Document v6Y8GMxr67821zdkMQ9eOemDq
VINYL RESIN
(Solveu. .olymerization) VMCA
Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
132 10,400 3-28-79
REJECTED* 3 (PDW)
Appearance (Whitepowded.soli i)
Size. % thru NCL._2Q-Slfi.ve. Heating Loss. % Polyvinyl Chloride. %_ Inherent Viscosity Foreign Matterr Slurry. Water.
(3.0 max.) (79.0/82.0) (0.30 min.) (8 maximum) (0 .5, max.)
Polvvinvl Alcohol. %
Heat stability.
Lead,, jpn.,
Solution Tests
,.yiSCQSj.UUCgS
Solar Turbidity
Insoluble Matter, %
10% Solution .Special Solvent
(15, nax.) (300/450) (80 min.) (85 min.) (0.03 max.)
.Apparent Density.... lbs/tm. ft,
Maleic acid, %
(2.1/2.5)
VCL Monomer, ppm
(1, max.)
PASSED 1.2 81.8 0.30 10+* 0.2
437 81 73* 0.016
1.94* <0.2
i PLAINT FPS lj E^E
"
lag) , r
Mr. R. M. Arnold, 133/515 Mr. W. T. Gray, 88/515 Mr. G. S. Peacock, 98/312 Mr. M. D. Pearson, 3001-7 Mr. P. D. Wegrzynowicz, 152-2
CONFIDENTIAL
PLANT tABORATdftY
4-b- 7L
UNION CARBIDE CORPORATION
CHEMICALS AND PLASTICS
SOUTH CHARLESTON, WEST VA.
109442 HRJf
"BAKEL1TE" VINYL RESIN
(Solvent Polymerization) VMCA
3 Lend Number
Blend Weight . Pounds.
Date
Laboratory DiSDOsit iorL
VMCA-
Batch Status
131 67,500 3-24-79
PASSED 8
ADDearance (White.Dowded.soli i)
Size, % thru No. 20 Sieve Heating Loss, Polvvinvl Chloride. % Inherent Viscosity _ _ _ _ Foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 min.) (8 maximum)
Water. %
- .................... (0.5, max. )
Polvvinvl Alcohol. %
Heat StablliJtv_____________________
Lead. nnm
( 15, max.)
Solution Tests
Viscositv . c.ps Color.
(300/450) (80 min.)
Turbidity
(85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Adoarent Density.__lhs/cn.ft .
Maleic acid, %
(2.1/2.5)
VCL Monomer, ppm
(1, max.)
PASSED
2.2 81.7 0.32 8 0.2
5 448 95 99 0.008
2.4 <0.2
'
Mr. R. M. Arnold, 133/515 Mr. W, T. Gray, 88/515 Mr. G. S. Peacock, 98/312 Mr. M. D. Pearson, 3001-6 Mr. P. D. Wegrzynowicz, 152-2
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PLANT LAB'ceAftBY 3-26-79 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS
CONFIDENTIALS0UTH charleston west va*
yCC 109443
Rlend Number
Blend Weieht, Pounds
Date
Laboratory
'Disposition
VMCA-
Batch Status
"BAKEL1TE" vinyl resin
(Solvent Polymerization) VMCA
128 83,250 3-20-79
129 81,000 3-23-79
PASSED 8
PASSED 8
130 72,500 3-21-79
PASSED 8
Aooearance (White,Dowded.soli i)
Size. % thru No. 20 Sieve Heating Loss. % Polvvinvl Chloride. % . Inherent Viscosity Foreign Matter, Slurry ........ _
(3.0 max.) (79.0/82.0) (0.30 min.) (8 maximum)
WaterL %
(.0.5, max.)
Polvvinvl Alcohol. %
Heat Stability.
Lead. DDm
.
Solution Tests
Viscosity r cps Color ....
Turbidity
. ( 15,max.) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Apparent Density.__lhs/cu . ft. .
Maleic acid, %
(2.1/2.5)
VCL Monomer, ppm
(1, max.)
PASSED
2.4 82.0 0.32 5 0.2
435 96 100 0.008
2.4 <0.2
PASSED
2.2 80.8 0.31 8 0.2
PASSED
2.3 81.0 0.32 6 0.2
__ 5_____________ ___6________ 365 425
94 96 100 95
0.010
0.008
2.4 <0.2
2.4 <0.2
Mr. R. M. Arnold, 133/515 Mr. W. T. Gray, 88/515 Mr. G. S. Peacock, 98/312 Mr. M. D. Pearson, 3001-6 Mr. P. D. Wegrzynowicz, 152-2
j jh
CONFIDENTIAL
pLaNt laboratory
3-28-7
UNION CARBIDE CORPCRATION
CHEMICALS AND PLASTICS
SOUTH CHARLESTON, WEST VA.
ucc 109444
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weieht. Pounds..
Date
Laboratory DiSDOSltiOlL
VMCA-
Batch Status
125 67,500 3-14-79
126 72,000 3-17-79
127 76,500 3-15-79
PASSED
PASSED
PASSED
_2______________ --s_____________ ___ 8--
ADDearance (White.powded.soli i)
Size. % thru No. 20 Sieve Heating Loss. % . Polyvinyl Chloride. % Inherent Viscosity ...................... Foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 min.) (8 maximum)
Wat r. %
.........
(0*5, max.)
Polvvinvl Alcohol. %
Heat Stability
I.ead . nnra
Solution Tests
Viscositv r cps Color
Turbidity
(15, m ax. ) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max. )
Apparent Density.__Ibs/eu. ft .
Maleic acid, %
(2.1/2.5)
VCL Monomer ppm
(1, max.)
PASSED
2.9 81.0 0.31 4 0.2
3 325 97 99 0.008
2.1 <0.2
PASSED
2.1 81.0 0.31 7 0.2
14 328 94 96 0.010
2.4 <0.2
PASSED
2.2 80.4 0.33 4 0.1
6 405 97 96 0.006
2.3 <0.2
Mr. R. M. Arnold, 133/515 Mr. W. T. Gray, '''8/515 Mr. G. S. Peacock, 98/312 Mr. M. D. Pearson, 3001-7 Mr. P. D. Wegrzynowicz, 152-2
jjh
>/ 't' /*.
>la&t laboratory UNION carbide corporation19
CONFIDENTIAL___ CHEMICALS AND PLASTICS S0UTH CHARLESTON, WEST VA.
109445
Blend Number
Blend Weieht. Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
122 74,250 3-6-79
123 67,500 3-7-79
PASSED 8
PASSED 8
Appearance (White.oowded.soli 1)
Size. St, thru No. 20 Sieve Heatine Loss. *?> Polvvinvl Chloride. Inh rent Viacositv Foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 min.) (8 maximum)
Water. %
(0.5, max.)
Pol vvinvl Alcohols.
Heat Stabilitv
............
Lead .__pom
ooiuxxon Tests
Viscositv P cps Color Turbidity
(15., m ax. ) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10?i Solution Special Solvent
(0.03 max.)
Apparent Density.__lbs/cu . ft. .
Maleic acid, %
(2.1/2.5)
YCL Monomer, ppm
(1, max.)
PASSED
2.2 81.8 0.33 7 0.1
5 350 97 95 0.006
2.2 <0.2
PASSED
2.3 82.0 0.31 8 0.3
10 366 96 96 0.01
2.1 <0.2
124 72,000 3-10-79
REJECTEE 2 (PDW)
PASSED
2.5 81.8 0.31 6 0.2
5 415 95 98 0,008
2.0* <0.2
Mr. R. M. Arnold, 133/515 Mr. W. T. Gray, 88/515 Mr. G. S. ieacock, 98/312 Mr. M. D. Pearson, 3001-6
/ --;/ t,__>
/> ,
Mr. P. D. Wegrzynowicz, 152-2
^ ^_ UV>
____________
PLANT LABORATORY
3-14-79
UNION CARBIDE CORPORATION
POMCIHrMTIAl CHEMICALS AND PLASTICS UVJimr 1 ULIm I IAL SOUTH CHARLESTON, WEST VA.
jjh
ucc
109446
t
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
120 76,500 2-28-79
REJECTED* 2 (PDW)
121 76,500 3-3-79
REJECTED* 2 (PDW)
ADDearance (White.Dowded.soli 1)
Size. 3, thru No. 20 Sieve
Heating Loss. 3, ................ _ (3.0 max.)
Polvvinvl Chloride.
(79,0/82.0)
Inherent Viscositv .................... (0.30 min.)
Foreign Matter, Slurry
(8 maximum)
Water. 3,
._
(0.5, max.)
Polvvinvl AlcohoL. %
Heat Stahi 1 itv _ . ... ......
