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REPORT #D.S.C. 67-3 1 - ' "CONFIDENTIAL DU PORT TECHNICAL INFORMATION" CC: J, W. NESTOR, WILM., F&F CC: C. W. STAHL, TOLEDO F. H, BEADLES, WILM., F&F F/ S. BAKER, TUCKER C. F, KALB, WILM., F&F C/. R. DlT BOW, DETROIT SALES E. T. BREUER, WILM. , F&F MULHOLLAND, FLINT DEV. LAB, C. W. THEOBALD, WILM., F&F " "LITT, JR., MAR. LAB. R. B. DAVIS, WILM.., F&F ^ ^RRELL, MAR. LAB. P. J. GRAHAM, EXP. STA. WILM. PIKEp-MARSHALL LAB. R. A. DE WALL, CHICAGO C./N. SWINEHART, JR., MAR. LAB. P. 0, PEASLEY, EVERETT JY W. BASTIAN, MAR. LAB. H. a. STINE, FLINT W. H. EDWARDS, PHILA. PLANT C. H. THOMPSON, FORT MADISON R. H. VINING, PHILA. PLANT J. F. MC GETTIGAN, PARLIN J. L. ABBAMONDI, MAR. LAB. W. H. BEUTEL, PHILA. PLANT W. B. CALLAHAN, PHILA. PLANT K. E. ACKLEY, SO. SAN FRAN. M. E. BARTON, PHILA. PLANT J. F. VOZZELLA, WILM. File: 1705 Marshall Laboratory ittiuftw T#-y 2S5, 1967 E, I. Iu AR^MA(c Ie jialfioiirfifMR^MPANY FABRICS AND FINISHES DEPARTMENT DIVISIONAL PLANTS CHEMICAL GROUPS Cs.y STABILITY REPORT SIXTEEN 330-LINE DISPERSIONS PERFORMANCE IN ALKYD AND NITROGEN-ALKYD PRODUCTS ABSTRACT: Prepared, by:. Date Issued: Project: Previous Reports: Notebooks: M. H. Schaffer P-63 DSC D.S.C. #66-2 7682, 7357, 3091, 8189, S196, S385, 8500, 8653, 8661, 8662, 8885, 9029 This report covers the stability performance of alkyd and nitrogen-alkyd products containing sixteen of the twenty-four dispersions in the 330-Line colorant gamut. Data demonstrate that products containing any one or a combination of the sixteen dis persions are satisfactory from a stability performance standpoint. Conclusions are based on the evaluation of over 3,500 laboratory pilots and on feedback from commercial experience. A report describing the performance of the eight 330-Line dispersions not covered herein will follow completion of a statistical evaluation program currently underway. REASON FOR REPORT: # "2- D.S.C. #67-3 This report is issued to: (1) Serve as a reference on the stability per formance of products containing 330-Line dispersions in support of the full scale 330-Line commercialization proposal. (2) Document a vast amount of experimental data regarding one stability performance of products containing 330-Line dispersions. (3) Eliminate superfluous 330-Line stability evaluations by providing comprehensive recommendations based on . experimental data, (4) Appraise Management of the satisfactory com pletion of the finished product stability evaluation work phase of the P-63 Projecto (5) Supplement and consolidate earlier correspon dence on 330-Line finished product stability performance . OBJECTIVES: (1) The overall immediate objective of the P-63 Project is to replace and subsequently obsolete 42 > 732 and 743-Line conventional dispersions by satisfactorily commercializing 330Line dispersions. (2) The specific objective of the stability evaluation phase of the P-63 Project is to determine if products containing 330-Line dispersions are equivalent in stability performance to conventional based analog systems. CONCLUSIONS: (1) Sixteen (16) dispersions in the 330-Line formulating gamut (See Table I) can be used to replace their 42, 732 and 743Line conventional dispersion counterparts in alkyd and nitrogenalkyd systems without any significant effect on finished product stability characteristics. (2) The settling performance of a finished product is directly related to the degree of flocculation of the dispersions which it contains. Due to their higher level of deflocculation (better dispersion), eight (S) 330-Line coarse pigment dispersions (See Table I-A) inconsistently display varying degrees of poorer settling resistance in finished products as compared to their con ventional based, more highly flocculated, counterparts.. A statistical evaluation program is currently underway to define the extent and determine commercial significance of the settling per formance in this area. Early results are satisfactory and con clusions, which will be based on these and longer term stability data from this statistical program, will be presented in future correspondence and in the Release Letter proposing full-scale c ommercialisation,, DUP030001698 FUTURE ACTION: -3- D.S.C. #67-3 (1) Work continues to commercialize 330-Line Dispersions, A Release Letter proposing full-scale commercialization -of the 330Line gamut - (24 dispersicns) will be written, (2) The coarse pigment dispersion statistical analysis program will-continue to completion with report on data to follow. * (3) No new stability evaluations are planned in alkyd and nitrogen-alkyd.. systems for thirteen (13) of the sixteen (16) 330Line dispersions classified in this report as satisfactory,- The other