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9osy,t,_ on_, _. A Ho_a_pmA. 19o44 TeJepho(n2e1:5)443-8710 r_: (2ts_443-8s87 ARGUS RESEARCH CharlesRiver Laboratories DiscoverayndDevelopmenStervices September 11, 2002 John Butenhoff, Ph.D., DABT, CIH o oate 3M Medical Department 3M Center, Building 220-2E-02 St. Paul, Minnesota 55144-1000 Telephone: (651) 733-1962 Telefax: (651) 733-1773 IF_/_ _ [_ _ _ ['_ _'_ ox [ 2 20ff2 I RE: Protocol 418-020 Dear Dr. Butenhoff: Oral (Gavage) Two-Generation (One Litter per Generation) Reproduction Study of Ammonium Perfluorooctanoate (APFO) in Rats Sponsor's Study Number: T-6889.6 Enclosed are the copies of the estrous cycle evaluation for P and F1 generation rats which you requested. If you have any questions, please do not hesitate to contact me. Sincerely, Ann Frazee, M.S. Study Coordinator Eric. 00294_ ESTROUS CYCLE EVALUATION P GENERATION FEMALE RATS ii "ix I_EXACTCOPY i Oc_q_q-7 _, PROTOCOL: 418-020 DOSAGE: 0 (Vehicle) MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: P Oral (Gavage) _TYPEOF TEST: EstrousCycleEvaluation SPECIES/STRAIN: Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ I.i-bl i,/,-0(1.3-_1_,'_-01/-_-o_t-_ _-q-oi-_,,L -,_-o,_.,0.01, -11olIIJz_ t'l_'_ :J-_ 1 2 3 4 5 6 7 8 9 10 11 12 13 14 . SaliTneecPhr/eT-iCmheeck 112.3 IIZ_ 11_]5 il7.,o tl_ t1,._... u,t'/ t,'_k _3 I1_'_ 113_ Saline PostCheckTech/Time IZ.eo 1155 @.._:_tl"3u I_o_ _tH'l Xl_ _:_ '_ _ 121_ _ _l_ X_=_"_ Smears Taken _J/_=_.._1,*,__.=1,., Smears Taken Time End SmearsRead fl_ _5_ _ I_51 ,._3,_ _&_,._ o_c U)__ _y_ _._ 3_ Smears Read ..... Time End It._.z_ /LH5 |_q5 _ .d_A tt'l'_ 11_1t_" "_;q I,_l_1_00_1_ i/.5"_ _t-0_ IzOI I1_'_ i_l "i2_ _ _P_ "_ Animal Number 13801 _ _ "_ F. _ _ 13802 "1_ "_ _.. _ _> _ ' F__m.. _ _ Z; _ D E_ _ _'_ I_ _ _) 138o4 C E, _ l'__ _ _ _ _ _' E _ [::, _P ,_ 13810 e _,-2_=. _p b _z E b ) F E b D O ' Review. By: _, _/'/_._..: Date: ,'[d'_R/ T 01.14.00 EC2_04a__/ _%_ ,/_/o, _5__'_._- _ _ ,._-.= _,,-,-0,__ '_,_'".,_,(__"Z"__0,l'_l_, N_'_:_o-_=,,l_-lo,;,_,,_._5_.b,I,_,itoF'0X_A_C,T,,,C._O" PY]: 002948 PROTOCOL: 418-020 DOSAGE: 0 (Vehicle)MKD = = Proestrus E = Estrus M = Metestrus D = Diestrus DATE AnimalNumber Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: P Oral (Gavage) TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD_ (SD) IGS BR VAF/Plus(D I-_-bl I.'_-t_ _-_,Oi ttqlbl _,_.o_l,f_,_ F'7-6( I._,_* 1..01 i.a.el i.i/.ol a'_.ol I-I_rdl H=l-_,x 1 2 34 5 6 7 8 9 10 11 12 13 14 13810 %E 0 _ E r_ _ .- 13817 IV_ _ (3 _ ,_ _ I-_ _, D _C_ _) _.._ 13820 P C- _ p -_ /v_ K P _ N i ..... 1_28 e C- ,b P ; _ E. "b b .i 13829 _ _ "b' b 1"3 _' /V_ b . P & N[ b _ ...::; 1383o E: b b _' _ 0 D P E ) t'> D ,r_ _ .. c. I-I-t31 Reviewed By: _ ' '/_, _-"_Z .. Date: :_: I-[f _ I ._ RT 01.14.00 EC2-04b - i EXACTCOPY 1 :_ 002949 PROTOCOL: 418-020 DOSAGE: 1 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: _ Oral (Garage) TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ l_l-_ll.;-bl1.5o'l1',1__t._.o_i._( _-_(_-z.o,,._._,1.,.o/,.zl.o,.l,=.6_,, I_,_, L 1 2 3 4 5 6 ,,,,, 7 8,, 9 10 11 12 13 14 AnimalNumber ......::... 1133883356 "p1_ i(:_:::: '_ ,,. (_.j - " 11338387.38 ,p _ -3_"L_ _ _ __" _,AA, E_ , _ __.. 1_D "_,_...b. _D_ 13849 _ "_ _0 '<C , ._ _) _. .._ J_ Reviewed By: _/ . (_) "_1'1' _ _ ,_ [. _/-oJ ' _.,,-o, I Date: /.- [_'.d/ RT 01.14.00 EC2-04b , _/t_"_ ' __"_:_e _/"/fEXACT COPY 1.i: 002950 pROTOCOL: 418-020 DOSAGE: 1 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE AnimalNumber Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: _ Oral (Gavage) TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/CrI:C,.D_(SD) IGS BR VAF/Plus_ I i-_.0.