Lead. ppm
Solution Tests
_.yiacflS.Lty.><ips, _ Color Turbidity
(.15, max.) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
103, Solution Special Solvent
(0.03 max.)
Apparent Density.__1 hs/nu,ft .
Maleic acid, %
(2.1/2.5)
VCL Monomer.. -PPJg_________________ (1, max.)
PASSED
2.5 80.7 0.30 8 0.3
5 277* 97 95 0.008
2.6* <0.2
PASSED
2.6 80.0 0.31 7 0.4
4 280* 97 95 0.006
2.4 <0.2
|
Mr. H. M. Arnold, 133/515
Mr. W. T. Gray, 88/515
Mr. G. S. Peacock, 98/312 Mr. M. D. Pearson, 3001-6 Mr. P. D, Wegrzynowicz, 152-2
J
PLANT LABORATdRY
___
3_6-79
UNION CARBIDE CORPORATION
CONFIDENTIAL CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA. j Jh
ucc
109447
I
. IN'fL REST*
* r. 'i . jjyvsriZsUr !
VVi
I 31(,.".v Number __________
| LI`.jr,d Wr;ifcnt , Poun-is_____
Lum___________________ _____
LBUorst. r>i"t LDmnojr ?. li-oa...
S Ba t cr S t r. i us
M-A:.
i
J.
Aor.c.'irancc ( wiii t <. h>wJ< u.mu i } i
4-2 1 -- 7 b
J2S 77,U00
M-25-78
Hx -TE:C i'hi ' '1 (PDW)
I"" PASSED
REJECTED*
3 (POM
PASSED
HeaUftfc.JLflss, Jf---------Polvvanv? Chloride, %
i 3.0 m3 v . ) (79.0/52.0 >
a;. AUUBcafiiA.v'--.................... (O.30 min.)
Foreran Ma_lJ2i2r2_.illnrxjr _____ ... ( S muXin:urn
*at_er^ .A.., ..
(!.0 mux.)
Polyvinv. Alcohol,.%
Heat Stability
T.eari . "nn--m 1 ----
Solution
Viscosity. cps__
Tests
Color___________
Turbidity
(15 maximum) (300/450) (80 min.) (55 min.)
Ins luble Matter, %
10% Solution Special Solvent
(0.03 max.)
Apparent Density., lbs/ru.ft. .
Maleic acid. \c
(2.1/2.5)
2.1 82 . n* 0.34 7 0,4
27* 435 96 Q4 0.006
2.0
J 1.2 j 80.6
0.32 : 10+-V; 0.4 ii *
12 363 78 * 79 * 0.008
2l2______________
:---------------
Mr.- fc. ,M. Arnold, 133/515 W. 7. Gray, 38/515 . G. S. Peacock, 98/3J2 *
Mr. M. D. Pearson, 3001-6 Mr. P. D. Wegrzynowicz, 152-2
Mr. R. N. Wheeler, 189-3
UCC - 10<3448
i CONFIDENTIAL
PLkUV LAbX?T-------
UNION CARBIDE CCBPCEATIOf
CHEMICALS AND PLASTICS
SCTTTW r-MAPT'RSTOW
VA .
B'j.-n'i : I v U-;.v ,
___
I L_ _ ....
iJ^-sj2Pe;.^-sa _ . .. ; .... .
tch.s
__________________
KZ ri-
..1
<r
, V'
T
I 1I
SOUTH CHARLESTON, WEST VA .
DISCARD
ORiGir:
RcPC. ,, i
vinyl resin
t t * Pi-j -/'f - . iza fion)
Blend Number
Blend Weight. Pounds
..lihXSk-----------Laboratory | Dieposi tier
Batch Status
..VMCA-
!
--- j
J ;
1
' -I
.'i 3,5 0 (. i
ft-20-78 j
fiL.T];riT,D` 2 (PDW
11?
i 85,500 . 8-26-76
REJECTED* 2(PDW)
1
Appearance (White, powdod. sol 1 I) Size. 1 thru No, 2Q Sieve
PASSED
Heating .j^sa ,_5L_ Pol vviny 1 Chloride. Jfc.
-Inherent _v;jjaj^aartx
(3.0 max.) j ^ (7*>. 0/S2.0 ) ; 81>3 ('.I, "JO min. ' 0.32
preign Marter, SInrry______
SI ater. S Polyvinyl Alcohol. %_________
( r i-.n \ i mum > (l 11 max . )
10* 0.5
r Heat Stability
; read. ppm
Solution Tests
Viscosity fcps
.Color, Turbidity
(25. max.) (300/450) (80 min.) (85 min.)
11
360 94 95
1nsoluble Matter, %
10% Solution Special Solvent
(0,03 max.)
0.006
Apparent density- lbs/cu.ft Maleic acid, %
(2.1/2.5)
2.5
,II PASSED I i 21 ! 81.2 ! 0.33 i 10*
u.3
26* 405 86 89
2.1
M. Arnold, 133/515 Mr. W. T. Gray, 88/515 Mr. G. S. Peacock, 98/312 ,
M. D. Pearson, 3001-6 . P. D. Wegrzynowicz, 152-2 Mr. R. N. Wheeler, 189-3
jjh
UCC - 109450
i CONFIDENTIAL
PLANT' UB<SXT<*T------- ST-3-7B"
UNION CARBIDE CCRPdUTICK CHEMICALS AND PLASTICS SOUTH CHARLESTON, WIST YA.
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Rlend Number
Rlend Weieht . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
113 81,000 8-18-78
REJECTED* 2 (PDW)
Appearance (White.powded.soli i)
Size. 1 thru No. 20 Sieve Heating Loss. % Polvvinvl Chloride. * Inherent Viscosity Foreign Matter, Slurry Water. *
(3.0 max.) (79.0/82.0) (0.30 min.) (8 maximum) (1.0 max.)
Polvvinvl Alcohol.
Heat St.ahilitv
T.earf . nnm
Solution Tests
Viscositv.cps Color
Turbidity
(15, max.) , (300/450) (80 min.) (85 min.)
inboluble Matter, %
10?i Solution Special Solvent
(0.03 max.)
Apparent Density.__1 bs/rn.ft .
Maloic acid, %
(2.1/2.5)
VCL MONOMER, ppm
(1* max.)
PASSED
2.5 81.9 0.32 10* 0.6
11 365 96 86 0.006
2.4 <0.2
Mr. R. M. Arnold, 133/515 Mr. W. T. Gray, 88/515 Mr. G. S. Peacock, 98/312 Mr. M. D, Pearson, 3001-6 Mr. P. D. Wegrzynowicz, 152-2 Mr. R. N. Wheeler, 189-3
j jh CONFIDENTIAL
UCC - 109451
PLANT LABORATORY '9-8-78 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
Til end Number
Blend Weight . Pounds
Hate
Laboratory
Disposition
VMCA-
Batch Status
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
111 74,250 8-10-78
112 83,250 8-12-78
rejected* 2 (PDW)
PASSED 8
Mr. R. M. Arnold, 133/515 Mr. W. T. Gray, 88/515 Mr. G. S. Peacock, 98/312
Mr. M. D. Pearson, 3001-6 Mr. p. D, Wegrzynowicz, 152-2 Mr. R. N. Wheeler, 189-3
PniurmriviTiai vUlNrlUui IIAL
UNION CARBIDE CORPORATION
chemicals and plastics
south charleston, west va.
Blend Numuer
Blend Vfeitiht. Pom:a&
Date
___ __
i.abora ten v j Disposition 1_______ ) )jCA_-____
Batch StatuF
V K } .t S< i. f Ii .
DISCAR-
ORiG!MM
VINYL RESIN
yB.rrissatior.) report
S'LA
!
I !'S i 109
110
o 7,7 5 O
87,750
69,750
8- - 7 8
8-8-78
8-9-78
i k;-.j ectld*
REJECTED*
; 2 (PPW)
i 2 (PDW)
REJECTED2 (PDW)
A dde r. ra nee ( 'irb it e . nowdfd . ;-ol i i)
PASSED
Size, JL thru.m.. 2Q Slevs-----
He.AU.ns .Losa. Polyvinyl Chloride^
nHerem yiauialuv "Rar.e,lg.a Jin ttfLiy-Siujuy...
Wat r.
(3.0 max. ) { 2.3
j(79.0/8*2.0) B2.0
(0.30 min.) | 0.30
(8 maximum) | ^
i(1,0 max.)
0.2
Polyvinyl AlcohoU %
Heat Stability Lead, ppm
Solution Tests
V13COS11V r CDS
Color Turbidity
(15 maximum) (300/450) (80 min.) (35 min.)
XL 282*
93 89
1n&oluble Sa t. t er, %
105, Solution Special Solvent
(0.03 max.)
