincnaghgrfecfomosrriichtmhapelel.eecreirtterraiNragouuutsaesecb:lddyTbbhycyiosEEnLPPiACsAe5iin0nntissswetiatittrinbhngigttrhuuaonnrsiyievvbeeurursssteaadnllobtttryreteoaEaottPmmiAenefncnototrnsscsttlaiasanntsddesaanirrtfddywssiintgh hBm(UaaazTamarmSrdasd)olo.usus,sI wwwtaooasxsuittceleidsst..ylik0FFeaacctaottqoouarradsstoithcphataottcrrgwiateneirssishhanoostuuh:lladdbibbiaeoerccecooosnninscmseiipnddtleeerrraiyintnegogtnafforopgrreuwwnaabatsslatytee,sscowwaninisttdihhstpleleeenrastscciwhhsaatibbtehllneectehfflolousfvtoeorhrouoecscehhldeeemmabicyichcaEealdlPssAlaaurrofe:or:rottcochlxoaeisscmsiiei.lcfyyatitlonosg mammals, toxicity to aquatic organisms; bioconcentration potential, and persistence of the leached fluorochemicals. o33f.. tWWhaesalstteeeasschtthehadattMllueeoaarccohhcssheeevvmeeirrcaaalllssppmeeciciitffiirccefMlcuuaoolrrcooucclhhaetememdiicacasllsssuiimfittnhhgee assduudmmiotofiftethhfeeoiirleltee.aacchh(eeTddoxccioocnniccteyenontrftraatttiihooennspsroiissduggcrrteeatcteaernr ttbhheaanenshtthieemaLLtCCedS500 uo(ussPfiitrnnhoggedttluhehceeatclohoLwewCedSes0sftlt,uLLoCCSroSS0cO0,h,,eEEmoCCriSc5aI.0lC, m5oor0rix)ICt=Cu55rS0e0UfcfoMaorlrc(ceuaaliacc)thhedccfooarmmsopspumoomnn=eiennn1tgt1aaa0nndddd=itfiitnsvsfeccoootronncxcfeiecnn=itttryrfaa.attcii(otoTinnoonixnnoicfttihhtyceeooppmrrfpootdohduneucetcp.nt.rtoTdTuhhincteehet eecqqaupunaratbtoiiedoounnecsuuttissameenddadtiiess:d:Ii = LaL(1cCC/cSP5oDr0u,on,dtEEnCaCcSnt5y0L0,,CsoyoSrnre0r,ICgCEiS5sCO0to5ico0f,foccrooormamn1ptCpoao5ng0noe)nenin=tsttSiicUnaneMddecn(nfti==s!lintn)huufammrtobbmmeearryioob=ffecc1opotmrmopespioeon=nnetnen.ntf)tossriifnni product. Thiscalculation docs not take into = fraction of component i in the product and product. This calculation does not take into li = accounl any synergistic or antagonistic effects thai may be present..) 4c4..itW Wraaosstnteessi ftthhoaarttuIIsnettwhheheTeTnCCLsLPPpeteessrt,, aoonrralaaynntieecqqauuliivpvaraloleecnnettdullereaeacschhtiihnnaggt tedeossn,t,oleteaaiccdhhenootirrfggyaannsipiccecffillfuuioocrrifinnueeoraaottc>>he33m00icmmakgl/ssk.gor. wNNohot1ete:: ettthhoixissincity cInriftoerrimoantiiosnfoiarvuasielwabhleenfosimhpelerleaancahleydticfalluoprrooccheedmuirceasl.lha~Thdios rtrion i not identifyalso arbitrary specific fluorochemicals or when no toxicivy information is available for the leached fluorochemicals. This criterion is also arbitrary. 3p5.e. rfW Wlauasostrteoesissttohhbaautttcyclooennntteaaii(nnPFavIvBoo)ilaaltti>ele ff|luumookrrooecc.hheemm(i1iccbaaellliaaettcvocenotcnhecenetenrxtarptaoitsioounrnsesglgriermeaiattteetrro thPhaaFnnI11i00s001tt0imePPesBs)i.ttss eexxNppootoess:uurreeThliienmilitto,gie.c.gh.,ere is pttahhbeaaortftulttuthhoteerhoewwiasTaossLtbteeuVtwwyboqoeueuilnnldedg (lleoPoxssFceeIeBethhd)eeeadttt,oe>xxmiiecc1amccsoougmmr/pkepogmon.enene(nt1ntotbfaaettleiaeamvirresaastteeihoettnhheafaxtat tpwweoososuuuwlrlodedullnndioomtbtiecct aatouunssePeecFettsIhhBseea rTiTsyLL1VV0 to be exceeded. PPB). Note: to be exceeded. If her ar doubts The logic here is If there are doubts abont the TLV being exceeded, measurement of emission rates would be necessary. Eric Eric 3M Internal Correspondence 3M Internal Correspondence To: TThhoommaas GsG. AAsshheennmmaacchhere/Er/TE-ETT-&ETSR/3SMAM!UUSS MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppePecacttliiomonenraavnn.dd3CCMo,oppyNyoii.nnggC2aa.ss0CC4o-on6nf3ifid0de9enntitiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000077 33MMAAO011441100773399 FDFrraoocmm:: EE1rr0iicc25AA.9.R6Reie1ni2ne:err8/EEPTTM--TEETT&&SS/3MMU!USS Date: 10/25/96 12:48 PM SSuubbjejecct:t: RRee:: SSuubbppaarrtt CCCC RReegguulalatitioonnss. Ton, "FOUl, 1dont think we should pur geting an exempiionfor alate fuorochemicls. I don't think we should pursue getting an exemption for volatile fluorochemicals. II3hhMaavvceeonsssttiaadrteteerddvwowlooartrkikliiennggMuooonnrotthcheheeddmrriaacfftatl33sMMascffollunuotorrroioccbhhueetmniiniccgaal(l0wwaVasOs.ttee cc1rrimittaeerdriieaa.thMMisyyrffciirrosstmt mrreeeccnoodmmlmmiecennnddabatteiicoounnswweaasosftthh3aatM,t,svepverenondiiufFcetexxsemmpplt,, 3M consider volatile fluorochemicals as contributing to VO. I made this recommendation because of 3M's product aewtatrdaschaihcpoepcdyofmomriymouer ni0nfomrmiantiimoin.ze perlorochemicalaiemissions. The crea are in an carly dra stage. bt| stewardship commitment to minimize perflnorochemical air emissions. The criteria are in an early draft slage, bul I hhaavvee attached a copy for your information. Frc Eric 3M Internal Correspondence. 3M Internal Correspondence TDTooA.:VE SPPCAAHTTULSSZHHEEE[LLHLLPEEDRREI[SHHKPPDDSEE0SS0KK.3UU5SS600]33226699H11o|]t@@maiHHloossttmmaaiill DRMRAAAARYYVDEDDIAASVJCVIAHISCSU[O[HHLBPSZPDEEDEN[ESHISKUPK.SDUS.UESPSSUOK07171..U11U1S3S803230]4]153@5a516HH1]o1o@sstt@mHmaaFoilosltsmtamiil l MARDI JACOBSEN[USSP01.US2485111 @ Hostmail ccJsc:O:EPPLHHIHILLEIIRPPUW WMIUIRRSEESYYP[[OHHLPPUDDSEEOSS9KK9.1UU5SS8221]1885@5775H8]o]s@@tnaHHioolssttnmaaiill HJTHOShSEEoELTmTTHTaLEGLEsR.EIAU[AAdLMLLa[LImUINaNSIcS1UP.hSU0e01Sr9.0U7E9S73T039-99696E]1]T5@a8&]SHH@GoosMsHmtUmaoSisatliml ail BTBDhRRAoEERmNNYaTTLs BGBHYY.USASGTTsGhRREeOOnTMmMTIaI[AcAALhLLeLLrLI/IEINNTNI1-.EUUUTSSS&222019S141/53852M 02060/])]U@@@S HHHooossstttmmnaaaiiilll DJJTOOaAHHrRNNaYHLHS.UUHSNNcUTaTGrEEEeRGsRJTE[AAT-LTLEL[LAITINNLSIL1S.IUNUASS1MO.0U11U6S66S62111664]]80@@6]HH@oossHttmoaaslitlmail TCJCOaAAmHMMNrIaILLPSLLI. YYLSNAAoEaBBrYe[RRsAY/YELAATLN-NITENTITI[A&ALUSLLS/LI32INM1NI4/18UU.0SUS73S]231421666H63o3]s] m@@ilHHoossttmaalil DJRDOOOOHUNUNGGKLPLElAAILSSCNHEJJOLYOEHH[RANNISLSHOLOPNINNDI[A1EA.LSULLKSLI2IUNN1SL4O1U87.US097OS3]I10791@)9006H@64o4]s]Htmo@@saiHtHloaoslsttmmaaiill RDKDOAEAVNNVIIKGDDRECCAICLNLIHTIFFILTTAEOOLRNNL[|H[IAAPNLLDLLLEUIINSSNLKI1UT..UUS328SS0521759]999395@18272]]]Ho@@@stnHHHaoooisssltttmmmaaaiiilll KW WJIEAAMNYYGNNGEESEREANINNAEELTUUL[MMAIANLANILNNLIIUNNSA[12AL.U2LL6SIL80NI49NL471U]3.S5U12S]22H9@2o29s28H8t1o1a)s]tlm@@aiHlHoossttmmaaiill ErEJJIiarMimcceGsAA.E.DR.RSeEeJii[onnAheeLnrr/EsLEoTITNn--EEE1T.TTU-&&E$S2ST2/M&36SM8U4M/4US]US@SHostmail JDaAmNesADM..JoShCnHsoNIOffBERTI-ECTH&IASL/3LMI/NU]S US239951] HOSTMAIL DANA M. SCHNOBRICH[ALLIN 1. US239951] @ HOSTMAIL This is an updateon Dan's merodated TSpheissiifscacnorurpedctaiteononfacDtaornsa"'sthmatemporodvaiteddf 10/1 o10/t1h8e relative fo the rcelliamtiivneattioonthoer cEEoPPnAAc/e/InlnntddruuasstrtiryoynNNaeedggjouotsititaamtteiionotnnoss foonnnoSSnu-ubrbpepagarurtlt aCCtCCed ""VccOooCnns'ststiittfuureeonntmt th. vspaleuceifimcecaosrurreecdtiofnorfaacwtaosrtse". that provide for the elimination or concentration adjustment of non-regulated VOC's from the value measured for a waste. 