Document v1ppamGvMOM36LkJM74OVQ4J6

j;q waiter c. mc crone associates, Inc. r&i as CONSULTING: ULTRAMICROANALYSIS MICROSCOPY' SMALL PARTICLE PROBLEMS' SOLID-STATE CHEMISTRY 14 June 19,77 Dr. Joseph P. Simko, Jr. Colgate-Palmolive Company 909 River Road Piscataway, New Jersey. 08854 Dear Dr. Simko: Using transmission electron microscopy and selected area electron diffraction, we have analyzed a sample of talc designated as Lot no. 6-1-2. We found no asbestiform minerals in this talc. A general description of this talc Is as follows: some of the talc showed shards and rolled talc, the level of fines was moderate and the talc particles were generally equlaxial rather than large thin plates. Thank you for consulting MeCrone Associates If there are any farther questions concerning this report, or the data herein, please feel free to contact me. Very truly yours, GRG:j d Ref. MA 5500 G. B. Grieger Senior Research Physicist CAM-95 PLAINTIFF'S EXHIBIT (s_ 2820 SOUTH MICHIGAN AVENUE 'CHICAGO, ILLINOIS 60616. 312/842.7100 CABLE: C}-IEMICROHE QE-cpc00004o7e I II e QE-CP000004077 PROJECT COST RECORD PROJECT TITLE: Talc samples SPONSOR: ADDRESS: COLGATEPALMOLflJE COMPANY 909 River Road Piscataway, New Jersey 08854 PROJECT NO.: MA3884 DATE RECEIVED: 3/12/74 P.O. NO.: 615139 COMMLTMENTS.$ Contact: Mr. J. P. Simko, Jr. Telephone No. SUMMARY OF PROBLEM: Lab Notebook References: No. pp. Initials No. pp. Initials No._____ pp. Initials Photomicrographic record no. Sample disposal: returned filed (where) discarded Individual time (Exclusive of oper. .h.me on Inst. below) Date Name H3ourrIs1 Charge tO DIRECT COSTS Travel Date Traveler Destination SEM TEM XRD EMP lIvIP ESCA time Outside Services Date Hours Charge Date 's/n/iq - vOf Photo Photo Materials Supplies (./-jYO Company Charge Summary Cost Individuals 1 $ Ins trtiment VTravel Outside Other Cost IrInstrument Total Charge $ OK for billing Project Ldr I Group Ldr PROJECT LEADER ROUGH DRAFT REPORT RECEIVED IMS TOTAL CHARGE $ C'..?) 770BILLED TO CLIENT $ . INVOICE NO.(S) 266 QE-CPC00004078 Res4ew waiter c. mc crone associates, Inc. CONSULTING: ULTRAMICROANALYSIS. MICROSCOPY SMALL PARTICLE PROBLEMS . SOLID-STATE CFIEMISTR<_ 26 March 1974 Mr. J. H. Simko, Jr. Colgate-PaLnolive Company 909 River Road Piscataway, NJ 08854 Dear Mr. Simko: As per your request, we have examined three talc sanples, 85, 120 and 123, that you had submitted to us for chrysotile and tremolite analysis using IBM and SALT) methods and have seen no evidence of chrysotile or of fibrous amphiboles in any of the samples. We noted fibrous inorganic material in all samples - some of which resembled chrysotile or tremolite. However, on consideration of the diffraction patterns from these fibtrs, we found them to be nonasbestiform mainly "rolled talc" or halloysite (one of the kaolin group of minerals). I have appended representative photoxnicographs in order to show typical material and how closely some of the fibers resemble (morphologically) chrysotile or one of the amphiboles. Thank you for consulting McCrone Associates. If you have any questions regarding the material contained in this report, please do not hesitate to call Yours sincerely, Enclosure PS: smg Ref. 3884 Richard Shinps Research Chemist u2O SOIJIII MICIIICJAN AVINUE CIIICACO. L.LINOIL CO(1G 312J$.12-7100 CABLE CIiLI1ICRONE QE-CF000004079 Memo from FRANCES EINOINDER Zc;I xTh9 QE-CP000004060 wafter c. mc crone associates, Inc. CONSULTING: ULTRAMICROANALYSIS- MICROSCOPY- SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 26 March 1974 Mr. J. M. Simko, Jr. Colgate- Palmolive Company 909 River Road Piscataway, NJ 08854 Dear Mr. Simko As per your request, we have examined three talc samples, 85, 120 and 123, that you had submitted to us for chrysotile and tremolite analysis using TEM and SAED methods and have seen no evidence of chrysotile or of fibrous amphiboles in any of the samples. We noted fibrous inorganic material in all samples - some of which resembled chrysotile or tremolite. However, on consideration of the diffraction patterns from these fibers, we found them to be nonasbestiform mainly "rolled talc" or halloysite (one of the kaolin group of minerals). I have appended representative photondcrographs in order to show typical material and how closely some of the fibers resemble (morphologically) chrysotile or one of the amphiboles. Thank you for consulting McCrone Associates. If you have any qstions regarding the material contained in this report, please do not hesitate to call. Yours sincerely, Enclosure RS smg Ref. 3884 Richard Shimps Research Chemist 21120 SOUTh MICHIGAN AVENUE - CHICAGO. ILLINOI!J 00516. 312/542-7100 CABLE. CHEkIICROtIE QE-cPc00004081 *ECI%O MAR 1 2 ism. COLGA TB-PALMOLIVE COMPANY.... A Dtlawan Corperatlo,, RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscataway, New Jersey 08854 March 8, 197k Mr. Ian Stewart Mccron.e Associates 2820 South Michigan Avenue Chicago, Ill moSs 60616 Dear Ian: I am enclosing three talc samples, labeled No. 8, No. 120 and No. 123, for analysis. We want you to determin chrysotile and tremolite. Please use TEM and SAJD as the method as you di& for the other materials we sent you (report dated 2/15/7k by Richird Shimps, Ref. 3805). Please attach the number 615139 on an charges bifle. to our company for this work. Many thanks. SSncerely, JPS: C 51374 QE-CP000004082 QE-CP000004083 PROJ ECT COST RECORD PROJECT TITLE: SPONSOR: ADDRESS: TEM and SAED of 7 talc samples COLGATE-PALMOLIVE CO. 909 River Road Piscataway, New Jersey 08854 Contact; J. P. Simko Telephone No. PROJECT NO.: MA 5259 DATE RECEIVED: 3 8 76 P.O. NO. :634965 1750 COMTVIITMENTSI (201) 463 1212 SUMMARY OF PROBLEM: Lab Notebook References: NNo.o__.___p_ ppp.. Initials Initials No._____ pp. Initials Photomicrographic record no. Sample disposal: returned filed (where) discarded Individual time (Exclusive of open time on Inst. below) Date Name Hours Charge DIRECT COSTS Travel Date Traveler Destination Instrument time Date SEM TEM XRD E1\&P IMP ESCA Hours Outside Services Charge Date Photo ;.m Photo ivlaterials Supplies Company Charge Summary Cost Individuals $ Instrument Travel Outside Other Cost Total .g!are I OK for billing Project Ldr Group Ldr PROJECT LEADER ROUGH DRAFT REPORT RECEIVED GG TOTAL CHARGE $ to'o BILLEDTO CLIENT $ - INVOICE NO. (5) QE-CF000004084 kYAYA ,sti waiter c. mc crone associates, Inc.A CONSULTING: IJLTRAMICROANALYSIS MICROSCOPY- SMALL PARTICLE PROBLEMS . SOLID-STATE CHEMISTRY 11 May 1977 Dr. J. P. Simko, Jr. Colgate-Palmolive Company 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko: The examination of your latest talc sample, utilizing transmission electron microscopical techniques, has been completed. The sample was designated: Colgate, MTB-Talc-Code M-6670--2, Lot No. 5-2-3, Date 5-3-77. This specimen was found to contain, principally, talc with a wide size range but without an excessive amount of material, at either extreme of particle size. Talc shards were found as were occasional talc ribbons. Goethite fibers were found with the largest one being about 1.6 X .15gm in size. Goethite is an iron oxyhydroxide and is associated with calcite, quartz, and other minerals. Additionally, goethite may be found as a weathering product of various minerals, as a direct precipitate in various water sources or from an iron gel. No asbestiform material was detected. If shy questions should arise concerning this analysis, please do not hesitate to contact me directly. Sincerely, RJS:jd Ref. MA 5500 Richard 3. Shimps Research Chemist 2820 SOUTH MICHIGAN AVENUE. CHICAGO, ILLINOIS 60616 .312/842-7100. CABLE: CHEMICRONE QE-0PC00004085 te Th-(Qz( 1 AlA waiter c. mc crone associates, inc. CONSULTING: ULTRAMIOROANALYSIS' MICROSCOPY. SMALL PARTICLE PROBLEMS . SOLID-STATE CHEMISTRY 9 May 1977 Dr. 3. P. Simko, Jr. Colgate-Palmolive Company 909 River Road Piscataway, lew 3ersey 08854 Dear Dr. Simko: The transmission electron microscopical examination of your latest talc sample had been completed. The sample bore the following designation: Cogate-presbipment sample, MTR Talc, Code M6670-2, Lot no. 4-26-27, Date 4-26-77. - This sample was found to consist mainly of nonfibrous talc with a wide particle size distribution but without an excessive amountof - fine thaterial. Fibrous aspect talc particles were also found to be present such as shards and ribbons. No asbestiform material was found to be present. Thank you for consulting McCrone Associates once again. If any questions should arise concerning this analysis, please do not hesitate to call. Sincerely, RJS:jd Ref. MA 5500 Richard J Shimps Research Chemist 2820 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS 60618. 312/842-7100 CABLE: CHEMICRONE QE-CP0000Q4O86 COLGA YE-PALMOLIVE COMPANY A DeIa,t'are Gpora:ion RESEARCH AND DEVELOPMENT DEPARTMENT 909 Rivcr Road Piscaraway, New Jcrsey 08854 June 3, ig6 Mr. Gene Grieger Mccrone Associates 2820 South Michigan Avenue Chicago, IL 60616 Dear Gene: Enclosed is one sample of talc for study by TEM and S$ED analysis, lot number 5-28-29. I will telephone you the Purchase Order number as soon as possible. Many thanks. 