Document vEwBx95gBR4xaJk8prdLdO8
CG 01 CODE YE-698-D
< DATE )
LZBZ7 ("l o t 7
5527* LBS, < EST WT )
PROCESSES < ) YE-698-D (T)
APPROVED &H-PUP 10/15/82
COMTYP JOB NAME: 01YE698DMT
BLENDED BACK:
(CODE)
EQUIP
USE ACCT
WENT
NAME: MOLYBDATE ORANGE
V\------------------ ~ l --
PREP
OBTAIN SODIUM SULFATE FOR S-13
"LB8S4--11
N-CODE
1 8-A
LBS
1 CALCULATE 6 SET ON BADGER METER F S-,16
gr 1 33-D(NITRIC ACID WEAK) 734 | 4-A 1 734OBTAIN SODIUM CHLORIDE FOR S-33 146 1 3-A i 146OBTAIN.SODA ASH FOR S-37 237 | 32-D 1 237OBTAIN SODIUM SILICATE FOR S-39 ' 350 1 3-A 1 350OBTAIN" SODA ASH FOR S-43 70 | 711-B 70OBTAIN ANTIMONY TRIOXIDE FOR S-46 mh 10-D |1 1885351 EIGH SODIUM CHROMATE INTO V-351. 1 12 OPTR____ , MK 'h/h
1 11 --OPTR___ MK_______ ,
!rr*3
\ --------\
11
Ii
423-D 1 303359 IGH IN SODIUM MOLYBDATE SOLUTION
13 OPTR.____ , MK kSL, T-3&_,4JSUtJX.
----- 1 i |1 ----wV;,OPTR____ , MK
T-_.___,______ %
358 RUN 10' <500 G) WATER INTO V-35B
4 11^4. Ru n v -359 in t o v-351 & p u mp in v-351
ADJ .TO 55* <2600 G>
SIFT IN N-108-A FROM Sir
STIR 5 MIN & RECORD : PH_/< 9/0-1 0.0)
ADJ TO PH 9,8-9.9 6 RECORD: PH_ZJ_7
(CAUSTIC SODA SOLUTION)
ASSUME 50%
I 7-D I
j ASSUME 66% .-TApfl 33--D I \4? ADD N-33-D FROM S 2 USING BADGER METER
i ADJ TO 66" (3121 G) AT 67-69*F
RECORD: VOL_A* 6 ___ ijLpF
L-.zx.jkii 8^1 STIR 5 MIN JL RECORD: PHJLJL (7 * 4-7,6) &
G/ML
080-1.083)
NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK LIST & ATTACH. TAKE 1 QT SAMPLE
Npy 5 J982;
,
sv RUN 20* <996 G) WATER INTO 5 RECORD N-4T-D STORAGE TANK TO PUMP FROM. (CLE ONE: 402 410 411 420 424 425
CHECK WITH CU SUPV:
^STORAGE TANK MUST CONTAIN AT LEAST 2376
GAL: 402-49*, 410=25", 411=48", 420=25*,
I------
424=25* t 425=31 * ^STORAGE TANK MUST HAVE STIRRED AT LEAST
20 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL
UJ
PUMPING FOR THIS BATCH IS COMPLETE SET METER FOR 300 G & PUMP TO SV
N40881
LOT,: __ EQUIP
---
COMTYP JOB NAME: 01YE69SDMT
MENT i
PAGE 02 `
------ _____----------------- ,--_______________________________
SV 122 AT APPROX i 00 G WHILE CONTINUING TO PUMP,
5|
CHECK PH & DENSITY, RECORD BELOW, IF NOT
CQNT |
IN RANGE, STOP PUMPING & SEE SUPV,
* PH:_____ (2.2-3,7)
DATE PRINTED:10/45/02 I USE 1 N- IACCT*
I LBS | CODE I LBS
I|
i.
1 ~" |
i "~
||
l\
* DENSITY: _______ G/ML (1 .270-1.323) 23 IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
I. |
DENSITY ______ G/ML ON TRAPPED SAMPLE
|I
|
FROM END OF S-21 PUMPING.
'll!
24 USING DENSITY FROM S-23, FIND METER SETTING FOR |
||
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
|
||
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21.
|
l|
CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
|
||
**** TABLE ****
111
G/ML 1 .270
1 .271 1 4'?7I 'A?