{ =14.-oIi,_l 1 2 3 V_l= i.(,_ _ 456 t-P( !_._, _._.6_I._.ol 1.1J_,t-0'_' I_ _, 7 8 9 10 11 12 13 14 ...... 13854 t'_ . _ I_ <_ f" 13858 _ _ b "b. b E _0 b b _;_g-"b _b B z, :: _ 5 Reviewed By: _-!ii /]1_, _. Date: I "! _'.(Y/ RT 01.14.00 EC2-04b .... 002951 ,,, PROTOCOL: Argus TEST ARTICLE/SUBSTANCE: :, TYPE OF TEST: 418-020 DOSAGE: APFO GENERATION: ROUTE: Estrous Cycle Evaluation SPECIES/STRAIN: 3 MKD P = Proestrus E = Estrus Oral (Gavage) R.at/Crl:CD_(SD) IGS BR VAF/Plus_ M = Metestrus D = Diestrus DATE B /--z-c/ i-2-Oi I._0t 123 V,_/_! l.s.ot /_-_1 V3-61 =3.o_ I.'_, 4 5 6 7 8 9 I..= /.It-el i.,;,.=, _-_1 _-_,_.,,_ 10, 11 12 13 14 Animal Number ..... 13866 _ !_ ,,,,, bE _ _ P g E ,E_) L._ 13871 _b P 13873 E b _> E __ 9 C) g _ .,: b _--:E) .i Reviewed By: - Date: 1"lS.d / ,,::_ RT 01.14.00 EC2-O4b ',,= = I-EXACTCOPY i " 002952 =ROTOCOL: Argus TEST ARTICLE/SUBSTANCE: TYPE OF TEST: 418-020 DOSAGE: APFO GENERATION: ROUTE: Estrous Cycle Evaluation SPECIES/STRAIN: 3 MKD _ P = Proestrus E = Estrus M = Metestrus D = Diestrus ._ Oral .(Gava,ge) Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ DATE //'_ l'2'0| /.'_.0| Vqlo_. ,.6,, t4.=_, I-"r,i f,'_._l I'c_'_l I._).oI _I'l.O( i.,z_, 1"/3-oil,-_,,, 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Animal Number 13882 -...... .,138s. 199 b _' _n, _) :_ & _ b _ _. lj_ ._ r_ _ _ _.. _ O t _ O I) _> 11) _- C) ,,.13887 E _ "b (,_.! e D _ P F_ m "b f __, 3 13889 _38oo _ _" _ _ __ _ .b _ _--_ _.,..b _ _) _ _ "_ "_ _._ ,_ F _ F_. _ "p _ ._ ,,,, _ ,, ,,, ,, , ,, ILl Reviewed By: /_ ,_" Date: 1"(5.(_/ RT 01.14.00 EC2-O4b _EXACTCOPY Lu/ ...................j.. 002953 PROTOCOL: Argus TEST ARTICLE/SUBSTANCE: TYPE OF TEST: 418-020 DOSAGE: APFO GENERATION: ROUTE: Estrous Cycle Evaluation SPECIES/STRAIN: 10 MKD P P = Proestrus E = Estrus M = MetestTus D = Diestrus 'Oral (Gavage) Rat/Cd:CD_ (SD! IGS BR VAF/Plus DATE j.i-ol i-2-b( I-3-_{ _/qJ61 |,..o1_-/,,-_i1.._ c._.o,' I._._L I-_.ol _.11.1)1i._;L.o, J"l_ I-_, 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Animal Number 138_ 13895 -_ t_ _ m _ -P F_...._.. b b E, _, -_ O -b _ _ m L_ _) "__....' _'_ b _ _ Cr3 _ _) 13897 L: ,.,_ "_ _) _ _ _) ._._ _' _) i'_ _ __ 1_02 -o _ _. _ 139o3 rn "_ _ & 13904 m b _ ; _ P E m_ _ o h P p b 0 .t_ lb E. _ _ '_ _ F_ _ 8. .,_ i) _ _ or Reviewed By: ,l_>l,I /_= _ Date: /'/',_-t / RT 01.14.00 EC2-04b 002954 PROTOCOL: Argus TEST ARTICLE/SUBSTANCE: TYPE OF TEST: 418-020 DOSAGE: APFO GENERATION: ROUTE: Estrous CycleEvaluation SPECIES/STRAIN: 10 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE Animal Number 13910 13911 13912 _ Oral (Gavage) Rat/Cd:CD_ (SD) IGS BR VAF/Plus _-I-Oit-21'oi(,_o(lY'llo, I._,.olp_,.,_[r_-_i I.t.o_i._.61 I,_._, /./(-0tl_""_=_f_oi l-,,l-_ 1 2 34 5 6 7 8 9 10 11 12 13 14 -_ P E _ b b F_. m _ _ _ N_ _ "P Z. D P b F_. b _ L: '% b O g (3 % b L F _ 0 C) b ) _ _ b ,D I_ 113399141_ ..._._. "bb _E,, _ Ie> Pg tP_ _P FL _ D_ gI) Pf _c- Jh 13916 E T_ _ f e 5 P. P g b "b P _- 13919 _ _ P E _ (_ P g b ) _ g _1 D 13920 -'_ b _. _ P'_ P ___. F__ _ _) _ (__.. _ _ ,, " '' Reviewed By: __ _ _ _ Date: (" t_.#/ ! RT 01.14.00 EC2-04b . I-EXACCOTPY 002955 PROTOCOL: 418-020 Argus TEST ARTICLE/SUBSTANCE: ;APFO ITYPE OF TEST: IEstrous Cycle Evaluation DOSAGE: :30 MKD = Proestrus E = Estrus M = Metestrus D = Diestrus GENERATION: P ROUTE: Oral (Gavage) .. SPECIES/STRAIN: Rat/Cd:CD_ (SD) IGS BR VAF/Plus@ DATE H-o/ i-_.01 ji._,0_ _/q/b_ ,.S.oJa-/,'=! ii_-m ,._.ot r.'ro, 1.00_, /./i.ot i.,=.o= H_o/ii-Pl_ 1 2 3 4 5 6 7 8 9 10 11 12 13 14 _,nimalNumber 13921 -_ _ _ o D P E z> _ _ _ b o P 13923 E_ _ -_ _ E _l_ b 3 _ _ _'_,,, _) .... 