three (3) dispersions are satisfactory in straight-alkyd qua lity .but have yet to be evaluated in nitrogen-alkyd quality. Plans have been made to evaluate these dispersions accordingly. (4) Stability evaluations already in progress will con tinue according to standard schedules and testing procedures. (5) Any new dispersions Introduced into the 330-Line ga mut will be evaluated in both alkyd and nitrogen-alkyd systems on a high spot basis only. ACKNOWLEDGEMENTS; The data presented in this report was planned and accom plished over the past several years. Many members of the Divisional Plants Chemical Groups contributed to the setting-up and conducting of the experimental program. PREPARED BY: APPROVED BY: MHS:JLA:CNS:jp 8/4/67 APPROVED BY; C. N. SWINEHART. SUPERVISOR DIVISIONAL PLANTS CHEMICAL GROUPS DUP030001699 -4- D.S.C. #67-3 DISCUSSION: Introduction; The immediate objective of the P-63 Project is to replace 42, 732, and 743-Line, conventional dispersions, with 330-Line DSC dispersionso To successfully achieve this objective it is necessary to establish that 330-Line dispersions perform equivalent to their conventional counterparts in alkyd and nitrogen-alkyd finished product systems. To determine performance, an experimental program was set up to not only evaluate initial film properties, but to also establish durability and stability characteristics of the 330-Line based systems as compared to conventional based controls. The data accumulated during this program demonstrates satisfactory durability performance of 330-Line dispersions, ref.; DSC Reports #66-4, and #67-2. This report summarizes the results of the stability evaluation phase of the experimental program. Results; Experimental data demonstrates that the stability per formance of products containing any one or a combination of sixteen (16) of the 330-Line dispersions scheduled for full-scale commercial ization are equivalent to their conventional based counterparts. From these experimental results it is predicted that there will be no significant commercial differences in stability performance between 330-Line and conventional based finished products. This forecast is supported by satisfactory complaint-free experience with many products manufactured on a commercial scale at Toledo using 330-Line dispersions oyer the past three years. A summary of the results supporting conclusions are presented in Tables II through XVIII. Tables II to XVII list individually, by Colorant , the per formance of the sixteen (16) 330-Line dispersions in alkyd and nitrogen-alkyd qualities. All of the finished products systems in this series of Tables either contain (1) the individual dispersion under .evaluation, alone, with no other Colorants in the system (masstone), (2) the dispersion under evaluation in combination with a prime white base (tint), or (3) the individual dispersion under evaluation in combination with other conventional dispersions. Systems* in any one Table are listed in numerical order by product Line Number. Line Numbers 15 to 699 represent straight-alkyd systems and 700 through 799 nitrogen-alkyd systems. Table XVIII shows the performance of combinations of the sixteen (16) 330-Line dispersions (gamut replacements) in alkyd and nitrogen-alkyd systems. Most of the systems used for evaluation here are active product formulas. DUP030001700 - 5- D.S.c. #67-3 Results in all Tables are expressed in terns of experi mental vs. control performance: a plus (+) designates experimental is better than control and a negative (-) designates experimental is poorer than control. Only those specific results showing a difference between experimental and control are recorded in the Tables. Where a specific result is shown, it should be understood that all other results of that evaluation are equal. Where there are no differences between experimental and control, results are designated as "equal to control." The results reported in the Tables cover the performance of prototype as well as the currently scaled-up, scheduled for commercialization, dispersions. Many of the earlier dispersions were similar in design to the present systems and results On these early systems correlate with, and tend to support data obtained from the current dispersions. Stability performance of products using any of the eight (6) coarse pigment dispersions in the 330-Line gamut will be pre sented in a separate report covering the statistical analysis program of these dispersions currently underway. Criteria For Analysis of Results: In most cases, finished products have numerically defined specification limits for controlling performance parameters and physical properties such as gloss, hardness, cure, gallon weight, viscosity, etc. In