3M testing has shown that when using the Method 25D analysis there are numberoflorinsted compounds measured ta3ThMhtaet taaterrhseeotiunnngogohttthccatoosnnasssihidadoeewsrreenddbtyhvvoaomltlaaatwktiiihlleenecgncooumtmhspiipsonogcuuontrnhdrdeesscMtuuinneoddtnheearorndoodtt2hhs5eeuDrrbtEEarPPnaacAAtlyirrsneeigggsuutlthlhaaetetsiireooennfsasr.r.oema number the total of fluorinated measured we compounds measured could potentially imine many ofthe waste from falling under the The thought that was by making this correction and eliminate many of the wastes from falling under the Subpart CC les subtracting these from Subpart CC rules. the total measured we could potentially MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000088 I3MMAAO011441100774400 Iusssap.kokeeAwwciictthhorKKdeeinnntKKgoaassKmtenneertarahellaFawwPyyAeerrdiionncsW Wanasosthhiuinnsgegittoohnne wwshahmooehhdaaessfbibneeieetnniowwnooorrfkkiVinnOggC'wistithhthatththeearEEePPfAAouaannndddiCCn MMotAAheroonnrettghhueelSrSuoubnbpspa.arrttACCsCC. roccounolltmelispin.noeeuAddnciidncnotitsrhhdgeeirnSSaguntbtbepopaaKrtrhtleannCCCtChrereeEglPaadAtaitdiooonnesss compound is considered1 not use the same definition a compound is considered a 1ovv8foolVlXaatOtii1lClee0'-soo6rtrhggaaaattnnmiioaccrsepiifhftotehurhesnsdHHaeeirnnnrarymoy'-t'shsmealnralwwere/gccnouosnln.asstttiaaoMnnnottss.fftooorAr fttshtheehe cfcMolounuomsorirpidionneauarttneeeddddpivpsrorelgodardtieiucaltcetsetsrnaatdnhndadenwwSaaussbtptearcctoonnCssttCiittuauennnditsscammneneaoasnsbuurreeesddutfoboiddraacteeehhdaavfvreeov1vm.aa8lltuuhXecessa1hh0ili-gg6hhaveeotrrmlatthothiasalpnnehshtehmiriee,sas,/sttghuhrreaeremredcf-fomforoeeorlthtehhe/eemyyw3wwa.isitllMlebboecs:t of the considered volalile uuder Subpar! CC and canno! be sublracled l'rom Ihe Iolal volaliles measnred l'or Ihe wasle. HcHaoonwwbeeexveearrbttthhieenerredeggbuuylalctaiootnniisodcndiosonaagllltoohwwe OffoforrfisspcpeeoccififfAiiccirecQxxueeammlpiplttiiyoonnassnodoffPvvlooallnaatntiiillneegccioonmmpRpoeousunendadsrs.c.h TCCrooimmapnpgooluuennPddarsskppeecNciCiff.iicc Haaddoujwuscsistmmeerennattsfowacictttoohrrss cmaoansondstbtleeaebxxooecbrmmatatppoiintrioyeodnnpberrryeesqqocuunoeennssetttlass.cottoEinttTghhSeeth,EEePPaOAAnfdfttihhcKiieessnowwfoKoAuaulsilrddtnQrreeeurqqauuliiiin~rryeeWaaeesnxxhtdtieennPngssltiaivovnenen.iddnoogcIcunuimnmiegRnehntetatsaeottafiiortochnnheaaTnnfarddicataanlholgoaltetooPtffhwawerockororNkktCoo.fnnorHtthhmoeeewppceaaivrrntetrgoofafSsppulwblaapninatthtrt aaCCnnCCdd rrlmeaeoqbqnonueriiaryrteoemrmityee_vnntoptssuelrwwsdioillncll nannetoolt,tfoEiinnTgcce&rreaSahsse,ee,a,enaaxdnncddKepmeminaaoyyKnsaaasccttunuaealrllyyinddW eeccrareesahassineegttthhoeen.ccoosIstntoolfifgwwhatsaisotefe disposal. | on think i's worth the fact that the cost for meeting disposal, I don't think it's worth he time. Subpart the time and money it would cost to get the exceptions. anyone has ang questoiwoonulsd ike me 0 pars his any frher please fet me knows If anyone has any qnestions or wonld like me to pnrsne this any filrther please let me know. 160 TGA 33MM tera Internal CCoorrrreessppoonnddeennccee TTRooo:berDt.SSecHoootnt BwB.lSSEtIrTaMn-dEE/ETTT&E-ESTTMR&USSS/3AMMFUUSS RDoAbVeErt DT.ERHMoOwNeTlFIEUTS-SEPTO&LSU/3SMIDATJSS73] @ HOSTMALL DAVE TERMONT[USSP01.US097573] @ HOSTMAIL cDcA: NA M.JJaammSeeCssHDDN.O. BJJooRhhInnCssoHornIffAEELTTL--IEENTT1&AUSSS/32AM1M9!UU9S5S11 @ HOSTMAIL DANA M. SCHNOBRICH[ALLIN1.US239951] @ HOSTMAIL FDFarrtooemm::: EE1rr2ii/cc0AA2.9.R6Rei0en5in:ee2rr8/EEPTTM--EETT&ESS/3MMU!USS Date: 12/02/96 05:28 PM Suet 127296 DratFluorochemical Waste Disposal Guidance Snbject: 12/2/96 Draft Fluorochemical Waste Disposal Gnid~nce Dave, Scott, Rober. Dave, Scott, Robert, Below, have made some additions and changes 0 the dra guidelines. Below, I have made some additions and changes to the draft guidelines. Please bring these guidlines withyou with our comments for our Wednesday December4 meeting from Please bring these guidelines with you with your comments for our Wednesday December 4 meeting from AAtt oouurr mmeeeettiinngg wwee nneeeedd 0to aallssoo ccoonnssiiddeerr:: 11.. DDeevveellooppiinngg mmoorre ddeettaaiilleedd gguuiiddelliinneess ffoorr rriisskk aasssseessssmmeenntt.; 2. Other uorechemica propertcs that noe tobsconsidered and included in thee criteria 2. Other fluorochemical properties that need to be considered and included in these criteria; 3 The cost ofthis policy and howtocalulate i. 3. The cost of this policy and how to calculate it. Eric Eric 5-10 AM. 8-10 AM. GGuuiiddeelliinnee OObbjjeeccttiivveess:: MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00000099 33MMAAD011441100774411 T"wThheeibooebbjrjeleeccdttuiivvcleeedooffbttyhhiissselFFeulcuotorirnoogcchdhieesmmpioicscaaalll oW WpaaissottneesDDtiishspptoosmsaaillniGGmuuiiizddeaannhccueemiiasnt0oorrreeednduvuccieerorinissmkeksnttoalppeeeoopxpllepaannoddtstothheeuoeenrnvovicirrhooennmmmeinectnl.ts. .RRioisskkss whraiaaielzrldadbr1deoourumessadknfMlecuueoodhrrioobsscyhhgeseumemiildeciaccantaliclntegtrrcaadonninssssfpfiooosrrstmmaealntatiotoipwontinitohppnrrscooudtdhurucaetctnstst,m, iraanennigmddulit0ozaoetotohthrhaeemrrreaqhunzaizaroaerrrmddeeononutvussis,croconobmmumptoepnhnoeatnanteltnssetsxoopofottfshtntherheeewwtpaoaussrfttlpeeusoosstretoorescfah.mtehm.eiW cWgaueelihsd,haaavtonvece.e t"rTiheodsetopemraskoensthdiisspgousiidnagncofetchoenswiastsetntwwilithrectuarirnenretsrpcognsuilabitoloitTy rfeoqrurireegmuleatnotsr,y bcuotmtphlaitainscneot the purpose of the guidance. Those persons disposiug of Ihe wasle will relain respousibiliU for regulalory compliauce. DDRRAAFFTT FFlluoorroocchheenmicicaall W Waassttee DDiissppoossaall GGuuiiddaannccee.. IIrnnevooirreddweoerrft1to0huuesseewatthhseetsseegeggunuieidrdeaeltliiinnneegss.,ptrthhoceeuusssseearrnmmduusistst cffiihrressnttvccshhraairrcaascc.tteerrWiizzieeettnhheesifMgluunoiorfrioocccahhnetemmdioiccuaablltwweaxasiststete.s. aTTbhohiuisst iitssheddoopnnreeebbsyyeaantthohroorroouugghh rccceoohvnenicmceeiewncntatorlrafatattiihnooaennlowyosfaficssctoooemfmgptepohnoneenewrenaanttstisstnegwwipit1rhhoacppseootsitesecnnattnisiaadrllcihhtaseemaaccllhottemhhmpoooirsrsiteertnniievvosiin.rrooW nnimmheeHennntetaasllligeetnffoffifebeictectsasv,,natridtthbhoiliusseb.ccthhedaaxroraiaschcttesteemrariibizzcoaaauttltiiootanhnessnhhpooreuuaslleddonlniicnnecycloslurusudfdeiicise cniunhubcemlmeubdierceraoalofnfadsnsaaaemmlvypapsllilueseassotiftfoootnhbbeeoeftwssuuharrseeetentt.hheaaeIttfdttwh1h0aeessrrtaeaamnnspggtlreeeeoaofamfnppdocososaismnbiablplleoeysczicoetoimoWmpnaopssitosiestislitikifooernnlosysmtiiosscauubcnnedhdeveprarsrrstiotaoocoboedldse.., cdoTTonhhticirsshiebccumhhtaaiircrnaaagccl et0aernriitazzhlaayettsiiwioosannsotsnsehhaootuurslluaddfmfaa.illcssioeont