13925 13926 E _ "_ ? _ _1_ r_ _ :_j _Y_ _ _ _ 0 "_ _ _ ('_ _) p _ _ _) _P _" _ _ .'_ 13927 -r_ _ i_ L_ p _ m _) _ _ _ "_ _ 13930 "_ _ _ _'_ _) P ..._ "_ __ _ r_ _ .._ 13932 _ _ P E. _ _ b E. _ b 3) E ,_ _ 13935 _" (_ _ # _P F_ % bZ _, m-_) 0 ':i. 13936 E _ "b o _ h P _ 'b P b _ 0 13937 'Z) "_ e Z, b p p ;. :b -_ "_ ;. o b .. _(_)])P I.It.ot ,-: RT01.14.E0C02_b ' EXACTCOPY_. 002956 , PROTOCOL: Argus : ......... TEST ARTICLE/SUBSTANCE: ,.,. TYPE OF TEST: 418-020 ,=,, DOSAGE: APFO ,, GENERATION: .......... IROUTE: IEstrous Cycle Evaluation SPECIES/STRAIN: 30 MKD .. , P : P = Proestrus E = Estrus M -- Metestrus D = Diestrus Oral (Garage) , , ,, Rat/Cd:CD_ (SD) IGS BR VAF/Plus , ,,, , m,,, .,. DATE Animal Number 13_9 t./-o/ _i-_.-ol _-_01 Y'f/ol I._.o, t-_'#( i'_ot 1 2 3 4 5 6 7 E 'b "b ib E "fq _ _'__. I,.o_ i.,o-m I.It.ot /.!_._.. H_( Hq.o, 8 9 10 11 12 13 14 "_ ? ? _ m -O ::.... _3_945 -_-o c#- E mb _O1).p _ Lrq. 0b ?, E_, , rzn::>D-_ # _o ...=., t:::, b : P E _ I::', E_. _ _, "b P' f_._f'4 ,_ ,,,, G@_.. _-5.o_ Reviewed By: '_ , __" ::, =. Date: [-!,._'.(_/ RT 01.14.00 EC2-04b 002957 3ROTOCOL: 418-020 DOSAGE: ',0(Vehicle) MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE Tech/Time Argus TEST ARTII_LE./SUBSTANCE: APFO GENERATION: ' I_OUTE: ... = .... Oral(Gavage) ......... ,,t<S.olm(,,,,I H?-o, !-4-'| /;/_,_, II1_1*,_//01 12 34 s _z 8 It ;3:)s_ V..c _ :7_ ds_ _./_.. TYPEOF TEST: EstrousCycleEvaluation !SPECIES/STRAIN: Ra..t/Cd:CD_(SD) IGS BR VAF/Plus_ / / 9 lO 11 12 13 1,4 I CheckTech/TimeiZ06 lit{?_. |_5"_, 1_0 I1_"_ "J_ .... I Saline Post- _L,/ '_ Y-._'tL _ IL_Ic I_'_(_!'_ / Tech/"l'imeStart li_, ?_lh_P'rT'"_" J_'/P_ "SmearsTaken '/ : -_. TeSchm/TimeeaRrSsetarat d'IvZo_l ( _3 I1_'_ _ '_12,01 _I_'_--'t- __I,'L_ __. ;_'_ ' , Time End I_'_ l/lvO tl_Lt |l_q _ _ IL_(Q IL_ / "; Smears Read' " _$ " I' Time End _2_ I?__.C_I_0_ ji_'_t 1_'_3 I"b3i'e i ii _ Animal Number P _803....... O E b b D E _: 13804 _'_ '_7 {9 .,_ _-) ,, / " '" " 13807 E (YI b _) E , ._. _). _8_o _-- _ t_ Reviewed By: ,--) 5 __ D.,. E b0 _ r_ t_ /_ e;D / Date: (_ A_;n'_ _ _r/_zumd,_/_'_J. _ 'h,t/a/ "_: !_ RT01.14.00EC2-04a ;'i_ ::; .... .. 002958 PROTOCOL: 418-020 DOSAGE: Argus : , TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: =, ITYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: 0 (Vehicle).MKD P P = Proestrus E = Estrus M = Metestrus D = Diestrus Oral (Gavage). Rat/Cd:CD@(SD) IGS B..RVAF/Plus@ 'DATE ,,, 1,1.%1I-J6ol I.iT.o/ 1.0'_._ I-I_q I.z,a.oI !-Zl,._e / 1 2 3 4 5 6 7 8 9 Animal Number 13813 i_ _ _ _ o P _ 13814 _ D _ ,o E ,_ ,O 13815 _" '_ m V_ D _p E 13816 P _. 011 _ _ ? 13817 e" _ rn b, E 6 .m 13818 P 21 01 "b P a m _,,_9 _ m-p y_.,E. _ D ....... 10 11 12 13 /4 / / / / /,,, / / 13821 h D F_ _'_ D p e / 13822 13823 _ 'J_ P_ p_ }_ D p _'_ D ;_ "L_ 7/ 13824 _'- _ _ _ O6 _ / / 1382_ _ _ b b _ _ m / 13826 _ _ _ _,, D p _, 13827 b _- _ _ J_ p I_ 13828 /1_ b ?_ PD P / 13829 I%j b P _J D D P / 13830 b _) 6 b PP 6/ '" 't J' .,, ,, ,., ,: Da,e. RT 01.14.00 EC2-O4b 002959 PROTOCOL: 418-020 DOSAGE: 1 MKD = Proestrus E = Estrus M = Metestrus D = Diestrus Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: _ Oral (Gavage) DATE AnimalNumber 1'15.oit._,._, t.m._ i_.o, 1 2 3 4 I-_-_ !-=,_1 t._I 5 6 7 13831 13832 13833 _ _ b_ _." "_ "_ "_2 E_ _ _ p O E rI") o_ e L-" r13 !E) TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/Crt:CD_ (SD) IGS BR VAF/Plus /,// 8 9 10 11 12 13 // "....... 13835 t_"_ _ _) p E _'_. ' 1133883634 c-- .m -_ P E E) E) / 13838 13837 113383_9o O f _ b _ -T_ p _ NE bP _) _ 0 O9 P _ _: LOr _b _E) ..... / 13843 b (2 E. _ o p g t 138_.5 r_vl _ pf g_- o _) pp / :-.