1 .273 1 .274 1 .275 1 .276 1 .277 1 .278 1 .279 1 .280 1 .281 1 .282
1 .283 1 .284
1 .285 1 .286 1 .286 1 .287 1 .288 1 .289
1 .290
SETTING 1 G/ML SETTING 1 G/ML 1678 1 1.291 1534 1 1.312 1670 1 1.292 1527 1 1.313 1663 1 1.293 1521 1 1.314
1656 1 1.294 1515 1 1.315 1649 1 1.295 1509 1 1.316 1641 1 1.296 1503 1 1.317 1634 f 1.297 1497 1 1.318 1627 1 1.298 1490 1 1.319 1620 I 1.299 . 1484 1 1.320
1614 1 1.300 1478 1 1.321 1607 1 1.301 1473 1 1.322 1600 I 1.302 1467 1 1.323
1593 1 1.303 1461 1 1.324 1586 1 1.304 1 455 1 1.325 1 580 1 1,305 1449 1 1.326
1573 1 1.306 1444 1 1.327
1 566 1 1.307 1 438 1 1.328 1566 1 1.307 1438 1 1.328 1559 I 1.308 1432 1 1.329
1553 I 1.309 1427 1 1.330 1546 i 1.310 1421 1 1 .331
1540 1 1.311 1415 1 1.332
SETTING 1410
1404 1399
1394 1338 1383 1378
1372 1367
1362 1 357 1351 1346 1 341
1336 1331 1 326 1326 1 543
1537 1532-
1526
I25| SET METER i, PUMP_______ G (RECORD FROM TABLE)
|
I I FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY |
I I 30 SECONDS
|-
1261 ADJ LEAD NITRATE TO 76' (3625 G) AT 67-69*F.
|
I I RECORD:_________ *F
|
1271 STIR 5 MIN 6 RECORD PH: _____ (2.2-3.7)
|
1281 IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 66% j__
I I 6 RECORD PH:___ __
ASSUME 50%|__
I I NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING|
1291 RECORD: ______ G/ML <1.143-1.144)>IF OUT OF SPEC!
I I FILL OUT CHECK LIST & ATTACH.
V
|
|30| STIR AT 67-69*F FOR S^31. TAKE: t-GTF SAMPLE.
j, f-
41 --D 57-A
33-D 7-D
51 f0~"
DUP050059674
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XDMTYP
JOB
NAME-*. 1YE698DMT sixVjT.
- PAGE
02
;. -^-.-" 'T - .; s i?:v.. . -T
| - TT- - .j> ,t
...
^ .' , -
I^TP APPROX;! 0 WHICONTINUING TO PUMP,
CHECK PH & DENSITY
) BELOW* IF NOT
IN .gg^g^STOP ; PUMg|j^g^E^U^?;. ..
DATE PRJHTEDjiiA02^e
1 I TJSE^r^-:^|ACCT | -LBS^^ODE^n__'
j -.-.av '.v str^y
?:S^22fOKM WHEN #g21CPMPUETEir RECORD
DENSITY!
^G/Wt^PNirRAPPED;5AMPLE^;
v..
USING DENSITY FROM%^3WiElND-/METER'SSETT.ING FOR
SECOND PUMPING IN/TABLE BEL0W.7 NOTE.;/TABLE-
ACCOUNTS FOR 3 ,G ALREADY PUMPED IN S-21. CIRCLE DENSITY ^^SETJTN&.IN TABLE BELOW.
****, TAELEs**** , i:
' .-
I v. ^Vrrvr*^'l .. -V* 3.s-;<288*M
-*?>. -|*| .V.V..V.yvl,~Y iv .
SS?-5* i - - ? SSfcS I1*!-. | ' ' V ~ ->" '
I ' -' S'V I:
1 G/ML SETTING ; 11'.27 1644 v
I 1.271 - 1637 1 1.272 163
1 1.273 1623 1 1.274- 1616 **Y* 1 .'275 * 1609 1 1.276. -: 1602
I 1.277 '1595
1 1.278 1588
1 1.279 : 1582 I 1.28 -- -.*..,1575 .
ms6&
.. . -^;.t.562 1:283^1555 1 284-. 1549 1 .285 *%?' 1542 1 .286 1535 1 .287:?' 1528 1.288. 1522 1.289. 1515 1 .29 151
1 ^;G/ML:aiSETTING i G/ML SETTING|
1 ;::iS29l|^154;;:-- i 1 i312* ; 1382 | --' Ki:
1 - Ti292-';^1487~ i 1.313^ .. 1376 |
' ; f' { 'SW,
1 1:293/.^im91 i 1.314 1371 |
.. ,rc..;1;-;.