UirUnennccdoldevueredrrsesytt,aaannntdddriienenavggtamthlehuneeatctcioooormnmdpioopssofpistohtisteiiaoolnnneoeoopfdtfiwwtooanassss.tatemFSsptitrlnreedeaiaamnmngssd awaaannnyddasltt{yhhez0eierirmwvivaanarsiritimaeabisbizilfleiribotwy~mawwseitilaellcl hgalelpnoloreowwrcaettthsihsoeencusossenherotrrutitlobodubssteeiellneeagccfttitoraapsptpthpreropoprwpriraioisarattyteee. srrterueusaseem, . recovery, treatment or disposal options. Finding ways to minimize waste generation should be a first priority. T"diThshpeeossseealcc.rriittheeerriiaasaaepprppsllyho1tou0lwwdaacsshttaeersa1nctsettrhhieezyye aatrrheee ffpiirnneaatllrllyyeaddtieisdsppooorssesedtaoobfif..lizTTehhduusws,a,stiifea.a wwaasstttheeessnttarreteauarmme oiisftsshttaeabbiwilliaziseztde ooafcrtppurraeeltltrryeeadattieesddpoppsrreioodfrft0ios Known. disposal, known. the user should characterize the pretreated or stabilized waste, so the nature of the waste actually disposed of is Disposal criteria Disposal criteria: FFdiiirrsssptto,,sccioonmmgpoplflyyuwwoirittohhcRhReCCmRRiAAcaaalnnwddasootttehhsee.rr applicable applicable regulatory regulatory requirements requirements or for orig. storing, trating. treating, lasing, classi~ing, recovering recovering and and disposing of fluorochemical wastes. "Then, ether perform risk assessment,orcomply with the mabered criteria listed below Then, either perform a risk assessment, or comply with the numbered criteria listed below. RRiisskk AAsssseessssmmenetn:t: IIaFfsppseesrrsffomorermmnetedd.a,s~krrciiasskknbaaessssfeeossrssmmmiedenantbtlddeee.tteerr1mmirinneeeqssuithhreeespprrfoobubalabcbihlialiirttayyocoifcfraaidzvdaetrirsoenoeefffftehcttes ctoohehhmeeiaacllatthlh acaonnmddpotthhseiteeinnovvniirraoonnndmmetnehtne.t.varTTihhaebeility of tah"hhseesaezwwsaasrasmdststeee"nossttftrtraetesaahkmme.wc.aasn""tRRbeiie.sskkf""Tohrddameettitdeeirar,mbmoiltihenn.aattIiitoocrnneaqrreueqmiqrueueisriearspeafarunsnollcuuecnshndapedrrraseectvtareennrdsitzsintaetgiaxoopofnnofsbooduofteitth,hhtnethohgecreheppmrrtoohibbecaaabwbililiclisiotteyylnooppfrofese"siexteixpnoptonsossunauornrhedee""tahanlentddvhattorhhrieeabili~ of e"hmaizraorndmse"notfatlhehawzaarsdtes.,Tmhoart iisk, eifxitshtes treatment process prevents exposure, or if the waste presents no health or environmental hazards, no risk exists. TaTchhteeuarrliissskkelaaesscssteeessdssmtmreeenantttmssehhntoo,uuklsddeevtvaaloluuaraotteeraexdgixpspapeososusu.arrleepfpaiattllhwewasyasy.stthIhtrrsoohuuogguhhdggcrroooununsndidwdaealtbre,ro, aaiirtrh,, elepaarcocbhhaaabtieelitrrtceyaaotmmfeienmntmtessdyyissateetmmes,se,fcefitcec.t.,saaatnttdhhee aeedxexcgptpurooaasslduuarsrteeeislseoacantnepddoronoftdrffeufacauttdtmrsuerefeno trrm,iisosskkvtsoserooafccgrcceouu,mrrortirihnndggisdoopivvoseepsrroaslttiamfela.ecF.ialciitliFFeiuutstyt.uunrrIeeftroisrhisstokkhuseslddedenepcpioeernnnosddnisdsmeeoornnnb.tothhtaehenpptdhootetteehnpnetrtioinaablelawffbooihlriatwwzyaaaorssdfttesimsspttmrrreeeeasadmmeiancctetoobmmeepdfypfoeoncnetesnntatnnadndd degradation degradation degradation products products to products. move from the disposal facility into the environment, and the new hazards presented by Select an alternative disposal approach orfacility ifthe is i deemed unacceptable Select an alternative disposal approach or facility if the risk is deemed unacceptable. Alternative Selection Criteria: Alternative Selection Criteria: BtBheoefrowraeestuuessiinngg tthheessee ccrriitteerriiaa oonnee mmaussttmmaakkeecceerrttaaiinn tthhaatt tthheerree wwiilll bbee nnoo uunnaaddddrreesssseedd ssaaffeettyy Bhaazzaarrddss t0o wwoorrkkeerrss hhaannddlliinngg. the waste. rNNeootcete:e: iTTshhkee 0ffoollallcoocwweiipnntggabwwlaeassettveeeddlii.ssppooOssanalel ssselhloecuctltiodonnnocctrieittteehrairat aahrreee raarrbteiittrriaarryy_usbbeuudttabaryreecEcoPonAnssiiidndeseretrdibenbdygy oouunuirrvpperrroosfafeelsssrsiicooanntaamllejjnuutddggsmimaeennndttarttodos reduce risk to acceptable levels. One should note that the criteria used by EPA in setting universal treatment standards MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001100 I3MMAAO011441100774422 o((UfUTiTsSSks))taoarrheeuaamllssaoonaarhrbbeiaittlrrtaarhryy.a.ndEEPtPhAAesetsntaavnniddraaorrnddmsseanarrtee bbaasseedd oonnppeerrffoorrmmaanncceeooffaa ttrreeaattmmeenntt tteecchhnnoolloogg9y7 rraatthheerr tthhaann aann aasssseessssmmeenntt of risk to human health and the environment. Do not andr Do not landfill: "11.T.hiW Wsa5as0stl0eessmwweiitlkhh cvvuootllaoatfliiflleewooarrsggasaenuliieccc(t(VeVdOOb))ecccoaonuncsceeentnnrlradatlieioonns4s,0, CiinFnccRll.uuddPiinangrg vv2o6o5lla,ltiSleeubflplouaoorrtroocCchehe,emmirceiaacltasmls,e,ntgg,rreaasttleoerratIgheha,non r5500i00spmmosgga/klsgf.aciNNlioottileoe:s: wT`swohhhmiiiscechh5q0ssu0tteaasbbmtiiillgioi/zznkeegwwwhcaeantssthtioeesfsrfwiintnahttesaaOnsncekktlssoebcmmetaerusd,sttb1pep9crro9ao6vuviisdudepeeudvxanaatdppeeoorrorf4e0SsmuCbiispFsoaRiron,tnPCccacorotnni2ttrn6ooc5llsl, ufiSfduttabehhlpeesaVVrvtoOOlCacctci,oolntnercceeMeanunttomtrrraaeottnciitoho,nensrsstioeecrxxaaccgleeesee,ddion55rt00dh00eisppp"ppomVms.aO.l fTaThcheielrrieetieiisss ccesooxonmcnclceeuendnqtetursraeattsthitiioeoosnnnebbwVeecOchaaCeuut-shseeeexrEEetPhmPeApAlOeelcxxtueeomobrreptorts,csh1sseo9on9mmi6eeculvvpsooldlaafatttriieolleemoffltluhuSeaourrbdooepfccaihhrneteimtCmiiicoccnaianlosscflffuVrrdoOoem,msttahthlehleidvsedocfelrifaiintntiielitertiiiofoolnnnuoaoofrfyosV"cVhOtOehCamC.ti."c"3aMlEEsvwviienelnnlthiinfefeEEv"ePPVrAAtOh"eaallsseooss tecrroexenacactltueaandlltellrsafMlttouhiroeoosrnoecochVhefeOmmiCwcia-casealtxlessemsmmtepeeataasfsmuln.urroeerddocbbhyyeM Mmeietcthahloosddfr22o55mD0 orthe or which have vapor definition of VO, which have vapor presses > 0.1 Tor, as this criterion says that pressnres > 0.1 Tom as contributing 10 the VO. 3M will nevertheless contribnting to the VO concentration of a waste stream. 