- 13846 L_-_" _, ri_ b 0e6 / +. 13848 ,0 9 g. h o e / 13849 P ,_f_.... m b f'ft / i RT 01.14.00 EC2-O4b = ,:_EXACT_"O_OJ',,v' _._..- qkilo _- ........ : _.' ....... : ........ 002960 PROTOCOL: _18-020 i= 'DOSAGE: 1 MKD = Proestrus E = Estrus M = Metestrus D = Diestrus DATE , ,. Animal Number 13850 13851 13852 Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: P Oral (Gavage) ' "I' I-I_ol, j.,_,_j _.61 I.,t ._ I-_.oI-_t=.ol (-_IPoI! 1 2 3 4 5 6 7 8 ., _ _ V C '_ r) __ _b _ i'n b o _ e, _ ['_ _ _ D_ TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD_) (SD) IGS BR VAF/Plus_) /t 9 10 11 12 13 /14 / / / 13853 '_--,--13855 13856 44 t::) P _ -_ P _ _4 D p _ D_ p OD P O D iP / ./ _r / 13857 _ "_ _ WI _, _" / 13858 _ 1;) _) E- 0 b D / 1385_ P F_.._4 b P ,_ _ / 13860 I'_ _ _,_ _1_ O P _ /" / ,, ,,, , ,,, ,i / / / ,,, / .../ , .... _ ,,, ,,, _ __ i,,, u _ Reviewed By: Date: .. > .i/- RT 01.14.00 EC2-04b .... ' _ ',F, _' t l;__u_ ...j; 002961 PROTOCOL: 418-020 DOSAGE: 3 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE !Animal Number Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: P ROUTE: Oral (Gavage) TYPE OF TEST: iEstrous Cycle Evaluation SPECIES/STRAIN: IRat/CrhCD_ (SD) IGS BR VAF/Plus_ 1.13_.0I.1,_,.m I._/.ai -,t_' 1234 1-1'1-_I-Zo_l I-_11_1 56 7 8 // 9 10 11 12 13 1 4 / 138612 b _P g_- b oo _pp ep / 13863 _ _ I-_ _2 _ _) _) /" -. 13862 _q _ P F. D _ p 13868 _ f _ b O p Z 1133886679 _1_ _"E) _CL_ mb DO b e_" / 1,33887710 I/3---T_b 3fP' __'. EP" D_ PD / -: 113387837. 13876 138n _ .4 b (vl _ __ f. OO _ P_, _ f'. o _ p P f. e- _ n 13879 I_ b _1 Db /_ / jf / Reviewed By: Date: .; -: i!. - :_ , ...y: ' }:i / RT 01.14.00 EC2-O4b I- XACcTOPY[ 002962 PROTOCOL: 418-020 DOSAGE: 3 MKD P = Proestrus E = Estrus M = Metesl_JS D = Diestrus DATE Animal Number 13880 Argus ,m TEST ARTICLE/SUBSTANCE: APFO !GENERATION: P ROUTE: Oral (Gavage) I.t_'_1 I.l,_l t.(I.O# l,il-_t I-Pi-o I-zo_ lill.=l 1 2 3 4 5 6 7 !._... _ P _ _ _ p TYPE OF TEST: Estrous CYCle Evaluation SPECIES/STRAIN: Rat/Cd:Cl_i) (SD) IGS BR VAF/Plus_ / 8 9 10 11 12 13 /14 / / 13883,,, rfl 0 _ _ 0 b _ f a,_ " " 13885 _ m _ E. _-",.e, 6 13886 E _- 171E- _ _ _ , / / / / 13887 _ P_ b0 9_ / :. 13888 D .... O. i-_") ,__... 0 _ p Z/ :" / / )1131 l-i_-='i e_ j,,,,,/'==. J_ ....... ::_:: .:.+:.:- ':_ RT01.14.00 EC2-04b ._, :i . _. _'-E-_ACCTOPY : 002963 PROTOCOL: 418-020 DOSAGE: 10 MKD P = Proestrus E = Estrus " M = Metestrus D = Diestrus DATE AnimalNumber 13891 13892 Argus TEST ARTICLFJSUBSTANCE: APFO ..... GENERATION: ROUTE: _ Oral (Gavage) I'l_:d I-Ila,o=Hq.OI !1,111..6..1PR-' _o_1 I-,11-_1] 12 34 5 6 7 ...8. ,3 D _ b T_ _ r_ o _ .D D ..._ p _ TYPE OF TEST: Estrous Cycle .Evaluation SPECIES/STRAIN: Rat/Cd:CD_ (SD)IGS BR VAF/Plus 9 10 11 .... , ?/ 12 13 / / / ' 13895 ,/v__ i_ ._ _ _'_ I_1 _) -- 13896 lE _ _X> E 1> tb 138_ _1 t> P Y__o. D ? 13899 P 3 h _ o d O 13..991 _ E. iXl _ 0 P e / / / / 13903 _3_ 13995 ... 13906 13997 IP ___.. I'_ "_) J_ _ m /3 5 _. _P F' o o, _ I) T) P E .6 _b 1# ., /' / / ._ _ __ r_ D _ _ 1/ _ _ t:::' ?_...D _ _ ... _' _:i Reviewed By: _ Date: '_: RT 01.14.00 EC2-04b 002964 PROTOCOl: Argus TEST ARTICL_SUBSTANCE: TYPE OF TEST: 418-020 DOSAGE: 10 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus APFO GENERATION: = ROUTE: Oral (Gavage) !Estrous, Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ DATE _)i_,-,_ 1 2 !.rl.01,1.ol i-_= 34 5 i.zool 1-31-el 6 7 8 "/ 9 10 11 12 13 / /14 Animal Number 13910 13911 13912 _ "b _ ,ITI _ D D _ _ B _ o 1_ 13 _I -_ _ _ E D i) / .,/ / / 13913 _" _- ('_ b O _ ]_ / .... 