Document wBd6Oy8Dg4MqBp0GNw7okRYd

AR A S - 0 7 & O MICROBIAL INHIBITION (DEHYDROGENASE ACTIVITY TEST) TEST SUBSTANCE____________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206 or L3243. (1-Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot number was not noted. The test sample is FC-206. Current information indicates it is a mixture of 0.67% PFOS, 17.5% diethylene glycol butyl ether, 78.91% water, 1.33% Sultone foamer, 1% sodium octyl sulfate, 0.04% sodium lauryl sulfate, 0.5% polyoxyethylene monooctylphenyl ether, and 0.05% benzotriazole. The following summary applies to a mixture with incompletely characterized concentrations of impurities. Data may not accurately reflect inhibition by the fluorochemical component o f the test sample. METHOD:____________________________________________________ Method: Not noted. GLP: No Year completed: 1973-1974 Analytical monitoring: % Transmittance Statistical methods: Results were determined by calculation of the % transmittance and comparison with the blank. Test organism source: Not given Contact time: Not given. RESULTS____________________________________________________ Nominal concentrations: Blank control, 0.01,0.1,0.5, 1,5, and 10% concentration during the study conducted in 2/74. Blank control, 0.1, 0.5, and 1.0% concentration during the studies conducted in 3/73 and 3/74. Element values: Not given. Remarks: Testing was conducted on the mixture as described in the Test Substance Remarks field. The values reported apply to that mixture and not the fluorochemical proportion alone. CONCLUSIONS_______________________________________________ No conclusions given. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 001452 DATA QUALITY Reliability: Klimisch ranking 3. Study lacks description and records of the method followed. The inoculum is not properly characterized. The sample purity was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution. REFERENCES________________________________________________ The studies were conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, Lab Request Numbers 2034, 2093, 1973-1974. OTHER______________________________________________________ Last changed: 6/28/00 001453 F O R M I0620-PWO cc: LAB REQUEST BOOK - 42-5W File: Water and Wastewater <2034- r REQUEST FOR LABORATORY WORK Lab Rec*uest No- TO: ENVIRONMENTAL ENGINEERING LABORATORY - BUILDING 53-6N Requestor Lab Personnel ne-X ) .''H Request Pete J_f'^' ^ ^ ' / 3 oDate Rec'd. Sample:___ Prob. No. * Code # _ 4 Z<ri> Analyst: Date Needed: Days Est. Tim e:. . Hrs. Y Date Completed:. Hrs. Spent: ____ B 8 ^4 ____________ _ ^ ------y . Sample Description 2^0 Fz Total Hardness, mg/l as CaC03 MU Calcium Hardness, mg/l as CaC03 "P" Alkalinity, mg/l as CaC03 "M " Alkalinity, mg/l as CaC03 _ C o A .fi. (5.017a Sulfate, mg/l as SO4 $, J Nitrate, mg/l as NO3 0, 5 Ya Chloride, mg/l