2t2..haW Wnaaststhteeessowtthehasat:iinnrettlhhieeabTTleCCLLLPtCteesSotf,soto0rhr,eaanuoeerqqo~uicfivhwaeqlmeleinntctallleeaa0cchhaiinqngugattteeisstct.,ollreegaaaccnhhisasmpsse.pceicfiNfioicce:fMluuaoTrrhooiccshheLemmCiSicc0aalliaatarabicctoornanrccyeennbttruraattniioootnn1gg0rr0eeaatteerr tihnaconnsthisetleonwt ewsitthreslioabmlee EPA TCL levels, LC50 of the fluorochemical to aquatic organisms. Note: This LC50 is arbitrary but not too inconsistent with some EPA TCLP levels. (`(OOmtathhmemerraltfhsac;cttoobrrissottchhoaanttcwweenetssahtoouhnldpboboeteecnoctuonisanlis,ldideaernriddinnpggeiirnsnissseeittteinnncggoccfnrtittheereriilaaetfaioecrrhwewdaassfttleeussowwrieitcthhenleieacacachlhasab.bll)ee ffluuoorroocchehmemiciaclsaalrrese:: ttooxxiicciittyy t(o0 mammals; bioconcentration potential; and persistence of the leached fluorochemicals. ) o33f.. tW WhaeaslstteeeasschtthehdaattMlkuenaerchohcssheeevvmeeirrcaaalllssmppieecctiiffriiccefMclauuloocrurolcoahtceehmdeicamasilssicuimtafihltnhsge assduudmmistoiofvftethhfeeoiircltleeya.acchhee[Tddocxcoioncncicteyenotnrftarattitihooennspsroiissduggcrrteeatcteaernr ttbhheaanensttthhieemaLLtCCedS500 ue(ussfPiitrnnhoggedttluhehceeatcllhooLewwCdeeSssft,ltuLLoCECrSCo5OSc0,h0,e,EEmoCCric5SaI0,lC, mSoor0rix)1[t=CuC5r5Se00fUcfoMaorlrcc(euaal1cach)thedccfooarmmsopspumoomnn=eiennn1tgt1aaa0nnd4ddd=itfiitnsvsecocrootfonncxc=eiecnnitttryrfaa.ttii[aooTnnocinxnoicftttihhtyseeoioppmrrfpootdoohdinencetcnp.at.rtoTdTinuhhthceeet eecqqauupnaratbtoiiedoounnecsuvttisaemenddadtiies:Id:i = LaL(lcCC/cSP5oDr0u,on,dtEEuCaCcSnt5y0L0,,sCoyo5rnr0er,ICgCEiS5sC00to5ico0f,foccrooormamnIpCtpoa5ong0noe)nenin=tsttSiicUaanncMdde(nfti-~!lintn)huufammrtobbmmeearryioob=ffecc1opotmrmoepspioeon=nnten.enntftossriifnni product. This calcudlocastnoittoakne ito = fraction of component i in the product and product. This calculation does not take into li = account aW synergistic or antagonistic effects that nlay be present.] 4c4.r.itWWearaisostnteessi ftthhoaarttuIIsnettwhheheeTTnCCsLLiPPmpetlesest,r, aoonrralaaynntieecqqauuliivpvaraloleecnnettdullereaeacschhtiihnnaggt tedesostt,,oleteaaiccdhhenootirrfggyaannsipiccecflilfouiorcriiMnnueeoraaettc>>he33m00icmmaggl//skksgo.r. wNNohotnete:o: ettthhoixissincity information iavailablefo the leached fuorochemicas. criterion is for use when simpler analytical procedures that information is available for the leached fluorochemicals. do not ident~ specific fluorochemicals or when no toxicib' 3p5..erfW Wlauasosttreeosssotthbhaautrtycclooennntteaaii(nnPFavIvBoo)ilaaltti>ele ff|luumookrrosocc,hheemm(1iiccbaealliaaettcvocenotcnhecenetenrxtarptaoitsoiounrnsesglgriermeaiattteetrro taPhaFnnI11i00s001tt0iimPmeePssB)ittss eexxNpoptooess:uurreeThliienmilitto,gie.c.gh.,ere is pthahbeaaorttfultttuhhoteerhoewwiasTasosLtbteeVntwwybooleueuinlnleddg (lleoPoxssFceeIeBetthdh)eeeadttt,oe>xxmiiecc1 amccsoousmmr/pkepomson.enene(nt1nottbfaaettleiaeamvirresaastteeihoettnhheaarxttaptwwoeoossuwuulorludedllnndiomobticect aatouunssePeeceFttsIhhsBaeerTyiTs:LL1VV0 0 be exceeded. PPB) Note: to be exceeded. If her ar doubts The logic here is If there are doubts about the TLV being exceeded, measuremem of emission rates would be necessary. Donot Incinerat Do not Incinerate: p11.o.llIIufttotioxoxinicccommneetatoalllsstaaoreperppersreeessneetnntht eiinnthie twhceaniwsssatisoetne. eg.(e.g., Hg. Hg, Pb, Pb, C4, Cd, Cr) Cr) an and the the incinerator incinerator seledcote enodt selected does not ave have appropriate appropriate pollution control to prevent their emission. 22.. IInniinncciinneerraattoorss tthhaatt ddoonndot hhaavvee aaddeeqquuaattee ppoolllauttiioonn ccoonnttrrooll to pprreevveenntt HHEF eemmiissssiioonnss.. a33..FiIInnnciionnmccpiinlneeerreaattcooorrmssbttuhhsaatttdidooonno(eIttCRhSaa)vvee aann aaddeeqquuaattee ccoommbbuussttiioonn eennvviirroonnmmeenntt ttoo pprreevseentt tthhee ffoorrmmaattiioonn ooffhahzazaarrddoouuss pprroodduuccttss of incomplete combustion (PlCs). Eric Eric 33MM IInntteerrnnaall CCoorrrreessppoonnddeennccee TTRooorb:ert D.SSccHoouotttwBBc.lSSVtIrEannTdE-/ETET-T-&EESTTM&RUSSS/3AMM!UUSS Robert D. Howell!ET-ET&S/3M/US MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppePecacttliiomonenraavnn.dd3CCMo,oppyNyoii.nnggC2aa.ss0CC4o-on6nf3ifid0de9enntitiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001111 I3MMAAO011441100774433 DAVE TERMONTIUSSPOL USO97S73] @ HOSTMALL DAVE TERMONT[USSP01.US097573] @ HOSTMAIL cJGca:mesD. DDJAAohNNnAsAoMMnE. STSCC-HHENNTOO&BBSRRSIICMCHUHIS[AALELLIINNL1U.SU2S32939995511]] @ @ HOSTMATL. I-IOSTMAIL James D. Johnsm~ET-ET&S/3M/US FFDarrtooemm::: EEr1ir2ic/c0AA39.R6Re0ei1inn:ee0rr2/EEPTTM--EETT&ASS/3MMU/USS Date: 12/03/96 01:02 PM Subject: Flnorochemical Waste Disposal Guidance Subject: Fluorochemical Waste Disposal Guidance Dave, Sot, Robert. Dave, Scott, Robert, AATrttcooauuurrme88n--t1100AlAAtMMrmaWWteidenndgenssedstdaoyahy,e, DDteeecmesmcwbeeecro4m4nsmmibedeeeteerit.innrgg., MMiikkee SSaannttoorroo ssuuggggeesstteedd tthhaat wwee aadddd FFlluuoorroocchheemmiiccaallWWasatsteePPrre- Treatment Alternatives to the items we consider. MesingTopics Meeting Topics: 1. Developing moredetailed guidelinesforriskassessment 1. Developing more detailed guidelines for risk assessment; 2. ter Nuorechemical properties that need tobeconsidered and included in these criteria 2. Other fluorechemical properties that need to be considered and included in these criteria', 3. Thecostofthispolicy and howtocalculate i; 3. The cost of this policy and how to calculate it; 4 Preisposal iraument alternativesfo Muorochemicals 4. Pre-disposal treatment alternatives for fluorochemicals. Eric Eric 3M Internal Corrsspondence 3M Internal Correspondence To: MardiJocobsen/US-Comporaie SMUUS DTDDoAAA:VNNEAA TMM.M E.RaSSMrCCdOIiHNIJTNNaIcOOoUBBbSRsRISeICrPCgIOUHHL[ISUAA-SCLLOLLo9IrIpN7NoS11r.7aUUtSeSS]/2323M3@99/99UH5511SO1|S@@TMHHAOOLSSTTMMAAIILL DKSKcEAEotNNVtNNEB.EETTTSEtHHRraMDDndOGGEONOTFTE-B[BEUETELS&L[SSUP[U0SMS1SS.PUUPOS0S1109.UU7S5SO70I319]999@5599H]] O@STHHMOOSASTITLMAALIL Scott B. Strand/ET-ET&S/3M/US cRco:bert D.DDHailolenlLc. lBBlauEccoTno-!nEEETT-T&ESETST&MESUS/S3IMM!UUSS James D. JohnsonET-ET&SMUS Robert D. HouclFET-ET&S/3M/US James D. JohnsmffET-ET&S/3M/US FFDrraoocmm:: EE1rr2iicc/0AA.5.R9Reie1ni0ne:e1rr1/EEATTM--EETT&&SS/3MMU!USS Date: 12/05/96 10:11 AM SSuubbiejeect:t: MMeeeteitinnggoonn FFlluuoorrooechheenmniiccaall W Waassitee DDiissppoossaall GGuuiiddaannccee Nardi, Dana, Dave, Ken, and Sct, Mardi, Dana, Dave, Ken, and Scott, PPadlledeaiasiseonllaoolookkaaovvleerrostthheeacfftooilllolonowwiiinenggsrreevviieewwooffoouurr meeting meeting on on Wednesday Wednesday 12/419, 12/4/96, and and let let me me know if know if I need need oto include include any any additional goals or action items. HeHrereeaarree aa ccoouupplee ootthheerr tthhiinnggss thhaatt I| tthhiinnkk itwwoouullddbbee uusseeffuull ffoorr tthhiiss ggrorupo1t0uoddpoo:: M11u))oPrPoelecaahsseeemciconocsanilsdidewrie,sr,ileliisssta,,raaenndddissspeonesdetd0notothfdphereoggprreooruuypp.aann(yyAaaddodduiitrtiiomoennaealtlciconomgmpowpneoennnoettnsetsndneteeheaddteetddhfefoporraoacpperrosocsechseosustl0sodeeinnssnuurreeedtthhmaatatking sure fluorochemical wastes are disposed of properly. (At our meeting we noted that the process should include making sure MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppePecacttliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3ifid0de9enntitiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001122 I3MMAAO011441100774444 fSMlhuuooourrloodcchhaeelmmsiicciaanlcllwwudaaesstuespperrooofpptaehrrteticedssisaaprroeesaaalddeesqqiuduaeatlecilyyneccsoommwmemuanurinecidcaaettceelddopttoionttghh.oo)ssee eselleeccttiinnggddisisppoossaall ffaacciililtiiess.. W Wee nnootteedd thhee pprroocceessss should also include use of the disposal guidelines we are developing.) 