these cases, performance of an experimental system can be measured in two ways: (1) Comparison to control and/or (2) Comparison to specification limits. Specification limits provide a basis for determining if an experi mental system is commercially satisfactory even though results do not duplicate control performance, e.g., if a product has a viscosity specification of 50 to 60 seconds and the experimental is 52 and the control 56, the experimental, even though it is not equal to control, is still considered commercially satisfactory since it meets product specifications. Where no specifications exist for a particular performance test, comparison of experimental to control is the only criterion for determining satisfactory performance. Tests such as viscosity, stability , seed and settling generally fall into this category of non-specification. To define performance of 330-Line versus con ventional based systems results were related to product end use, duration of stability and importance of the specific tests in relation to what is required by the customer of the product. DUP030001701 -6- D.S.C. #67-3 The ratings given for a particular evaluation are a composite of the performance of the experimental versus control over the entire duration of testing rather than expressed as results at any single interval, e.g., seed resistance of an experimental system slightly poorer than control at one month; slightly better than control at two months; and equal to control at six months is considered equivalent to control. Rating stability in this manner eliminates slight variations in performance due to: (1) sampling inconsistencies;: (2) batch-to-batch raw material variations; (3) testing reproducibility; and (4) use of several subjective type tests. Experimental Design The target area for commercialization of 330-line dis persions is alkyd and nitrogen-alkyd finished products. In carrying out this commercialization, 330-Line will replace 42, 732 and 743Line dispersions in approximately 100 different product lines encom passing close to E,000 formulas. To determine if these replacements could be made without affecting the present level of finished product stability performance, experiments were designed as follows: (1) Quality of Products a. Masstone and Tints - Each Colorant, where applicable, was evaluated in alkyd and nitrogen-alkyd quality, masstone and tint vs. conventional based controls. The 15, 93 and Idl-Line Formulating Tables were used to develop data for straight alkyd quality and the 7dO and 7dl~Line Tables were used to develop data for nitrogen-alkyd quality. These Lines were selected as representative of alkyd and nitrogen-alkyd quality, respec tively, because of the high volume position they maintain in our production pattern and the fact that nearly all dispersions in the 330-Line gamut are included as Colorants for these Lines. In the few areas where a particular 330-Line dispersion was not used as a Colorant in any of the above Lines, masstones and tints were selected from other Formulating Tables, e.g. 195-Line, 794-Line, etc. b. Active Product Formulas - All dispersions in the 330-Line gamut were evaluated in active product formulas, metallic and non-metallic, straight-alkyd and nitrogen-alkyd quality. These evaluations included single replace ments and gamut replacements in many of the Lines which will ultimately be converted to a 330-Line formulating basis. DUP030001702 -7- D.S.C. #67-3 (2) Evaluation Intervals and Duration Stability of each sample was routinely run up to six months. Where dictated by product end use, stability was either curtailed or extended. Testing intervals varied with the specific product, but usually included evaluation at one, three and six months. Oven stabilities (12GF), low tem perature stabilities, and shelf stabilities were run as related to product end use. (3) Evaluation Testing Routine quality control tests such as gallon weight, viscosity, settling, seed, gloss, hardness, flexibility, adhesion, and color were used to define initial product performance. Settling evaluations, as well as all or a portion of the aforementioned tests were used to define performance at each stability testing period. Non-routine tests specific to end product use were also run when and where required, e.g., appliance enamels were evaluated for humidity, salt spray, grease resistance and stain resistance in addition to the routine tests listed above. Visual and microscopic analyses were made on wet samples and dry films to determine floccu lation and pigment orientation characteristics. MHS:jp DUP030001703 TABLE I 330-LINE DISPERSIONS SCHEDULED FOR FULL-SCALE COMMERCIALIZATION STABILITY PERFORMANCE COVERED IN THIS REPORT 330-LINE CODE 