I i:294^^85-i;' r 11315- 1367 |
1 1^295;sf-;l^79::-- i 1.316 1361 |?
i 14'296 :::^1473 i Ti317 1356 |
i 1J297:4SlA67 ' i 1.318 : 1351 1
! 1.319 .1345 1 1 T559I.. -1455 '\ r.3i ~ ^m |
1 1 r3e ;T 448 j : 1 32.1 1335 |
1 ,1^|U^1r444r l 1.322, v- -.133 | - ? U;vvv:;-I. *11*323*# 1324
324. V/ 1319 1315
I 1;.32js' 131
.1 .. .>. frt--m-- P----^A-- J;'r a!*** J
II
;-.|.'-l327~' 135
1:301
I .11328 13
1^3b 1
h"1L329 1295
1I3<
1:^3 1290
ilfzmj
. I 11331 1285
1*311
I 1.332 128
I25TSET METER 6 PUMP UfcLLjZ (RECORD FROM TABLE)
| | FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
| ( 3 SECONDS
I
^ISiirr'ADJ LEAD NITRATE TO 3625 G (76*'-242/245 6 74.5* 1
I
| | -247) AT 67-6gF I L-RECORD: ___ 6_Jl -*F 6 ICE CONSUMED <334=/BL0CK)
l2<| STIR 5 MIN * RECORD PH: _0_ <2.2-3.7)
|330XJL I
* ,L ***# USE TITRIMETER TO ADJUST N-41-D PH ***
IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 66%
| & RECORD PH:
^
ASSUME 50%
NOTE: DILUTE N-7rD 10:1 WITH WATER BEFORE ADDING
RECORD: Jl L1i 2l G/ML (1.143-1.144) IF OUT OF SPEC
FILL OUT CHECK LIST 6 ATTACH. STIR AT 67-69WF FOR S-31 . TAKE 1 QT SAMPLE.
41-D 57-A
33-D 7-D
j 511 \2JLjL
I---- L.
.k
DUP050059675
LOT: EQUIP
COMTYP JOB NAME: 01YE69SDMT PAGE 03
DATE PRINTED:10/J 5/82 USE N- | ACC? LBS CODE J LBS
TAIN 1 GJT SAMPLES OF S-18 & S-30 SOLUTIONS & TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
7,1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0,10 ML N-10-D <IF YES, FLUSH ALL EQUIPMENT , REPEAT TITRATIONS), DO NOT
PROCEED IF N-10-D TITRATION IS OUT OF RANGE ADJUST V-358 FOR A TITRATION PH OF flnCO.Tfr-2.20 FROM FINAL IN-LINE TITTRRAAI^^OIOJi^, RREESCORD LOWEST PH & ML N-10-D
it
33-D | 7-D i
WHEN S-31 TITRATION OK , STRIKE V-358 THRU
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN RECORD: START
/fTOTAL MIN.
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
6 BUBBLES APPEAR IN SIGHT GLASSES
IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER
FOR 15 MINUTES
DURING S 33, WASH IN V-358,
Jr_STIR 2 MIN 6 RECORD PH__A
PBXS,__
(MUST BE + )
(1,8-2,5)
STIR TOTAL OF 15 MI^JROM S-33 & RECORD: TEMP__/-A__tfF (67-73*F)
DUMP N-3-A FROM S-4
STIR 3 MIN
POOR IN N-32-D FROM S-5
STIR 2 MIN
RUN IN LIQUID ALUM USING BADGER METER
STIR 3 MIN & FLUSH ALUM LINE WITH WATER
DUMP IN N-3 FROM S-6
STIR 4 MIN FOR S-48
734 115-0 367
Ii I WT\
f
RUN IN HYDROCHLORIC ACID USING WEIGHT i, FLO
CONTROL PANEL `
MK
MK ______ ,
._____ %
DURING S-44 SIFT N-711-B FROM S-7 INTO V-390
WITH AGITATOR ON IN 1-2 MIN
STIR 1-2 MIN TO MILKY SOLUTION
S3J&S.
28-D 28-D
105
WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES.
niiMp TW Rl AWP FTXF N
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP OF PAGE 1 -
___
RECORD: CODE
LOT
STIR 20 MIN / ^
RECORD : PH_________ < 5,8-6.0) .
! 53'' IF NECESSARY, ADJ TO PH 5.8-6.0
ASSUME 50%
& RECORD: PH-___fcssr^__.
ASSUME 66%
154' FLOOD TO 153* (7298 G) & STOP AGITATOR
jr
330v I 1i 28-A 33
7-D 33-D
1
DUP050059676