139126 _b f__.. N_ _b oP p_ _em 139178 __ b(_ _- ',bb _o _p P_, / / 13919 {._,_ _ _ _'_ I_ E" ITI H ,, ,,,, _ _0 V-I'rf.ol ReviewedBy: Date: i, .::il '_ RT 01.14.00 EC2-04b ;._._--!_,_-..--__-:-:-->._,.-_ 002965 PROTOCOL: 418-020 DOSAGE: 30 MKD ....... P = Proestrus E = Estrus M = Metestrus D = Diestrus Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: P Oral (Gavage) TYPE OF TEST: tEstmus Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD(D(SD) IGS BR VAF/Plus_ DATE 1.1";,0]1l,l,e! il-r/.OI I._._1 |-Ppot I-zo.=111-31.o ., 1 2 3 4 5 6 ,, 7 8 9 Animal Number 13921 13922 13923 ...... _ _ _ "_ .__ -_ D _ _- ,._ 1_ T') _ E" _) _:) _ .__,,, O _ 13924 _ "_ f _ D E, P 13926 13927 _ mb 0 E" D '_ _ "_ "_ _ E" _) =p 13928 13929 IN'} _ _ _, D _ i? .... L_. _" _ E, {Vl _ _: . ,. 13930 t_ m __ _ E" p I 13931 _ I0 _., i'_ O _ .... 13932 P _ b o b, 13933 t_ .-_ ?__ nl c, _ .,,_ /,/ 10 11 12 13 // // / /,j '" / ... / / / 13935 _ _ i(_ _ &-- D ] _ ./ 13936 _ _ __-_ D {{_) _ / 13937 E _ "T_ _ I_ _ !_ 13939 _," IT) b .ev,ewe_: __ - P L--" D n / 0--: _ _-._._ .-._-..d RTo1.14E.oCo2-_, 002966 , : PROTOCOL: 418-020. DOSAGE: 30 MKD P = ProestnJs E = Estrus Argus ., TEST ARTICLE/SUBSTANCE: APFO GENERATION: _ ... ROUTE: Oral (Gavage) , TYPE OF TEST: Estrous Cycle Evaluation ISPECiES/STRAIN: Rat/Crt:CD_ (SD) IGS BR VAF/Plus_) M = Metestrus D = Diestrus DATE .,o I1_-01 i.,_,'__..,_.o,.,_.o,i._-ol,,z,,oI_-'_ b 1 z 3 4 5 e 7_ _s._, 9 lo // 11 12 13 A4 Anim1a3l N9um4b0er 6 F/ _ D P _, _ 1394_2. _m'I -_P _ __, oo __b ?P .... ._.._ 1_3.9343_ __- "m_ "-__ _fj> E0 ,,,m_ ,_ _._ 13943 d t4 _ "b e m n .... / / / / 133994487 1P3 E_, P_ q Ib-) _o Ip_ _: / 13950 I_ _ ,P., _) _ _) _ !/ .... ,, ,,, _ Reviewed By: %_ O_o RT 01.14.00 EC24)4b ,I,/ol Date: ,/_._ '_' I EAoOOfP,,q 012431 ESTROUS CYCLE EVALUATION F1 GENERATION FEMALE RATS PROTOCOL: 418-020 DOSAGE: 0 MKD P = Proestrus E = Estms M = Metestrus D = Diesltus DATE" Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: F1 ROUTE: Oral (Gavage) 012432 TYPE OF TEST: Estrous Cycle Evaluation SPECiES/STRAIN: Rat/Cd:Cl_b (SD) IGS BR VAF/Plus_ J _-z-ol 4/_, _/_j _t_t :_'l_'O_15Lz"_i_-_,I-- _;s-al S'-M-e__-n-_l _J_0t F-_J __o_ _--_i 1 /2 " 3 4 5 67 8 9 10 11 12 13 14 Saline Pre-Check _'P" _ TecW13me /23S ,_ _ (}o '(_ _/.t= _ _ ._C _ _ _"_-"_ NIICF _) iz4L- tl,it# 19=j_ _a_l ._., "Q't_ i,15,,l e3._ j_b ![.!S<. '_ ,ao_ l;_'fo CheckTech/Time Smears Taken _% SmearsRead ,uP,, SmearsRead lifO0 t3o_ ' _' _' " 1" b iVt_ (I_ .4u_f' bc D ,Z.ET:'._%__=I_._%, /,3(.// _fz_ Animal Number _2_'<,_/=_ FS/o .ffl _ f', E b P ? E b ReviewedBy: /' LI Date: _;-/z. _//0 t l V' @(_ V ,r/J,o]} C _. i_,,,,=j._e=.,N._ RT 01.14.01:) EC2-O4a _/A\ _r-','_L.!,! L._.,.../,r i 1 012433 Argus pRoO:CrOL_ : " :T"ES'T " " ' ARTICLE/SUBSTANCE: " "TY'PE O"F TES.T.:.. 418-J0, 2i 0 DOSAGE: ,, [APFO GENERATION: ROUTE: ,,, EstrousCycle Evaluation .... :SPECIES/STRAiN: 0 MKD F1 Oral (Gavage) Rat/Cd:CD_ (SD) IGS BR VAF/Ptus_ P = Proestrus E = Estms M = Metestms D = Oiestrus .....O. ATE_t,/o_,17_1'/_,.,/.,,X_,_ _"_s',,.o_,-,_5.-,,__-.,7, -_0._. ,._,,.,__.,_L.,I, 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Anima.,.l Number @ , ,, ., /33& _ t> i' _- p o ? c p4 b /_ E /'ft. 'D ,,,,J 13ql -o _ ,_" _. 'z) f b b fl _ j_-b D _ e _ t> _ p. _ _4 t_ _ _ :_ P /350 e ,_ _, _ .,,,_ b " nO:_ P f' I..3__$3..-_._bz, .D P _" _ D p E_._ _ D t 13,55 r4 D /_ e" "p o _. _ .... 1_ J_ _ E T'_ D I_I _ ,,,'_ _ E" :.. _ .,, _ _,,, __ D r c_r,..o, _-',-o., _9e3_;-_-o_ @_z_-,-_-_, ., 4 _..,." 