22h))tPPl1leesaaussbeemsiseetnenddd.mme(eAxccoooppuiireessmooefcfytyoiounugrrcwcooemlndmmiednenntotsst aarnnevddiessuuwgggygeoesustrtiioosnnusgsgffeoosrrteiedodinitstoororiinaalltohoerrssseuugbbussittdaaennlttiiinvveees.cchha|anwngileglseittsooncttlhhueededdrryaaoftutrggusuuiidgdgeleliisnnteeissons otrhaart rIasnugbemtithteedm. f(oArtdoisucrumsseieotninagt awneudpidconmoitnrgevmieiwnygou)r suggestions on these guidelines. I will include your suggestions r arrange Ihem for discussion al an upcoming meeling) Ihhaavvee aasskkeedd aaffeeww ootthheer qquueessttiioonnss iinn tthhee mmiinnuutetess,, plleeaassee rreessppoonndd t(o0 tthhessee aass wwlell.l. Thanks, Thanks, Eric Eric MMFILINNUUUOTRTEEOSSCHOOEFFM11I22C//4A4/91L69WMMAEESEETTTEIINNDGGISOOPNNOSAL GUIDANCE FLUOROCI-IEMICAL WASTE DISPOSAL GUIDANCE AATTTTEENNDDEEEESS,: SKScecoonttttGSoScttbraaenln-ddC-- hEESeS&mAAFiGGlrrmoouu&pp,AEEllTTi&AedSGSSSroup Compliance KDDDaaeanvnvaeeGTTSoeceerhrbmnmecolobn-nrttiCc--hhCCem-hEemnFmvi.lFFmOiipll&memr&A&atlilAAioellndleiseGddGrroGGoururpoopuu,CppoECCmToRopmSmpliSlap.inlaicanenccee. DM EMraaiarncrddaiRieSJJicaanhccenoorobb-sbseerEinncSh--CCA-ooEttGnatravggo.eueOpGG,preroEorvavTete.i&oSnSs Group, ET&SS Eric Reiner - ES&A Group, ET&SS BBAACCKKGGRROOUUNNDD:: DDaannaa ggaavvee tthhee ffoolllloowwiinngg bbaacckkggrroouunndd: FFullnuusoorriooacshhieelnmziictechaasll iiinnnccciiinnneeerrraaatttiiooornnpccoHsotscstosnt~-roS$l.80000F/lddurraumrmn,o,clhaleanmndifdcifalillliccnoocssittnsse<<Srt1$i01o00n/0id/ndrcrurumema.s.esIInwnccaiinsneetrraavttoiiolonunomoeffhhfiriggohhmllyy1fM1luu.oor1riinn4aait1eebdd, wwaanasdstteetsshe uccMaanullsocctiariubuomimclifzhflleueusomotrrihiidcedeeaicnslsalcsnuhidndgeeaeramfftaooogrrrmempeeHtddheciionrnnettfthrhroeealc.iitnnoccFriyilnnucelorrraaiottcoonhrreiossmfccntrriuuchgbbabbleieinrnrcssciinnmnemuresarsttatobtrbieo,enhahilaantnnchddroleleueadgdshesasashwdhadazaisazntaregrddvsooioululsiuscmawwatesatsfkerteo.e.meBBp1uurlrlbnni.iqintunoiggd4 lbs, sag and can the frdalenuuddoucrcioegecnihththcieindss.fiddcaaammIlasnajgcugeare.yn. fdAAranonmmaiinengccxeiipddtoheesnenuttrroecocfc0rccauuchrrtreeoeddureiilninsnuwhilniihgncicgohhfftdduhiimessecscionotschheieennrtremrmsaet((vosseprpr,eaellalliliatnnhggno??u)d)gwwlhaasawstdtoeedrsskinfefrgrrosomsmi0liCCctoaohrrteddooohkovvseaapeiprrteaealaa.cclttie(eqddDuiiwwdsiiottshhtlahkKgeiillrcnnamnddiussstt ta{prraneesdaasttiemgmdenetnintthterdppo.rruoogchcIenesajssusrttcyhhraafuttrbobbbmooeiirlle)ssxoopfAfofrfsvsvuoeolrnleaiatcttiioll(eetAh)cce,oommreNpipso.uonlnaeteinnndnt.gtssfoCuofrmfafMerluuseoorsrmoeoecnchttheaseresmmviheiccraaaatlll cwlxaaavnsnatdsetbfseie,sll,pwer..ego&s.rkeffoenorrsir8ntohblrurthoaaerttoh33co00hs0e0pim1iitt0oacla.04l00(D0w;aii.ssOciOFoefFstfhgageanarsmdseessmisaaayraree make these wastes hazardous passed through a scrubber.) Arsenic make these wastes hazardous. (As), Ni, and Cr are metals that can be present in fluorochemical wastes and may GoaLs: GOALS: "TwTioollddenveoelCovapaseaepprltroosaocucitivpvepero""bpperrnoonccsee.sss"" 0to ensure ensure that that fluorochenical fluorochemical wastes wastes ar are disposed disposed ofpropery of properly and and 0to nue ensure that that they they will uot cause future problems. TtThooismmpaarkkoeceerrseesaassoonnaabbllee fflluuoorroocchheemmiiccaall ddiissppoossaall gguuiiddelliinneess ffoorr ppalannttooppeerraattoorrss aanndd wwaasste ccoooorrddiinnaattoorrss t0o ffoollllooww aass ppaarrtt ooff this process. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001133 I3MMAAO011441100774455 ArAfeftcteeorrmgmgueuinidddeealltiinineeossnsaarrweeeddeegvvieveleloop(pe0eddo,u, rttoocummsatakokmeeerccsee.rrttaaiinn tthhaatt tthheeyy aarre ccoonnssiisstteenntt wwiithh ((nnoot mmoorre sstrrinnggeennt tthhaann)) MMSSDDSS recommendations we give to our customers. Tm"TahhkeesseeesgguuurieiddeuelslieinrnseesscossnhhsooiuudlleddrsshehoovwwanhhootwwhettooalccthhhaaarranacdctteeernrivziiezareaonfMmluueoonrrtooacclhhecenomnniciccearalnlsww,aassttee,, aanndd sshhoouulldd iinnccluludde gguuiiddaannccee qquueessttiioonnss ttoo hheellpp make sum users consider relevant health and environmental concerns. Provide those classifying wast streams with aceess to all needed dat sts hile rotting against ease ofconfidential informationoutside the company Provide those classi~ing waste streams information outside the company. with access to all needed data sets while protecting against release of confidential HHbyaavveeendpprrooorpphoossieeddd pqpurroaocrceeesrss ww19ii9t7hh. ift'ss fulouroorocchheemmicicaall wwaasstte ddiissppoossaall gguuiiddeelliinnees rreaaddsyffoor ssuubbmmiissssiioonn ffoorr mmaannaaggeenmneenntt aapppprroovvaall by end or third quarter 1997. DDeevveelloopp a ddaattaabbaassee 0to sstiorree iinnffoorrmmaattiioonn oonn pprrooppeerrttiieess ooff wwaassttee ssttrreeaamm ccoommppoonneennttss tthhaatt hhaavvee bbeoenn cchhaarraacciteerriizeedd.. DISCUSSION ITEMS: DISCUSSION ITEMS: ApAronnseoeeeds eesxxhiiostutssltdtooLdadeyevoveueltloolpplaat"h"peprrtoocccpeessss""tt0ao eemnnusssuutrrbeeetththaaatktettnhh.esseeAfHmluuooonrroogocchthehememiriccatalhliwwnasas,stteethssitsrerparmoscsesaasrreeshddoiisusplpodossceedduroofefssaahela~lytl.y.disTTphhoiisssal pfcbaercioticwleeietsseisenss(ph(aeloaonunpdllddiefillaFlysa)moiaaulrrteieaaeslelwllitechtcheitedtsdtheettphhwsaaatitshuutasestesmaaippusppsratroombppercrihtiaaaatrkleaeecnttte.eeccrhiAhsnnmtooillocoosngggyaynottdotohhmmeoirisnnthieimimnsiigczzlseec, tirtihisskniks.g,ptaarhnnoeddcdettishhssapaioshsttahohleeurrlfeedaciieisslniccstoouesmmr.emmuthnuaintcicadatisliipooonnsal betxveen people familiar with the waste stream characteristics and those selecting the disposal facilities. AAsisiggnnififiiccaannttrnoeoedd eexxiisst ffoorr iinnffoorrmmaattiioonn cchhaammccileerriiziinngg ffluuoorroocchhememiciacl wwaasstteess. TM"Tuhhciirssinnnaeeteeiddoinincncecllluluddseeassnccdhhaadrroaawcctnteesrrtiirzzeaatatiimoonnlooofrfowwcaahssettmeeisscttarrelea-amumsssiffnrrgoompmraaollcll effsllusuo.orroocchheemmiiccall procsses processes inching including electrochemical electrochemical fluorination cells and downstream fluorochemical-using processes. wCCuaursrrretennettllsyytmmreaaannmyyprffolufuioolrero,occbhhueetmmitichcaeallhawwzaaassrttdesossttfrreteahamem apprsorificoleasfnaadrireervlivasagkegsuduesue..riTTnhghiiassnmmdaalakeeess iitdicesaapsosysat1ol0 ppmllaaaycceevafaarlfyuluosorigronocicfhhiecemamnitcilcyaa.ll wwaassttee ninttoo