6ncere3r, 3. P. Slanko JPS : da Enc. C 5137-3 QE-CPC00004087 c. mc crone associates, inc1 'AMwafterCONSULTING: UUTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS - SOLID-STATE CHEMISTRY 8 September 1976 Dr. Joseph Simko Colgate-Pahnolive Company 909 River Road Piscataway, 1ew Jersey 08854 Dear Dr. Simko: Using transmission electron microscopy and selected area electron diffraction we have examined a sample of talc designated as 8-14-15. In this sample we found no asbestiform minerals, neither amphiboles nor serpentines. We found that this sample was very platy and did have a large number of fines. We also found that in some cases in these fines there were some indications of rolled talc fibers, which we identified as talc with selected area electron diffraction. If there are any further questions concerxng this report or the data contained therein, please contact us. Very truly yours, ene R. Grieger enior Research Physicist GRG:fe ref: 5500 2820 $011111 MiC:IiIUfN AVRNL)E ChICAGO. ILL b140I8 GOGICI . 312. 342-7100 . CAOLC: CIIEMICRONU QE-CF000004088 IYiYA '.AIrlI+or rAYAVV'..A11\..tI 'r..',. rIin1n'..r..r.In'..n#icI".r.''so.QnrintcQ ;IInr a CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS. SOUOSTME CHEMISTRY 6 August 1976 Mr. J. P. Siniko, Jr. Colgate-Palmolive Company 909 River Road Piscataway, New Jersey 08854 Dear Mr. Simko; Using TEM and SAED, we have examined a sample of your talc designated as Lot 7-24-25. We found this to be an excellent quality talc, free of asbestiform minerals, both amphibole and serpentine. The talc was generally quite platy and quite acceptable. Thait you for consulting Mccrone Associates and if you should have any questions concerning these results, please contact me. Yours sincerely, Gene R. Grieger Senior Research Physicist GRG :fe ret: 5500 2020 SOUTH MICHIGAN AVENUE . CHICAGO. ILLINOIS 60616 312/042-7100. CABLE: CHEMICRONE QE-0PC00004089 kYAYA waiter c. mc crone associates, inc. CONSULTING: ULTRAMICROANALYSIS - MICROSCOPY- SMALL PARTICLE PROBLEMS- SOLID-STATE CHEMISTRY 6 August 1976 Mr. j P. Simko, Jr. Colgate-Pa]molive Company 909 River Road Piscataway, New Jersey 08854 Dear Mr. Simko This letter records the results of our analysis of a sample of talc designated as Lot 7-18-19. In our first examination of this talc we found a single fiber of chrysofile. The SAED pattern was extremely weak and does not show up on the print; however, under a lox magnifier on the negative we were positively able to confirm the fact that this is chrysotile. This would put the relative percentage of chrysotile at approximately 1-2 ppm. Upon request, we subs equently re-examined this material and in our second and third examinations of the same material, taking different samples and .1i fferent lots from the sample, we did not find any further examples of chrysotile, thus the chrysotile observed in our first examination may well have been contamination from the atmosphere or some other source. In out third examination we did find one particle of antigorite, which is also a serpentine but is not classified as an asbestos mineral. Electron micrographs of the chrysotile fiber and the antigorite particle are also included with this report. We did find a high percentage of talc shards, blocky talc and fibrous talc in this sample and 1 would estimate that between 20 and 35% was non-plaly talc. We are also including some SAED patterns which we feel may help in your future examination of these minerals. Enclosed is a standard talc electron diffraction pattern and a standard chrysotile diffraction pattern, both taken at 200 kV. Thank you for consulting MoCrone Associates and if you should have any questions concerning these results, please contact us. Yours sincerely, rGeRt:Gbt0e 0 2820 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616 Gene R. Grieger Senior Research Physicist 312/642-7100 CABLE: CHEMICRONE QE-0PC00004090 a c) 3 0C) a (0 a(00n, C) a C C-) -u C0000-) 0 (-0s r -: Sample 7-18-19 (50,000X) 1st run waiter c. mccrone associates,.inc. QE-CP000004092 SAED Talc standard waiter a mc crone associates, Inc. QE-CP000004094 2: 0o (D 2 :/ (3Ofc' waiter c. mc crone associates, Inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY. SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 8 July 1976 Mr. if. P. Simko, Jr. Colgate-Palmolive Company Research and Development Department 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko: Using transmission electron microscopy and selected area electron diffraction we have analyzed the sample of talc designated as 6-13-14. In this talc we find no amphiboles or serpentines. We do however find a rather high percentage of fines, some fine rolled talc and fine talc ribbons. This material is not very platy. Repeating again, we did not find any asbestiform minerals in this talc. Thank you for consulting McCrone Associates. If there are any further questions concerning this report or the photographs contained therein please feel free to contact me. Very truly yours, GRG:jd Ref. MA 5259 Gene R. Grieger Senior Research Physicist S. kD4bMPL .'f // 2820 SOUTH MICHIGAN AVENUE. CHICAGO, ILLINOIS 60616 312 '842-7100 CABLE: CIIEMICRONE QE-CPC00004097 ft \VAV/LrA4I II+cIr rL'. IrnI nrL''lr'.r.JnI IckLin\)os)e\J\n...r.I-\.IAn1+.cn)c1 nrLI IL', LA a i CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 24 June 1976 Dr. J. P. Simko, Jr. Colgate-Palmolive Company R&D Department 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko: Using trsnsmission electron microscopy and selected area electron diffraction, we have examined a sample of talc designated as 5-28-29. In this talc we did not find any asbestiform minerals. There were, however, a high portion of fines and an indication of fine talc rolled into fibers. This talc was platy and we have noted in the past that many of these platy taics tend to form rolls and talc ribbons. Enclosed with this report is a photograph of one of the fine rolled talc fibers. When rolled so tightly the electron ffiffraction pattern does show some streaking of the spots similar to that of chrysotile which, of course, also has a rolled structure but on an even finer scale. Calculation of the interplanar spacings, however, hows excellent agreement with ASTM data (card 13-55 8) for the <002> axis of talc. Thank you for consulting McCrone Associates. If there are any further questions concerning this report or the data contained herein, please feel free to contact me. Very truly yours, GRG:fe enclosure ref: 5259 Gene R. Grieger Senior Research Physicist 2820 SOUTH MIChIGAN AVENUE - CHICAGO. ILLINOIS 60616. 312 342-7100 CABLE; CHEMICRONE QE-0PC00004098 2 3 C) C) J (0 0 Cl, 0Cl) C-) 0 - -- We* 4W1 aC) CD d Cl) 0C,) C) 0 3b r kTYA waiter c. mc crone associates, Inc. a CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 24 June 1976 Dr. Joseph P. Simko Colgate-Palmolive Company R&D Deparbtient 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko: Using transmission electron microscopy and selected area electron diffraction, we have examined a sample of talc designated as 42728 4-27-28. This talc contained no asbestiform minerals, neither amphibole nor serpentines. This talc was extremely platy: there were fines in this material and a few ribbons, and we found this to be excellent quality talc. If there should be any questions concerning these results, please contact us. - Very truly yours, Gene It. Grieger Senior Research Physicist GRG:fe enclosure ref: 5259 2820 SOUTH MICHIGAN AVENUE CHICAGO, ILLINOIS 60616.312/842-7100. CABLE: CHEMICRONE QE-CF0000041 01 waiter c. mc crone associates, Inc.-VAYIAAII CONSULTING: ULTRAMICROANALYSI5. MICROSCOPY SMALL PARTICLE PROBLEMS . SOLID-STATE CHEMISTRY 24 June 1976 Dr. Joseph P. Simko Colgate-Palmolive Company R&D Department 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko Using transmission electron microscopy and selected area diffraction, we have examined a sample of talc designated as 4-29-30. We found no asbestiform minerals in this talc, but it did seem to have rather a large number of talc shards and there were some indications of bacterial contamination as shown in the accompanying photographs. There were fines in this talc which did not show such morphological perfection and .was not as platy as other talcs because of the lack of platiness of this talc. If there are any further questions concerning this report or the data contained herein, please contact me. Yours sincerely, Gene R. Grieger Senior Research Physicist GRG:fe enclosure ref: 5259 2820 SOUTH MICHIGAN AVENUE. CHICAGO. ILLINOIS 60616. 312/842-7100. CABLE: CHEMICRONE QE-CPC000041 03 0 c 0 ES. C) -4 0- a C0) aC(0') ci) C p0 C-) E 0 N t COLGATE-PALMOLIVE COMPANY 4 Delawat. Corp.rati*.s RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road . PiJ-cat4wa,, New Jersey 08854 May 27, 1976 - Dr. Ian Stewart Macrone Associates 2820 South Michigan Avenue Chicago, IL 60616 Dear Ian, Enclosed is one sample of talc for study by TEM and SAED analysi, lot number t-29-3O. I win telephone you the Purchase Order number as soon as possible. Mazy thanks. JPS: is AEnclosure 3. P. Bunko C0000) C 0 0) QE-0F0000041 07 RECEkt(to; COLGA TB-PALMOLIVE COMPANY A Delawart Corp.ratien RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscatawy, New feast, 08854 79 May 7, 1976 Dr. Ian Stewart Mccrone Associates 2820 South Michigan Avenue Chicago, U 60616 Dear Ian, Enclosed is a sample of raw material talc for TEM, SAED analysis, lot number l-27-28. I will telephone you the Purchase Order number as soon as possible. ny thanks. JPS: is Enclosure 3. P. Simko C 5138-2 QE-CPC000041 08 COLGATE-PALMOLIVE COMPANY A De/awo,j Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Fiscatawa, New ferny 08854 May 27, 1976 Dr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, m 6o616 Dear Ian, Enclosed is one sanle of talc for study by TEM and. SAD analysis, lot nwnber lI-.29-30. I will teleDhone yott the Purchase Order ntimber as soon as possible. Many thanks. JPS:ls .Enc]osure 3. P. Siflo C $I3S-2 QE-CP0000041 09 V y 'VAVFLr44III+Ot-IrLC. .I-I rI'r-.'rL' -rI'L.r'rI.