0.004
Apparent Density Ihs/cuft Maleic acid, %
(2.1/2.5)
2.4
PASSED
2.7 80.9 0.31 10* 0 .3
8 250* 91 95 0.004
PASSED
2.6 79.8 0.30 7 0.9
13 275* 91 91 0.004
2.3
2.3
Mp-^k. M. Arnold, 515
M11Xr. W. T. Gray, Bldp. 88 - Texas City
ft G. S. Peacock, 312
*
r, M. T. Pearson, 3001-6
Mr. P. D. 'tfeprzynow!cz, 152
Hr. R. N\ Wheeler. 189
4--
ucc
109453
CONFIDENTinL
/
PUKT 'OTafUT^^^y^-76"
UNION CARBIDE CCKPOUtlCN CHEMICALS AND PLASTICS SOUTH CHARLESTON, VEST VA.
Blend Number
Rlend Weieht . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
(a) A CORRECTED REPORT
"BAKELITE" vinyl resin
(Solvent Polymerization) VMCA
105 90,000 12-10-77
106 69,750 12.12-77
107 90,000 12 -13-77
REJECTED * REJECTED *
4 (CEF)
4 (CEF)
REJECTED 3 (CEF) (s
Aooearance (White,Dowded.soli i)
Size. % thru No. 20 Sieve Heatine Loss. *1. Polyvinvl Chloride. % Inherent Viscosity Foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum)
water. %
(1.0 max.)
Polvvinvl A1 cohol. %____________
Heat Stability
Lead. Dom .
Solution Tests
Viscosity r cps Color Turbidity
(15 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Anparent Density.__Ibs/cn.ft .
Maleic acid,
(2.2/2.5)
VCL MONOMER, PPM
(1 maximum)
PASSED
2.3 81.9 0.32 5 0.3
7 440 96 96 0.008
2.6 * <0.5
PASSED
2.3 82.2 * 0.32 5 0.3
6 348 88 92 0.004
2.8 * <0.5
PASSED
1.8 80.7 0.33 10+ * 0,4
7 390 91 98 0.006
2.9 * <0.5
(a) Reclassified. Please di scard origins ,1 report, da ted 12-19-77
Dr.J.J.Brezinski,511 Mr.C.E.Fry, 152 Mr.W.T.Gray,Bldg,88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr .R.N. Wheeler, 189
raf 1
UCC - 109454
PLANT LABORATORY UNION CARBIDE CORPORATION
CONFIDENTIAL CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
"BARELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weieht. Pounds
Date
Laboratory Disposition
VMCA-
Ratch Status
104 85,500 12-3-77
PASSED
Appearance (White.powded.soli I)
PASSED
Size. 1 thru No. 20 Sieve Heatine Loss. 1, Polvvinvl Chloride. % Inherent Viscosity Foreign Matter, SlurT-y Water. %
(3.0 max.)
(79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
2.8 81.4 0.31 6 0.3
Polyvinvl Alcohol. %
Heat Stabilit.v
Lead, pom..........
Solution Tests
Viscosity.cps Color Turbidity
(5 maximum) (300/450) (80 min.)
(85 min. )
5 381 94 96
Insoluble Matter, %
101) Solution Special Solvent
_Aucar ent. Density.__lbs/cn . ft .
Maleic acid, %
VCL MONOMER, PPM
(0.03 max.) 0.006
(2.2/2.5)
2.5
( 1 maximum) <0.5
1
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 TC Mr,G.S.Peacock,312
Mr.T.J.Salernn,212 Mr.R.N.Wheeler,189
mf 1
UCC - 109455
J/ 7*. CdJLJ" PLANT LABORA'l'ORY 12-7-77 UNION CARBIDE CORPORATION
CONFIDENTIAL CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
103 96,750 12-8-77
REJECTED * 4 (CEF)
ADDearance (White,powded.soli i)
Size. % thru No. 20 Sieve Heatine Loss. % _ Polvvinvl Chloride. % Inherent Viscosity Foreign Matter. Slurrv
(3.0 max.) (79.0/82.0) (0.30 rain.) (9 maximum)
Water. %
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stability
Lead. Qnm
.
Solution Tests
Viscosity,cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution
(0.03 max.)
Special Solvent
Apparent Density .__Ihs/cu . ft. .
Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(1 maximum)
PASSED
2.4 80.6 0.32 2 0.3
5 315 97 100 0.006
2.9 * <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mfl
. 109'156 ----------
CONFIDENTIAL
PLANT LABORATORY 12-13-77
UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
(a) A CORRECTED REPORT
R1 end Number
ft 1 end Weieht . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
"BAKEL1TE" VINYL RESIN (Solvent Polymerization)
VMCA
102 49,500 12-13-77
REJECTED * 3 (CEE) (a)
Appearance (White,powded.soli 1)
Size. T> thru No. 20 Sieve
Heatin? Loss. % _ Polvvinvl Chloride. %
(3.0 max.) (79.0/82.0)
Inherent Viscosity Foreign Matter. Sltirrv
(0.30 min.) (9 maximum)
Water. %
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stability
Lead, ppm
...
Solution Tests
Viscositv,cps Color
Turbidity
Insoluble Matter, %
10t Solution Spec! a 1 Solvents
Aoparent Density.__1 bs/cti . ft . Maleic acid, %
(5 maximum) (300/450) (80 min.) (85 min.) (0.03 max.)
(2.2/2.5)
VCL MONOMER, PPM
(1 maximum)
PASSED
2.8 81.5 0,34 8 0.4
40 485 * 90 99 0.006
ft . ft * <0.5
(a) Batch Status changed fron 4 to 3.
Dr.J,J.Brezinski,511 Mr.C.E.Fry,152 Mr. W.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T,J.SalenD,312 Mr.R.N.Wheeler,189
PI =ase discard original rep art, dated 12-15-*?
"PLANT LABCRStCRY 1-9-78 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
ucc 109457
WW I
Blend Number
Blend Weieht . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
"BAKEL1TE" VINYL RESIN (Solvent Polymerization)
VMCA
101 69,750 11-30-77
REJECTED * 4 (CEF)
Appearance (White.powded,soli i)
Size. 1 thru No. 20 Sieve Heatine Loss. 1 Polvvinvl Chloride. 1 Inherent Viscosity Foreign Matter. Slnrrv Water. 1
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polvvinvl A1 cohol. 1____________
Heat Stability
I.pari . ppm
Solution Tests
Viscosityr cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
101 Solution Special Solvent
(0.03 max.)
Anna rent Density.__1 bs/mi. ft .
Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(1 maximum)
PASSED
2.5 80.5 0.33 6 0.3
5 350 98 90 0.006
2.7 * <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry, 152 Mr.W.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mfl
ucc 109458
CONFIDENTIAL
PLANT LABCkaTinx 22-2-77 UNION CARBIDE CORPORATION
CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA
mend Number
Blend Weight . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
"BAKELITE" VINYL RESIN (Solvent Polymerization)
VMCA
100 85,000 12-2-77
REJECTED * 4 (CEF)
Appearance (White.powded.soli i)
Size. % thru No. 20 Sieve
Heating Loss. % Polvvinvl Chloride. %
(3.0 max.) (79.0/82.0)
Inherent Viscosity
(0.30 min.)
Foreign Matter, Slurry
(9 maximum)
Water. %
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stablli.xv_____________________
Lead.__ppm
(5 maximum)
Solution Tests
Viscosity,cps Color
(300/450) (80 min.)
Turbidity
(85 min.)
I ni.oluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Apparent Density.__lbs/cu.ft.
Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(1 maximum)
PASSED
2.3 80.9 0.31 10 * 0.25
5 401 92 94 0.004
2.5 <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr,R.N.Wheeler,189
mf 1
UCC - 109459
1
r_
PLANT LABGRATCRY 12-7-77 UNION CARBIDE CORPORATION
CONFIDENTIAL CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
Rlend Number
Blend Weight . Pounds
Date
Laboratory Disposition.
VMCA-
Batch Status
"BAKELITE" VINYL RESIN (Solvent Polymerization)
VMCA
99 81,000 12-7-77
REJECTED * 4 (CEF)_____
Anoearance (Whitepowded.so] i 0
size. % thru No... 2d. Sieve Heating Loss. % Polwinvl Chloride. % inherent Viscosity
Foreign Matter, Slurry.
Water%_
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polyvinyl Alcohol. %
Heat Stability
T,eadf ppm
Solution
Tests
I nt.oluble Matter, %
YjLscQslty.cps -Colon. Turbidity 10% Solution Special Solvent
(5 maximum) (300/450) (80 min.) (85 min.) (0.03 max.)