as Cl { Silica, mg/l as Si02 S* Ya Fluoride, mg/l as F Q Ortho Phosphate, mg/l as P C .O rt4 yo l - * \L + U j >0*ptl / Total Phosphate, mg/l as P - *t.T zb ____ I 7 ____ 1 2 .S 4i.fr ZU AmSSm -- =ssss 7T / 3>4i hS ZL "f.T /4 J3 z t ___ 1 43.5T U ZU V Total Chromium, mg/l as Cr Hex. Chromium, mg/l as Cr __ Total Cyanide, mg/l asCN Ferrocyanide, mg/l as CN Iron, mg/l as Fe Manganese, mg/l as Mn Surfactant, mg/l as LAS __ 1 Phenol, mg/l BOD, mg/l COD, mg/l (Short, Long, Dilute) __ Total Suspended Solids, mg/l 4.740 Volatile Suspended Solids, mg/l Turbidity, mg/l Silica Total Solids, mg/l Total Volatile Solids, mg/l IH H V T s J__*_LJ__ --^ , ,, Conductivity, mhos Total Bacteria, No./100 ml Total Coliform, No./100 ml Fecal Coliform, No./100 ml Fecal Streptococcus, No./100 ml Ammonia Nitrogen, mg/l as N Kjedldahl Nitrogen, mg/l as N Oil and Grease, mg/l Comments:. e' / Wt/W>-L -r- ' V. 7 7 % j /a , IS CM ~LsC'fa dC--__ 001454 3D)Cartunits White -- Environmental Engrg. Lab Canary -- Environmental Engrg. Lab Pink -- Environmental Engrg. Lab Goldenrod -- Requester* Copy $* s ^ X i ic-t> PRODUCT ECOLOGICAL ASSESSJCNT REQUEST FOR LABORATORY WORK h -. _ S Q B 3 S ^ -- N t . <- Q I *jiaT C-^'^'Vtv' RH'-UFSrOR NAME: -..j REQUEST DATEPROJECT S O . : COLE S O . : SAMPLE DATF: DATE. NL'EDLD. PROB. NO. DCSCHC riON: PURPOSE OF Tl.STS: LABORATORY L 3z4S DATE RECEIVED SAMPLE: - 2 14ANALYST: DATE COMPLETED:\ %f2Zj74 HOURS SPENT: ISA, Y __ G ?- BEST CORY AVAILABLE v ^ BEST COPY AVAILABLE SAMPi.:TTC SU<y? ^ File: Page No. i'IL i.N(jP. IAB - WORK SIP'-CT BEST COPY AVAILABLE bate Hrs. F c -?o 2 u r *>1 U as _ .. ... .. M . . . .. ... CM 0 /5 7 .. 6 .' %T 'US 10 Ai.Z 34 ' fo _ .A 2 -1 C . ' 5c .. L-Z2A1 ..............r A? i.t ._. 1..4 ............ _ 1 _ ` 4 (* t c - ^ o c- ___ _ __ _ ........... . C.3*i4v ^ _____ 45 U:.irh-a----- l/.A ' ----- W .jiiM s M iX --. Hr. Ip i t l ~ [ / A 3 .1 OS' u 3S 4 .4 6 , 5 .... ? ?7 "i Z l , S ...____________ ... . o../ ........ ...... -6 , ______ j..-, i.o 6 .t AS i-i" 3 8 . 4 35 ZZS 4 6 _ ... . g*. ? A UA Z 1 0 4 J C - ./fr : a 'Z iE;..:' 4,0 1 5 fdm/i ..... _ j s i s . _ j . t - ___________ ....................... . .. .- -- J ................. Reviewed bv: 001457 :v, TJC. Lii: -oh 1Lr :>' fV1(2 -P V wv A-'. V? B ,, V.f . --s/i v' VC- 20-i /*/'* 0 U I t *' //'6 ... IO-i<//0C; . . 1* ' / C 2 . File: rage N o . L'a te: ___ S^2ofl3 A r a Lv r,f : C, J H r*. : t '/ tf)ti t 4.5 ; U_ ..? 0,5 /6 *//6 ...... ///6 ///4.... _ , 7 M' 1,1 71 96 : A7 _ 74 77 y/i u r ir/,/f.l........ ;.o - !/ > ....... 77 *6 W") 1v_$! ' //O . cjia .. .!/!& J-i ____ . 6.S f i 7 / 4 Wo lie 74 crzm t/fo _ 6 9 ._ 11 75 T ~ ......... " __ _ . 7^ 3 ... Cl ^ 'ft 0,C ,j` / t Co ]fih . ..... 7- .... 76. C 74,6 EUd Ifa 7a 74.-r<H H1. Z4.*'V\ C V5. MU ( .2 1 0228 74. <822 M: C- Q ? l ! . W < . / iV z tX J J 0,0 Z l f il -7 Reviewed bv: 001458