-lnr nLe1eO'i .)LL.I-.L-I-Ar..I-.,- II IL.-. I CONSULTING: ULTRAMICIROANALYSIS MICROSCOPY- SMALL PARTICLE PROBLEMS . SOLID-STATE CHEMISTRY 3 May 1976 Dr. 3. P. Simko Colgate-Palmolive Company R&D Department 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko: This report covers the results of the transmission electron microscopical examination of your four talc samples: JF-4-10-11, JC-4-11-12, 12-10-11, and 2-13/14, for asbestiform material. No asbesfiform material was detected in any of the four samples. The sample descriptions are as follows: - JP-4-10---11 - Platy to chunky talc particles which vary widely in size (small submicrometer to large multimicrometer sizes). Talc shards and some rolled talc are to be noted as are occasional small blocky inorganic particles. No asbestiform material was detected. JC-4-11-12 - The size ranges from quite small (<1/3 gin) to large multimicrometer particles. The talc particles vary in morphology from thin platelets to substantial chunky particles with talc shards fairly common and some occasional rolled talc being noted. Small (<1/3 gin) blocky inorganic material is also present. No asbestiform material was detected. 12-10-11 - Platy to chi.mkier types of talc particles. Some talc shards and ribbons noted. Some quite small blocky inorganic material present, occasional organic material. Infrequent, poorly diffracting, high aspect ratio (>10:1) fibers of uneven morphology (sometimes jagged) which can be positively shown not to be asbestiform material (most likely silicates of varying composition and crystallinity). 2-13-14 - Platy to chunky material is present which is mainly talc but some of the chunky materi*l is not (? quartz or carbonates). Some fibrous aspect ratio talc particles (shards, etc.) are noted which range to quite large sizes Also noted were occasional non-asbestiform non-talc fibers. This sample is pre- dominantly talc with the other materials occurring at very low concentrations. 2820 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616 312/842-7100. CABLE: CHEMICRONE QE-CP0000041 10 Dr. a. P. Siniko Page two Thank you for consulting Mccrone Associates once again. If you should have any questions regarding these analyses, please do not hesitate to call. Sincerely, Richard 3. Shimps Research Chemist RJS:fe ref: 5259 / QE-CPC000041 11 ('OLGA TB-PALMOLIVE COMPANY A Dd, wan Corporacio RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Fiscataway, New Jersey 08854 April 6, 1976 7 9?6 Dr. Ian Stewart Mecrone Associates 2820 South Michigan Avenue Chicago, IL 60616 Dear tan, Enclosed is one sample of raw material talc for TEM and SAD analysis. l-6-7.Lot jumber is I will telephone you the Purchase Order number for charges as soon as possible. Sincerely, tt. P. Siito Enclosure QE-CP0000041 12 COLGA TB-PALMOLIVE COMPANY 4 Delawarc Corp nt&n RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road . Pscataway, New Jersey 08851 March 10, 1976 Dr. Ian Stewart Mecrone Associates 2820 South Michigan Avenue Chicago, IL 60616 Dear Ian: Enclosed is a single talc sample coded CE MS No. 1. Please rim TEM-SD studies. Determine all asbestos minerals especially amphibole Please expedite this eample, I wifl phone you a purchase order No. to cover costs. Sinqerely, 3P3:ls Enclosure 3. P. Simlco, Jr. -c 5137-2 QE-CPC000041 13 /a4 t'Z /0 'J a7 Zr25?:at ,-hst4o9z-eL4LCZc..ta6OCt1#jt"Z I ci34Cia.ctC. A,4 cay4tc,_c*6.d70 ttOy ,&c( c&erzena, cAte &4- 7Lr QE-CPC000041 14 LbLJ kQ - '-1-10 II 4'VP, ztSthattAASO 'Q- o &h - c aA4 oaQ on TL& #4iA9tjeD /ta1M-$nal cf 4 to Qe PMt%A.Ctt - /. I ca9 (L IPfr.,> +cv4 ct&w -I A 9p ow4Q 1 ctl2a- (p'u..ce.ct. i(1, '' / QE-CPC000041 15 DRIGINAL PURCHASE- okbER 05217-9 :-n.. ........-------- Show this mmbet cxl Prefix c# int'osces, packing - slips and packages. eacalO COLGATE-PALMOLIVE COMPANY A DELAWARE CORPORATION 105 HUDSON STREET. JERSEY CITY, N,J. 07302 ATTEa1 DAT/////77 SHIP TO Mccrone Associates 2820 South Michigan Avenue 25j 5JE4 RGSREAYNDCISTTY.. N.J. 07302 909 RIVER RD. PISCATAWAY. N.J. 08854 13 2JE0RGSREAYNDCISTTY.. N.J. 07302 Chicago, Illinois 6o6i6 - Attn: DISCOUNT TERMS I D2110 N/3D 2 ON/3D 3 1/10 N/3D 4 Net Cash 5 Trade Dr. Ian Stewart SHIPPING TERMS I FOB Destination 2 f] FOB Shipping Pt. (Pre-Poy& SilOSee Be(ow 3 FOBShippingPt. (Collect) City WANTED SV FROM: 1/1/77 TO: 12/31/77 IF ABOVE DATE CANNOT BE MET NOTIFY 16 RJEEfClEERFVSINOGNSVTILALTEIO.N INDIANA 47130 19 RECEIVING STATWN KANSAS CITY. KAN. 66105 710 CARLrOH Sr. 221 1 BERKELEY. CALIF. 94710 26 3N0E0WPYAORRKKA. VNE.Y.. 10022 23j ATTN: Receiving Clerk YOU ARE AUTHORIZ 0 TO FURNISH THE ARTICLES LISTED HEREO IN ACCORDANCE WITH THE TERMS AND CONDITIONS OH THE FACE AND BACK OF THIS ORDER. QLJAMTITY AND UNIT SYMBOL NUMBER . PRICE This purchase order issued to cover the following analysis: (as required): - 1. Transmission Electron Itcroscopy ana Selected Area Blectron Diffraction Analysis on tale samples (TEMaAn;) . 2. X-ray analysis $oo. eac) sample 50. eac) This cancels and supersedes P.O. 635737 TAX EXEMPT -. .- VENDOR TO PROTECT ALL METAL PARTS AGAINST CORROSION BY SUITABLE PROTECTIVE SEALING. :atEF. or.? of Thwcic3s IhOHnCldCOUIbOr!Xed original bill oF lading. konspnriotion chqrg ,isit hiupore:i iQ preefrI fre -t14,?I .. COLGAfl.P4LMOLIVE Co PANY .AZtC pAcc,es with porchosa crder number, symbol n.-umber, contenft ond quantity. - Acceptance o .:jer is to bo doomed a certificqilon that YOU kayo read and ct0read Ia ib5 terms and conditions on the back IIEOCI. PAYMENT WILL NOT BE MADg AGAINST PRO FQOItA INVOICE. WSRyg Ut'tOADlNG space and thus lot heavy loads bj telephonins; 201.4324300 extonsion 309. tP.....-- 4NItQl - .. . - -- n:*r Ji:sy SLLE tio: 1J3T BE BILI.Efl ur ;-:ss XE:.:PTED BY i.TIACHED cnirtvr'-ir: 4 QE-0PC000041 16 COLGA YE-PALMOLIVE COMPANY. A Dc/a roan Crpnation RESEARCH AND DEVELOPMENT DEPARTMENT 909 Rivcr Road Piscataw4y, Now Jersay 08854 April 20, 1976 Dr0 Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, fl 60616 Dear Ian3 Enclosed are 2 raw material taics, lot nmnbers 12-10-fl and 2-13-11 for T2M and SAD analysis0 P0 nwaber tLfl foflow. Many thanks. 3, P. Sisnko Enclosure C 5138-Z QE-CPC000041 17 \t'QiE3r 'c 1:iJrE?: C 5259 resptrable CE MS no. 1 talc QE-CFC000041 18 5259 respirahle CB MS no. 1 50,000X waiter c. mc crone associates, Inc. QE-CF0000041 19 5259 CE MS no. 1 sediment amphibole \%.Q!ltv C;, mc; crone assodaic-c ii QE-CPC00004 120 A 5259 sediment CS MS no. 1 talc \!vt?i!1E3r C;. nccrcne CssoCicytc: IF QE-0P0000041 22 resp ftable CB MS no. 1 talc mc: OtC)flG c:ssc)cic)1ss; Inc, QE-CP0000041 23 rA - )- - ('- -U -I p ( C a 0 0 Cl) aC/) ci) C 20 C) E 0 I) 'TA waiter c. mc crone associates, Inc. CONSULTING: ULTRAMIGROANALYSIS- MICROSCOPY - SMALL PARTICI,E PROBLEMS SOLID-STATE CHEMISTRY 31 March 1976 Dr. J Simko Coigate-Palmoliye Research & Development 909 River Road Piscataway, NJ 08854 Dear Dr. Stnko: We examined seven samples of talc labeled "0925AX6, 02l5DX, 1971CB4, 04143 (we believe this should have been identified as 0413), 0326 and 3214." - These samples were examined in the TEM at approximately 17,000X inag- nification and also using selected area electron diffraction (SAID). We were primarily concerned with the amphiboles and serpentines which we might find in the form of fibrous, asbestos minerals. None of these were found in these samples. - We did, however, find two other unusual materials, photographs of both of which are included. One which appears to be organic from its morphology and diffraction pattern we believe to be a zinc stearate; the second we found was sodium chloride. Enclosed with this report is a SAED pattern of the sodium chloride which we have indexed positively as sodium chloride. We also examined this material using the electron microscope microanalyzer (E?5MA-4) and we did, again, find sodium and chlorine as the only elements present. Samples 0925X6 and 3214 showed less of the sodium chloride than the other samples. Thank you for consulting McCrone Associates. If you have any questions concerning this report, please feel free to contact us. Very truly yours, Enclosures GRG smg Ref Mk-5259 Gene It. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE CHICAGO. ftLINOIS G0616 3fl 042-7100 CABLE: CHEM)CRONE QE-cPc00004l 26 NaC1 (25,000X "1 - waiter c. mccrone associates, Inc. QE-CP0000041 28 tO 5217d0 a ORDER - Va., Show ibis numbet prefix on I 13- packing. 'y,QMsPIfiqA '445 COLGATE-PALMOLIVE COMPANY A DELAWARE CORPORATION 10$ HIJDSON STREET, JERSEY CITY, N.J. 07302 NIfiTI -2a 4 SHIP, TO MeCrone Associates Si'd Cfln 86 GREENEST. 251 JERSEY CITY, N.J: 07302 14 909 RIVER RD. PISCATAWAY. N.J. 08B54 j2B2OSoUth Michigan Avenue ia iso GRAND ST. JJERSEY CITY. N.J. 07302 IChicago, Illinois 60616 DISCOUNT TERMS J2/1O N/SO N/SO 1/10 N/SO Net Cash Trade SHIPPING TERMS 1 fl roe DestinatIon 2 JFo8 Shipping Pt. - (Pre-Poy& 811 !)See Be low 3 FOBShlppingPt. (allect,t CIty WAItI.TED BY RUSH IF Aea%.oAffE C.