Apparent Density, Iba/cn.ft Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(1 maximum)
PASSED
2.9 80.6 0.32 8 0.3
314 93 97 0.006
3.0 * <0.5
Dr.J,J.Brezinski,511 Mr.C.E.Fry,152 Mr.V.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mf 1
ucc - 109460
"^Unt^A bcr^r?^
CONFIDENTIAL
12-13-7 UNION CARBIDE CORPORATION
CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
61 end Number
Rlend Weieht . Pounds
Date _ .
Laboratory DisoosiiioiL
VMCA-
Rat.ch Status
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
96
81,000 11-30-77
97
87,750 11-22-77
98
87,750 11-23-77
REJECTED * 4 (CEF)
REJECTED * REJECTED
4 (CEF)
4 (CEF)
AoDearance (White.Dowded.soli i)
Size, $ thru No. 20 Sieve Heating Loss. ..?> ... _ Polvvinvl Chloride. % Inherent Viscosity Foreign Matter, Slurry Water. %
(3.0 max.) (79.0/82.0)
(0.30 rain.) . . (9 maximum)
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stability
Lead, nnm
Solution Tests
Viscosity,cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Apparent Density.__lbs/cu.ft.
Maleic acid, %
(2.2/2.5)
VCL MONOMER. PPM
(1 maximum)
PASSED
2.5 81.0 0.33 7 0.2
5 390 98 90 0.006
2.6 * <0.5
PASSED
2.5 79.3 0.32 10+ * 0.4
PASSED
2.4 79.3 0.32 10 + * 0.2
10 * 301 91 97 0.006
2.5 <0.5
_ 315 88 93 0.006
2.5 <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg,88 TO Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N,Wheeler, 189
mfl
UCC - 109461
CONFIDENTIAL
PLANT LABORATORY 12-2-77 UNION CARBIDE CORPORATION
CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
"BAKELJTE" VINYL RESIN
(Solvent Polymerization) VMCA
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
3lend Number
Blend Weieht. Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
92 22,500
7-29-77
REJECTED* 4 (CEF)
93 76,500 7-27-77
PASSED
94 54,000 7-28-77
REJECTED 4 (CEF)
Appearance (White.powded.soli 0
PASSED
Size. % thru No. 20 Sieve
Heatine Loss. % Polvvinvl Chloride. % Inherent Viscosity foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum)
2.4 81.2 0.34 7
Water. %:
(1.0 max.)
0.7
Polvvinvl Alcohol. %
Heat Stability
T.eari. nnm
Solution Tests
Viscositv r cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
a,
365 90 88
Insoluble Matter, %
10% Solution
(0.03 max.)
Special Solvejrt _
0.01
Aonarent Density.__lhs/eu.ft .
Maleic acid, %
(2.2/2.5)
2.9*
VCL MONOMER, PPM
<0.2
PASSED
2.6 80.7 0.33 7 0.4
PASSED
2.0 80.0 0.33 4 0.3
_3_____________ 315 97
3 365 90
_24____________ 80*
0.008
0.006
2.4 <0.2
3.0* <0.2
Dr.J.J.Brezinski,511 Mr.M.E.Eisenhour,5IE
Mr. W. T. Gray, Bldg. Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,189
88 TC
jjh
ucc -
/
CONFIDENTIAL
PLANt LABORATORY UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
SI end Number
Blend Weight . Pounds
Date
Laboratory
Disposition-
VMCA-
Batch Status
91 85,500 7-24-77
PASSED
Appearance (White.powded.solii)
Size. % thru No. 20 Sieve Heating Loaa--SL Polyvinyl Chloride. < inherent Viscosity Foreign Matter,__Slurr.y. Water. %
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.).
Polyvinyl Alcohol. %
Heat Stability
T,eadr ppm
Solution Tests
Viscosityfcps Color Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Apparent Density, lbs/cn.ft Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(1 max.)
PASSED
2.5 81.3 0.33 8 0.3
300 92 91 0.01
2.4 <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 TC Mr.G.S.Peacock, 312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mf 1
ucc 109464
_
plAnt laboratory
7-26-7
mWFinFWTIA! UNION CARBIDE CORPORATION
vvm lULmlML CHEMICALS AND PLASTICS
SOUTH CHARLESTON, WEST VA.
(a) A CORRECTED REPORT
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Appearance (White.powded.soli 1)
PASSED
Size. % thru No. 20 Sieve Heating Loss., %_ Polyvinyl Chloride. % inherent- Vigcogitx. Foreiyn Matter. .Slurrvwater. 3l
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
2.0 82.0 0,32 7 0.2
Polvvinvl Alcohol. %
Heat Stability.
T,eadf ppm
Solution Tests
In&oluble Matter, %'
Viscosityrcps
ColQrTurbldity 10% Solution Special Solvent
(5 maximum) (300/450) (80 min.) (85 min.) (0.03 max.)
308 (a) 92 85 0.004
Apparent-Penally.,__Ihs/cu-ft.
Maleic acid, %
(2.2/2.5)
2.4
VCL MONOMER. PPM
(1 maximum) <0.5
(a) Reanalyzed and redisposit toned. Pleasie discard report dated 7--21-77
Dr.J.J.Hrezinski,511 Mr.C.E.Fry,152 Mr. W.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mfl
CONFIDENTIAL
UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
ucc 109465
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Date
Laboratory DisoosLtioiL
VMCA-
Batch Status
89 119,250 8-1-77
REJECTED 4 (CFFl
Aooearance (White., pQwded.soli 1)
Size. % thru No. 20 Sieve
Heating Loss. % Polyvinyl Chloride. %
(3.0 max.) (79.0/82.0)
Inherent Viscosity
Foreign Matter, Slurry
(0.30 min.) (9 maximum)
Water. %
(1.0 max.)
PASSED
2.5 80.1 0.33 10+ * 0.3
Polvvinvl A! cohoL. %____________
Heat Stability
Lead. oom
Solution Tests
Viscosity rcns Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution
(0.03 max. )
.Special Solvent
Apparent Density, lhs/on.ft.
Maleic acid. %
(2.2/2.5)
3 325 81 88 0.01
3.05 *
VCL MONOMER. PPM_________________ (1 maximum) <0.5
Or.J.J.Brezinski,511
Mr.M.E.Eisenhour,515
Mr. W. T. Gray, Bldg, 88 TC
Mr.G.S.Peacock,312
Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
PLANT iABORATdRY 88--110--7' 7 UNION CARBIDE CORPORATION
CONFIDENTIAL CHEMICALS AND PLASTICS
mfl SOUTH CHARLESTON, WEST VA.
ucc
109466
ri.W.Ot.*..
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Rlend Number
Rlend Weieht. Pounds
Date
Laboratory Disposition-
VMCA-
Batch Status
88 94,500 7-7-77
PASSED
Aooearance (White.Dowded.soli 1)
Size. thru No. 20 Sieve Heating Loss. % Polvvinvl Chloride. < Inherent Viscosity Foreign Matter, Slurry Water. %
(3,0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polvvinvl Alcohol. %
Heat Stability
lead. oom
Solution Tests
Viscosity r cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
I ns,oLuble Matter, %
10?i Solution Special Solvent
(0.03 max.)
A noarent Density.__1 bs /o u . ft .
Maleic acid, %
(2.2/2.5)
VCL MONOMER^ PPM_________ __________ (1 max.)
PASSED
2.7 79.9 0.36 7 0.3
5 310 97 100 0.008
2.5 <0.5
Dr.J.J.Brezinski,511
'BARELI TE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
._
Blend Weieht. Pounds .
Date
Laboratory DiSOQSitiOJL
VMCA-
Batch Status
87 81,000 7-22-77
PASSED
ADoearance (White.Dowded.soli i)
Size, % thru No. 20 Sieve
Heating Loss. %_ _
__
Polyvinvl Chloride.. % _ . _ _
Inherent Viscosity . _ _ _
Foreign Matter. Slurrv . _ ...
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum)
Water. %
......
(1.0 max.)
Polyvinvl Alcohol. %
Heat Stability
Lead. QDm
Solution Tests
(5 maximum)
..yiscositx^ps____ Color Turbidity
(300/450) (80 min.) (85 min.)
Insoluble Ma 11 er, %
10% Solution
(0.03 max. )
SDecial Solvent
.Aonarent Density.__1 bs/nu.ft.
Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(1 max.)
PASSED
2.0 80.9 0.32 4 0.3
3 305 91 93 0.01
2.5 <0.5
Dr.J,J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 TC Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mfl
OZl plANt iabotatcry 7-26-77
CONFIDENTIAL UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
ucc
109468
(a) A CORRECTED REPORT
"BAKEL1TE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight, Pounds
Date
Laboratory
nisoosltion
VMCA-
Batch Status
86 81,000 7-15-77
PASSED (a)
ADoearance (White.powded.soli 1)
PASSED
Size. 1 thru No. 20 Sieve Heatinsr Loss. Polvvinvl Chloride. 1 Inherent Viscositv Foreign Matter, Slurry Water . 3,
(3.0 max.) 2.1 (79.0/82.0) 81.0 (0.30 min.) 0.31 (9 maximum) 8 (1.0 max.) . 0.5
Polvvinvl A1 oohol. %____________
Heat Stabilitv
I.eari. nom ........
