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ARQ26- 0722 ACUTE TOXICITY TO FISH (RAINBOW TROUT) IESTSUBSTANCE Identity: A mixturecontainingperfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot number was 4. The test sample is FC- 2di0e3t.hyCluernreegnltycionlfobrumtaytlieotnheirn,di3c7at.e8s5i%t iwsaatemri,x2tu0r%e oefth1y.l3e4n%e gPlFycOoSl,, 35% 2.66 % Sultone foamer, 3% sodium octyl sulfate, 0.1% sodium lauryl sulfate, and 0.05% tolyltriazole. The following summary applies to a `mixture with incompletely characterized concentrationsof impurities. Data may not accurately reflect toxicity of the fluorochemical `component of the test sample. METHOD: MeTytpheo:d:Acute Not given. static YGeLaPr:coNmopleted: 1974 Species: Salmo gairdneri Supplier: Not given. Analytical monitoring: Temperature, pH, and DO Exposure period: 96-hours TSetsattifsitischalagmee:thJoudvse:nilNeot given. Length and weight: Average length = 1.5 in Average weight = 0.9 g (wet) Loading: Not given. Pretreatment: None. Test conditions: - DDiilluuttiioonn wwaatteerr:chCeamribsotnryf:ilteNroetd city water, given. St. Paul, MN Lighting: Stock and Not given. test solution preparation: Not given. Concentrations dosing rate: Once SEtxapbiolsiutryeofvetshseetless:t cNhoetmgiicvaenl.solutions: Not noted. or NNuummbbeerrooff friesphlipcearterse:pl1icate: Not given. Number of concentrations: five plus a `blank control `Water chemistry during the study: PH range (0-hours only): 71-72 000584 Temperature range (0-96 hours): 48 --49 F Dissol4v.e7d-o5x.y7gmegn/rLa(ncgoentr(o0l-9e6xphoosuurrse)): 42-52 mg/L (1250 mg/L exposure) RESOWYTS Nominal concentrations: Bk control, 125, 312.5, 625, 937.5, and 1250 mg/L Element values: 96-hour LC50 = 1250 mg/L Element values based on nominal concentrations RSuebmsatraknsc:eTReestmianrgkwsafsielcdo. nTduhcetveadlounesthreepmoirxtteudraepapslydetosctrhiabtemdixintutrhee aTnedstnot the fluorochemical proportion alone. conclusions The test sample 96-hour LCso for rainbow trout was determined to be 1250 mL. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 paraQuautY Raenldiadbiolciutmye:ntKaitiimoins.chSraamnkpilneg p=ur3i.tyTwesatsinngotlapcrkosperrelcyocrhdaorfacmteetrhiozdedolaongdytuhseed Study lacks analytical confirmationofthe amount of fluorochemical proportion in the solution. REFERENCES ~~ This study was conducted by the 3M Company, Environmental Laboratory, ~~ St. Paul, MN, Lab Request number 2103, 1974. OTHER Last changed: 6/27/00 000585 - c fe-t [---- 3 Request Fon LasoraToRY work Lb ewette. S10 70: ENVIRONMENTAL ENGINEERING LABORA--TBUOILRDINYG 536N Sen bs TEEHh dy, | YEA Ero Name: [DON ROSON RequestDate Project No. ____, _Prob. No. _, de fy SampleDate HoldSample ______DateNesdedi For____Days Est. Time: eo Date Rec'd.Sample: Analyst: MTEL OateCompleted: __2= =e |e J sTimp Diupia n Calcium Hardness, m/l 35 CoCO3 "F Alkalinity, mg/l as CCO3 WM Alkalinity, m/l as CaCO3 oH Suifatc,mg/i 95 S04 Nitrate, mg/l as NO3 Chioride, mg/l as C1 Silica, mg/l as $102. Figoride, melasF Grtho Phosphate, mg/l as P `Total Phosphate, mg/1 as P. Total Chromium, ma/t as Cr `Hex. Chromium, mg/l as Cr Total Cyanide, mg/l as CN Ferrocyanide, mg/l 2s CN Tron, mg/t as Fe Manganese, mg/l as Mn_ Surfactant, ma/l 2% LAS Phenol, mg/t BOD, mg/l TOD, mg/l (Short, Long, Diluter Total Suspended Solids, mg/l Volatile Suspended Solids, mg/l (Nlessetyes YFeeaztoss[ [TTTT] Ne--ATTT 11 Tr IrT Tr Tr rrr rr TTT rT Tr Tr 17 Ir T1 TTT T7 } rTTT 11 TTT 11 rrr 11 TT T7 rrr Tr TT 1] [I | BESTCOPYAVAILABLE rr rrrr TTT rTTTT T1 rT IrrrTTT 11 oT I TTTTT rT TT 11 He Turbidity, mg/l Silica Total Solids, mg Total Volatile Solids, mal Conductivity, mhos `Total Bacteria, No./100 mi 1 TT 11 TTT rT TTT T1711 rTTT Total Coliform, No./100 mi Fecal Coliform, No./100 ml Fecal Streptococcus, No./100 mi Ammonia Nitrogen, mg/l 3s N Kiedidah! Nitrogen, mg/las N Tat rE Tee aE | [ICOSS0y 9% ho - S= o_ m ---------------------- Comments: 1 rT rrr 1 rrr 11 rrr 1 1 TTT 11 1a XI 180 IX 50 TATEM I I Zp LL -- 11 TTT ts omni on St Eman En i Es Gr, Glin Re BOS56 30 carsomiess 0 3 ldpsw JWIThosoae 3 a Y J. 1e cot tat? or rE :.$ oF, Tr i ey SiN A [AE :4 F BARE NS aT02 nT h i PEE TL ` ba E&d IS 3 lselwi[Jo voc1| 56ib:u hd Eb g 3 42 ERE EoE n | E 7 : IF: 3 Ba 2 R3 EE pi | cooe fod [oo 1 ool _) vas ee 1 LL ! ap Fl Es 3 Ct---- ol bod * - Ls A a 1 1 . Bre Los IA H gE bce a-s ; =" dd of BES COPYAVAT ILABLE FERE TET 00055% ~ M8