<11N0T CE MET NOTIFY 161 IIJREEYCFEErVRI5NOGNSvTIALLTEIO.N INDIANA 47130 'I RECEIVING STAtION I KANSAS CI.TY KAN. 68105 710 CARLTON ST. 221 I BERKEL.EY., CALIF. 94710 26 I 3N0E0WPYAORKRKA,VNE.Y. . t0022 ATTN: Recelvng Clerk YOU ARE AUTHORIZED TO FURNISH THE ARTICLES LISYED HEREON IN ACCORDANCE WITH THE TERMS AND CONDITIONS ON THE FACE AND BACK OF THIS ORDER. .IANTITY AND UNIT SYMBOL NUMBER PRICE Transniission Electron Microscopy and selected area electron Diffraction analysis of 1 talc saiple: :- s This is a onetime sample ATTENTION: Dr. Ian Stewart Necrone Associates - VENDOR TO PROTECT ALL ME TAX EXEMPT PARTS AGAINST CQRRO$J.tfl BY SUITABLE PROTECTIVE SEALING. oSELLERS INVOICES iliaC lncludo authorized transportation charges, must be supported by prepoici freight bill copy of original bill of lading. MARX PACKAGES with purchasearder number, symbol number,, content, and quantity. Acceptance ci this order h to be deemed a certification that you have lad and agreed to the terms and conditions on the bock hereof. PAYMENT WILL MCI BE MADE AGA NST PRO FORMA INVOICE. RE5RVE UNLOADING specs end time for heoy load, by tslcphoning: 201-4324300 extensIon 309. -COLGATE- PALMOLIVE C'MPANY a I- ---.-..2,w .nSSEI SM.ES TAX MUST BE BILL'ED UNLESS EXEMPTED t'UiGItAlC OCPAU IMENT CSPY BY ATTACHED -. CFRTIFICATE; ......-. - QE-CP0000041 30 COLGA TB-PALMOLIVE COMPANY 4 DJeUMTC Corporally, RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscaraway, New Jcrsy 08854 February 27, 1976 Mr. Ian Stewart Mccrone Associates 2820 South MLchgan Avenue Chicago, ii 60616 Dear Ian, I am enclosing seven talc samples fo' TEW-SAE)) analysis. These ifare finished products and I am interested in determining any chrysotile or amphibole, apecificafly tremolite or anthophyflite, are present. The sa1e codes are as foflows: 0925AX6 0215DX 19T1CS 0316CX 0i.JA3 0326 321h I tfl contact you concerning, the purchase order munber f this work. I need theie results as soon as possible. Any questions please contact me. Sincerely, Jbp Simko tTPS:ls QE-CPC000041 31 c1 r .d "P En 01.0'! Cc 000010 000cIe3aD I o(- .3 is f. ORIGINAL PURCHASE ORDER - S2i7-lO :4 z a';: , .!wz z qr4&-ry;jr &tZ4sch Show this number and prefix on /n- tones, pack/ng '' ;tr'i,ic.. q'- -t ' 63496S COLGATE-PALMOLIVE COMPANY A OflAWARE CaRPOR&TION NISS 105 HUDSON STREET. JERSEY CITY, N.J. 07302 AUENTi0N j-Jj. S724, DATS/3/ Sill! TO 0RtE5t. 251 JJE9SEY CITY. N.J. 07302 NOrone Associates 2820 South 1!ichigar Avenue Chicago, Illinois 60616 114p S, J9,4, DISCOUNT TERMS I J2/iO N/SO 2 jjN/3O 3 1/10 N/So 4 p Net Cash 5 >fjTrade SHIPPING TERMS 1 D FOB Destination 2 jFOB Shipping (Pce-Payc Bill)See Below S fl FOBShIppingPt. (Col!ect) City ANTED BY S. IF AB'QVE DATE CANNOT BE MET NOTIFY r14IXIOIPOIS9CRAwTEARWRADY.. N.J 06858 120 GRAND ST. IJERSEY CITY. N.J. 07302 .161 IRECErVINIS STATION IJE F FE RS ON VILLE INDIANA 47130 RECEIVING STATION KANSAS CITY, KAN. 60105 22j 710 CARLTON ST. BERKELEY. CALIF. 94710 26 300PAR)<AVE. NEW YORK, N.Y. IODfl 23 ATTN: ReceivIng Clerk YOU ARE AUTHORIZED TO FURNISH THE ARTICLES LISIED HEREON IN ACCORDANCE WITH THE TERMS AND CONDITIONS ON THE FACE AND BACK OF THIS ORDER. QUANTITY AND UNIT SYMBOL NUMBER PRICE fransrnissjon Electron Mieroscow and, selected area electron diffraction analysis of 7 talc samples, Note: is a one tie request. ATTENTION: Dr,. Ian stewart NeUrons Associates est. cost: $1750 & VENDOR TO PROTECT ALL PETAL PARTS AGAINST CORROSI caN BY SUITABLE PROTECTIVE SEALING. SELLERS INVOICES that include authorired transportation charges, must be supported by prepoid freight bill or copy of original bill of lading. ' -ILGATE-PALMOIII'B CnMPANY' tMARK PACKAGES witlf purchase order number, symbol number, contents and quantity. Acceptance, of this order is to be deemed a certification that you hove read ond agreed to the terms and conditions on tho bock hereof. PAYMENT WILL NOT BE MADE AGAINST PRO FORMA INVOICE. RESERVE UNLOADING space and time for hea loads by telephoning1 201.432-1300 extension 309. S .. ..- - %e' -' ''?Il'F-J 'I'?C nFr'r"n QE-CP0000041 33 TERMS AND cONDITIoNS WARRANTY The Seller expressly warrants and agrees that there has been compliance with and no violation of any trademark rights, patent rights, copyright or of any rule, law or regulation of the Federal Government or of, any State or any of their respective agencies or political subdivisiosis, in the marnifacture, production, sale and or shipment of the goods hereunder; and the Seller will indemnify and hold Purchaser harmless Prom any or all costs, damages, fines or expenses (including counsel fees and tees of expert witnesses) which may be incurred by the Purchaser by reason of any claim or suit arising out of the infringement of any trademark, patent right or copyright and/or by reason of any citation, claim or suit for damages and/or penalties 'orought against the Purchaser based upon any injuries, damages or violations resultingorclaimed to have resulted from any alleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY - The Equal Employment Opportunity Clause Section 202 of Executive Order 11246 as amended related to Equal Employment Opportunities and Implementing Rules and Regulations of the Secretary of Iabor are incorporated herein by specific reference. CHANGES IN ORDER This order cannot be changed, snodifiea or discharged in any manner except by agreement in writing signed by a duly authorized representative of the Purchaser. The Purchaser reserves the right, to (I) make changes in the order (2) cancel all or any part of the order at any time by notice in writing. The Purchaser shall not be responsible for costs incurred by the Seller in connection with this order, after the 'date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser an itemized statement of claim against the Purchaser within twenty (20) days after the receipt of notice of such change or cancellation, the Seller shall be conclusively deemed to have waived all claims against the Purchaser with respect thereto. CANCELLATION FOR SELLER'S DEFAULT Should tile SeUer fail (I) to etlect delivery on or befova the speothed delivery date(s) (2) to delivet goods in all respects conforming with the requirements (3) to duly perform Seller's obligation under each and all of the' terms and cdnditions df this order; the Purchaser may cancel this order in whole or in part. Without prejudice to the foregoing, the Seller agrees to report promptly to the Purchaser any delays in performanc:e or in slupment of the goods covered by this Order. SPECIFICATIONS, DRAWINGS, ETC. - All specifleations, drawings, plans, designs, samples, or other documents referred to in this order shall ha deemed an integral part of this order as fully as if set out in full herein and Seller warrants that all deliveries and/or performances hereunder shall conform thereto, each delivery and/or pef. formance being subject to the inspection and approval of the Purchaser, whether or not any rn'ior payment shall have been made thereon by the Purchaser. NONCONFORMING MATERIAL .- If Seller delivers defective material or mateijal not conforming to the a'ee-upon specifications, Purchaser may (I) hold such material at Seller's expense pending instructions as to disposal. (2) retUrn it to Seller at Seller's expense, or (3) utilize it in the rrni received or erter up-ading or other operations are performed on it, Os utilize it inc different manner or in different proportions with oIlier products than ynts intended, and Seller will be liable for any diminution in the 'ialuc to Purchaser at the material and for any incidental or other damages suffered by Purchaser resulting from such defectiveness or nonconformity. No replacement of defective or nonconforming niateiial will be made by Seller unless authorized by Purchaser. LIABILITY FOR DAMAGES Whenever Seller hall, by virtue hereof, have property of the Purchaser in its possession, the Seller shall be deemed an insurer thereof and shall be responsible for its afc return to tile Purchaser. ASSIGNMENTThis order shall not be assigned or transferred without prior written consent of the Purchaser. WAIVER -- Purchaser shall not be deemed to have waived any of its rights hereunder unless such waiver shall have - been signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated therein, shall be effective as to any delivery or other transaction which may occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL - With respect particularly to ordcrs covering labor and material, Seller agrees to start work :isnmpdiatel, to proceed with the utmost dispatch and to complete all of the work under this order. All such work shall be performe4 in strict accordance with Purchaser's "General Conditions for Contract Work" Specification -No.0920-CE, nor shall 'work be permitted to start on Purchaser's property until required Insurance Certificates have been relied b Purchasdi Time is hereby declared to be the essence of this order. Prices shown are firm and not subject to adjustment because of increase or decrease in material prices and/or wage rates and/or freight rates and/or other items of cost. The acceptance of the final payment by Seller shall be held to be a waiver and discharge of any and all claims gnd demands again&t the Purchaser for cQmpensation and darnges on aCeo.uxit of any matter irising