330-32^3 330-3300 33O-23I2 330-1362 330-1393 330-1505 330-1550 330-1559 330-2582 330-1588 330-1612 330-1658 330-1785 330-1818 330-1819 330-1830 DESCRIPTION Carbon Black Dispersion Bon Red Dispersion Thlo Red Dispersion Red Iron Oxide Dispersion "Monastral" Maroon Dispersion "Monastral" Blue Dispersion "Monastral" Blue Dispersion Indo Violet Dispersion Milori Blue Dispersion Indo Blue Dispersion Green Gold Dispersion Ponsol Orange Dispersion "Monastral" Green Dispersion "Monastral" Violet Dispersion "Monastral" Red Dispersion "Monastral" Scarlet Dispersion -9TABLE I-A 330'-LINE DISPERSIONS SCHEDULED FOR FULL-SCALE COMMERCIALIZATION STABILITY PERFORMANCE TO BE COVERED IN FUTURE CORRESPONDENCE 330-LINE CODE 330-1355 330-1384 330-1622 330-2630 330-1655 33O-I679 330-1686 330-1687 DESCRIPTION Red Iron Oxide Dispersion Medium Light Cadimum Red Dispersion Molybdate Orange Dispersion Ferrite Yellow Dispersion Red Toned Molybdate Orange Dispersion I^ght Chrome Yellow Dispersion Medium Chrome Yellow Dispersion Light Chrome Yellow Dispersion DUP030001705 REMARKS' ; TABLE I I STABILITY PERFORMANCE OF 330-3243 IN STRAIGHT ALKYD AND NITROGEN ALKYD ENAMELS MASSTQNES. TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS PW * r** pppp H H H -H i~l rH r-1 iH Prl PH PHPH CO G G G G CO p p p p o co to CO w bO > r> > > pppp H *H H H -rl CtJ CO CO (0 CO HOOOO POOO O H CO tO tO tO stttt ppppp s pppp bO h0 bD bO bO rl H H 'rl *H i--I rH t--I rH rH CO to to tO CO +++++ P rl CO Q CoO. bO H rH CO CO b|)SCO OH H 8 H 8 HO fcr HO tr HOHO HOHO f-i fr t-r tr P Cl PO bHO O HO o o Cl 0O O t3 0O O *5 t3 t3 0O-O00O0O OO O O CO p p p p p pp p p I II II II II II II II II CO CO CO CO CO ooooo a a aaa (AtnN c m c m oto oto oto oto o(0 oCO oto o otooto SESE0SEEES \0 tCHM SO M3 VO <A<AH CAMO 3 rH rH S 6-rJs; Eh -r Q XroOHN oOn O H OOOgEHgttCJOO *r< O rH *P G G > 2a- a G O bD H pG o Or G p HP to b&H rl |3 0o Or G Hoo O CO rl G PO G *h oH G tO H O o rl P0 Ho Otor P O rj td to P* G H P <A -4 ttoJ CM CA oSt 1 O H <A H (A O <H bO H G P rl GG rl P G O II O 6-t oo Ho Go O Pttoo o tl) 2 h II so 1 CD H P O rH rl P-4 (D 0) ag > rl *H U -P G G p, G bO G GH G * G pGHo *a" air o tSo to) Pto o >> GO GHr CO a H G P H B G CO 1 GH > O <a Pto Hi W (A >-,0 G G to CA G <AH PG H POG 1 n Hto PpOc a O G CA Gw G 0,0 G OM P (GS tH) Go P a G O. rofi P G CrH O GU OOP G P P Or GG IrP P U Gp G H (0 Id GOGO IrPPO G Or W-rJ G M G W3 m G IrH G G G ra p H O oO8rXG GGbO O OH H to W H WH G rd q| MG 1 CO P u Ga G Or W\ UMT\ U\ 1A 4NNOOOOOOO' rH rH H rH rH o H VYCO <0 -CO to -00GO ON rH OJ STABILITY DURATION PILOT TYPEum 7 PRODUCT LINE NO. DUP030001706 TABLE I I I STABILITY PERFORMANCE OF 330-3300 IN STRAIGHT-ALKYD AND NITROGEN-ALKYD ENAMELS MASSTONES. TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIOHS 02 CO fed Ph Ph Qrf HH OO PP O0 O OO PP !l II S25 o H E-t Ph g .C*3 * 01 01 >h o o Eh s S M P VO VO W m a! Eh CO P P P ro O P o O P *k 60 P P W 1 0) to OHrl POO 60 PP P P60 V O r) . POO . Wpp + II II , W 01 2s 2s s2 PvOvD P &a EH Eh o PQMh Eh O SOJS 3 gw Ojas O,H.-3 3 *ss'v o ON SJEh vt \w n HH * O PV. oo OS Eh OOO to to>-t!o>- 01 - o -- r4 P 01 B CL 60 W pP P,> H p P S o Se p 'n .P P CD 2 fib HO C6 . xJ P P Ss O' i-I OO OP P bn O fi H OP PS PO O _ >>P P O XJO <rv is O1 rH O H rv O cr\ P hO P *H H EH p , Uo o EH O H O O O P XJ 01 to M Si! II II So 1 E&h pPOH rl 04 rH***% 0} p w 60 bflP Hrl O 01 P XJ W SH 60 H CLP CO 04 * *H H- : p * S P 60 P w^. . t>p WO p a POP Hon 1 w * O 01 0, B C<-\ P WP P pw i a o P r*YP 0 ooy 01 P 6% C0 (D CO o P fl P a, 1 C0 p P Eh op O XJ 1 P o 6H o<n <*> OB P p PP OP P P p O {> O P 04 O OO POP P P S P PO WO P P P CO s rs P CL O46P0 P S 01 0 O H O O I 01 MB PS ca DUP030001707 STABILITY PERFORMANCE OF 330-2312 IN STRAIGHT-ALKYD AND NITROGEN-ALKYD ENAMELS MASSTONES. TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS { 1> PP rl *rl rH H H rH Pp p 43 CO W rH I--I N SO , H *H P P OOw OOm pOO pOO CO CO rH *H O O > > .p P + + II II s o HE-* B CO CO CO CO oooo ft a a a a >H4 'SO'OvHOH'O H -PaQ! E-t CO m ft <PE> Ml CP EOpQ>-i OtP M Q w525 CPP oO rH ON Oo O' t H WAmn t H rH On On S> P H rH H P P CO w n OH O P hOf-t O P o p o u 2 P p p +2 p P p PS PP OP o o o o o o Mo o o o o H pO tHopO pO o p o p o p + II II II II II CO CO CO CO CO CO CO 2a 2a 2a 2a 0a 0s0a n Ov Os OmOs O'-HO''rH OOo ON %* ON N oOo H rH O' o s e-* is ih S3 e-< 01000044 VN-Cio to to *0 0vQ\ (0 pO *H CO S3 P Pt B52) >CHO h gg H O X3 *H >>. PS p 0 8o WO H PiP p *tJ *sH p OP rH O O -H Op * P H > p 1 I--I -H CO *2 CO >0 P CO 3P 0H CsO *PHi Pi*H XPi -> >rl --a_ -re` pto +3 ~P to--1 . Pc IT -p a p ;p HO P o<n g w cr* P W H P S>MI pwia o P cr\p O Of'VCO H l> CD O PP P P Pi P g WCM.H P -H O P O TJ 1 P) O p H o ro P(A Pi P SO 1 & p o rH H A* Pp OP P o p P<HpPei Op p Po _ p <H P pp p ^pwippo nXJ pPop( P g-O P Qi psp P bo rH * Oao0*fr0wC poo0. 