Solution Tests
Viscositv r cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
5 305 (a) 100 100
Insoluble Matter, %
101 Solution Special Solvent
(0.03 max.) 0.004
A DDarent Density.__lbs/ru . ft. Maleic acid, %
(2.2/2.5)
2.5
VCL MONOMER, PPM
(1 maximum) <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr. IV. T.Gray, Bldg. 88 TC M^.G, S, Peacock, 312 Mr.T.J.Salerno,312 Mr. R. N.Wheeler,189
mf 1
Redisnnsit- nned. Please
irt Hatpri
/} j
c
A ft irinri-r, . LUNr UrNT A
iwuiunL
y-~i '
PLANT LABORATORY
8 9 77
UNION CARBIDE CORPORATION
chemicals and plastics
south charleston, west va.
ucc
109469
Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
83 79,200 3-21-77
84 58,500 3-18-77
REJECTED * REJECTED *
4 (CEF)
4 (CEF)
85 63,000 3-19-77
REJECTED 4 (CEF)
Appearance (White.powded.soli I)
Size. % thru No. 2Q Sieve
Heating LPSS,-.%_____________ Polyvinyl Chloride. % Inherent Viscosity_________
(3.0 max.) (79.0/82.0) (0.30 min.)
Foreign. Matter^ .S-Lurry------
(9 maximum)
Water. %_______________________
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stability________
Lead, .ppm.. _
Solution Tests
.Visapsity.cpa .. .Calox_____________ Turbidity________
Insoluble Matter, %
10% Solution Special Solvent
(5 maximum) (300/450) (80 min.) (85 min.) (0.03 max.)
Aaaaxfiat. Density Ibs/cu. ft, Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(DAR)
PASSED
1.8 83.0 * 0.32 10 * 0.25
10 * 480 * 85 93 0.01
2.2 <0.5
PASSED
1.5 82.1 * 0.32 7 0.3
5____ 400 82 90
oToT
2.0 * <0.5
PASSED
1.7 82.4 * 0.31 6 0.3
Q* 350 83 91 0".008
2.1 * <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg. 88 Texas City Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
CONFIDENTIAL
PLANT 1XB0RATCR Y 4. x 3.77
UNION CARBIDE CORPORATION
CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA
mf 1
UCC - 109470
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number Blend Weight . Pounds
Date
Laboratory Disoosition
VMCA-
Batch Status _.......................... .
82 117,000 3-11-77
REJECTED * 4 (CEF)
ADoearance (White.Dowded.soli O
Size. $ thru No. 20 Sieve Heating Loss.. $ Polvvinvl Chloride. inherent Viscositv Foreign Matter, Slurry............... Water_L_i
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polvvinvl A1 COhoi. %_______________
Heat Stability
...........
Lead, oom
Solution Tests
.
Visoosity,cps Color
(5 maximum) (300/450) (80 min.)
Turbidity
(85 min.)
Insoluble Matter, %
10$ Solution Special Solvent
(0.03 max.)
ADoarent Density .__1 bs/cn.ft .
Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(DAR)
PASSED
2.4 82.0 0.31 8 0.2
8* 341 92 97 0.004
2.25 <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 Texas City Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
CONFIDENTIAL
UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
mf 1
ucc
109471
"BAKELJTE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weieht. Pounds
Date
Laboratory
Disposition.
VMCA-
Batch Status
80 36,000 11-16-76
81 33,750 11-15-76
REJECTED * REJECTED *
4 (CEF)
- 1 iCEEL... ,,
Appearance _ fWhite.powded.soli 1)
PASSED
Size. Sf. thru No. 20 Sieve
Heatine Loss. %
__
Polvvinvl Chloride. % _ _
Inherent Viscosity
Foreign Matter, Slurry
Water.. %
. (3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
1.2 82.0
0.32
6
0.3
Polyvinyl Alcohol. % ..........
Heat Stability .....
Lead. nnm
............... (5 maximum)
Solution Tests
Visfiositv,cps Color . _
(300/450) (80 min.)
Turbidity
(85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
13 * 315 87 94 0.006
Apparent Density.__lbs/cu.ft .
Maleic acid, %
VCL MONOMER. PPM
(2.2/2.5) (DAR)
2.2 <0.5
PASSED
1.3 81.8 0.33 10 * 0.3
13 * 370 87 92 0.006
24 <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 Texas City Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
raf 1
UNION CARBIDE CORPORATION
WIVriUtlVlIALPfilUnnrMTm CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA
ucc 109472
Blend Number
Blend Weight . Pounds
Date
Laboratory Disposition.
VMCA-
Batch Status ______ . . .
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
78 13,500 11-9-76
79 87,750 11-12-76
REJECTED * REJECTED *
4 (CEF)
4 (CEF)
Appearance (White.powded.solin )
Size. % thru No.. 2Q Sieve Heating Loss^ _%______________ Polyvinyl Chloride, %_____ Inherent Viscosity__________ Foreign Matter. Slurry-----Water. %_______________________
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polyvinyl Alcohol. %
Heat Stability-----------Lead, ppm ___________
Solution Tests
-Viscosity ,,Cfls.
Color Turbidity
Insoluble Matter, %
10% Solution Special Solvent
maximum) (300/450) (80 min.) (85 min.) (0.03 max.)
Appaxsat Density, Ibs/cn.ft Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(DAR)
PASSED
2.4 81.0 0.33 10 * 0.35
16 * 308 93 99 0.006
2.4 <0.5
PASSED
2.6 81.9 0.31 10 * 0.30
10 * 325 93 93 0.008
2.3 <0.5
Dr.J.J.Brezinski,511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 Texas City
Mr.G.S.Peacock,312 Mr,T.J.Salerno,312 Mr.R.N.Wheeler,189
mf 1
plant labgratUw
.
UNION CARBIDE CORPORA TI OP
CONFIDENTIAL CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA
"BAKELJTE" vinyl resin
(Solvent Polymerization) VMCA
R1end Number
Blend Weight . Pounds
Date
Laboratory nisposltlon
VMCA-
Batch Status
77 78,750 11-18-76
REJECTED * 4 (CEF)
ADDearance (White.Dowded.soli 1)
Size. thru No. 20 Sieve Heating Loss. Polvvinvl Chloride. inherent Viscosity
Foreign Matter, Slnrrv
Water., %
. (3.0 max.) (79.0/82.0)
(0.30 min.) (9 maximum) (1.0 max.)
Polvvinvl Alcohol. _%
Heat Stability...... .
Lead. nnm
Solution Tests
Viscosity r eps Color Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Ma 11 er, %
10^ Solution Special Solvent
(0,03 max.)
Adoarent Density.__lbs/on.ft . Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
(DAR)
PASSED
1.9 82.2 * 0.32 8 0.3
14 * 275 * 92 98 0.006
2.1 * <0.5
Dr. J.J.Brezinski, 511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 Texas City Mr.G.S.Peacock, 312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
mfl
mm
11-23- 76
UNION CARBIDE CORPORATION
OAMrihrMTi A l CHEMICALS AND PLASTICS UUImNLJlN AL SOUTH CHARLESTON, WEST VA.
UCC - 109474
"BAKEL1TE" VINYL RESIN
(Solvent Polymerization) VMCA
! Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
76 74,250 11-15-76
REJECTED * 4 (CEP)
Aooearance (White.Dowded.soli i)
Size, * thru No. 20 Sieve Heating Loss. S> Polvvinvl Chloride. % Inherent Viscosity
Foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum)
Water.. %
(1.0 max.)
Polvvinvl A1 cohol. %____________
Heat Stability
Lead. DDm
Solution Tests
Viscosity f cps Color ......
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10?> Solution Special Solvent
(0.03 max.)
Apparent Density.__lbs/cn.ft . Maleic acid, %
(2.2/2.5)
PASSED
1.3 83.7 * 0.33 10 * 0.3
13 * 355 89 91 0.006
2.3
VCL MONOMER. PPM
(DAR)
<0.5
Dr,J.J.Brezinski,511 Mr.C.E.Fry, 152 Mr.W.T.Gray,Bldg.88 Texas City Mr.G.5.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
CONFIDENTIAL
mfl
UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
UCC - 109475
''BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
._
Blend Weight . Pounds____________
Date
Laboratory Disposition
VMCA-
Batch Status
74 27,000 11-8-76
75 92,250 11-9-76
REJECTED * REJECTED *
4 (CEF)
4 (CEF)
. .Appearance (White Dowded soli 1)
Size. * thru No. 20 Sieve Heatirwr Loss. 1 _ _ Polvvinvl Chloride% inherent Viscosity
Foreign Matter, Slurry
Water. %
(3.0 max.) (79.0/82.0) (0.30 rain.) (9 maximum) (1.0 max.)