out of '-'-Or in conn' ctron with the Conti,aet or the performance of the 'work. Any extra or ddditidaal work performed by Seller shall b isa a'fixed prica basis or c6st' plus fee basis and must be in each dase, first authbrized in -writing 'by Purchaser. Seller'i tates for such purposS shall be as set forth in a quotation from Seller prior to starting any such extra or addijonl'work asll Confirmed by Purchaser's prior written authorization. ' - QE-CP0000041 34 ST 4 (1Q13. R-I) Ic be completed by purchaser (Ted given Ia o..d domed by v..jder. lead inuiructtoni Ol back of this C.rlitkol.. IHIS CERTINCATE MAY NOT IF USED IN CONNECTION WITH THE PURCHASE QE SERVICES MAY E REPRODUCED *thtr uf Writ' rrflrfl DIVISION OF TAXATION SAtES TAX EXEMPT USE CERTIFICATE FORM SN PuRt IIASFR S CERIItICAIt cfl AIIIIIORIIY NIIMbtN 131-815-595/001 'fio 4" L/ L477tZ,a (Horn, of Vendor) Address City Date Stet. Vp The undersIgned purchaser certifies that it Is not required to pay the New Jersey Sales and/or Us. Tax on ik. purchase or purchases covered by thIs Certificate because the tangible personal property purchased will be Used for an exempt purpose Said tangible personal property will be used for the following exempt purpose- ...for. 1se...or.... consumption dfreeti,y and exclusively in reseaa'ch and developtent in the experimental or 1bbfltorvaie. The exemption on the sale of said tangible personal property to be used for the above described exempt purpose is provIded in subsectIon N.J.SA. 54:326.( 8N (See reverse side for Siding of principal exempt uses of tangibl, personal property and fill in the block with proper subsection citation). I. the undersigned purchaser, have read and complied with the instructions and rules promulgated pursuant to the New Jersey Sales and Use tax Act with respect to the use of the Exempt Use Certificate, and it is my belief that the vendor named heroin is not required to collect the sale, or use tax on the transaction or transactions covered by this Certificate. The undersigned purthaser hereby swears (under the penalties for perjury and false swearing) that all of the information shown in this Certificate is true. A VENDOR SHOULD READ AND COMPLY WITH THE INSTRUCTIONS GIVEN ON BOTH SIDES OF AN EXEMPTION CERTIFICATE COLGAPE-PAI14OLIVE C0lTh'ANY NAME 9 P7RCMASRR (as t.gjs$s w CivI,1o, of Taxation) Dy ((4 (Signature of owner, partner, officer of corpo -Walter L. Born- PurchasiWMartment lo5jLudaon St;eet (Address of Purchaser) Jersey City, N. J. 07302 QE-CP0000041 35 -4. 51.4 INSTRUCTIONS FOR USE OF EXEMPT USE CERtIFICATES 1. Good FaithIn general, a vendor who accepts an exemption certificate in "good faith" is relieved of.liability for collection or payment of tax upon transaction; covered by the certificate. The question of "good faith" is one of fact end depends upon a consideration of all the conditions surrounding the transaction. A vendor is presumed to be familiar with she low and the regula- tions pertinent to the business in which he deals. - In order for 'good faith" to be established, the following conditions must be met: . The certificate mvst contain no statement or entry which the vender knows, or has reason to know, is false or misleading. The cerlif icote must be an officially promulgated certificate form or a ubantial and proper rocluct1on theteaf. The certificate must be datid and executed in accordance with the published instruct lohs, arid must be complete and regular in every respect. The vendor may. therefore, accept this "good faith" Exempt Use Certificate on a basis for exempting sales to the signatory I'ur. chaser provided that: The purchoser's Certificate of Authority number, indicatin9 that the purchaser k registered with the New Jersey bivision of Taxation, is entered an the face of the Certificate. The purchaser has entered all other information required on the farm. {f) The vendor has no reasop to believe that the property to be pvrchased Is of a type not-ordinarily used itt the purchaser's business for the purpose described in this Certificdte. 2. Imptoper CertIficate Sates t,onsaalens which are nat supported by ptoperly executed exemption certlfleates shall be deemd to be taxable retail sales. The burden of proof thatthe tax was not requIred lobo otlected is upati the v6tdor, 3. Correction of CertificateIn genrol, vendors have 60 days alter dote of sale Ia obtain a corrected certificate v?here the original certificate locks material ipformation required to be set forth in said certificate or vhere stich-inforntation is lnc6rrectly stored. . - 4. Additional Purchases by Same Purchas.iThis Certiflcqte will serve to coveradditknal purchases by the sam purhaser of she sonic general type of property. However, each subsequent sales slip or purchase invoice based on this Cirtificate must ,how Ihe purchaser's name, address arid Certificate of Authority number for urpbses of verification. 5. Retention of Certificates Certificates must be retained by the vendor for a period of not less-than three years from the date of the last sole coveiedby the ceTtificate. Certificates must be In the physical psssslon of the vendor and avoilable far inspection on or before the 60th day following the date of the trcnsactio to which the certificate relates. 6. The most common exempt uses for which the Exempt Use Certificate (Form.ST-4) is applicable are th following: Sales of machinery. pparotu or Muipment far use or consumption diretly and primatily in theproduction, gcnration, transmission or distribution of gos,-eleclricity, refrigeration, steam or water far sole or in the operation of sewerage systems. jN.J.S.A. 54;328-8 (m) (2)! . - Soles of taniblEpersonal property purchased for use or consumption directly and exclusively r research and development in the experimental or laboratOry sense- Such research and development shall not be deemed to include the ordinary testing or inspection of. ,paiic4s.or poducts for kuality control, efficiency surveys, management studies, consumer surveys, edvertising, promotions or research in connection with literary, historicaJorslmilarprojects. fN.J$4:54r3288 (11)1 Soles or use of wrapping paper, wrapping twine, bags, cartons, tape, rope, labels, nonreturnable containers, reusable milk containers anctall other wrapping supplies when such use is incidental to the deliveiy of paronal projOiljs which has been sold. jt4.iS.A. 54:328-B ()I Sales of materials, such as chemicals and catalysts, used to induce or cause a refIning or chemical process, where such materials are on integral or essential part f the processing operation, but do not became a component part of the finished pro- duct. lN.J.SA. 54:328-8 (t)J The sale of advertising materials to be published-in a nowpaper. IN.J.S.A. 54:-8 (eefl - The use of property for market satiipling by the purchaser. (NJ.S.A. 5432B-1 1 (4)J REPRODUCTION OF EXEMPT USE CERTIFICATE FORMS: Private reproduction of Exempt Use Certificates may be made without the prior permission of the Division of Taxation. STATE OF NEW JERSEY, DEPARTMENT OP THE TREASURY, DIVISION OF TAXATION Post Office Box 999, Trenton, N.J. 08625 QE-CPC00004I 36 L fP rt tftHfft:i rJ4I { rt H+t4*''I ' I L 1r 1- Tfr :FijfP T '1' r 'ik ' JJri Irfrfi41J4J4' Th' I 1+w;w1cItl_LIiit1*i J4I i''Li j r $PJ4'fft4. rtcp' -'r u1t14vh1iIThirftiHjtThfl V i-f4i-Rf:2TiW! fT LI !111 : '- ii vyiTTn*1; 1- - 1j4; j 'z d 'R nFli-iI,Lrnr AriHir T bkl I rII Ir' W1I1WNL ( .Ij1HThft jj1ij E'*f$fflt c* liii, -+ r iiTTlhP r +i[T1rri'*i frfi,rFh 4IT1T1rrdtjrf4nl!rHLI 4rHri,t1RirHfl] - Im 4J1 I jj1 HF'44L 2 ' ci cPdft :+rti4f] F r -H4tif! 1 [ 11 Th'TtVill rn ry:;t: 4rr4I ft4I1t 'if r44f: k:- ir: i;r'i''1-'Hrrtt 4frr : H4jti. jI [ -t Ht 1 14 'j 1 rnTTrt r Jrrm 1 Jl(l Tkr,jr-tyn-r r1:r r1minrrrm rq t ItI;LHIrHtIiI?rTnc 'iTIY rjrTrr41 dr4. ;E1' hT1 :4r4TTHft;r:u; rrIII sx'rTrrjm 11 i 1J +'4I T!V'Ttf 5;:-ttT1*---I-rHrr-JI1Ipf H4r-1F R Jf941[I4 - -1- 1rj-'- iIIrTTIJriHrnrr1'4LLJTHhthyJhLr1qr'rLIjcn(tr4rr-brd-. - -r' rm- r I RI 1 L-1dThTf:fl 4mT1T4]n1tihrwjttLIIt1i 'hTf ii-itP:iftt:pTt:'t:T:TrIRTI*t4IlutLiLthi tfJi :L4Lri ' rJH Mk4ttf rr+441,rt4..!.i c ' i J- r : f'rp F41 L411 *4H} --v ]: j1}jfri, 1411j4h4-H. 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IUiJVSSI!l9tI5g5ujflpl USUhlhKInhI 155 $58 iiuijtungjgssg 'iTh!J!5 519511ff IM!IIflUuIIUwj a' !15fl SMwksssi$ I E EURSUS8ISI 58 II 155 EHNliKNliuSIa I iN EMSSSSMIisgssui !ISSaIntSIsSIius lEIMIE!I5SEPBL SARI S ff1111 HIS llIL N! fluluslins flhI!3NI III 1551 !SEIhIgSvS d":1!UflaI3RMWIQK5!IEuIII!II!SS!II,RSINIINHISUISfEEPS!SESH!I 5ARNSSO .SNIIflIIfls. 