00 ,, RT 01,14.00 EC2-04b _) : PROTOCOL: 418-020 DOSAGE: 1 MKD P = Proestrus E = Estrus M = Metesb'us D Diestrus Argus TEST ARTICLEISUBSTANCE: APFO !GENERATION: ROUTE: F1 Oral (Gavage), ,, 1 2 34 5 6 7 AnimalNumber 012434 TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ .. 8 9 10 11 12 13 14 152'7 J'bgl I'bggl%$b __ _ 1) -_ D j_c E ,D p F__ D o ? E. o E E-'b P /-I,,_b tp b t' E L_ L/_ F b E I_ /q 0 _ ? {_ /'_ _ _ E E; _h p b _ _ 6D E ]) t?z, D L} f' l"Z_-j?2 _ Revi.ed By: P E __ Ua f E h D p r--,-_ Dale: I/ ,_'_/I'_ I--RT / 01.14.00 EO2-04b ,_ , PROTOCOL: 418-020 DOSAGE: 1 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus 012435 Argus " ",',",, ," , ,',,,,,c ' TEST ARTICLE/SUBSTANCE: TYPEOF TEST: ,, ,_ APFO ,GENERATION: ROUTE: EstrousCycleEva,l. uationn SPECIES/STRAIN: F1 Oral(Gavage) Rat/Cd:CD(_S)D)IGSBRVAF/Plus@ 1 2 3 4 5 6 7 8 9 10 11 12 13 14 , ,, ,,,, , Animal Number I,,40,'?_ _ e,,_<'-b D P ,,_ b_ D D E b D -h iIq'/O-/o7__.,,f _ Up. _c--bb oD _? ee _E bb 0D. _<, PC..,,K.E lqlZ e _ D F,..E.. o ) u g b _0 'P E D I_!5 _ E m _,b P _ b b E _ E n_ _ Iqlk -P c D _ P d g _ p _ _. m g C _ ., ,, , ,,. ,, .... . . .,. -"-,_, / RT/ 01.1" 4,00EC2-04b 7! ql_.i {o:)- _) 012436 j PROTOCOL: Argus TEST ARTICLE/SUBSTANCE: TYPE OF TEST: 418-020 DOSAGE: IAPFO GENERATION: ROUTE: Estrous Cycle Evaluation SPECIES/STRAIN: 3 MKD F1 t '_L P = Proestrus Oral (Garage) .,., Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ i , E = Esirus M = Metestrus D = Diestrus '_ _/./o,';d/4/,_t,_o,,/'.,_,__o.,_r,._.._,-,_s,-ro.!,,-,_,._d, ;'/., 1 2 3 45 6. 7 8 9 10, 11 12 13 14 AnimalNumber D, f _ t4 _ ,,z_ , /42H,, _ _ _ .r..-- E _- r lqS-_ "-O _C ,__ _ ]) E _ . UP ff i_ ReviewedBy:. ,j. Date: , ./ O(./ RT 01.14.00 EC2-04b _AO_ 'OPV:I 012437 j ,, .... , PROTOCOL: 418-020 DOSAGE: 3 MKD -P = Proestrus E = Estrus M = Metestrus D = Diestrus ,,_ ,. i ,,,,, , Argus *TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: F1 Oral (Gavage) , ..... .,, TYPE OF TEST: Estrous Cycle Evaluation SPECIES/STRAIN: Rat/Cd:CD@(SD) IGS BR VAF/Ptus@ ,.'.. : , ,, 1 2 3 4 5 6 .... 7 89 10 11 12 13 14 Animal Number ,, )'-!74 I/-/;)2 _c _ "b' e s .r)_ 9. 5 O _ _- _5, .J_ t M b ? o E _ [.)_ ,_ E o ,, ,, ,,] ,u ReviewedBy: i__._ .J U# Date: , %/:2_//o( RT 01.14.00 EC2-04b 012438 _) ...... PROTOCOL: 418-020 DOSAGE: Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: TYPE OF TEST: EstrousCycle Evaluation _SPECIES/STRAIN: 110MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus _,_ AnimalNumber F1 Oral (Gavage) Rat/CrI:CD@(SD) IGS BR VAF/Plus_ g,/o4.!.._/_. i/._. ' _,.',""_o,,',__-'_5-,=s.,_,:._r._, _, 1 2 3 4 56 7 8 9 10 11 12 ! 3 14 /qTq -_ _ e p e a .o e ,_ D 147) 15o0 /for I_135 1507 s _ D P 7> ,,,a,, "_ $ E N ID P. _ D _ d E D b f g 0 b P _E B D _ D __ p _ _ o g e 12_D D _ I) P _ rb o _ g b_ b D E '.b D e- D D P ff D b E 6 _ 19 'P g 15,1 _ ,_ _ _ "b ? _ a _ E ,__ .D P 1.5i& e D .,_ e p.. o P p DE o C_O_r,,,..rp__- #'-o, ReviewedBy: __-_j _ /'/" Date: .5"/z.-,_/0 ( RT 01.14.00 EC2-04b O12439 PROTOCOL: 418-020 DOSAGE: Argus ITEST ARTICLE/SUBSTANCE: APFO , ,i ,,, GENERATION: ROUTE: TYPE OF TEST: EstrousCycle Evaluation SPECIES/STRAIN: 10 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus DATE .. , F,,r:1 Oral (Gava.ge) IRat/Crl.'CD_(SD) IGS BR VAF/Plus_ 5//!/5o",/=//Q_i/',,oZ_/,'., _1,'1S0_0_','O5J'=0_.*0_''_ S'=_, _/J0. 1 '2 3 4 5 6 7 8 9 10 11 12 13 14 Animal Number 15_3 _ JSP-P. e D D _ E _" _ _ ,,i o _ _ d _ D _M P N l_ P F-_ _ nt ._ ]6"_q --_ E D _ P E p_ 0 P. E .0 .b _@ ).5_'/_?e ,o o p,,I> P _; _ p g _-:._1) _ ,, ,..b .