Polvvinvl Alcohol. %>
Heat Stability _ .
Lead, ppm
Solution Tests
,Viscosity cps
Color Turbidity
Insoluble Matter, %
105fi Solution Special Solvent
Annarent Density.__lhs/cu.ft .
Maleic
acid,
CL
to
(5 maximum) (300/450)
(80 min.)
(85 min.)
(0.03 max.)
(2.2/2.5)
VCL MONOMER. PPM
(DAR)
PASSED
2.1 82.4 * 0.32 10 * 0.3
11 * 445 95 96 0.006
2.2 <0.5
PASSED
1.9 79.6 0.33 10 * 0.3
13 * 390 94 99 0.008
2.2 <0.5
Dr.J.J.Brezinski,511 Mr.C.E,Fry,152 Mr.W.T.Gray,Bldg.88
Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,189
Texas
City
mf 1
CONFIDENTIAL
vjjAn r ukBQftATQRY ,
-
UNION CARBIDE CORPCRATrON
CHEMICALS AND PLASTICS
SOUTH CHARLESTON. WEST VA.
ucc 109476
Rlend Number I
Rlend Weight . Pounds
Date
Laboratory
DiSDQSltiOIL.
VMCA-
Batch Status
"BAKELITE" VINYL RESIN (Solvent Polymerization)
VMCA
73 81,000 11-11-76
REJECTED * 4 (CEF)
Aooearance (White.Dowded.soli i)
Size. thru No. 20 Sieve Heating Loss. ?. Polvvinvl Chloride, t inherent Viscosity Foreign Matter, Slurry
(3.0 max.) (79.0/82.0) (0.30 rain.) (9 maximum)
Water. %
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stability
Lead. not!!
Solution Tests
_y iscosily,cps____ Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min. )
In^oluble Matter, %
10?> Solution
(0.03 max.)
Special Solvent..
Apparent Density.__1 ha/cu . ft .
Maleic acid, %
(2.2/2.5)
VCL MONOMER. --PPM__________________ (DAR)
PASSED
2.1 82.0 0.30 4 0.3
16 * 283 * 95 98 0.006
2.2 <0.5
Dr.J.J.Brezinski, 511 Mr.C.E.Fry,152 Mr.W.T.Gray,Bldg.88 T^xas City Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler, 189
. .CONFIDENTIAL
raf 1
________ PLANT LABORATORY\ 1-19-76 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
ucc 109477
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number Blend Weight . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status
72 20,250 11-3-76
REJECTED * 4 (CEF)
Appearance (White.powded.soli 1)
Size. % thru No. 20 Sieve Heatine Loss. % Polvvinvl Chloride. % Inherent Viscositv Foreign Matter, Slur-ry Water. %'
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polvvinvl Alcohol. %
Heat Stabilit.v
Lead, oom
Solution Tests
Viscositv r cps Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max.)
Apparent Density.__1 hs/cu ft .
Maleic acid, %
(2.2/2.5)
PASSED
1.6 84.7 * 0.34 10 * 0.35
9* 725 * 95 95 0.10 *
2.4
VCL MONOMER. PPM_____,,_________ __
<0.5
Dr.J.J.Brezinski,511
Mr.C.E.Fry, 152 Mr.W.T.Gray,Bldg. 88' Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,189
Texas City
CONFIDENTIAL
mf 1
>LANT LABORATOCRY 111--55--7' 6 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA,
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status_______________________
71 99.000 3-1-75
REJECTED * 4 (CEF)
|1j
Appearance (Whi t e . oo^di-d . so 11 1 )
PASSED
Size. % thru No. 20 Sieve Heatine Loss. % Polvvinvl Chloride. %
lherent Viscosity .
Foreign Matter, Slurry
Water. %
Polvvinvl Alcohol. %
(3.0 max. )
(79.0/82.0) (0.30 min.) (9 maximum)
(1.0 max. )
1.8 80.7 0.31
8 0.2
!
Heat Stability
I ,ea d nr,m
Solution Tests
Viscosity.cos
Color
Turbidity
Insoluble Matter, %
10% Solution Special Solvent
Apparent Den sity. lbs rii ft Maleic acid.
(5 maximum) (300 '450) (80 min.) (85 min.) (0.03 max.)
(2.2 '2.5 >
17 * 420 93 94 0.01
28
2.3
t
1 i l
I
VCL MONOMER, PPM
*.0.7
------------------ ------ _ ... -- --
Mr . G. P. Bigel ou , N'YO Dr.J.J.Brezinski,511
E.Eisenhour,515 5 .C.E.Fry,152y
Mr.G.S.Peacock,312 Mr.T.J.Salerno,312 Mr.R.N.Wheeler,159
UCC - 109479
CONFIDENTIAL UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA .
i ,
'BAKELI TE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Date
Laboratory
DisDosition
VMCA-
Batch Status
70 161,700 3-4-75
REJECTED 4 (CEF)
Appearance__(White.powded.soli i)
PASSED
Size. 1 thru Nq_._2.Q Sieve Heating Loss. 1 Polwinvl Chloride. 1 `nherent Viscosity Foreign Matter, Slurry Water. 1
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max. )
2.3 81.0 0.32 9 0.2
Polwinvl Alcohol. 1
Heat Stability
Lead. Dom
Solution Tests
Viscosity.cps Color Turbidity
(5 maximum) (300 /450) (80 min.) (85 min.)
12 * 390 97 97
Insoluble Matter, %
101 Solution Special Solvent
(0.03 max . ) 0.004
Apparent Density.__lbs ru.ft __
Maleic acid. ft
(2.2 /2.5 )
30 2.3
VCL MONOMER, PPM
<0.7
Mr.J.P.Bigel ow,NYO Dr.J.J.Brezinski,511 Mr.M.E.Eisenhour,515
.C.E.Fry,152 ' Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,1S9
ucc--
4AAA
CONFIDENTIAL
5-7-75 UNION CARBIDE C GRPORATION
CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
"BAKEL1 TE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weieht. Pounds
Date ........
Laboratory
Disposition
VMCA-
Batch Status_______________________
68 90,000 3-2-75
REJECTED * |
4 (CEF)
j
Appearance (White . oowded. so.li i)
Size. ?> thru No. 20 Sieve Heatine Loss. 1 Polyvinyl Chloride. <1 Ail. rent Viscosity
(3.0 max.) (79.0/82.0) (0.30 min.)
Foreign Matter, Slurry
(9 maximum)
Water. %
(1.0 max.)
Polvvinvl Alcohol. %
Heat Stabilitv
Lead. nom
Solution Tests
Viscositvf cps Color Turbidltv
(5 maximum) (300 '450) (80 min.) (85 min.)
Insoluble Matter, $
10% Solution Special Solvent
(0.03 max.)
Apparent Den sitv. lbs/ru.ft.
Maleic acid, %
(2.2 '2.5 )
PASSED
1.8 81.5 0.33 10 * 0.15
9* 365 94 95 0.006
31 2.4
. VCL MONOMER. PPM__________________
<0.7
|
1 i ! !
Ucc
Mr.G.P.Bigelow,NYO Dr.J.J.Brezinski,511 Mr.. E. Eisenhour, 515
i. L . E. Fry , 152/ .G.S.Peacock,312 Mr.T.J.Salerno ,312
Mr.R.N.Wheeler,189
CONFIDENTIAL
3-11-75
UNION CARBIDE CORPORATION
CHEMICALS AND PLASTICS
SOUTH CHARLESTON, WEST VA .
"BA KIEL I TE" VINYL RESIN
(Solvent Polymerization) VMCA
ADDearance (Wh i te.powdcU.soll i)
PASSED
Size. ? thru No. 20 Sieve Heatine Loss, ? Polvvinvl Chloride. ''herent Viscosity .
Foreign Matterr Slurry
Water. %
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
2.5 81.0 0.32 7 0.2
Polvvinvl Alcohol. % Heat Stability
Lea d. nom
Solution Tests
^Viscoa.! t,y. cps Color Turbidity
Insoluble Ma t t er, %
10?. Solution Special Solvent
ADDarent Density.__lbs/ru__ft. Maleic acid, %
(5 maximum) (300/450)
^ ^io v
^345
(80 min.)
96
(85 min.)
