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SvV* V C 46
CODE YC-11-A
PKG ____
WL
( DATE )
~T,l d t *'n u me e r )
EST* WT* 2126* LBS*
PREPARATION NOTESi_______
D*V{ 300,)f31j5>, 317*v 322, gg*^
PROCESSES (C)YC-I1-A ( >
TYPED BY: JHH > STANDARD HRS* ____ __
APPROVED BY JJG 6/10/81 EWK 10/21/81
t ih e ^X.m ,
BLEEDING
EQUIP MENT I
NAME: DALAMAR YELLOW
USE i N-CODE } ACCT
LBS j ______j
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LBS
PREP 1
. DV 2
OBTAIN 5-NITR0-2-AMIN0ANIS0LE FOR S8
j 557-C
1O-0 OBTAIN ACETD ACET ORTHO ANISIDIDE FOR S22
I 46-C
><? | CLEAN, DRESS, CLOSE 24* CLARIF PRESS -
| |15 FRAMES
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1
_______ ___________________________________ __a_
2~j l
RUN 17* (595 G) WATER INTO V,,,3fr.6>,.
WEIGH IN HYDROCHLORIC ACID FROM V-324 *
m_3__l __,
28-D
I DUMP & RINSE IN .5-NITRD-2-AMIN0 ANISOLE
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f0"| STIR 30 MIN AT 28-32 DEG F MAINTAINING"
I + CR, + KI FOR S 12 _
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` I RECORD : TIME START
CR_-=t__( + ),
T k i 14- ( + )
NOTE:< 1) IF CR-, KI-, ADD 204 'AS'IS*
' INCREMENTS' HYDROCHLORIC ACID
ASSUME 323 ____ i
RECORD: CR________ ( + ), KI__ ___( + )
l! (2) IF CR+,KI-, ADD 20# "AS IS" INCREMENTS
SODIUM NITRITE
ASSUME 33* ______ I
RECORD: CR________ ( + ), KX_____(+)
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1 l .i 57-A }
I 725-A |
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EQUIP MENT
PACE 2 OF 3 CG 46 CODE YC-41-A
I USE 1 N-CODE | ACCT
<C> I LBS I
I LBS
MISC
SLURRY IN 40 GAL WATER IN DRUM & PRECOAT
.3 l I: CLARIF PRESS WITH DICALITE FILTER AID
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STIR 30 MIR AT 28-32 DEG F MAINTAINING
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RECORD: TIME START^Zj&5?J CR;fc_.< + > ,
Ki..r*r_<+) . . ^
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NOTE: (1) IF CR^, KI-, ADD 20* "AS IS?
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INCREMENTS HYDROCHLORIC ACID
I
ASSUME 32X l_______ I
RECORD: CR______(+)i
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(2) IF CR-KKI-, ADD 200 AS IS'INCREMENTS l.
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SODIUM NITRITE
r ASSUME 33%
RECORD: CR______<*> *
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RUN 10* (97Q;G> WATER INTO
TALL TEMP CHART
UR IN -SODIUM HYDROXIDE M.
DJ TO 40* <39O4^:-^:fe3:-:'46'-70'iDE(ferfe
OSE STACK' DAMPER^ V ,, :
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I WHEN, S 14 STIR COMPLETE, TESTEDV ,4 RECORD 4 i CR...( + ),TEMP:^tet28-32 F) | : T\ |
I NOTE: Cl) IF CR-, KI~,' ADD 200 ?AS ISV
1
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INCREMENTS HYDROCHLORIC ACID
K? I
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CASSUME32X I
r e c o r d : - CR^r^c^:,i
IF CR+/KI-, ADD 200 *AS IS* INCREMENTS!
|
SODIUM NITRITE
ASSUME 333
_____l
RECORD: CR___;_( + >, KI,,^< + >
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TURN ON V-2at AGITATOR, CHOP & ADD ICE. J 2X330|
!N SHUT (OFF AGITATOR... ..