9I- unlshiissu IVIlifu S5ifllh!5I5H H IIiD fl'1Rsg RS SII!S51WUISSHP{5N!IUlIh5lIlIIIlI5IIIi!5IsHim551l8RIaI5u5I1z5I155!l1!niI5Iupf5lhplulI!fflgl555pHE5vu5g55Jfl5a5595E51l1R15I551 S lSiJftfiCa t IU UH9li5J q IJ!U 1I Ilk 551551 UqSqI t'1II5tIiIffIIliIuIiailSsuursiptsitEtfitlhIiIIlilihiIiNIiI$IuI IJIIUIkflI IS OI J5S IIIusnq us p RIlIlIESSlI lhiIhHlUEfHlhllhIlIIIfJlfIf! hi lIfl!HhIHIifl UhIiUhIII8I55IfthI IOHJIIISJEUU ,5Snwuniip iffill Ills SIP IlPOEILNWN!SNHQ15g5M5IBgMfluun58255S'fS5SlIl5S55UliiaE1IUfIREnln!iUfIIS3QlU5BUIIUFIEaE5SfBl9lUlSSJqKnUhUImSfflIINtUlr,IIuonEuIiRlInnEISws,NUI%sh1HIqlaI1uiuUJhulIiUJIhiHIJ5InIlnIjiIIIUpIhjIfIIplSutlNISImIrIjI5f9hns5IuIl1IfuhrIpultln0IhlUf,,UIIi*1utlJmi5l1isI1uJluJf1ml1ijplIluI1hJ9IJuIIIil1lIa,AJIgI1IuI!1IIph*tLIIIlIII1lIJIliIll11IpJllul1II1h1fll1IIIllII11u1INIuh"IlI11I*MI,I1ISl1upt11IiJll1fI,lpiu!l1ilIH1lIIUn1JlDD1uhuI1Ium1jUFa10UAIUm1si5ISf5g!SfNliII1lIIiuIIJIIEfPII1I1I1IIl1III0IN1IhI1IRNIli!1PIIIl1Ii!IEJHIISI1EJ1AEIO5IIUI0fIIl1HIIsiJSIrSkJUN1fHJ'IUUISf1IUIEIIPlIISIIUHC1LHM!UIfU15UlJfuEhEII!llIAI1Upp5IIJlURSIUIJIu51fISIJ5IlIpilIU85p'SHUhuSIIE5lSuIIlhNIII5IJNII5IIlIIlfIAIlIJ1IIJIIlIshIIfISII5II5JIlIfA951IflM5IlI1I5lEjHI5ili11lI5iIISfEIih1I1IU1lJi*IPluII11I1fI1IlJIgh85l11lRIIU1iJ5IPII1l1Ia1puaJIf1I1sllI1sUtUSIuI005IHIHaShSI1lII1IIIImpIII!SII5ISSJIIIIUSU1sUISf9QURIlhI1IIIj5JNRIIIIIIIIpIIlMIUIIl5pIIIIIII5uUIIIISIfEIfSIliIIUIlIhlSuIIInISfEIIIlSShlJJ1lIHIplIIIIMSBOfIll%S1lp9IEIE1UI!lJ4Ij5JlIK5fJ1tI1llUIES1hfS1IJi1Jm1IfUJSplmUf1IuIflI59EfSmIJU1lIAJlShIJ5ulIIfifg1iiIIJfEIg1fjlupg;R5EuiH1MlUa1i'1!lHIhIu1SI1mlhISIIIHSaHI!IijihlislUlIuEufBliBIlIsSsI-sIElssISS5sI:58 18 VU 51fl JIg UH11 Usun nan Anun 52 flUH qNSa UiJMH5SE UUEt55Ufl55flg8pli5q 5UuSauuwnaunu'su S i SINS 15W U en: COLGA TE-PALMOLWE COMPANY A D.ltuvasr. Cnprat4n RESEARCI-I AND DEVELOPMENT DEPARTMENT 909 River Road . Piscnaway, New Jersey 08854 February 27, 3.976 Mr Ian Stewart Mccrone Associates 2Q20 South Michigan Avenue Chicago, IL 60616 Dear Ian, I am enclosing seven talc samples for TBM-SAM analysis. These are finished products and I am interested in determining if any chrysotile or amphibole, specifically tremolite or aaithophyflite, are present. The sample codes are as follows: 0925Ax6 0215DX lgTlCth 03160X okl!t3 0326 321A I flfl contact you concerning the purchase order number of this work. I need these results as soon as possible. Any questions please contact me, Sincerely, 3, P. S1ko JPS:ls S QE-CPC000041 41 -I QE-CP0000041 42 PROJECT COST PROJECT TITLE: analyze for asbestos SPONSOR: fl4TF_pAT?VflTTVE CO. ADDRESS: gO9RLvetRd lJiSLcLLcjWdY, NJ 0885'i RECORD NA 7673 PROJECT NO.: 2 7 79 DATE RECEIVED: P.O. NO.:3 9.c.s COMMITMENT $ Contact: j. p. s:into Telephone No. SUMMARY OF PROBLEM: Lab Notebook References: No. pp. Initials No. pp. Initials No. pp. Initials Photomicrographic record no. Sample disposal: returned filed (where) discarded DIRECT COSTS (Exclusive of open Individual time time on Inst. below) Date Name Hours Charge Travel Charge Summary Date Traveler Destination Cost Individuals $ Instrument Travel Outside Other Instrument tine Date SEM TEM XRD EMP IMP ESCA EMMA MOLE C). (33 C\ .\c \ Hours Charge Date Company Photo Photo Materials Supplies Total Cbirge Cost $ OK for billing Project Ldr Group Ldr - \L+a,j Ps&s C \L-dcz-4 CHARGE $ sca1q - BILLED TO CLIENT INVOICE NO. (5) 1 'a, $ PROJECT LEADER: QE-CP0000041 43 ,J waiter c. mc crone associates, inc.A A I CONSULTING: ULTRAMICROANALYSIS MICROSCOPY. SMALL PARTICLE PROBLEMS -SOLID-STATE CHEMISTRY 13 February 1979 Dr. Joseph P. Sinto, Jr. Colgate Palimlive Company 909 River Road Piscataway, New Jersey 08854 Dear Dr. Sflrko: Using transmission electron microscopy and selected area electron diffraction we have analyzed a sample of sodium carbonate for asbestiform minerals. The procedure we used for this sample was to dissolve the sodium csrbonate iri approximately 500 ml of water and filter onto a 47 urn filter. We then washed the fi,lter to remove any excess sodium carbonate and, using a$oxhlet extractor, dissolved the filter. We did not find any asbestiform mineraj.s in this sample, either amphibole or serpentine. In fact, the filter was extremely clean indicating that the predominant portion of this sample was water soluble. We thank you for consulting Mc Crone Associates and if there are any further questions concerning this report or the data contained herein, please feel free to contact me. - Very truly yours, ORG j d Ref. Mk 7673 q.c. 63b-r\o Gene R. Grieger Senipr Research Physicist 2620 SOUTH MICHIGAN AVENUE. CHICAGO, ILLINOIS 60616.312/842-7100. CABLE: CHEMICRONE QE-CFC000041 44 PURCHASE REQUI$TiO:ETROPULITAN AREA dRIGI&AL PURCHASE ORDER b521 t- Ii Show this nnrner and prefix on invoices, packing slips and packages. BILL 'TO COLGATE-PALMOLiVE coMpA4j,4: A DELAWARE CORPORAtION 105 HUDSON STREET, JERSEY CITY, N.J. 07302 ATTENTION; - --I DATE //a3f7 SHIP TO Mecrone Associates 2820 South Michigan Avenue Ohicago, flhinois DISCOUNT TERMS 2/10 N/SO N/3D 1/10 N/SO Net Cash Trade SHIPPING TERMS flI rOB Destination 2 0 EOB Shipping Pt. (Pre.Pay& BilflSeeBek,n 3 FOBShIppIngPt. (Collect) city IF ADOVEOA1'E CANNOT BE MET NOTIFY 251 IIOJEGRGSREEYENCEITSYT..N.J. 07302 14 909 RIVER RD. PISCATAWAY, N.J. 05554 20 GRAND ST. 13 JERSEY CITY. N.J. 07302 16 RECEIVING STATION JEF FE RS ON V IL i.E INDIANA 47130 RECCIVING STATION 191 KANSAS CITY,-.KAN, 66105 itO CARLTON ST. 221 BERkELEY, CALIF. 94770 1 261I 300 PARK AVE. NEW YORK, N.Y. 10022 231 I ATm: Receiving Clerk YOU ARE AUTHORIZED TO FURNISH THE ARTICLES LISTED it REON IN ACCORDANCE WITH THE TERMS AND CONDITIONS ON THE FACE AND BACK OF THIS ORDER. QUAWTITY AND UNIT S'(MBOL NUMBER PRICE Microscope studies to confirm presence of asbestos in Sod&ihrn - Carbonate sample, CQSt: approx. $300 Sample sent under separate cover to &Orone Assoc., ATTENTION: Mr. Ian Steimrt 0TE This is a one time request9 . I. 7 TAXEXEMPT VENDOR TO PROTECT ALL MET.L PARTS AGAINST CORROSION B ,v UITABLE PROTECTIVE SEllERS INVOICES that include authorized trantporlotion charges, must be supported by prepaid freight bill copy of orgInol bill of lading. MARK PACKAGES vhh purchose order number, symbol number, contents and quantity. Acceptance of this order is to be deemed a cerlificotibo thot YOU hove read and o0reed to the terms and condilions on the bock hereof. PAIMBHT WILl. NOT BE MADE AGAINST PRO FORMA INVOICL RESERVE UNLOADING space and time for heosy loads by telephoning: 201.434.1300 extension 209. 0I C ATE- PALMOLIVE CQMPANY QE-CFC000041 45 TERMS AND CONDITIONS WARRANTY - 'The Seller expressly warrants and agrees that there has been compliance with and no violation of any trademark rights, patent rights, copyright, or of any rule, law or regulation of the Federal Government or of any State or any of their respective agencies or political subdivisions, in the manufacture, production, sale and or shipment of the goods ltereunder and the Seller will indemnify and hold Purchaser harmless from any or all costs, damages, fines or espenses (including counsel fees end fees of expert witnesses) which may he incurred by the Purchaser by reason of any claim or rmit arising out of the infringement of any trademark, patent tight or copyright and/or by reason of any citation, claim or suit. for dathages and/or penalties brought against the Purchaser based upon any injuries, darnage; or violations resulting or claimed to have resulted from any alleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY -.-. The Equal Employment Opportunity Clause Section 202 of Executive Order 11246 as amended reInsert tc Equal Emn!oyinent Opportunities and Implementing Rules and Regulations of the Secretary of Labor arr incorporated herein by specific reference. CHANGES IN ORDER This order cannot be changed, modified or disc'harged in any manner except by agreement in wilting signed by a duly authorired representative of the Purchaser. The Purchaser reserves the right to (1) make changes in the order (2) cancel all or any part of the order at any time by notice in writing. The Purchaser shall not be responsible for costs incurred by the Seller in connection with this order, after the date of receipt of the change or cancellation notice. Unless the Seller ln'esents to the Purchaser an itemized statement of claim against the Purchaser within twenty (20) days after the receipt of notice of such change or cancellation, the Seller shall be conclusively deemed to have waived all claims against the Purchaser with respect thereto. CANCELLATJON.FOR SELLER'S DEFAULT Should the Seller fail(1) to effect. delivery on before the specified delivery date(s) (2) to deliver goods in all respects conforming with the recjutvenients (3) to duly perform Seller's obligation tinder each and all of the terms and conditions of this order, the Purchaser may cancel this order itt whole or in part. Without prejudice to the foregoing, the Seller agrees to report proniptly to the Purchaser any delays in performance or in shipment of the goods covered by this order. SPECIFICATIONS, DRAWINGS, ETC. - All specificatiOns, drawings, plans, designs, samples, or other documents referred to in this order shall he deemed an integral part of bUs order as fully as if set out in full herein and Seller warrants that all deliveries and/or performances hereunder shall conform thereto, each delivery and/or performance being subject to the inspection and approval of the Purchaser, whether or not any prior payment shall have been made thereon by the Purchaser. NONCONFORMING MATERIAL - If Seller delivers cicfectivc material or material not conforming to the agree-upon speoifications, Purchaser nay (11 hold such material at Selter's expense pending instructions as to dispomi, (2) meturti it to Seller at Seller's expense, or (3) utilize it in the form received or alter up-grading or other opeiations are performed on ii, or utilize it in a different rhanner or in different proportions with oilier products titan uns intended, and Seller trill tic liable for any diminution in the value to Purchaser of she material and for any incidenlal tsr other utages sntThrerl by Purchaser resulting from such defectiveness or nonconformity. No replacement