1 n Xd jPrt 5 rH CM I cm DUP030001708 STABILITY PERFORMANCE OF 330*1362 IN STRAIGHT-ALKYD AND NITRQGEN-ALKTD ENAMELS MASSTONES. TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS CM SP rl i--I P P rOH HO 0) M U PP PPWC) ooS?oo HOO 03 p p I II II o) w co ii CMvOMD wCM o $>H e-i Ho g H? BSm H Ph M0nOt=> OSm2 H Ph i-? O ON ON drlrl 222 ooo o o t> ooo ppp II II II to w to oBoSoS vOsOco, 8 O* ON g Eh O OOO axoto cvC'-r^ 8 ****'o-{ pa0) w m I) to* ri *rl OtT) H P CD ^PSS3PS-S>H3 iErl.ba<o3 Mo rOH O O -H *Ho P<c3 01 cd rr*a--ft*-HW03) PS0 r<PItS3 Mr? SV0r3t a, --X- *-f*pH* - * 5# 0) rl w P -0 tO^H. ! !>r-l tf CO of-l 03 P a a ft 2 0) 03 rl O P P IJ-? vO 0>3, 0>}. o a to to 03 03 P S3 S3 0O3 01 -rl -ri P 01 | I ,o O Pnn O C*N <n rl 0> t0 03 O M|3 J3 S3 0fL, P p a 03 0-1 O-i M -H O O I mH I *ESHh3 Ctf II Eh f--foHI 0) O SO3 O P -tJ to WX S3<MM M U > s3 p, a fr II gO I 03 & EH iPpOrl Ph 03 *2 a P3 H CM DUP030001709 STABILITY PERFORMANCE OF 330-1393 IN STRAIGHT-AlKYD AND NITROGEN-AT.KYD ENAMET.fi o 0o) b tv <3 Ctf pp CHO *<H0 CQO) Wa> In B *OT3 H O to n h p + p 60 hO rl rl HH O Mp + + II aoH E-*i W CO M OOO 3 a6a <c*a: vOvOvO Eh to g & oH* OHaPEh, IS Eh O EH O 8B CJM 02 Ql M (Vt4 r've'sH o *c mci--l HH B8 +OB2 *OB2 0o PO P0 II II oo aa SO NO oo tHoOOss pvt'- B O . . .h PB B B. a bO-rl H -0 a r-i P S3 as i o OH .P P HOOO *+0r>i tH S O oH P*eOrl PB O B X> Ot*s\ TJ m o2= oHl H Ho cn --Cm :Mri -B P -rl B H P EH B 8 Eh rUOH O Ofi O P'0 co X II II SO i ft Eh Po r--I *rl P-. ra <3 _ B bO iH *H P B aS So *H BcH Ba. X >- -Prl B*H bO P**>- B* 5>>ruOH pBH pOB0 Pa Pa i > ** l> t O MW n*-%\ a P -BH -H PP >WP1 P1J OO O 'HO o'SctN o B si A g pp Oi a Be Cm *ri 0 O rC .. . . . Poo B BH <BH B BB B.l P... MB.PO PP OOBCk Pi P M B gj * P P sss B H PbPO*brCfl E r-<t O O "O "O I W s a ce; tv H-4- DUP030001710 H 2 ir\ i-I & CQ < E-* !> P H rH H P P W O S3 rH 2 o o o p P to fa> 0 ft P H AH H <0 fOt Oft Oft fOt H OH O O P O OO S3 *H 'HOP o o P P -H p p + H II II O O 22 ss { SB *A NO M3 WNUN rH H m *: Eh CO w o. E-* O gh^OO i-l H (ft Eh O O S3 S3 ss QS5 CH W P.P UNVrvfr^frjj-J HHONONtO rH >. p pp rl H t>* rft ft H p bD ho p H H *H H rH rH H p 0 P 1 p 1 rH rH o 5 .--* Or, O ft ft ft o ft p-q P rH ft ft rH O o SOSO ft o 1 O1o ft > 0 A. Pft o :4K rH ft H ft 0OO N ft * ft P P -ft ft S> ft > O P (1 oo 2 ob.ob> ft H-r p v-rp ft H -H H rH rH ftHftH $ P P H O to p to p 50 ft CO CO ft, o ft 2 P P p s O H x? H-h t> a. a OrH bOO p p 0 H W'H 0" o H H O ft O P CQ p *H p'd I II II H OOO o oo sag g a a ii c -C'-n o vO IAV\ rH rH O to 8 oo to On o' CM SO $SJ Eh S Eh S Eh - OOO to to to C>-Cn .Cv - too CN- O O -d CCONt-oCvOtv' * ft O .H --s 0J P ft ft iPii hO-H H XJ Pi rH P ft H O PH P ft ft ao 50 O *H p XJ iH 9 ft O ft rH O O-rt OP O *H oH -Oa2 Po sft* f_Ht p ir\ O TJ ITN H OO rH cr\ I--I o H "ft PP ft H P EH ft .. o II O EH ft O rOH ao o Pt J 00 WX II II SO l ft Eh P O rH <H (X. W P ft ft 50 rr. tU).H HvH B 01 0 P XJ ft 0 ft ft SH faO H Pi*X ft a, x *> -H --r P B -H taO P "ft ^-* : i>H O ft " PS ft ft H O P HoiQ I J> O _ fA s p ft -H p t>.p p oi 0H oft 0<r^\ H >> V ftp ft P Pi ft S H >H rl OH PH oii Pi ft oa -H ftp PP OP P H ft C-t O>O P ft Pi ft O O tp P ft Pp P S ft PO W O <h Mft P xj p fat, B ft ft ft ft b0 . 9*'d ft HI S O HO O CX W U i a{ CM DUP030001711 STABILITY PERFORMANCE OF 330-1550 IN STRAIGHT-ALKYL AND NITROGEN-ALKYD ENAMELS ..... MASSTONES. TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS 0 0O 4- + PP *rH *H O Pi S-i Pi X3 x3 P fc 5, 55 O O oo r-l i--I O OO 0 OP 1 I II a oM-> $ iQ=> N Me-i 0) CO CO H*4 o o o a aa < ^OvOvO Eh CO & El Eh s Eh O 03)23 og A**-) O CM to <Acr\r-| q\o<o tH CO 5O3 rj CO P Pi S3 A aw bO'rl rl X3 A, r-l P 53 rl O .rl p 0) 53 > 2 53 ) 8 x3 ^ >Qb4 O53 p-H PP ua O *rl -O oa rl O PO . Pi rl -O Otf\ X3 HWlV OO rH Cf\ i--O( o"\ A bO --- 53 Hp Eh S3 . II 8 Eh p, O * H O SO3 O P x3 cwo m sgo I fc Eh PO r-l rl PL. bo r-l *H P fa-t i SW3,> rl fieri Pi CO 53, X > *rt P * S'H to- (aW4) fWeOH H *-- * P 3 3 S3 r~l OO P PW 1^ S o ra w r-\ a <*\ p S3 S3 W -H -H 43 |_3 P 1 1 . ^oo H S3 O C'NC'N rl O Pi 3 -S3 S3 A ,P P Sh *ih rl O O ri POO S3 Ch <h Pi t, S3, A Pi Pi P P JOt POOA. MO J4 P W W P, X3 P P P S3 3 P< bO bO A6 -rl *rl O 0X3X3 MU a Pi c* VO r-l DUP030001712 9 rt O H w P rt p rt rt p ft rt rt p I 01 rt bO Ko -h w h *d ft H -H rt toraot H rt fl *rt rt P rt rt rt H P H O Ih w ) S H W -H O CO 3 ft CO M + Ok Mrt 0 fl 2, cv *rrat 01 xs H <j) M .rt H <Jfc.P P rt > rt ft? So H ft.fl - H ft'H rt rt ft w > *H wp rt S H bO O ** + P P *rt n -h . a o H rt S'H rt Ho HO PH k rt o rt Ho o rl r*H O rt * p ,, CP .EfsaHtt-;' Q O p P Oo H O H O rt rt H 42 73 P P H rOt 13 O pp { * rl 0's HOP HO o^ crr^sv B oP H O p rt ft Eh rl -H o p o p + + II o p PP t rt ft P ra-H o0 S M fl <r*\ p M JQ CN o 0!