a waste stream profile, but the hazards of the waste and risks during and after disposal may vary significantly. OOnnee rreeaassoonn fforr tthhiiss iiss tthhaatt iinntteerrnnaallMMSSDDSSdedsecsrcirpipttiioonnss raree ceqaulalllyy vvaagguuee.. T("TChhoeetrraeegiiessGarnnoeeveeeddhffaoosrraccoonnnesswiisstwteeannsccyyt iisnntrddeeeavvemellpoorppoiifnniglgewwsaaysssttteeesmsitrrtechaaammpirsporlfoiifnlikleeessd fftroooCmmoraaplllolrfMaluutooerrDooascthheaemmBiaiccsaasll.mmaaMmnafnrifdcaitcumwirrliilnnbggeffaapccriiellsiitetiineetssi. ng hCiosttasgyestGemro1v0ewhaassteacnoeowrdwinaasttoersstraetaCmorpdroovfialeansydstDeemcatthuart is linked to Corporate Data Bases. Mardi will be presenting this wstem to waste coordinators at Cordova and Decatur. WWIohhmiiloesttthheeMrroeeraaerrecchmmeoomrrieecthlhaawnna1s10t0e00(flpluurooorbroaocbchlheycrmn5i5icca%all)ww.aasste sstrteaamm pprrooffieless,, ccuurrercnmtllyy aa ffeew pprrooffilkess ((pprroobbaabbllyy <<20 2%))a0cacccoo%uunntt for most fluomchemical waste (probably >85 % ). DDwaSSsCCt((cDDoiifufflfeedrcreehnntatiinaaglleSSsccaaatnnnniainnggpCCoasalsloiorbrilimemetaermtyrb)yi)enisstaateteemtsptertthahtaauttrcceoso.ulldd bbee uusseedd 0to eevvaalluuaattee ppootteennttiiaall rreeaaccttiivviitUy aanndd aallssoo wwhheetthheerr tthhee waste could change state at possible ambient temperatures. MaMnaadnnynyotllaabibnoorcraiatntooerrryyataaednndd mmaannaaggeemmeenntt ppeeooppllee pprroobbaabbllyy aarree nnoott aawwaarree tthhaatt mmoosstt ffluuoorroocchheemmiiccaall wwaassttee sstcreaammss aarree llaannddffiilllleedd and not incineraled. e`SSvuuabblppuaaartrttedCCaCCccddoeerffiidnnieenddg VtVoOO40lleoCvvFeelRss.mmPaWayrtbb2ec65ee,xxccSseusebddpoeaddriitnnCmmCa.annyy lffluueoodrroosbchehcecammuisicceaalol fwxvaVasOsttee>sstt0rres0aammsps..pOOmfF8 fulouroorocchhecmmicicaall ssaummpplless evaluated according to 40 CFR, Part 265, Subpart CC, 5 failed because of VO > 500 ppmw. T"stThahbeeilcicthhya,arraacctteesrrtiiazzbaailttiiitooynnooovfefaratwiwmaaess,tteeisssttrceehaaemmmisschhaooluuallddndlIissptth:ys11i))cawwlhhapatrt owwpeeekKrnn,oowwanaabdboo1uutt haaawwzaaasrsttdeeousssttreeparaommpeinrntifteeser.mrassnoodffi2it)tsswtthhheearrmmraaellmains (0 bc known that i relevant 0 poental health and environmental impasts stabili.ty, its stability overtime, its chemical and physical properties, and its be known that is relevant to potential health and environmental impacts. hazardous properties; and 2) what remains to WWaassttee tstrreamnnss mmaayy iinncclluuddee hhaazzaarrddoouuss ccoommppoonneennttss,.e..g..ssoollvveennttss., ootthheerr hthaann ffluuoorroocchheemmiciac'asls.. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001144 I3MMAAO011441100774466 W Wee nneeeed 1to0 ddeevveelloopp ecrritteeriiaaffoorr wwhheennaa wwaasstee ssttreeaamm iiss aa ""fulouroorocchheemmicicaall wwaassttee."" Pot Shale is Waste Coordinator at Cordova, Ray Davi Decatur. (I this DAVIS, PHORNICE R.2) Pat Sheller is Waste Coordinator at Cordova, Ray Davis @ Decatur. (Is this DAVIS, PHORNICE R.?) `Are Volatile Fluoroshemicals VO? Are Volatile Fluorochemicals VO? DFDeaadnnearaannlooRtteeegddittshhtaaettr rr(eeMvvoiisnsiidooannyss,t0oNotthhveeesmsitbaaennrddaa2rr5d.dss 1kK9nn9oo,wwnnpaccgooellslloo$qqu9ui9iaa3ll2llyy03a5ss9tt9hh9ee7)"".SSuubMbpypaarruttnCCdeCCr*"stwwaeenrrdeeinrrgeeccoeefnntwtllhyyapptuubDblaliinsshaheesddaiiidnn wtthhaees that FaausscedrrreeoevvrciaihssleeedRdm,,iegcSSiauusbltbpespararw(rtoMt uCColCnCddopoarynlo,lybyNaccboolovnynessmioiddtbeeerrbreeedd2i5sss,ppiee1cec9idif9fiai6ccn,aadlplllaywygoleiuisstlted5edd9n9cco3oo2mmbetppoooi5unu9ncn9lddu9ssd7e3a)d.s My understanding of 1V5O.VO,At the meeting. VO. At the meeting, | thought that what Dana said I thonght that was that fluorochemicals would probably not be listed and would not be included as VO. F"FToohrrecclclaoarnriiiffisicciaaottinoionsn,maaffsteerrtotthhheeamvmeeeeerttiinenggsI| rreefvvriieoewmweetddheSSuFuabbcptpaatrrhttatCCCSC.u.bpaMMryty CrreeCvviienewowwsshhaoolwlwoeewddsttehhaarttitthhniissauunannlddyeetrirsscttaaalnnpddriionncggedwwuaarssesnnooatts aaccccuurraet.e. TaaSelhtrleefrcnccaaotrtniifvouanes,sitot0tonuihuessseesieiennsmeggslMMtyeoetathhhadoovdddee22rde55saDDullyfftoeotrdricddfiarirroleemccattltmhmteeeeaafrsasnucuartrteethmmiaevaetnenntSstuooobfnfplVVayrOOtbeCccooCunnsccneeedonnwtftroraaratltsliioopoewnncisiifnnciceaarlthhlaaayizznalaiarrsdndtooaeudluyssctwiowcamasapltsoetpue.rn.odcsWeW.diiutthrhBeouosutuotatsnffuuprratthhgeeerr 39942 10 the verification, 59942 in the ectiontitled F. Waste Determination Procedures" It ls these newly added analytical alternatives can only be used section titled "F. Waste Determination Procedures" It also sacs the following: for specifically listed states the INlowing: compounds. But on page "w"FFauursrtthhteer,rt,hffaootrrhtthaheevpapeuurrFppeoonssreey'oosffaLaawwwaassattelddueettaeebrmomivrieantatithoieonn0..,1tthhYee/ooXwwnneeorrfoofr(0oo.pp1eerrmaatotoolrre-mnrumassctttevivoaanll-uiuanteehett-hhgeeammsa-aspsshsoaosffsaa/llmlllVVe-OOacccootmmoppnoo-uuinnndd-ss iinn tafhhoewerl-aialisqqatueuisidtdhe--appthdhaehatsaseever))em. iaTTnhHhaetereireneofrfonyor'rseies.L,sathuhweecveooawwnluntneeertraboooorrvveooapptehterereaat0tooa.1rrliiYossf/rrXeetsspchpuoonatnospsifpifbblli(le0ec.af1fboolrmeddooeerlttegee-arfrnmrmiaiiccnnctiiioonnmnggp-titohnhu-attnthdttehhs-eegataashmn-alaptylhytaaitrisceceaac/llmonmmoteleaetti-hhnooferdddacibbtnieeohiinnne-gginus-soedd for a waste determination is sufficient to evaluate all of the applicable organic compounds that are contained in the waste." And on page $9943: And on page 59943: E=" PATThhieeammmaeaiinnndipponoiginntttthhheaatrtummlueus1st0t babeelorreweesmvmapprhhiiaoasusisizzteeeddstrremegegaatrrhddoiidnnsggoddtiihrreertc.tthmmaeneaaMsseuurtreehmmoedenn2tt5ooDfftVVoOObeccoounnscecedennttirrnaattaiioownnaiissstihadtae,tt,eaarmlltithnhoaotuuiggohhn,tthhetehe EowmwePitAnheeorisdoo(arr)moopuepesneredraaditntoofgrrormmtthuuhesesttrwouaulssseeetateoadteaeesltsltotewrmmmeiventatahrhtoiooidduo((snss))tmettushshtaamtbsieestshaauoppidpptrsraoobopplrthreiifeaarotteertfhfaoaonnrdttMhhmeeuestcchtooommdrpepf2ool5ueucDnntddotssorccaboocenncuottasuiiennndteedfdoiniinnaattlwhlheeacsowwtameaspstdoteee.ut.enrdTTmshhieennattiohen, the mwaethdodw(ist)huasHeednrfoy'rsthLeawwasctoendseatnetrmqiunaaltioonomrugsrtebneersutithabalenf0o.1 rYa/nXdam12u5sdt eregfrleecetsoCrealcsicuosu.n"t for all compounds in the waste with a Henry's Law constant equal to or greater than 0.1 Y/X at 25 degrees Celsius." T"iTnhhcuulssudiisisnaagpppppaeeraatrirssalttlhyhaaotrSSufuubblplpayarrlttuCCoCrCiiainntccellduuddceeossmAApLoLLuLnodrosgr,gaannaiiccVccOoo.mmppoouunnddss with with units unitless