--.... _,k." H 'L.._xW_'IF '! : PROTOCOL: 418-020 DOSAGE: 30 MKD .... P = Proestrus E = Estrus M = Metesb_JS D = Diestrus DATE Argus TEST ARTICLE/SUBSTANCE: APFO GENERATION: ROUTE: -, F1 Oral(Gavage) 012440 !TYPE OF TEST: 'EstrousCycle Evaluation SPECIES/STRAIN: Rat/Cd:CD_()SD) IGSBRVAF/Plus@ T.#1/5.19.Ol U(J RT 01.14.00EC2-04b : LJ- 01244j _/ -., ., PROTOCOL: Argus TEST ARTICLE/SUBSTANCE: ., TYPE OF TEST: 418-020 DOSAGE: A,,PF..O..... GENERATION: ROUTE: Est.rousCycle Eva,!uation SPECIES/STRAIN: 30 MKD. F1 P = Proestrus E = Estrus Oral (Gavage) , RaUCd:CD@ (SD) IGS BR VAF/Plus@ M = Metestrus D = Diestrus DATE Animal Number 15P_ _J_(/P' g'k_ 1 2 __ _;_/_,1_'f,/o, g-ia_i..sI,,]o,]6'_-' 3 4 5 6 7 ,_ > e _ !Y"D_"fi-'.'-off 8 9 ,_0..,_ -`1"'` 5,/f9:5#._""_"' _._tY 10 11 12 13 f/za_i 14 _ _ '_ _ .? l g%q ) 5 %_ p g _ ,3 > g > so p E/"_ E .b C & b D P ,,E . D b e E b 1__ D /4 ',,," 1_5-_,q--o e f _ '> a , j _ D _) .? D .5 3 .I_GI _ ? E" D 17 D ? D h p _ D 43 P I._T5 ......P. E" _ _ 7' _. w o p E 2_) D .P _- _5<7_ -"o _ P g....m _ > P E b _ P E D , ,,, _ ,,_,j RT 01.14.00 EC2-O4b | | i coPYI J//'_-i SXqiuAloCa-T O12443 'PROTOCOL: _ 418-020 DOSAGE: 0 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus Argus Test Article/Substance: ..... APFO GENERATION: ROUTE: F1 Oral (Gavage) Date Salin'e Pre-_heck Tech/Time _0i 1 _0 I_. 5_-I?2'1 _ 1_ 3 _ s'_q'_3l _ _,23 _ W'_"4l _ /1_( 'Saline Post-Check _ _ 'I =_ .... _ Type of Test: EstrousCycle Evaluation Species/Strain: Rat/CrI:CVDA_F/P(lSusD_) IGS BR _?-_5'_15A,'_/6, 6 T'z,_r _ 0 7.4 ,_/-/ _/'0/./1 Is/_lo7! 1150 __d (_ _" ' B._ Tech/Time Start _.#Z ""_- IHq _1 i 13":'_ IIlOb _,]L_'3 SmTeimaresETnadken i_,'_ ]3_n- 1%9_ 115t ,_ f_i'_ _.-' ir,_ liS"o .... Tech/Time Start .i_ji/_ l_,_, 13_ /;Z0:Z.... -- Smears Read I tE'_ Time End ANIMAL NUMBER /_1 ii / _J-_} /_1") [_6_L ii i ii ia,_ } Z _a.- 17_.?-_ i i iiii ii i_ III 13o_ E m. nq o, _- .. (_q o ,,. __i3 b ,b _ F" ,_, _ P I.'bf b _ F E ,,',,n o b l%n-5 i%50 Do p E_ b E m D_ e_D_/,J_/_ iz_-__-'='"_/" "'_"_ _" E I P_ /_ RT 01.14.00 EC1.04a 012443 PROTOCOL: 418-020 DOSAGE: 0 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus Argus Test Article/Substance: APFO GENERATION: ROUTE: F1 !Oral(Gavage) Type of Test: EstrousCycle Evaluation Species/Strain: Rat/Cd:Cl:_ (SD) IGS BR VAF/Plus_ Date ANIMAL NUMBER __L.%31 ._._/._b_ 1 _ 5"-_.ol 2 _ _,_'-/.o/ 3 P 5-2_'.0/_;-0,.,-.,. 4 5 __ S:;_7._, 6 _-Z_.c_ 7 _ P ___L_O __L_5 _0 b b__c--E-- _ r_ _ p_ __ _12 --P-_q _4 _. _F eveweO Oa,eRT 01,14.00 EC1-04b PROTOCOL: 418-020 !DOSAGE: 1.0 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus Argus ,,-' Test Article/Substance: APFO GENERATION: ROUTE: F1 Oral (Gavage) O12444 Type of Test: EstrousCycleEvaluation Species/Strain: Rat/CrI:CD_ (SD) IGS BR VAF/PIus@ Date .... ANIMAL NUMBER 13_ )_b_ __,z.'_i=t 5._3.ot 1 2 L _:_,/.ol 3 D p. E b m J':'oT_.ot 4 o" _._.,-,., 5 _5":_'7. #' _5 _e..pi 6 7 _1 o De DE _D I."a._? b P /__S P _ 1%7/ _). P _1 _ o m D_ g mD pE F_ D b .E 15;_ 152_/ I_.. _ bP _ Eo _'"' ' 1 rn o 1"5_ , p ibSD b IbgY I:b_7 fit f. /71 DD _' P DP D_ o_ P E: ,__ De DE _ O r DD D 1_'_3 I'b,_1 9_. m _ ,p F_- m p_ bD _a E z; RT 01.14.00 EC1-04b ... _;_ _lul_. 'i PROTOCOL: 418-020 DOSAGE: Argus Test'Article/Substance: APFO GENERATION: ROUTE: 1.0 MKD F1 P = Proestrus E = Estrus M = Metestrus D = Diestrus Date ANIMAL NUMBER 5z_t 1 Oral (Gavage) 5.,_%.of 2 _.;tL/'os 3 5".Jf.d/ 4 ' 012445 Type of Test: Estrous Cycle Evaluation :Species/Strain: Rat/CrI:CD (SD) IGS BR VAF/Plus -:._-_) _._.2,.'_.oI ._.,_5._ ! 5 6 7 I_c,7 ;flip p r_.. f_ D _ t4 D b ... _ ,, _ .... 