92
(0.03 max . ) 0.008
(2.2 2.5)
2.3
Iron, ppm (DAR)
2
VCL MONOMER. PPM
<0.7
Mr.G.P.Bigelow,NYO Dr.J.J.Brezinski,511 Mr.M.E.Eisenhour,515 i . C. E.Fry,152 ` Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,189
UCC - 109482 ------
CONFIDENTIAL
UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
"BAKELl TE" VINYL RKSIN
(Solvent Polymerization) VMCA
Blend Number Blend Weight . Pounds
Date
Laboratory Disposition
VMCA-
Batch Status_______________________
67 40,500 2-26-75
REJECTED * 4 (CEF)
Appearance (Whi te . powdt. d . sol i i)
PASSED
Size . % thru No_.__20 Sieve
Heating Lose ___________________ (3.0 max.)
Polvvinvl Chloride. 1
(79.0/82.0)
nherent Viscosity
(0.30 min.)
Foreign Hatter, Slurry
(9 maximum)
water. % ______ _
(1.0 max. )
2.1 80.8 0.32 3 0.2
Polvvinvl Alcohol. %
Heat Stability
t.eari . nnm
Solution Tests
Viscosity.cps Color
Turbidity
Insoluble Ma tt er, %
10% Solution Special Solvent
^ vJ
(5 maximum)/ 35
(300/450)
445
(80 min.)
98
(85 min.)
97
(0.03 max . ) 0.01
Apparent Den fiitv, 1hs/en _ ft. Maleic acid, %
(2.2 /2.5 )
2.4
VOT. MONOMFR. PPM____________
<0.7
l'
Mr.G.P.Bigelow,NYO Dr.J.J.Brezinski,511 'r.M.E.Eisenhour,515
. .C. . Fry , 152 1 Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,189
-
ucc 109483
CONFIDENTIAL
3-7-75 UNI GW CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WIST VA.
\'
"ELAKEL1TE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Dat e
Laboratory Disposition
VMCA-
Batch Status
60 81,000 2-23-75
REJECTED 4 (C. F.F) .
Appearance (White.powdedsoli i)
Si2e. % thru No. 2Q Sieve Heating Loss. % Polvvinvl Chloride. % j, herent Viscosity Foreign Matter. Slurry Water.--%
(3.0 max. ) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max. )
Polvvinvl Alcohol. %
Heat Stability
Lead, ppm
Solution Tests
Viscosity r cps
Color Turbidity
(5 maximum) (300 /450) (80 min.) (85 min. )
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max. )
PASSED
1.3 81.1 0.31 5 0.3
365 97 92 0.006
Apparent Density.__l.hs/cu. ft Maleic acid,
(2.2 /2.5 )
2.3
VCL MONOMER, PPM
<0.7
^l ^ ^ \,Y
*w
Mr.G.P.Bigelow,NYO Dr.J.J.Brezinski,511 V M.E.Eisenhour,515 M- .C.E.Fry,152 t Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,189
ucc . 109484
CONFIDENTIAL SDCTTTTiraJfTaST---------- 2-27-75" UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA,
Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
"BAKELITE" VINYL RESIN (Solvent Polymerization)
VMCA
66 103,500 2-22-75
REJECTED * 4 (CEF)
! Aooearance (Whlte.oowded.soli 3)
PASSED
I Size. ** thru No. 20 Sieve j Heating Loss. 1 _ 1 Pc' -vinvl Chloride. % L nherent Viscosity
Foreign Matter, Slurry Water. %
(3.0 max. ) (79.0/82.0) (0,30 min.) (9 maximum) (1.0 max. )
2.6 79.1 0.31 4 0.2
Polvvinvl Alcohol. %
Heat Stability
l ea d . nnm
..
Solution Tests
Viscosity.cps Color
Turbidity
Insoluble Matter, %
10% Solution Special Solvent
(5 maximum)/ 16 *)
( 3'450 ) ~3~0"cf
(80 min.)
98
(83 min.)
97
(o.o3 max . ) 0.004
Apparent Density.__1 bs,'cu . ft . Maleic acid, %
(2.2 '2.5)
2.67 *-----
VCL MONOMER, PPM
<0.7
) 1
----
Mr . G. P. Bi gelow , N'YO Dr T.J.Brezinski,511 )4r.-,.E.Eisenhour,515
r.C.E. Fry, 152^ tyr.G.S,Peacock,312 Mr . T.J.Salerno,312 Mr.R.N.Wheeler,,189
-
ucc
CONFIDENTIAL
>LANT LABORATORY 3-4-75 UNION CARBIDE CCRPCRATICH CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA
"BAKEL1TE" VINYL RESIN
(Solvent Polymerization) VMEA
Blend Number Blend Weieht Date Laboratory Disposition Batch Status
Pounds VMCA-
62 81,000 2-18-75
63 81,000 2-21-75
REJECTED
REJECTED *
ADoearance (White.oowded.soli 3)
PASSED
Size, % thru No. 2Q Sieve
Heating Loss. %
.
P-'vvinvl Chloride. 1
llnnerent Viscosity..
.
Foreign Matter, Slurry
Water.. % Polyvinyl Alcohol. 1
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max. )
2.9 80.2 0.33 io * --
0-2_
, |#
Heat Stability
Lead, onm
........................
Solution Tests
Viscositv.cps Color Turbidity
(5 maximum)^ 8
(300 /45U )
325
(80 min.)
99
(85 min . )
92
)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max . )
0.004
Apparent Density.__ 1 ba ,'cu . f t . Maleic acid, OVf
(2.2/2.5)
2.5
VCL MONOMER, PPM
Iron, ppm
(DAR)
<0.7 1
PASSED
2.7 80.3 0.32 10 *------0.2
> (
313 96 99 0.004
2.6 --<0.7
2
Mr. G.P.Bigelow,NYO Dr T,J.Brezinski,511 *.Mi .. E. Eisenhour, 515
r.C.E.Fry,152 S Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr . R. N. Wheelery 18-9
ucc
CONFIDENTIAL
kBOUfTSfT 2-27-75 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA .
"BAKELITE" VINYL RESIN
(Solvent Polymerization) VMCA
Blend Number
Blend Weight . Pounds
Date. r-- Labors tory
Disposition
VMCA-
Batch Status
65 128.750 2-19-75
RF.JF.rT7n *
! 4 (CEF)
|
j1! i i ;
i
Appearance (Wh i11.. dqu deu . a-ol i i)
PASSED
Size. 1. thru No. 2Q Sieve Heating Loss. % Polwinvl Chloride. %( Inherent. Viscosity .oreign Matter, Slurry
max.) 'K2.0)
(1 >,3 o min.) (9 maximum)
2.6 80.2 0.32 10
Water. %
i1 0 max . ) 0.2
Polwinvl Alcohol. T
Heat. Stability----------Lead, ppm
Solution Tefts
I n.` ol ub 1 e Ma t ter. %
.Yis-coslly , cca - _ Caior
Turbidity__________
I 0^ Solu,tJ_on____ Special Solvent
(5 maximum) iluo o.vi) ; v> m l r , ) ( *3 nn:.)
( i.' i;; tnx . )
315 97 95 0.006
Apparent Density.--Lbi... an. ft.. Maleic acid. 0
VCL MONOMER. PPM
Iron, ppm. ___
U.. d.a
1 2.5 4--------i < 0.7
I 1
1
Mr . G. P. Bigel ou . NY0 Dr.J,J.Brezinski,511 Mr . M, E. Eisc nhuiir,, 515 "r.C.E.Fry. 152 j .r . G. 5. Pea cut. k , 312 Mr.T.J.Salerno,312
Mr.R.N.Wheeler,189
UCC - 109487
CONFIDENTIAL
PLANT LABORATORY2-27-75 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA .
Blend Number
Blend Weiehi . Pounds
Date
Laboratory
Disposition
VMCA-
Batch Status
'BAKELITE" VINYL RESIN (Solvent Polymerization)
VMCA
64 99,000 2-15-75
PASSED !
Appearance (Whi te.powded.sol i 1)
Size. % thru No. 20 Sieve
Heatine Loss. % Polvvinvl Chloride. %
T herent Viscosity .
Foreign Matter. Slurrv
Water. %
_. ...
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max.)
Polyvinyl Alcohol. %
Heat Stability
[.pa ri onm
(5 maximum)
Solution Tests
L.,.YiscQSiiy.,LCH5____ (300 '450)
Color
_
_ (80 min.)
Turbidity
(85 min.)
I ns-oluble Ma t t er . %
10% Solution Special Solvent
(0.03 max.)
Apparent Density...__lbs cu.ft .
Maleic acid, C
(2.2 '2.5 )
VCL MONOMER PPM
PASSED
2.9 79.8 0.32 9 0.2
<.
2 313 J 92 94 0.002
2.5 . <0.7
1i
----------------------------------------------------------- ----------------- -------- . .