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PNPTE: ^-BREAK UP ;
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NECESSARY,- ADJ TO PH 5.8-SvJi^i^'
SODIUM HYDROXIPE';->.^m|AS^UHE: 50%
V-, ^ ACETIG ACID
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RECORD: PHL-Jz I C3.8^3>'
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4
CG 46
MAKING INSTRUCTIONS:BATCH UNIT
USE
n -c o d e "7~a c c t
CODE YC-i 1 -A <C) LBS
1 LBS
DV 12
WHEN S 21 CLARIF COMPLETE, WASH DV (S 4)
3 I LINES, PUMP 6 PRESS FOR 20 MIN OR TO A -CR
) TEST' ON A SAMPLE TO TOTAL PRESS EFFLUENT, 1
l WHICHEVER COMES FIRST* . COLLECT WASHINGS
I IN DV <S21B>*
_v
ORD: TIME START_C.ifI_CR_J!-l_(- OR +> .
f STIR 5 MIN & RECORD;' TEMP_____ (28-32 DEG
57-A
1 FUf IF NECESSARY, ADJ TO 28-32 DEG F
I J^ECORbt X&. .DEG F . J; V:,
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SULFAMIC ACID* TIR 5 MIN 6 RECORD:
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10^ 395-D 1 10
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SULFAMIC ACID/
395-D
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i WEIGH SODIUM HYDROXIDE IN DRUMS FOR S4J- ,
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J38'HD ISSOLVE IGEPAL CD630-IN~20 GAL~WATER IN~' T I DRUMS FOR S43
7-D I* 296 979-D !' 62
1 1
I WHEN S 33 COMPLETE, ADJ CV TO 48* (4685 G)
UAT 80-84 DEG F
A>-
CHECK ACCURACY: HT_Jl X.~-DEG ? h
RECORDER__|C&?_ DEG F
IMMEDIATELY RUN IN DV THRU UNDERSURFACE
DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV .
I AT 80-84 DEG F '
L^REGORD.% TIME STARTS--^T, TOTAL MIN_J'JL__
&r\ WHEN S 38 COMPLETE, STIR 10 MIN `
^ 1 NOTE: IMMEDIATELY AFTER COUPLING DISCONNECT
TRANSFER LINE AT CV
J-SfO J RECORD: DIAZO__r_L_<->, BASE___ !__(+),
PH (4*3-4*?) > ,,,
NOTE:
(1 ) -IF DIAZO +., BASE -, AND PH BELOW 4,3:
(A) ADJ TO PH 4*3-4*? SODIUM HYDROXIDE
J ASSUME 50%
(B) RECORD: PH_JL6__
(2) IF DIAZO +, BASE -, 6 PH 4*3 OR ABOVE:
(A) ADD Si 100% N-7-0 SODIUM HYDROXIDE TO
A 55G DRUM
(B) ADJ WITH WATER- TO 25G
(C) ADD 20# 100% N-46-C ACETO ACET ORTHO
ANISIDIDE
<D) STIR TO DISSOLVE
(E) POUR INTO CV
(F) STIR 1 MIN
(3) REPEAT (1)6 (2) ABOVE AS NECESSARY
1^-"'
TO - DIAZO, + BASE
POUR IN N-7-D SODIUM HYDROXIDE FROM S34 6
ITR 5 MIN-
I RECORD: PH_4b5_(8*0-8*5) 6 IF NECESSARY ADJ
| TO PH 8*0-a.5* SODIUM HYDROXIDE*. ASSUME 50%
J RECORD PH_Jj||J HYDROCHLORIC ACID,ASSUME 32%
7-D 7-D 46-C
7-D 28-D
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jar iimpriN N-979-D ig e p a l c o -630 f r o m S35
M^HEATTO 200-204 DEG F IN 58-62 MIN #rj 'SIXR%MIN AT 200-204 DEG F
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