Henrys Henry's lav law constants constants at al 25 25 C of 0.1, of> 0.1, including partially or fully fluorinated compounds, as VO. `GUIDANCE QUESTIONS (for those evaluating fluoroehemical waste steams): GUIDANCE QUESTIONS (for those evaluating fluorochemical waste streams): W Whhaatt t.tyyppeessooff ttrreeaattmmeenntt sshhoouulldd bbee aavvooiiddeedd wwiitthh tthhiiss ssppeecciiffiicc wvaassttee sstcreaamm?? Issiitt rreeaaccttiivvee?? mCCoeouu,lldd(ttShhhiiossuwwladassottteehssettrrremeaaamtmerrriesasalccstt dbdaeannaggdeedrroeoudussollyytwwhiiistthhstmm?aa)tteerriiaalls that that maybe may usdfo be used for wast waste treatment? treatment? c.g. e.g., Kiln Kiln dust dust, fy fly ash, ash, lime, (Should other materials be added to this list?) How schHE docs it contain? How much HF does it contain? How much PFIB docs it conan? How much PFIB does it contain? W Whhaatt iss tthhee ssitabbiilliibty~ oofftthhee was waste ssttrreeaalnm ccoommppoonneenuttss?? MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001155 I3MMAAO0114411007744T7 W eWnhvhaiatrt oaanrrmeeeppnoottt?eennttiiaall ddeeggrraaddaattiioonn pprroodduuccttss oofufnusnistaabbllee ccoommppoonneennttss., aanndd hhooww ffaasstt ccoouulldd tthheeyy ffoorrmm iinn a ddiissppoossaall ssiittee environment? HHooww vvaarriiaabbllee sis tthhiiss wwaassttee ssttrreeaamm?? IIs tit tthheessaamme eeaacchh tiimmeetthhee pprroocceesss sis rraun?? (Phaseaddadditions guidance questions that mibegvalhuabtle) (Please add addilional guidance queslions Ihal mighl be valuable.) ACTION ITEMS: ACTION ITEMS: oAAfsseaacpphiillolltupoprrrooojjecechct,te,mMMicAAaRRDwDaIsIteJJ:AACWCOoOrBBkSSEEwiNNthwwiplillr:lo:cIdedseesnnietfinfygyineceaaeccrhhsfll0uuoosrrootcchhheeammtiiccamalalypprrbooecceecssossntwwaaaissnttee:d; EEinssttiiimcmahatteeWattshhteee;a(anSnnonuruaalwl))asvviooellsuumimieeo Rated of each related caegorics. fluorochemical categories. waste: Work with process engineers to list what may be contained in each waste; Sor~ wastes into EEareriircciRRaeleisinn.eerr wil will conduct conduct a a erature literatnre search search for for reviewsatclscovering review articles covering treatment treatment technologies technologies for for halogenated halogenated organic organic materials. D`Daannaa wwiillll shi schedule nneexxtt mmeeeetitinngg,, aanndd rreessuultss oofafcatctiioonnss sshhoouukldd bbee rreeppoorrteedd 0to DDaann.a. EAR EAR 33MM IInntteerrnnaall CCoorrrreessppoonnddeennccee Tor KATHY JURSIKIVAXMAILUS2S1952] @ HOSTAL Tol KATHY JURSIK[VAXMAlL.US251952] @ HOSTMAIL DANAM SCHNOBRICHIALLINLUS239951] @ HOSTMAIL cc~ DANA M. SCHNOBRICH[ALLIN1.US239951] @ HOSTMAIL FDFrraoocmm:: EE1rr2ii/cc0AA59.R6Reie1in0n:ee4rr4/EEATTM--EET&TSS/3MMU!USS Date: 12/05/96 10:44 AM SSuubbieieect:t: SSeeaarrcchhffoorr HHaalloooorrggaanniicc WWaassttee TTrreeaattmmeenntt MMeetthhooddss Kathy Kathy, Please do the folowing litcrure sarch for me. Please do the following literature search for me. T`"Tw~rayystt0eosfofiirnddisrrecevaiireedwweadratratiilccoll-eeossroognnanmmiecetthphrooodddssucttthhsaa.tt ccHaanlbaobe-eousrngseendidc0towrtarcesaatt,,eapprrsree--wttareesaattte,,s ddheesasttrrocooyynotorarirrneecocorovgnaeenrirrceesscooouumrrccpeeossufnfrrdoosmmwhailtaholo--oorrggnniicc wccinooatvvseaatrleleeessnnttotellrdyydibbnistoocruuaennradddtehhmdaaellhnootaggleeoonnr-sos.d.rigsTTapnhohiseecalmmpoarosolstdteumcccoaotsmtm.immeHoosannlfohho-raaollhrooaggglneeoinncgssewnaaaarrteseeteffdlsluuwaooarrrseiitnnweeesa((stgFto))essccthhtahllnooadrrtaiincrnoeden(i(tCCna1c1i)in,)n, eoaarrnnagddtainbboirnrcooomcmroiinmaneenp(o(dBBurlrn)).d.psaI1wcaaiimtmchepp.rriimmMaayrriillyy pipanvrritaimeimrlaaearrsbyytl,eediinoiitneneerttesrrsetetaaisltsmmfeuelnountrotoaro-olor-trodgrriagsanpationvcsiesca,ssl,afbblouturettrcnbboaemtcipaveoueussensofdoofsrfeaehsnnauvvlciouihrrgooaennsnsmmaPeteneCnsdttBaa~llv(accpsoootnenlscycecetohrrlnnsosstramminnaadanntayyerddmmbioniorpcreheiennrreeyerlllaesetv)vioaa.nnntCtFoppCarapslpe.aernrsdsfaailrelepleriaklcetyliycefto.obbMeey a(cvhaiiloarbolfeloornotcraerabtmonesn)toaltefronraftuivreansofrordcioomxipncoounntdasmsiuncahtaesdPwCasBtess.(polychlorinated biphenyls), CFCs (chlorofluorocarbons), or for furan or dioxin contaminated wastes. 10 you nes futher information to help develop thi search. pise cal me on -5079. If you need further information to help develop this search, please call me on 8-5079. Thanks, Thanks, Eric Eric HH1i0isEEorrimicce..onIleloionoktehdeo2aat0t 1tkthhiisTseescseehaandrriccchhalrreeLqqiuubeeassrttayannwddhtothhohouaugsghhmttoiirtebbeecsshtteiimfi|Icpaplaasbssaedcskiiegttroodonnund than| do. Mary Hansen to someone in the do. Mary Hansen (sou may have 201 Technical (you may have worked Library worked wwwihittohh hehas her n the pis) has agreed 1 more chemical background in the past) has agreed to than I MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001166 I3MMAAO011441100774488 ccfooormmtpphlleeetitenftthohirissmarrteeiqqouune.essttHffoeorrryynoouuu,, aamnnddissshh1ee 7wwi4illl8l ppifrryoobobaulblyywbobuselcdcoonitnateacct0tiinngggivyyeoouuefforoarr cal. Tam sure she will do an excelent jobfor yon. fiwther information. Her number is 3-1748 if you ~vould call. I am sure she will do an excellent job for yon. like to give her a IlIooppee hthiiss iiss ookkaayy. Kathy Jursik Kathy Jursik 3M Inter Corraspondence 3M Internal Correspondence To: DANA SCHNOBRICHIALLINI US239951] @ Hostnail To: DANA SCHNOBRICH[ALLIN1.US239951] @ Hostmail cFcr:om: ErSSeeieecBBAeellRooewwiner ET-ETAS MUS FDartoem: : 12/1296 03:49 PM Eric A. Reiner/ET-ET&S/3M/US Date: 12/12/96 03:49 PM SSuubbjjcetc:t: RREE:: MMeeetingosonnFtFlluuooirrocchnheemmigcicaall WWeasstte DDiissppoossaallGGuiudidaannccee Dana, Dana, IShhaoavuveerll,ooookakeeddlettahhsrtrofouougghhletthcheerorrseghgueuinlamaittocorayylsseclctutoiirooinnnssarhtihaoatnteyyeooluu paposoiiinncttso.ouuctoiirnnreyycootuuarrlmmeaaelnmonog.aattStaoacrcrhhyee!dd bbeellooww:. 