Document v1wQmjnErKBj7gjGx43nnbXp6
Mass Spectrometry Gas Chromatography Leak Detection
Yq. Mr. E. K. Borch Amboy Terminaling Company 560 State Street Perth Amboy, New Jersey 08861
47 INDUSTRIAL ROAD BERKELEY HEIGHTS. NEW JERSEY 07922 TEL (200 464-3331
ANALYTICAL REPORT NO. G.A.S. 33549
MATERIAL SUBMITTED:
Date Reported: 5/3/75
Date Requested: 4/29/75
P.O. No.
Verbal
Monitoring for Vinyl Chloride Monomer.
INFORMATION REQUESTED:
Gas Chromatography Analysis
NOTEBOOK REFERENCE:
NB 350 page 84.
RESULT OF INVESTIGATION:
This investigation was undertaken to determine the concentra tion of vinyl chloride in the Warehouse Area at Amboy Terminaling.
On April 29, 1975, Mr. J. Traina of Gollob Analytical Service visited Amboy Terminaling and monitored the Warehou ambient air with NIOSH approved charcoal tubes. In addition, several grab samples were taken in special evacuated glass containers. All samples were then returned to the G.A.S. Laboratory and analyzed by Flame Ionization Gas Chromatography for vinyl chloride. All data are presented in the tables.
Continued
RNW 3561
GOLLOB ANALYTICAL SERVICE CQRP.
Mr. E. K. Borch Amboy Terminaling Company
2- -
G.A.S. # 33549
Area Monitored Bay 640 & 641
Bay 664 & 665
Time
0916-1016 1019-1118 1122-1220 1221-1329
0920-1021 1021-1126 1129-1225 1228-1332
Vinyl Chloride Monomer
Concentration ppm Volume/Volume
.25 TWA'.
.39
.73
.61
.24 T^A1
.31
.35 . V7
.37
Bay 618 & 619
0907-1007 1008-1107 1112-1213 1217-1324
.18 TwA-
.23
.69 . 'U
.34
Bay 542 & 543
0933-0949
.55
564 & 565
0957-1012
.52
518 & 519 *
1038-1053
.19
418 & 419
1150
ND .1
-464 & 465
1145
.1
440 & 441
1143-1158
.33
340 & 341
1236-1251
.25
318 & 319
1239
ND .1
364 & 365
1244
ND .1
240 & 241
1302-1317
.40
218 & 219
1305
.18
264 & 265
1352
ND .1
ND *= none detected, less than
NOTE: Except for the grab samples all other samples were collected
on NIOSH approved charcoal Lot #105 with Sipin pumps calibrated at
50cc/minute.
* Door opened before this sample was taHen. Mr. Traina requested
that this door be closed before sampling was started. ach 5/5/75
RNW 3562
Gollob Analytical Service Corp.
--------------------- .Mass Spectrometry Gas Chromatography Leak Detection
Mr. E. K. Borch TO: Amboy Terminallng Company
560 State Street Perth Amboy, New Jersey 08861
47 INDUSTRIAL ROAD BERKELEY HEIGHTS. NEW JERSEY 07922 TEL. (201) 444-3331
ANALYTICAL REPORT NO. 33549 G.A.S.
MATERIAL SUBMITTED:
Date Reported: Date Requested: P.O. No.
5/3/75 4/29/75 Verbal
Monitoring for Vinyl Chloride Monomer
INFORMATION REQUESTED:
Gas Chromatogrdphy Analysis.
NOTEBOOK REFERENCE:
NB 350 page 84.
RESULT OF INVESTIGATION: This investigation was undertaken to determine the concentra
tion of vinyl chloride in the Warehouse Area at Amboy Terminallng. On April 29, 1975, Mr. J. Traina of Gollob Analytical Service
visited Amboy Terminaling and monitored the Warehouseambient air with NIOSH approved charcoal tubes. In addition, several grab samples were taken in special evacuated glass containers. All samples were then returned to the G.A.S. Laboratory and analyzed by Flame Ionization Gas Chromatography for vinyl chloride. All data are presented in the tables.
Continued
.A
RNW 3563
By. GOLLOB ANALYTICAL SERVICE CORP.
Mr. E. K. Borch
Amboy Terminaling Company
-2-
G.A.S. # 33549
Area Monitored Bav 640 & 641
Time
0916-1016 1019-1118 1122-1220 1221-1329
Vinyl Chloride Monomer Concentration pom Voluee/Volume
.25 .39 .73 .61
Bav 664 & 665
0920-1021 1021-1126 1129-1225 1223-1332
.24 .31 .35 .37
Bav 618 & 619
0907-1007 iooa-1107 1112-1213 1217-1324
.18 * .23 .59 .34
Bav 542 & 543
0933-0949
.55
564 & 565
0957-1012
.52
513 & 519 *
1038-1053
.19
413 & 419 ,, . -454 & 465
440 & 441
1150 1145 1143-1158
ND .1 .1 .33
340 & 341
1236-1251
.25
318 & 319 ' i 364 & 365
1239 1244
ND .1 ND .1
.
240 & 241
1302-1317
.4
718 & 219 264 & 265
1305 1352
. .18
ND .1 '
/V
ND a none detected. less than
-
NOTE: Except for the grab samples all other samples were collected
on NIOSH approved charcoal Lot #105 with Sipin pumps calibrated at
50cc/minute*
* Door opened before this sample was tatfen. Mr. Traina requested
that this door be closed before sampling was started.
ach 5/5/75
RNW 3564