*\ M JBS o u\ T) v\ S I 3. M Eh H >I rt rt ft p 8^ Eh H O U c CO .00 rt ft H c*\ p <M H.. I H rr\ rt-H OH O <M bO COM -p OI *-- rt rt H P cA O S BBSS i -'S Pe *rrtl rt flen ftrt rt Hoprt.rt fl P O P O VOv> HH CM 6h 3 II p p O P <mrt OM ft Eh rt HOO jj rt P rt p rt .fl P _ rt P rt co ft 65 ft P *P rt o M P rt rt S (X, rt *fl P ft CO fc sfiSt. CO Eh So fb cftd*Hbp frfti Q 1--i S Eh 6-i q O a, o aI OB OO 0*0 ft ) p rt {OCE0oO=hC-rs6tJOfHs5Ht cOn' cOnNeOnNCOO^|H0 too fHt ft H2 DUP030001713 designates b e tte r performance o f the 330-Line system; a-negative sign designates s a n ta l) sig rim en p lu s pe a x , .e e( rsoyl)st,e im. t ine on 0-L (c the 33 system re fe r to the performance o f the conventional dispersion STABILITY PERFORMANCE OF 33Q-25S2 IN STRAIGHT-ALKYD AND HITBOGEN-ALKYD ENAMELS ...... MASSTONES. TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS o* T3 ts r4PbHr30l r4pbHr3Ol H- p4PP>rrH3ll p4P>rrH3ll> Pra el co pci o rPCOOoHt PO rPPOOOotHal H4HPpmWOBpHlor>3l>.HPPOHosOO3o HH4pp>bCOtro3HQ*O 11 II + II + o tQ= >H mWHM<6 W 01 01 0e e0 s6 0e 0d v0 vG NHN E-i CO H "w ft' O 'EH R OE3H H Sh OOO Pt Eh O orraatwa gsa PL.ra 0tne^r^WH 'OO'>Htq HH 00 CQ rObHflbpOHO p4pWHH3)r4<phHH3b + H* pSCH3J -p0OSHh rpPOoIooHH roPPOOoHurpPO0oHM4H'pCMH3lHM4-t+WH3t5.OrPpOcyots orpPO0oH (I II II + + II II ^ S w ffl tn d) ra to a j) ooooo S E S E EE ^ oisO <nvO vO -Hd-f\ o CH R uoo'g^oo CO 0 oH "8 05 0Uq3, S-5 H TJ '^ippgi N* i.,oir>l 1H 8*5 0,43 P *0 *rf 0O iHOO pOH OH H P0H ! o g 0rl 43 <\J to TJ V\ Oi o9 oI pH &\ rOH c p, --%' WH) P ri o ErHl II PO0o ^ ptOOH. O O P TJ 03 X Hu So i ft rlNOOOO' lf\ UNvO to to to o r HH A. 03 "p 3 A ll remarks compared to - .emarks DUP030001714 TABLE X I STABILITY PERFORMANCE OF 330-1533 IN STRAIGHT-ALKYD AND NITROGEN--ALKYD ENAMELS MASSTONESt TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS O d 0 % 0) d n 0 w p d S CM "cO co co CD id d *53 d iH pS dO WH) O H O W 43 I II oa S MCQ 0O ss HH -a! Eh co W (X, HH O M4 (X. HO o ss Q 03 fQtjSM5 Id HI oo HcH 0M6Q CO d o "rl CO Pd d0 a, 1. w H T3 SS rl O a*03 0 I o,d o p 2* o rOH d0 rl O 1Od IO iH P Oo gd rl d faO-rl i--1 -rl CO 0 CO 0 p TJ dW 0dd Br-i bS) H CL-H dW K0. 0*> . rl vDP *0 0.H W> 00 p "d w-- t*r-l 0 WO d " PS dd H O P >4 O W 1 --* }*> ow tn S r*\ 0 0 Pd W rl, d >HI P _ W. OI O O CN W rl CO CO odd d 0P 0 0 a< d i wd.H d*H Od O -O 1 H 0O d r-l O <*\ 0d a,d 0 op H dd dp op PCJd d<d O !> O p d a, 0 O d 4-t d Pp 0a dP 0 d dO WO d XP W d d 00 0-0 P (2, S00 dd d d 0 W> Qrrl d HSW0 HO0O 0 *CJ Id 1 to * 1 cd cJ DUP030001715 TABLE X I I STABILITY PERFORMANCE OF 330-1612 IN STRAIGHT-ALKYD AND NITROGEN-ALKYD ENAMELS MASSTONES, TINTS AND IN COMBINATION WITH CONVENTIONAL DISPERSIONS rilHHHHHHrlH pppppp+app ododododododododod ooooooooo ooooooooo pp pp pp ppp II II II II II II II II II S3: oM Eh 2 B Eh ra w w ra n 0a 0a 0a 0a 6a 0a 0a 0a 0a S *! fS o Sn OsO NO sO >0 CM CM iH rH Eh CO PS PHEh-, o so oo vs Os O vs vOs o op vsH O vs ovs H4 S Eh g Eh Eh g Eh g Eh (X, Eh O tOoSWS 0 5 01 m vs vs Vs vs Vs vs vs cs cry i-H rH rH rH rH rH rH Osps fH W rH rl r*| pH rH rH rrl 200000000 ppbi pJh pIH pfn pU pIHpu pu ddddddddd OOOOOOOOO ooooooooo ooooooooo ppppppppp II II II II It II II II II 3 ,, *OH .-- Pd d a, am bO-H H Xi O. rH pd h o XI -H J* +3 S >g rl CXP rTJoOHOOh *Oh PboHn *PkH **P;PVddOaOdHH w `cl X3 CHM 03 P d d bO --* bO-H *--i h m m P d * dd a rH bp rl CbtWH / 8* P a rH bO *<O.ooXpp0M>c4H1Hss,>--WrpWdoOfdO_O_apHHnrr->oooa*P*WdPHdisv">P>a*. mom o IH xi <o p 0) 03 01 M 03 05 0) ffl OasOaOOa Oa Oa Oa OaOa CNt CM CM sO >0 CM CM <\ r*S HHH ..Irlrl oOO Os vs NO >N o O o' H vs Ht g OO.gfrng Engfr* Ht-4-O-O ' 0 00' H d P -H d as H P Eh d II Oo Eh d O O do O P Xi 03 X II II gP I 0) B p f--ol PrHh Jh h om d <*s Cb d OS H Gxs X5 P O P p d <n fHH 0> O P C O, O bubo d oh J4P 8 It IH 8u tJ P CH ....... IH bO rH aCVH SH <H0 O O XJ O, OJ 13 P5 CM DUP030001716 oo CM a CO p p w 01 01 H *H ra oi Pi Pi ert T00a1)iC0MJ)r0U-IH0Pi PP HrH Op U PP XPbtOXPbOOo o 0 oo o r) irl H.rl O O oo p p pp * + ii a II II H S3 a KO 0 HM M Eh PQ t 1 -< t=> Eh n O >H O Eh M a t4 01 01 to CO 01 01 H t--1 2ss2 s2a2 OO aa Q a Eh OnOnOnO vOvD < CO co M Eh CO (x) 1 Eh fWc CO Eh ooo H On cr, O ON CO Eh O ood ON|-l WN $ 4 H CU S Eh Eh Eh S Eh Eh O Is o Ai t4 U-VLTN UN UN HHHH tDoOto C-0>* W o *H . 