Document wDyykLJZrkwYNz1xwL3pJ5g3d
FORM 5455-A
;
ANALYSIS FORM
1 A/-40
2
3 42- Ad
4
5 03 -AO
6
7 0/ 'AO
8
9
to
11 03-/}/?
12 t3 01-40
14
15 02-A P
16
r 43-40
(8
19 &I-40
20
21 02-4-0
22
23 fa'AP
24
25 STA*i/0 4409 *2/
26
27 2
28
29 3
30
31 # /
32
33 2
34 35 36
37 ^5? A/Art/4.
38 39
'i 41 43
43 44 45
file
ENG.
DATE
SHEET
>*&
S/(4>0 wee 73? reim Hf urn t.im (11*28 (. 737} t/ftm !, 7171
WOO 0.CW7 10,135 77o
twHo O.eszf <o,toc 2.7C>
(hObO 0,07tO (0266, 270 2x>7V0 don? tOJK 27<?
n/po O.OBtff (O.cvr 270
16/to O.OTiS' to.otx 2?/>
32(3 0,0(47 tttl A7o
o/>m r'n/ 27o
ivm 0.057}
270
f/8?8 0,0718 97Til 27a
3689 o.oi(3 3733? 2?e
/of$ o,orv
270
3erfr 30.23 nu SsTff XI.b# 28, /l V^v/ 17.X6 Wy? #>5" */Ac3 27.C7
X 2- 304/
SO c{V
z.
*
23 trn
7Sb-
SAL
t 27.6
n i.lO 2.7?
t HNFH ENT1A LMAT :rial SUSIE A pi OPRC TECTI /E OR. 5ER
jr *uy/o
_____ L
i
/
S..tvrSvifto;- ...
>$&;> i?, >.''
i
EXTINCTION METHOD WORKSHEET
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Th1 method of calibrating the 3M Brand Organic Vapor Monitor No. 3500, 3502 depends on adding a known mass of solvent or solvent mixture to a known volume
of air.
i# The known amount of solvent Is determined by the change In weight of a syringe upon solvent Injection. The known volume of air comes from readings from a positive displacement flowmeter.
The solvent(s) are diffused through one of five alimlnum columns. The small bore column Is #1 and Increasing bore sizes are numbers 2 through 5.
m
Position
2 '>io
Monitor Mce. found Flowmeter (ft j(1)
Diffuser Used FF
Date of Test s-n
Solvent(s) _.fiV -JJ. Temperature______ _ Syringe Used ----------
Mean: Standard Deviation: Coefficient of Variation:
Syringe (gr)
Coaments
*2^ 7<r<rc>
ecu
m
W&7\ O
' 2yo CALCULATIONS :
i
't jj j*
FLOW RATE:
%08t 1/,
^MILLIGRAMS. OF SOLVENT;
3
(METER)J OF AIR:
frs" (3
Fch
^
Ai-.Ztf.7jL AsL&A iA.
/2
CONCENTRATION:
fez
EXPOSURE TIME:
tOi <37~ geti S't S'G X
%7d
PPM: PPM-HOURS:
CONFIDENTIAL MATERIAL SUBj TO PROTECTIVE ORDER
3H 108971
960
- pi p
iME1 . 5
hT 1 3 3T r,~| p I I D ctf
' ^ MC
>* ~i
-j P t r-i # 3 3 INJ/'BTLf STROKE! 12 3
ijELt i h. CHRNtit RUN 3
CHANGE RUN 0 3 CHANGE RUN 1 B STOP
SB 34-6
HP RUN # BOTTLE 1 HRER `s.
1
'
RUG^31773
RT.:
RRER
HRER.; y.
0.28 S-36 0.46 1.15
lilt FhCTQR!
485 11380 81580
1242
0^512
12.003 36.173
1.312
4- ^ \
1.3000'" E+ 0
RHTE 133
TEMPI
270
TEMP
Q.^7
i.
r
80 73 MS=
TIME 14:17:36
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
l. 14 3-56
HP RUN # . BOTTLE RRER '<
RT '
fiEEfi
HUG73\s79 RRhrt
TIME 14:38=41
3H 108972
i 27 -- l:
46 14 :-"i CT
75 56
4y4 i i -j i s.1 3 .Cl v f?
1 244000 1 30 346
515600
0.027 0.621
^4 4
67.095 0.007
0,019 27.S09
jIL FhuTuRi 1.0000 E + 0
o CD --sJ
HP RUN # BOTTLE 3 BRER
3
HUG-31 79
RT
hREh
HRER "c
0.22
0.28
0.37
0.46
3 r' f
3 Q7
4
j.
4i C_*
I
1,70
1,90
2`. 23
2.83
3.58
3,93
4,15
4,46
5,39
_iO=.
_
.