5 oD ,, _ ,,, ....... ,, Reviewed By: ,,, ..... , ,, , .. _ _,. , '-- _ Date: _--/,_P//_a / RT 01.14.00 EC1-04b EXACT COPY i 0124.46 ,.. == PROTOCOL: 18-020 Argus .... . Test Article/Substance: APFO Type of Test: Estrous Cycle Evaluation DOSAGE: 3.0 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus GENERATION: FI ROUTE: Oral (Gavage) Species/Strain: Rat/Cd:CD@(SD) IGS BR VAF/Plus Date j_.Z_ 1 b'-;_%-ot 5.-_'o) 2 3 _-=ls'o) 4 _-z_-,I 5 _'t.o/ 6 _:-ZS_I 7 ANIMAL NUMBER /._,FI)- D D f-- _ ,_ Igg_ h _) P F-- ,',' ,r) z; o , e%o _ m D !_'_1 h o _' f' IH_ .p.. _ .m 1.'--/"3G b E iq3? % _4 _ . ,_J_ b E ,_ . f'......._ E ...._. ', __ ,m _ .ff _ _ ") nn P Dp EP DE g /4 _ _.... lgZ/(o ,.., E m o e g F__ t.,--/'-/.,._ b 1'45b b _ D '_ _ .m ,_ E m ._ .._ _ o 1'45_. b m b _,.... _ _b 1_5_, b p ,P ,. E e IgS_ _ O ?. E 9 IH_ b D _ Pe fn DO DP Reviewed By: ..___--=o-_I ._.' __L.d_ Date: R,T_40[1,/.Z1'44A."0_0 /EC1-04b ., 0PY PROTOCOL: 418-020 DOSAGE: 3.0 HKD P = Proestrus E = Estrus M = Metestrus D = Diestrus Date ANIMAL NUMBER I_(_3 Arg_ Test Article/Substance: APFO GENERATION: ROUTE: El Oral (Gavage) ..5"/.../-.Lq _97. o! 1 2 5.=1q.I 3 _'-,_'oZ 4 & m P F_ 012447 Type of Test: Estrous Cycle Evaluation Species/Strain: Rat/CrI:CD_ (SD) IGS BR VAF/Ptus f-z t,-''i 5 E._7.ot 6 ._.ze._i 7 _ mO /_7 b E r_ '4 _ , _ ,,,192/ _ rB .b.... f' P- mD ' 1'-/?_ b f' lg 9 _ FE 1q77 b r _ _ v Pd ,,, Reviewed By: Date: ,_,_"/2.t.'*/ RT 01.14.00 ECI-O4b _ __,,_._;_,,, _ROTOCOL: 418-020 DOSAGE: 10.0 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus Argus Test Article/Substance: APFO 'GENERATION: 'RouTE: F1 LOral(Gavage) 012448 Type of Test: Estrous Cycle Evaluation Species/Strain: Rat/CrI:CD@(SD) IGS BR VAF/Plus Date ANIMAL NUMBER P/%_ /_._b _$Zbi 1 D p 5.,23.01 2 _ _ E.,,lq,O) 3 _._-c_l 4 _.7,/oi 5I_'OJ 5 6 P E ,_ D m D_ E _--Z:_I 7 E D Iq'_ l atlq b D g Eb b _ ffl b _ D _. F_ E. I.qoc_ f_ E m p E d __ ..... 15o5 ) _ D v 'y_. /,,,l /5o$ _ P' 15 m _ 15l/ _'. ffl '_ _4 _ 15__ [_ D D p _ _q_,-t & m o.... F-- .v) f" = PP Z_ D pp 5i7 _ p U _F b DE Reviewed By: ,..__ _'. _ 00 Date: "_/_"A l RT 01.14.00 ECl-04b !_'_'; .L".,'-:'>=_ ,_:"';,;_,..':_:'_.i,':" :,-.-_;"_,,'-_,=:;:: -',-..',,_.M _i ti : qluio_, _,L; ........ ! - I 012449 PROTOCOL: 418-020 DOSAGE: Argus Test Article/Substance: APFO GENERATION: ROUTE: 10.0 MKD F1 = Proestrus E = Estrus M = Metestrus D = Diestrus Date _ 1 ANIMAL NUMBER Oral (Gavage) E._3,0) 2 5.;_LI'ol 3 _.a_.ot 4 Type of Test: Estrous Cycle Evaluation Species/Strain: Rat/Crl:CD (SD) IGS BR VAF/Plus 5"'z_'_I 5 5.9,7.oi 6 _k':ZB-O# 7 ___t_5,?_t,__. _ _ _4 _g e e Eb e t go ;55L/ _ D P r_ _ ep 5'i O0 PE '_'Reviewed By: _,._,._ ,_ _ (,2o Date: ,.,_/,_../f# / RT 01.14.00 EC1-04b E_ACTC0IPY PROTOCOL: 418-020 Argus Test Article/Substance: APFO O12430 Type of Test: Estrous Cycle Evaluation DOSAGE: 30.0 HKD P = Proestrus E = Estrus M = Metestrus D = Diestrus GENERATION: F1 ROUTE: Oral (Gavage) Species/Strain: Rat/Cd:CD_ (SD) IGS BR VAF/Plus_ Date _ 1 ANIMAL NUMBER _-=_3.0___.5_.___L./!._o_/ _.o_E.o/ 2 3 4 _'.'?._-0l 5".;}?.d) _.ZS-o t 5 6 7 D___ ____m [L_ D ____ _ _ --LI..ss b b D L_ -_ _B__ D E -I )___15Z3___ __I___#__6 io __ +b P r m _D__ _ RT 01.14.00ECI-O4b _om _ PROTOCOL.: 418-020 DOSAGE: 30.0 MKD P = Proestrus E = Estrus M = Metestrus D = Diestrus Argus Test Article/Substance: APFO GENERATION: ROUTE: F1 Oral (Gavage) .- i_,m - 012451 Type of Test: Estrous Cycle Evaluation Species/Strain: Rat/CrI:VCADF_/P(lSuDs) IGS BR ii 1 2 3 4 5 6 7 ANIMAL NUMBER J5% b _ m D P e )5_7 _- _ m D p g /5_ p _ m D D eN p5_",7 _ _ D _ p ..F.. D /5) g. _ P e E m o l_q'_? _> e P E r,n o 0 .j5"_ ,_ P m /2 _ e -_ luoo .b e - m D _- _-, '% ..,, -.... -.,,. "x RT 01,14.00 EC1-04b ,.hs qi,,lo_ it