01 P Pi 2a &oi Sb'H H X) 'g P H O a -H 9P 0) S3 > 0) c o bO O s o rH O O -H P <H O H X oa H O P U *nl XiO vrv O 2H HH3ot focAnI , O <H M H * C2 Pfl *H SO H Eh C! O Jh O -rH O O 0 P XJ l iX II II So i Eh P O H H CH 01 bO --* bO-rt r--i H W P an gndpbt Phi < -H --* p a "H cbtof p ~ w -h f*>rH 01 O Pi * pa c HOP 4 0 1 N->* O 01 c\ a p 01 -H Xt r-ll4 p i a o S\ P O Ocr\ 0} CO O Pi P OP 8 CIQPCh c .H. Pi -H O t4 O X) I H O Pc pHa O Mn -ori pfi* xl p 0 p p *h Pl % o p CP Pi Pi o Ph P ; 43 8 up C ^3 O O H JilPtlP u XJ P CP a Pi Pi bO CP*H Pi h aO HOO aj XJ Oi 1 3 S pH CM H . CM S-x* DUP030001717 ro S3 o H --m P Pc ro 43 S3 ro cd A cd S3 -p X XH F>1 HP PHP rl *rl M M HP H H rl cd H P P PP cO cd ro cd t PP mow S ! J ! > P rl rH H is<d ! . m w Q H H OH H O OHO U Pc bOPi PP S3 d P o O oP o 0 O bOU o *H OHO p P TO p g $ o o o p rl HXJ A 'H p cfdi H O P-rl N^Cl P CD aps rl AP P XdH ? Pc 0d H0 OH 0p H Sd3 f3 bO rr h mbO-rHo cd ro P s3 ro XJ n S3 B H bO rl AH Pc ro cd A CD X " > CD H w CD P _ <4. fi rl ro CD CD P -0 ro--c S H cd ro 0 Pc V' P B dd rl 0 P HOW 1X >u M >< m h 03 < (r< It 1 II II pX w m ro W * H O 0 rH M H H in h ro M P P P (UP 0 p Pc Pc Pc d fl Pt d H <D O <1> xs xJ xS X Ao HoHo oA Ao oAHo Pi cd Pc cd A Pc H O cd OH Pc Pc Pc Pc Pc Pc Pc PP PcP Pc *H APd Pa A A APa P P A P P dP H cd Oo O i--It--i i--I 0 <d cd cd o o p PHP bO bQ cd bD OP O bO rl H H M H H H H *rl P O O P P P O rlri Arl OH '`""aaa ro ro .rj m p m 8u U H H M II + + H I II + !> >* > PPP rl *rl -H Pc Pc Pc H cd cd cd H r-i t~i r-i r-i ri OH HH Pc 0 0 0 O Pc PPi HO OPc O Pc O Pc P P PP P P d S3 S3 P d P d OPPP O O O O o o 0 bO bO bO 0 O O O O 0 rl M "rl OHHH O 6 o o o o prom ro p p p p p p + + + II II II II II II 0H p OB rl 0 p0 cd Pc d PlfN 0 xsc^ H >1 00 Hcr\ Hcry 0 H bO S3 H 0 H6 CT\ Pd H P Sd * p ro 1 g O CD H S3 O' p O O fry ro rl >> 1 ro ro O Pc P CM d p CM S3 Ad WH rl Sc H O H 1 OP 1 O Pc H O H CD Cd S3 cry rp A w cd PH O B CD d cd CD M Pi P H P P P O P M d P S3 H ,HS5 MO HM m e-i PQ HO 03 Q w ro ro ro ro ro ro Ii o o o goo SBB t B6S i III i C'-c- I I H CM CM I CM C*- CM I r HH ro ro ro ro ro ro ro ro ro ro o o o oo o oooo BBBBBSBBBB O-'O'O 'O'O 'O 'O'O'O |>- II O M Pc O rHo do o PXJ ro c d o g> * Pc H CD O p S3 A O CD Pc O Pc CD CD H c d p cd CD P P S Pc P CD Pc PO ro o h ro h p ro Pc Pc fx) A o goo oo M O' cv 4-vO M-0N E-* N. E-f 9H b.oo to v>^ do vOH OO cd-eo oo VO CM cd x3 P A S rt , o ii it Pc C Pc v\ Pc cd bO X .So AH Pc o HSMO if' i H O O s < Ox> A CD H SJSlMSME-cMSBE-cE-iOpiS; O JB M M O O S E-c O O I a E-c ro x P Pc MO g* O H i rl QW os 03 JH MM u mj t \ w\uvir\ir\irvicMA<r\H crym HHHHHHHHH O''00 O' O' HHH A HOOOOOHcncn-dOtOtOlSOtOtOO'O'O'O' ........................................... fc'-C'* 03 CM. DUP030001718 STABILITY PERFORMANCE OF 3 3 0 -lB lS IN STRAIGHT-ALKYD AND NITROGEN-ALKYD ENAMELS . MA5STONES. TINTS AND IN COMBINATION WITH CONVEMTIONAL DISPERSIONS i-1 O rOH rOH i--J O rH O rOH r-( O +G2 +c3j -p g -pt5 +6> +> g +o3s 0 0 0 0.0-0 0 oo oo oo o po po po po po po po II II II II II II II H rH oo PG PG oo oo p0 po II II 5s: o M Eh 05 C3 Q CO TO TO TO TO CO H oog o o 6 o Eh Saflgg'SB H *4 'O iHvOsOvO 'C CO HH CQ si Eh CO CO CO oo SB \On O Kft) oO H rH &H Eh O O On ON El O 4 SE-f St<OOU Hft Eid ots E? QM O3 05 H Oh i4 f*V'Y<yN COtOHrl On On On On On CO -60 rH rH o ON o rH cO g o *H CO P go <d a sw Eo -h HO ft , rH (D PG *H O ^ *H P G P G> G SO bb o H P.A P XJ *rH ? O ft rH O O -H OP <H c! O *H A OS H O PO _ G H ad o t -H xJto H 1 oo rH rr\ rH or* O *M bp >-r G H " G PP (5 H P Eh St ,,O II o Eh O **rH O ft O O PCQ X(DJ TO * J!i! II II So 1 o* t*. Eh P O rH H ft rH P CO C G bO Cj O-H i--i -H W P X* G GG g rH bO H ft*H TO ft -rl M- P S -H bO P Br. !>rH O In * PS gg H O P t4 O TO 1 -- >, o<r\ g <r\ P S3 TO -H C >m4 P 1 S O bn fi CVP O O rH TO H 5S TO TO Jt ft P ft G S mc h -h h o 4 Ot) 1 bn O rH ocn (3<H ft os -H fi jd 45 P O P P <H Cm O>O P G ft O Oo G H P A3 P S P AO TOO <h AIPB XJ P ft S G bO ft*H H S TO O HOO <5 O XJ ft 1 TO s P5 oi DUP030001719 STABILITY PERFORMANCE OF 330-1319 IN STRAIGHT-ALKYD AND NITROGHN- ALKYD ENAMELS a) as P to H VCO p xj , O Ho H rH HiH rH HI opppoo to P P P P p p p PPPPPP p ** aH s fl o o B o p fi o p fl o p fl o p pj o p HOoooooo W P p p 43 ,p p p 4- II II II II II II || a oM <Eh O3 >e-h> Ht totooitotototo 06S0S0S0S6S0S00S HI Mm HHn Ov On On OnOn Os O < EwH; w OO O 0 Eh ,HOn OOOH HH Oo ^^ O O' Eh OH Eh O O HI a. g; M PH t-q w n H\h \ cn H\ <*><*% H H OOOOOn O'CO n h > PP rt H HH H rt -rQt -rQt p ,P to CO fi p 00 HH OO PO 4- >+ >> rl rl fi fi a as p as fi H fi H rt 0 rt p pP to xj W XJ H fi-H fl rt w as P to p to to to xs 0 xJ 0 H H H H bO bOO O W , CO P P + +PP P fl Pi Ort fi bO rl 0H3 bHO rl CO p oo pp I II II to to co to O 0 22 a a aa NO n O 'OvO rH QO H ON N. 'NX. O0 ON <> H 'X-- S Eh EH O O O ~*On 00 <0 On On I>- o- c*-t>* to rt 0 "rl --- to P fi rt a, i to hOH H XJ 0. rl as p rt H0 -fi H <.rpt a> rt > rt So 60 p H _ Oort P XJ H 3C pz O rt HO O H Pp oS OH 0 rl P oap> f! rt H P O'* H xJ -00 H H H\ OH c n Vt hO -- * fl -rt PH rt as Eh ^ II P Eh p O O oP o P Xj CMO K II II So 1 Eh P <3 rt A to p to rt rt rt bO --' taDH HH W rt to p xJ fl w rt fl S H bO H Pt I P to Oi >< >> H H- P as a *h bo pW---s rt k*H rt to 0 P pa rt rt H O P Hon 1 -- >> 0h \ a to 0^ ffl p rt -fl t!