Mr.G.P.Bigelow,NYO Dr.J.J.Brezinski,511 Mr.M,.Eisenhour,515 ! C. E. Fry ,152 Mr.G.S,Peacock,312 Mr.T.J,Salerno,312 Mr.R.N.Wheeler,189
ucc - 109488 _
CONFIDENTIAL
TLaht umutATUn 2-18-75 UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
Blend Number
Blend Weight . Pounds
Date
Laboratory
Disposition....
VMCA-
Batch Status
"BAKELITE" VINYL RESIN (Solvent Polymerization)
VMCA
61 101,250 2-11-75
PASSED
Appearance (Wh i te.powded.sol i 1)
Size. * thru No. 20 Sieve Heating Loss. 1 Polvvinvl Chloride. 1
ierent Viscosit.v Foreign Matter, Slurrv Water. %
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1.0 max. )
Polyvinyl Alcohol, i
Heat Stability
Lead . DDtn
Solution Tests
Viscosity. cns Color
Turbidit y
(5 maximum) (300/450) (80 min.) (85 min.)
Insoluble Matter, %
10% Solution Special Solvent
(0.03 max. )
A oparent Density. lbs cu . ft___
Maleic acid, CC '
(2.2 '2.5)
PASSED
2.6 81.4 0.32 8 0.2
5 320 98 96 0.006
rj^
2.3
VCL MONOMER. PPM
Mr.G.P.Bigelow, NYO Dr.J.J.Brezinski ,511 Mr M.E.Eisenhour,515 M. E.Fry, 152/ Mr.G.S.Peacock,312 Mr.T.J.Salerno,312
Mr . R. N. WheelerM.l89
<0.7
-- Uc - I094fto
-----------
CONFIDENTS
PLANT CJbcKAtCFY 2-18-75 UNION CARBIDE CGRPCRATICN CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA.
Blend Number Blend Weight Da t_e Laboratory Di s_oos i tlon Batch Status
Pounds VMCA-
"BAKELITE" vinyl resin
(Solvent Polymerization) V MCA
51 ' 81,00'j :9-29-74
1 ' REJI-.C 1 I'D '
' 52 101,250
, 10-1-74 '
REJECTED *
53 81,000 10-7-74
REJECTED *
ADDearance__Wh ite.oowded.>oli i)
PASSED
Size. thru No. 20 Sieve Heating Loss. % Polvvinvl Chloride. % Inherent Viscosity 1F =ifn Matter Slurry Water. %
(3.0 max.) (79.0/S2.0) (0.30 min.) (9 maximum> (1.0 max.)
1 . 82.2 0.34 3
0.2
Polvvinvl Alcohol. %
Heat Stability
Lead. nnm
Solution Tests
Viscositv r cps Color
(5 maximum) (300/450) (80 min.)
Turbidity
(85 min. )
Insoluble Matter, %
101) Solution Special Solvent
(0.03 max. )
...
ADoarerrt Density__lbs/cu. ft___
Maleic acid, 'O
(2.2/2.5)
10 * 495 * 95 93 0. u 04
2.5
VCL. MONflMFR,
1.5
1 PASSED
PASSED
: 1 -9 i H1,6
2.5 81 .1
; 0.32
0.32
;3 1 0.3
9 0.3
, i
!9 * : 380
22 `__________ 335
i 95 97
! 98_____________ 33_____________
' 0.006
0.0U8
_J_________________ I
o3
2.8 *
< 1 .5
v 1 .5
V r . G . P. B i e 1 ir* . NYO Dr.J.J.Brtzinski,511 .Mr.M, E. i~( r.hour ,515 -Mi1. C . E. Fry .152 Vi . S. Pc-acock. 312 It. T. J. Salerno, 312
Mr ,R.N. Wheelerl`189
CONFIDENTS
PLANT JlBOfuOiRY
UNION CARBIDE CCRP^KaHoN4 CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA .
1 .i B1end Number ! E1 n d W e 1 e' .
Pounds
' DC-r e
i 1 a oora iorv
1 -s --- *t~ v 1 L-IQL. _ . . V'>`CA- _
: rj a t c n Statu?
"BAKELITE" VINYL FES IN (Solvent PnlyBfrizj1
^i,
JM . "3 l-i-O 7 i
55 1 -.750 <'-27-74
56 81,000 10-4-74
T; A v I
EEJECTED * 1 <CEE)
REJECTED * 4 (CEF)
[); .J.J.Q]cZin>ki,511 Mr M F.. t.ot nhuur, 315 *rr r i. Fry , 152 Mr . S. Pt acor k , 312
m . T.J.Salerno,312 .R.X.Whe c1e r , 189
CONFIDENTIAL
PLANT LABoftATCR Y^^* ^ 10-18-74
UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA .
Blend Number
Blend Weigh! . Pounds
Date
Laboratory
DlSOOSltdOr.
VMC A-
Batch Status
"BAKEL1TE" VINYL RESIN
(Solvent Polymerization) VMCA
i1 3` \ 92,25*
!10-5-74 |
`rejected
58 118,600 10-8-74
59 33,750 10-5-74
REJECTED * REJECTED *
ADoearance (White.Dowded.soli i)
Size. 1 thru No. 20 Sieve Heatine Loss, i Polyvinyl Chloride. 1 Inherent Viscosity
.irei gn Matter, Slurry
Water. %
(3.0 max.) (79.0/82.0) (0.30 min.) (9 maximum) (1,0 max. )
Polvvinvl Alcohol. 1
Heat Stability
T.eflri nnm
Solution Tests
Viscosity,cps____ Color
Turbidity
(5 maximum) (300/450) (80 min.) (85 min . )
Insoluble Matter, %
lOI Solution Special Solvent
(0.03 max.)
Apparent Density.__lbs/cu.ft.
Maleic acid, %
(2.2/2.5)
VCL MONOMER, PPM
PASSED
2.7 82.0 0.31 3 0.3
7* 296 97 98 0.004
2.0 <1.5
PASSED
2.9 81.2 0.34 5 0.3
PASSED
2.8 80.2 0.31 3 0.2
10 * 365 93 88 0.008
2.8 * <1.5
31 * 302 93 86 0.008
2.8 * <1.5
Mr.G.P.Bigelow,NYO Dr.J J.Brez1nski,511 Mr.M.E.Eisenhour,515
-.C.E.Fry, 152 .G.S.Peacock,312
Mr.T,J.Salerno,312
Mr.R.N.Wheeler,189
UCC - 109492
CONFIDENTIAL
PLjTnT LABORA'TCfcY iU~-T8-74
UNION CARBIDE CCRPCRATION CHEMICALS AND PLASTICS SOUTH CHARLESTON, WEST VA ,
\ J
Lr.tr-
,i i
REJECTED * vCEF)
PASSED
] .2 ;,1 .7 0.32
' 'J J. v
-
!j .:1... ^ i. - . ___
j Lift c. .
t S'! ,i : - | It- = *
} ! i ': ` O 1 u L . h | <*.: i r
* n ^ i-
L O ',- * . i , i, p;
> * : y ; of, ) ' ' ~ r ; ' v_ i j i ScT \ ' : . . ii>y i u ;
^"iron, ppm
'Vinyl Chloride Monomer , ppm I
'': . 0 . P . J. J
\.i . m. y:
''ri . T. .1
l -i. CD ; !v . ; '>
..r *
' v.. W ;, . I .
> .2
20 * 3B(
1 M 0.00:}
2.3
6 1.5
UCC - 109493
CONFIDENTIAL
?r.N 1
^m . ' PC
i _l
: * 4 **
' '
^ ~^k TCrV ' 6-3-'tT"
,! ; '*PCR.\T1 'J*
' PLASTICS i ' TON , *ET A .
r
U* X F i
r f ' ' j: - : t: j >
REJECFED .CEE)
PASSED
# ,o.t ' I .... i- i: 1
Sc I v. t ; -: It'' -
i O :it; J V.j. : u:- 7
w'-: vr T j -;;i i J i I i'_ i i ' EoliJ 1 U.M
i A j. pa r c: ' l v r h l i v., : i .
j Iron, ppm
l Os, l l
' Vinyl Chloride Monomer, opn
' .U. i . J. '.
V. 1
,j V
; .\ '*
A.
-i.O
* 370 >7 s' sJ 0.00.
2.2 3 '1.3
3v
CONFIDENTIAL
A- '
. t)9
49 96,000 5-27-74
REJECTED * REJECTED * (c&f) ... ;_.iCE),
PASSED 3.2 *
PASSED
2 . ei 23 .4 '*.32 1 0.3
2 *
! 15
-o
* 305
1 09 0.004
2.6 4
1.5
UCC - 109494
'' (
1
- ' -r J ' ' 6-3-74
. r . e> > SA 71 ON
I , ` iJ r i_ \ > : J C T-
s \ i\\ t,s rc*i*,
r /A .