1It nnooww aappppeeaarrss toommee tthhaatt you were, a! least for electrochemical lluorination cell wastes, correct all along. Sorry! Y`taYbooluue:aarr"eeTrrsieiggahhtttm,eeenllteeccSttrtroaocnchdhaeermmdiisccfaalolrfvlHouarosirainnraaditoioounns wwWaaasssttteeesss.ww"oouIulnlddfanrsott,t cc| soocnnataariicnnheaadnn,vhaootrrggtaaannbiilcce mmcaeatctsterrriioaanllissclaliilsstyteeddfoiinn"tthlheoerSSoeec"c..a22n66d88..f44o00und tcaobmlep:o"uTnrdesattmhaetnwt Sotaunbdleariddns feolrecHtraozcahredmoiucsalWfausotersn."atIonnfaccetl,l Iwassetaersc.hed that table electronically for "fluoro" and found no compounds that would be in electrochemical fluorination cell wastes. BcBeuultt,poorttohhdeeurrctfflsuuoowrirootchchhoeetmmhieicrcaaollrwwgaaasnstiteec,sm,attthheoorssieealffsoo,rrmcmoeeuddldffrrcooomnmtrareieanacccttiionnmggpecoelullnl dppsroidrutcdtoswiwiditthhhiausobtSheececrr.oort2rg6ga8ans.ni4ic0c mmaabatletee.rriiaaWllsseoorwroffuoolrrmdmuuhllaaavtteiinntggo check or thi possibility on a case by case basis. cell products with other organic materials, could check for this possibility on a case by case basis. contain compounds listed in this Sec. 268.40 table. We would have to 1Iwohcuyoluylddounnorotefffieinrnddedrree0ffeer"reeUnnTccSeeot0rogttahhneeiUcUTsT"SStiatnabybloleueriinnfiSSnuaulbbpppaaarrrttaCCgCrC.a.ph((T.ThhaeelsUUoTTsSSeattraacbbhlleeediistihinins SSaceb.cl.e226f68o8.r.44"88)i.)ToThrhs"u,s,TI1hddioonn'a'tbtluuennddaeesrrossdttoaancndds votcontain any components that wobueprlesednt in clectochenmical luoronatiosln waste. why you referred to "UTS organics" in yonr final paragraph. I also searched this table for "fluoro." not contain any components that would be present in electrochemical fluoroination cell waste. This table also does Eric Eric Eric, Eric, T""T5hh0iis0s EEp--pmmavaiillsdtdaiinssdccauurssdss"ee.sstthhSeeeceetxxieeomnmp2pt6tii5oo.nn1o0of8f3flluSuotoraronocdcahhrcednmsiiccGaaellnsserffrarolomm tthhee ipp"s5aaer0rxaa0eggprmrapapppmthhvf((rcso))tsamtsnatdsattateearssdnd""".aAArdSttsaeanncskktp.ie,ocnssiuuf2rir6ffeaad5cc.e1ien0iim82m36pp5ooSuu1tnan0dnd8mdm5eanetrtdnh,rst,:oGuoorgrehncceoo2rnn6at5tlaa.ii1nn0ee8rr5. iomosfaftenthhxaiiegssmeSSmpuuebtbpnfaprtroatrmu.tn, aisaattspaipnasldpoipancrleidaocbsaflbseplt,ehee,cppifFrriooeolvdvlioidiwndeiden2g6tt.h5h"aa.t1t 0Stte8hhz5eetiwwthoaanrssot(tueecg)h4)2(6)5.1088 omocfofanttnthhaaaaitgtneppemararrefttnosrstttuawatthneeiisstcttihhshaatotlnl""ehAAaozttfaaatnnhrkkde,,ofussousullrrowffaawccsieetnegiim:mp"lppaooScuueenndcddtmiimeonnnettnh(,tec,)u(oo4nrr)t(ic)iter cT0(io)a)naMMtreadeieneotteussrsttfhhoceeornwnmsuthiemitcuehrerniatccslal,l haccapoozpnnalccireedcnnaotbturrlasaettwii1oo0annstthlleiemiphilstaasczeaffoodrrrdiooonurrstgghaawenuaiiuscctnei,t either as hssTppaaeezbccaliireffdii"eoeTdudrsiiennacto44mn00esnCCtittFFuRRSetnpaptasnar,drttaarp22dp66s8l5i-cf-LoarLbalHaneandtzdoaDDrtihdisseoppuohossasazaWlalarRRdseeoissu"trsriciwcnitai4oos0nCntess,FuuaRnnsddeerr 26840..% Table "Treatment Standards for Hazardous Waste" in 40 CFR 268.40 ..... " MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001177 I3MMAAO011441100774499 Tr"Tehhceeeippvrrieenaagmmwbballseetesssttaahtteeassttthhsaatat,, si"itttiisshEsEPePAAs't'ssanffdiinandrddiinsnfggohheoorrergttahhnaaittcusnnintietssed rnapeloocrttbeebaievedyicncoogrnntewtrrdaoouslltlceeesddttffohi~alerettvhseraeltrsi,ssfwsyhii_nentcrhseeettshhteeehsootearranggdaapnaornicdsissediifnnobryhthoereregwwlaeaanasssitcteeeosssfnaaehrreeeed organics has been already reduced to organics has been minimized." levels where minimized." threats posed by release of the IoItrigisanmmiycysbbeaelnliideeffftothrhaattthifMlsuuoroerraoosccohhneemmtihicecyaallarwweaasestxteeessmpddtoo nnfootrt ccoootnhnmttaariiunnlttehheeveUUnTTSS totuhnhrogiouqauunggehihcnstethhsaeesnoVdVfOOfoFrccCootnhcntithseenenrtetmammisaosaynytbbytehe(eoqqsyuuu)iraitrtweee hehaixiggeshhm.d.tpoAtAenfggrosiaotnimn,f,ittbbhneeeecaratcuullsyaeeoeiuonfvtfsetotnhheee uttihhnneeciqorrruuupleloeenrsse.a.stseTThohtifhisseFCmmSa0acy0yhapealmlplbimbseetarylaci(camsadi)dteoem1muir0cicw,,3addsMeetepp'seennpdoddoliiinnncggoytuufppitoonnnehhaootlwwy iwwneeto incorporate the 500 ppmv limit into 3M's policy. cDcA: VE TM EMRaaMdrdO:iNJaTacIcooUbbSssSeerPgVOUULSSU--SCCOoo9rrp7po5orr7ata3et]/3eMM@I/UUHSoSstal DKKScEAEotNNVtNNEB.EETTTSEtHHRraMGGnOOdOEEENBTBET-LEIEUILTUS[U&SSSSPSP0SMO1P.10UU.1SU.SU0S9SO7015197993931599@]] @@HoHHsotomtsmtamialiaill DDRSoacabloleeettrLLtB..DBB.SaatHcrcaooonnnwd!EcE/ETlTT-V--EEEETTTT&-&RSESS/T3/B3MAMMS!UU/SUSMSSUS RJaombeesrtDD. .JHoohwnseolln/EETT--EET&T&S/S3SMM/UUSS James D. Johnsm~ET-ET&S/3M/US DDiissppoossaall ooff SSppeenntt SSccoottcchhggaarrdd TTrreeaattmmeenntt SSoolluuttiioonn 33MM rreeccoommmmeennddss mmiinniimmiizziinngg ddiisscchhaarrggeeooffspe spent SSccooticchhgagradrTdMTM ttrreeaattmmeenntt ssoolluuttiioonnss.** AAss pprraaccttiiccaall., effffoorrtss tfoo rreedduucceewwasatsetewwataeterr ddiisscchhaarrggee ocouulldd iinncclluuddee:: pprreeppaarriinngg oonnllyy aas mmuncchh ttrreeaattmmeenntt ssoolluuttiioonn aas nneecceessssaarryy foorraaprporodducutcitioonn un: run; Storing treatment solution remaining froam rnfor use inanotherapplication storing treatment solution remaining from a run for use in another application; usssoiilnnuggiowwna:atteerr ffrroonmt wwaasshhiinngg liinneess ccaarrLrMyinngg tthhee SSccoottcchhggaarrdd pprroodduucctt 0to mmaakkee tthhee etnext SSccooitchhegaarrdd rtrsesattmmeenntt solution; uusssoiilntngigpophny,hsyidsciicasalplo/cschihenegmmithcicaalslowwlaiadsssttbeewwyaatiteenrrcittnrreeeraaattmtmieeonnnttmormeientthaoonddsapotporroeepmmroioanvteee SdSccoicthclghgaarraddndssoodlliiiddssschffarroromgminrrgeesspiidrdutuaaellattirrceedaattmmeenntt wastewater 1.4 asieaer ratment system: solution, disposing the solids by incineration or wastewater to a wasteuater treatment system; in an appropriate landfill#, and discharging pretreated + using S c at c ha r d co nt aining w astewa ter a make wer for Scoichgard spay or bah: using Scotchgard containing wastewzter as make-np water for Scotchgard spray or baths; mmiinniimmiizziinngg oovveerrsspprraayy oorr ccaarrryyoovveerr aanndd ssuubbsseeqquueenntt ddrraaiinnaaggee dduurriinng aapppplliiccaattiioonn. pS*eSorosmimseieeSnStccoomtatccthheggraiaarrldd wppirrotohdduuaccpttosstmemnaatyyiaddleefggorrraaddbeieoiianncctfurremeaualttmamteeinnottn.ysyssteimss aanndd iinn rrecceeiivviinngg aaqquuaattiicc y systemssoorri sseeddiimmseennttss 0to a persistent material with a potential for bioaccumulation. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001188 33MMAAO011441100775500 #ImanItncecirinineaerlrasa.ttiiooInnnciisintthchreeappirreoeffneeyrrraeedd fmmaoocddieeloiofsfdddiiesssppioogssnaaellfdfootrorsssooalflieiddlyooircnoccnoicnneecrneatntrteraahttaeelddogSSeccnooalttchehgdgaawrraddswtwaesatbsetesecsaauassseiitodfdefe-ssgttrarosoyeysss tithnhecelppueedrerssiisstteenntt hydrogen foride. 17 andl disposed. ined landfill wih leachate collection and ream preferred materials. Incinerate only at facilities designed to safely incinerate halogenated waste because off-gases include hydrogen flnoride, lt'landfill disposed, a lined landfill with leachate collection and treatment is preferred. MSMauadbdeejeAAcvvtaotaiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliiomonenraavnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4o-on6nf3fiid0de9ennttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 11446677..00001199 33MMAAD011441100775511