>onH P w oI a o p H mp S to to P P -fi p p as A P aw PH o xj <hO.*. OH,;HI P H O Hi os rt h n Art rt OB h P jrt si p 0 p p rt H PH O> 0 p rt ft 0 POP P Ch i p <P0 .fi P 5 P,, P H fOi WO H H CO ttS m 1 a Oto* wM cos S3 >4 E- aH -65 O M CP Ei S3 65 <g BO wO 1-9 *4 ce i Eh N H M o ]a > I*! M 2? ao H W E-> Eh i-9 CO U m 65 H Eh 65 H M O o n CP t H 65 1H O on CO 6; <; Cos CO EH w S3! oM j65 EH CO B!0. W 'a EH o CO to bH Eh M i-9 H CQ d *N CO p b0 rl r--I to + a) 2 B +* -h PH W *rl rl 3> 93 -H X Pi 03 i--1 . " H O UW P bp O 33 O bO . rj OH *P CO M+ HSO3 << E- . 93 MCQ Os Os S5 ON ON CO) w PHh h O*ME4h o o Ph HO OoS3sKaI Oo.raM-9 UN H r9 tO H 03 C! O "H 0) P Pi C3 I aH>* S0*rt H a. r-1 PB *d o 33 *H p Nfl P B l> 9 iO S) rl Pi33 P ?< Pi OB HO O -H t> P <H PS O -rl -2 oS rl O PO Pi B rl 330 oN "OtC r4 1 OO iH o n H (*\ O <h faD B H B P -r-l B rl P h B .I.I O Eh Pi O -H floo o Pm XJ wX s, seJ II II So >> Eh P o H *H 04 H (0 p 03 B B t>0 bjO-rl r--i *H 10 P B ra BB 0rl bO H Di*H Pi VJ Pi 14 -> l> -H -- P S *H bo P * B W-^. birl MO Pi * - PS BB rl O P oon i >-- S O CO S ON PB *H rB r'll-Q PM | O H B (NO O o ON M rl !>* 03 03 O Pi 33 B P Pi B B 03 <h *H M 'rl O 1-9 O' J b-l O Pi H O ON B ON Pi fi OB -rl fi33 33 P O P P B Ch Pi Cm O> O P B Pi O Pi O Pi O B *H P 33 P S Pi P Pi 33 O SO O <H 34 P M Pi P, Q> CD "OP Pi B Pi B Pi Pi bO h Psi*arl Pi o HOMO <4 o Du II 01 t i aj e/ I u\ CM I DUP030001721 TABLE X V III STABILITY PERFORMANCE OF STRAIGHT-ALKYD AND NITROGEN-ALKYD ENAMEL PILOTS CONTAINING! COMBINATIONS OF 330-LINE DISPERSIONS AS REPLACEMENTS FOR CONVENTIONAL DISPERSIONS 3a bO faQ Hrl rl rH co CO I CO co O HbO P PbO. H HCO t* > !>> > S P rl HP PP d rl PP rl >H fiSp r* P P co rl rH CrOl H 0) PU 0$ P xf CO 0 . S>vO M P f* WOotra't Pd H0t O-rl P PH rl o d >PH pOH p o P pOH p o p >% p rl H H P at P co >>rPH pOH PriPi Pf-i w dd pm Oo ` oo pp pH 2 p o p pH 2 p o p o d at p <0 rl CO IH'rHH W)Od Hd S3 P P O 1h PO O pOH PP H rH Prl at Prl at pw pco s N p PP wH o H<H St p P 'P CO rH CO 22 2*fc P P .rH dOPp cOPp oP p hOo bQ rl *H O pH OpH p OTp CO ait % rl GO u tp H PH O CO 6 p PO bJOO rl HO CO p H H P at p co > * PP H H 8O1 Hf-t S'0 H PO 'o H r--i co HH rl `H PP at at pco p m > t*. pP rl rl CO CO Oo o H O H O H p H p H O H O H O H O GO ?' COUOHHUO pppppppp PP dddddddd OOOOOOOO oooooooo M Pp odod bo o o oooooooo -HH rl H O O p p p -p p p p p CO CO p p + fl i il II + II II ll ll i ll + II I il + + il + ii ii II II II II Ik II I + II II |Hg &- O PhMiEM-s*! <e-! & q CO to co co co co co cow co co co co co co co co 000.0 00.000000 0 0000 B 6 S 6 S fi 0S E S fig E EB a E mmcNPPPPPpNmpPHP CM CM CM H Hrlrl co co co ooo BSE CM CM 01 rlrlrl m-4-mco PCMI PCI^ woirawwMrawwcowwP 000000.0 00000?* BBBBBEEEESEE( CM (MiOM) CMP CM CMPPPIN rH rH rH H H CM o OVCM m m O' miSO so inminin CO H m rlHOIOrlCftH tototocoto o cn o ON moo cMm rn H to m m tO-4- E-f PP HO (ACACvtO mP P Cn -O- O-Cv . i i i i i i i i i II II 1 p1 p1 t1o C^PP I1 1 mN ii S3 3 S3 SO 3 S3 S3 S3 & ppp p p p p p p p p PP M M A M A M A K S 23 mcM into mmmCM O On On CMO O OO O No n O MMnoN-toOOCMON-4-Oino O topiryMN-4-eooPmHCN-cMmmmmm fr-mPP CM CN-inmtOtOPPPPPPP rl f'<H Pto H mmmH mmm NO P p v Cn-P p p p nO p mppp I I I I I I I I 1 I I I II I I 1 S3 S3 S3 S3 S3 S3 S3 S3 S3 S3 S3 S3 EPS3S3 S3 III I I I I I I I I I III S3 3 S3 3 S3 3 p S3 S3 S3 S3 S3 S3 S3 S3 S3 M1-3 mmo c m in c m mP c m mmmmmmcM m mirvm mmcM c m mmmino c mpc m I 440'OOH4NH014-44'44'H4 toto.4- 44HH44tOOPHH oml c m c m cn c*Mn m c m n o m cn c m c m c m c m c m n o c m II I I I I t I I I I I I I I I I fN-CN-CM N CM mcnCM CM C^CN-cniNTCOP III I I I I I I I I I III m S3 S3 S3 S3 S3 S3 S3 S3 S3 S3 S3 S3 S3S3 S3 S3 S3 ppp pppppppppppp a M hO w" 3 . ap ao a CL. . . rl rl Hrlrl rlrr\OVYNr'M*N4,-4' ON ONONtOtOtO tOtptOtO On ON O' QN On O O HHrlHrlrlHrlHHrlH:CNCN CN-CN-C^ OOO C^Cn -Cn - Cn -Cv C-Cn -CNINNNCHWO HHHHininmininino-to CN-s-l^~t^->-C*-C^C^CN-Cs-L"CN. 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ABSTRACT----------------------------------------------------------------------- 1 II. REASON FOR REPORT------ -----TM 2 III. OBJECTIVES------------------------2 IV. CONCLUSIONS---- ----------2 V. FUTURE ACTION--------- ------ 3 VI. ACKNOWLEDGMENTS------------ ---------------------------------------- -- 3 VII. DISCUSSION------------4 A. Introduction--------4 C. Criteria for Analysis of Results--5 D. Experimental Design----6 VIII. TABLES-- ---*.-TM-- g I - 330 Line Dispersions Covered Herein--- S I-A-330 Line Dispersions Not Covered Herein-- 9 II to XVII - Tables Covering Performance--10 DUP030001724