*
1138 ^ L* T
12690 82620
3067 1201 44510 J'D^L7 3727 4374 1 026
8012 17900
2977 4382 9294 2114 1852
0.555 0. 333 6. 193 40.323 1,497 0.586 21.723 1.62 5 i1 i Cu1 4i O/ >1.1 3d 0.501 3,910 8.736 1,453 2. 139 4.536 1.032 0.904
TIL FhlTuR: 1,0000 E+ 0
TIME 14:49:19
HP RUM BOTTLE 4 BRER
RT RREfl
0,22 0.28 0.37 0.46
0.73 0.96 1.14 1.37 1.68 1,89
1065 668
12530 32520
3236 1507 43750 3723 4146 5015
HUL.^31^79
RRER *4
0,520
0 326 6. 123 40.324 1.531 0.736 21.379 1,819 2,026 2,451 =35 A =-
MM|p
TIME 13:01:54
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 108973
pjwyggjLiv wjwi.i l uj ijj
098
Z< "* ~Z* "7 "t V "7 Ql
4.14 4.54 ^ . 3d 5 - fe 7
*4- 4 y 1 7440
2800 33
8590 1633 1779
DIL FACTOR: 1.0000 E+ 0
i. i- l ,
8.522 1 * 3dd 1.889 4. 198 0 0.369
=; T M R T --r
pp i Qf,
00 3?6
HP KUH #
BOTTLE 5 flREfi L
D
ti AREA
H U ij 31 79 AREA X
23
393
0.821
37
1 1600
8.616
46
88640
4.279
14
1264000
67.879
86
643
0.034
74
367
0.819
56
5,26780
27.951
FACTOR: 1.0000 E+ 0
irt TIMt 15: 14:2 o
HP RUN #
BOTTLE 6 area y.
6
RUG'31-'79
RT
AREA
AREA X
0.22 8.28 8.37
0.46 0.76 0.96 1 . 14 1!-_?{ 1.63 1.39 2.22 2.82
. 58
3.93 4.14 4.55
5.48 5> * 6 r
1102 678
12380 83080
4842 1671 42140
4249 4531 5215 1129 3198
16068 2406 3012 7036 1344 1246
0.553 0. 340 6.287 41.617 2,027 0.838
21.129 2, 130 OC_ * -i7->l7?02.615
0.566 4.111 8.053 1.206
1.518 3.528 8.674 8.625
L FACTOR: 1.0000 E+ i3
TIME 15:27:02
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 10S974
099
HP RUN *
SOTTLE 7 'rl K E H '
7
RUU-^31 - 79
RT
E- ">
3.28 3.36 0,4 6 8.76 8.96 1-14 1.37 1,68
89
81 57 92 14 54 39 67
RKER
1284 760
11750 84320
3637 i =OQ
53148 3933 4413 5481 1079 9784
28740 2790 3622 8180 1520 1 684
rrlh
0.585 0.346 5.358 38.383 1.656 0.724 24.196 1,791 2.889 2,496 0.491 4.413 9,443 1.270 1.649 3.725 0.692 0.767
DIL PHCTORs 1.3080 E + 0
SThRTi
T I HE 1 6: 34: ,i6 1 1^
HP RUN # BOTTLE 8 RRER 2.
S
hUG/31--'79
RT
RRER
RRER ms.
8.28 0.37
0.46 1 . 15 2.76 3.57
494 11838
S1580 1250000
346 509708
0.827 0.638
4.396 67.427
0.019 27.484
DIL FACTOR: 1.0000 E+ S
HP RUN tt BOTTLE 9 RRER X
a.ujT_,
9
RUG-'31 '79
TIME 15:52s 11
CONFIDENTIAL MATERIAL SUBIEC : TO PROTECTIVE ORDER TIME 16=04:44
3M 108975
F
'' 1 ........
' T fi<Ti_ 11
i IPiLI k '
3.22 0.23 3.37
3.46 3.75 B. 96 1.15 1.37 1 ^ j-j I'-i
1. 3.23 -1' * C> -_i 3 .58 3 * 8 2L
4. 14 4.5^ 5.40 5 , b8
1043 6 F0
12600 02760
3433 1362 4493B
367 4
4181 5053
929 Fbifid! 17100 2074 2696 6 1 58 i1 41 C3J I
888
8,5260.338 6.351 41.715 1.730 8.687 22.647 1.352 2.107 2.547 0.46S 3.642 8.619 1.045 1.360 3. 104 0.553 0-504
1 L FfiL-TUK S 1.0000 E+ 8I
TflPT^ st
5
'
jj. ^ 9
I- 1f
?r# 0 5.63
HP RUN * TILE 10 EH Z
10
HUG
RT
HREH
HREH >.
0.22 0.23 0 2* i' 0.46 si-'?` W 7* Q
0.93 1.17 1 - 41 1.71 1.92 -_* i-_j J=: 2.35 3.60 3.95 4. 16 4.57 5.68
1 163 680
12368 83160
267 1 1 324 43340 2945 3297 37 43
717 6596 16160 170S
2060 4791 1937
0.619
0.360 O'. jDi, 44.030
1.416 0.702 22.973 1.561 1.743 1.934
0.330 3.496 3.566 0.905 1.092 2.540 1.027
XL FBC-TOR: 1.0080 E+ 0
TEMP 1 T I ME 1 RHTE TEMP2 T I ME2 IN-J TEMP FID TEMP ru:k TEMP
270 80 0.50
10.00 270 115
2.00 350 200 350 258 480 115
CHT 3PD ZERO mTT kj v f-
0.30
10.0 V.....
38
280 250 1 15
TIME
17: 13
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3H 108976
100