of defective or nonconfonning mnnierial will he made by Seller unless authorized by Purchaser. LIABILITY FOR DAMAGES ...Wltencver Seller shall, by virtue hereof, have property of the Purchaser in its possession, the Seller shall be deemed an insurer thereof and shall be s-esppnsible. for its safe return to the Purchaser. ASSIGNMENTThis order shall not be assigned or bansferred without 1hhor written consent of the Purchaser, WAIVER - Purchaser shnll not he deemed to have waived any of its rights hereunder unless such waiver shall have been signed by a duly authorised representative of the Purchaser. No such waiver, unless expressly stated therehi, shall be effective as to any delivery or other transaction which may occur subseqnent to tho date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL - With respect particularly to orders covering labor and material, Seller agrees to start work immediately, to proceed .:with the utmost dispatch and to complete all of the work under this order. All such work shall be performed in strict accordance with Purchaser's "Genera) Conditions For Contract Work" Specification No.0920-CE, nor, shall work be permitted to start on Purchaser's property until 'reaired Insurance Certificates have been received by Purchaser. Time is hereby declared to be the essence of this order, Prices shown are firm and not subject to adjustment because of increase or decrease in material prices and/or wage rates and/or freight rates and/or other items of cost. The acceptance of the final payment by Seller shall be held to be a waiver and discharge of any and all-claims and demands aainst the Parehaser tot compensation and damages on account of any matter arising out of or in connection with the Contractor the performance of the work. Any extra or additidnal work performed by Seller shall be on a fixed price basis or cost plus fee basis and must be in each ease, first.ai.ithorized in writing by Purchaser. Seller's rates for such purposes shall be as set forth in a quotation from Seller prior to starting any such extra or additipnal work and confirmed by Purhaser's prior written authorizatipn, - QE-CFC000041 46 V. b. c.nqpl.sd by pvn$....s o,d r' I. end rsfelnsd by .544w. 5.44 infl,wdS,s en bat .4 01. C.,iUIt.w. Nil CIflI$CAYI MAY NOT U 1550 IN CONNeCTION aWItH THJ MI*CHAU ISYICtI MAY II REPRODUCID tat, ui Nnu 3rrer DIVISION OP TAXATION sAID TAX IXIMPT Un CUTIflCATh FORM ST-4 q PUlL IIASI1 tllIItItAt (it AIIIIII*IIv NI$MII'P a131-815-595/001 (Maui .4 Vend..) The undersigned purchaser certifies shot it Is not required to pay the P4w Jersey Solse cr4/or Use laM on the purchase or purchase covered, by this Certificate because the tongiM. personal property purchased will be used for on etsempt purpose. Said tangible personal property will be used for vhs following enmpt purposet for uee or consaoption dfrectly and exclusively li research and d.veinrient in the exl,etimentII or iaorstory inst. The exemption on the sale of sold tangible personal properly to be used for the above described eicempl purpose Is provided in subsection N.J.S.A. $432b.f 84 lsee reverse We for IWIna of principal enmp( uses of tangible personal properly and (UI In the l'iock wiSh preper subsection citation). - I. the undersigned purchaser, have read and compiled wish the Instructions and rules promulgated pursuant to the New Jersey Sale. and Use Tax Act with respect to the use of the Exempt Use Certificate, and it is my belief that the vendor named herein is not required to catted she soles or use tax on the lrcsnsacelon or. transactions covered by this Certificate. The undersigned purchaser hereby swears (under the penalties for perjury and false swearing) that cli of the information shown in this Certificate Is true. A VII400* INOUtO HAD .U40 COMPlY WIN THS IN$TRUCTtON5 O1YN ON ION MDII 0 AN LIIMPIION CIITWICATI. COLGATZ-PAZMOLIVE Cc*WMT NAMI RCNAUI (is ngi.isrQt GOIvItien of Toxafi.,.) ly IlWlwicaI.aleteeOrf SLW.iftB1 noetrtmn.-r, iAds.s .4 Pusdues) Jersey Cit', N. J. 07302 QE-CPC000041 47 Sf4 I,, INSTRUCTIONS FOR USE O EXEMPT USE CERTIFICATIS I Good Faith In 9tn!rOI. a vendor who accepts on exemption certificate in "goad faith" h relieved of iobiiijy fat colfection Oc ptynwnt of (Ok upon transactions covec.d by the certificate The question of "good faith" is one of foci and depends upon a consideration of all thr condition. surrounding the transaction. A vendor is presumed to be familiar with the law and the regt4i. lions pertinent to the business In which he deal;. In order Par "good faith" to be established, the following condition, must be met Ike certificate must contain no slatement or entry which the vendor knows, or has reason io know, is false or'n.is. leading The certificate must be on officially promulgated certificate form or a substantial and proper reproduction th.rsof. The certificate must be doted and executed in occordanca with th. published instructions, and muit,bitmp4ete and rguiar in every respect. The vendot niay, theret ore, accept this "good fa;tw' Exempt Use Certificate on a bails for enniptlrtg she to the signatory pur chaser provided that: The purchaser's Certilitate of Authority number, indicating that the purchaser Is regIstered with he New Jersey Dividon of Taxation, is entered on the face oV the Certificate. Thu purchaser has entered oil other information required on the form. - (f 3 The vendor Isos no reason to believe that th. property to be purchased Is of a type net ordinarily used in the purthasec's business far th. purpose described In this Certificate. IMproper Certiftcote - Sales transacttons which ore not supported by properly executed !x,mp$on certificate, thoU be deemed to be taxable retail soles. The burden of proof that the lax was not required to be collected is upon the vendor. Cerrectian of CertIficate '-In general, vendors have6O days after dale af sole to obloin a corrected wrtlficote where site original cerlificote lacks material information required to'b. set forth in said cet-sificoteor where such information is Incorrectly stated. AeIditienelpurshas.s by Sonic Purchaser--Thu Certificat, wIll sen to ovr addfttonOl puichii by the same purchaser of thE. Seine general type Of property. However, each subseqUent sales ii$ dip hse'ln*TS'&SSd'en this CI$IR1S must show she purchaser's name, address and Certificate of Authority numbeVforpoiftirifiatian. . - S. tetenlien of Certificates Certificates must be retained by the vendor tarn period of not len than three years from the date of she IaIsoie covered by she certificate. Certificates must be In tti. physical pqssusion of the vendor and available for inspeclion on or betote the 60th day following the date of th, transaction to which th, certificate relates. 6. Itu' oiol ,on,oton oxempt uses for which the Exempt Use Certificate (Form ST-4) is applicable ore the following: Sok at machinety, apparatus or equipment far use or consumtion directly and pilmorily in the production, generiilin 'transmission or distribution of gas, eluctricily, refrigeration, steam or water for sol, or in the operation of sewerage systems. IN.J.5.A. 54;328'8 (in) (2)! Sofas of tangible personal properly purchased for we or consumption dIrectly and exclusively In research and development it. the .xperimentai or laboratory s,ns,. Such research ond development shall not be deemed to include the ordinary testing or inspection of materials or products for quafity control. efficiency surveji. s.Onoj'emont it.dles, consumer surveys, -adtertising, promotions or research in connection with literary, historical or similar prolects. INJ.S.A. 54s321'B (nfl Sates or use of wrapping paper, wrapping twine, bags, canons, tape, rope, labels, nonreturnable containers, reusable milk containers and all other wrapping tupplies wheit such use is incidental to the delivery of personal property which has been sold. IN iSA. 54:3218 ()I SaLes of mojerials, such as chemicals and catalysts, used to induce or cause a refining or chemical process, where such materials are an integral or essential part of the processing operation, but do not become a component part of the finished pro' dud. IN,J.S.A. 54:3218 (t)J The sale of advertising materials to be published in a newspaper. IN.J.S.A. 54,'e (,efl Th. use of property for market sampling by the purchaser. (N.J.S.A 54,321.11 (4)j 4.4 RIPROOUCIION Of EXEMPT USE CERTIVICM( FOIMS. Prtvolt reproduction of Exempt Use Certificates may be mode without the prior permission of the Division of Taxation, STATU OP MW JIUSUY, aPARTMENT OP THE INEASURY, DIVISION OP TAXATION Poet Office kx 999, Trenten, NJ. 0142$ OE-CPC000041 48 kIA5Y1A !VI 1 V,.V,rSiIHII-VJcIr.r, I'I mI'n.r,I''..r./ni nILc, \r4iQccnr'.eiIn'..+4Ia\_ciJgiIInr1'.'. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY - SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 13 February 1979 Dr. Joseph P Sinko, Jr. Colgate Palnolive Company 909 River Road Piscataway, New Jersey 08854 Dear Dr. Sinko: Using transmission electron microscopy and selected area electron diffraction we have analyzed a sample of talc designated as #32. We found this sample to be extremely platy, although there were indications of rolled shards because of the platiness, but we did not find any ashes tiform mirieral. We thank you for consulting McCrone Associates and if there are any further questions concerning this capon or the data contained herein, please feel free to contact me. Very truly yours, S GRG :j d Ref. M& 7673 Gene R. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616 3121842-7100 CABLE: CHEMICRONE QE-CPC000041 49 PURCFIASE REQU!SiT!OW - METROPOL1TAH AREA ORIGINAL PURCHASE ORDER I -tI Show this number avnodicepsre, fipxaocnkning slips and packages. RPA 89982 COLGATE-PALMOLIVE COMPANY A DELAWARE CORPORATION 105 HUDSON STREET, JERSEY CITY, N.J. O73!'... Heorone As'ociates 2820 South M1chigan Avenue Chicago, flhinois 1 25!I BBGREENEST. JERSEY CITY. N.J. 07302 909 RIVER RD. 14 PISCATAWAY. N.J. 08854 20 GRAND ST. a JERSEY CITY. N.J. 07302 161 I RECEIVING STATION .JEFFERSONVILLE. INDIANA 47130 RECEIVING STATION KANSAS CITV.ICAN, 05105 DISCOUNT TERMS 1 fl/io N/3D 2 []N/30 S Eli/SO N/SO Net Cash Trade SHIPPING TERMS 1 fl FOB DestinatIon 2 FOB Shipping Pt. (Pre-Poy& EiII)See Below 3 J FOB Shipping Pt1 (Collect) CIty 221 7B1E0RCKAERLLETYO.NCASrL.IF. 47i 0 I 26 300 PARK AVE. NEW YORK. N.Y. 10035 231 I ATTN: Receiving Clerk YOU ARE AUTHORIZED to FURNISH THE ARTICLES LISTED HEREOH IN ACCORDANCE WITH THE TERMS AND CONOITIONS OH THE FACE AND SACK OF THIS ORDER. QUANTITY AND UNIT SYMEOL NUMSER PRICE - 1. Sample of Talc Code #32 for Microscope and Selected Area ...................ectron Diffraction analysis for asbbatos r:dnerals. Cost Sample sent under separate cover e approx. $300 / NOTE: This is a one ti:e requestj -. I - -. K4AIL lNVOcT) o: .- -.cvflg .......... ................. TAX EXEMPT c CJ210 ? ........-. rUvOr Roa N.J. 08054 VENDOR TO PROTECT ALL METAL PARTS AGAINST CORROSION B? SUITABLE PROTECTIVE SEALING. .- SELLERS INVOIdES thotinlude aUthOriZed trorisporlotion charges, mdsbbe supported b' prepaid freight bill copy of original bill of lading. MARK-PACKAGES witli-purchaseorder number, symbol number, contents and quohtiIy Acceptance -of Ibis order isto be deemed a cortificationthot you hove rood and agreed to the terms cod conditions on the bock hereof. PAYMENT WILL NOT BE MADE AGAINST PRO FORMA INVOICE. RESERVE UNLOADING spoce and time for heavy loods by telephoning: 201-434-1300 e3ctension 3D?. LGGATR-PALMOLIVB doisPAlyi'e I: C QE-CPC00004I 50 TERMS AND CONDITIONS WARRANTY - The Seller expressly -warrants and agrees that there has been compliance with and no violation of any trademark rights, patent rights, copyright, or of any rule, law or regulation of the Fedeial Government or of any St-ate or any of their respective agencies or politil subdivisions, in the manufacture, production, sale and or shipment of the goods hereunder; and the Seller will indemnify and hold Purchaser harmless from anS' or all costs, damages) fines or expenses (including counsel fees and fees of expert witnesses) which may be incurred by the Purchaser by reason of any claim or suit arising out of the infringement of any trademark, patent right or copyright and/or by reason of any citation, claim or suit for damages and/or penalties brought' against the Purchaser based upon any injuries, damages or violations resulting or claimed to have resulted from any alleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY The Equal Employnent Opportunity Clause Section 202 of Executive Order 11246 as amended related to Etjual Employment Opportunities and ln,plcmentintc Rules and Regulations of the Secretary of Labor arc incorporated herein by specific referenca. CI-IANGES IN ORDER - This order caurnot. be changed, modified or discharged in any manner eicept by agreement in writing signed by a duly authorized representative of the Purchaser. The Purchaser reserves the right to (I) make changes in the order (2) cancel all or any part of the order at any time by notice in writing. The Purchaser shall not he responsible for costs incurred by the Seller in connection-with this order, after the date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser an itemized statement of claim against the Purchaser within twenty (20) days after the receipt of notice of such change or eancellatioa, the Seller shall be conclusively deemed-to have waived all claims against the Purchaser with respect thereto. CANCELLATION FOR SELLER'S DEFAULT - Should the Seller fail (1) to effect delivery on or bcf ore the specified delivery date(s) (2) to deliver goods in all respects conforming with the requirements (3) to duly perform Seller's obligation under each and all of the terms and conditions of this order1 the Purchaser may cancel this order in whole or in part. Without prejudice to the foregoing, the Seller agrees to report promptly to the Purchaser any delays in performance or in shipment of the goods covered by-this order. SPECIFICATIONS, DRAWINGS, ETC. - All specifications, dcawings, plans, designs, samples, or other documents referred to in this order shall he deemed an integral part of this order as fully as if set out in full herein and Seller warrants that all deliveries -and/or performances hereunder shall conform thereto, each delivery and/or performance being subject to the inspection and approval of the. Purchaer, whether or not any prior payment shall have been made thereon by the Purchaser. NONCONFORMING MATERIAL - If Seller clelivcrs defective material or material not conforming to the agree-upon specifications, Purchaser may (1) hold such material at Seller's expense pending instructions as to dispol, (2) return it to $eller at Sellcr's,epcnsc, or (3) utilise it in the form recoivcd or after tip-grading or other operations are perforned on it, or utili-ce it In a different manner 02 in different proportions with other products than was intended, and Seller will be liable for arty diminution in the value to Purchaser of the material and for any incidental or other damages suffered by Purchaser resulting from such defcctiveness or nonconformity. Nn replacement of defective or nencenfonning material will be made by Seller unless antI-tented by Purchaser. LIABILITY FOR DAMAGES .-- Whenever Seller shall, by virtue hereof, have property of the Purchaser in its possession, the Seller shall be deemed an insurer thereof and shall be responsible for its safe return to the Purchaser. ASSIGNMENTThis order shall not he assigned or transferred without prior written consent of the Purchaser. WAIVER -- Purchase,' shall not he deemed to have waived any of its rights hereunder unless such waiver shall have leen signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated therein, shall be effective as to any delivery or other transaction which may occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL - With respect particularly to orders covering labor and material, Seller agrees to start work immediately, to proceed with the utmost dispatch and to complete all of the work under thi. order. All such work shall b? performed in strict accordance with Purchaser's "General Conditior1s for Contract Work" Specification No.O920cE, nor shall work be permitted to start on Purchaser's property until required Insurance Certificates have bedn received by Purchaser. Time is hereby declared to be the essence a1 this order. Prices shown are firm and not - subject to adjustment because of increase or decrease in material prices and/or wage rates and/or freight rates and/or other items of cost. The acceptance of the final payment by Seller shall be held to be a waiver and discharge of any and all claimi and demands against the Purchaser for compensation and damages on account of any matter arising out of - or in cqnnection with the Contractor the performance of.the work: An extra or additional work- performed by Seller shaH -be on a fixed price basis or cost plus fee basis and must he in each case, first authorized in writing-by Purchaser, Seller's rates for such purposes shell be as set forth in a quotation from Seller prior to starting any snob xtra Or additioDal work and confirmed byPurchaser's prior written authorization. . .- QE-CPC000041 51 MAY RE REPRODUCED 555 iD73. * I) V. bi aa.pi.ie4 by p.nties. iS she. I. iS ..S,S by .sedet. le.d lflnnWi.. en Seb .4 Mi Cr H tkew. btatr sit Nra' trsr DIVISION OP TAXATION SAt,, TAX THIS CI5TIPICAYE MAY NO? Ii USID IN cONflICTION WITH TNt PUICHAM 04 SNV1CI$ lUMPY USI CEITWICATI FORM ST4 0' kt &d44aS (tiuneef Yl Clip Pult It ASPI' siulititAlt sit AIliuItiIliv I4ltMflI zip The undersigned purchaser certif I., that It is not required to pay the New Jersey Sales and/or U.. lax on th, purchase or purchases covered by this Certificate becaus, the tangIble personal properly put chased will be used for an escempt puaee. Said tangible personal property will be used for th, following exempt purpoeei fat' use or conrntiptton dtnotly aM exclusively ih reasa.reh sd developtent in the experiaentir or 1*bor*tory ann. Tb, exemption on the sale of said tangible personal properly to be used for the above described eampi purpos. is provided in subsection P.U.S.A. 5432LJ 8-n J(See revers, side lot list Ing of principal esenspf use. of tangible personal property and till hi the black with proper subaect Ion citation). I. the undersigned purchaser, have read and complied with the instruction. and rules promulgated pursuant to the New Jersey Sales and Use Tax Act with respect to the use of the Exempt Use Cerlif lease, and iii; my belief that the vendor named herein is not required to collect the soles or use tax on the transaction or. transactions covered by this Certificate. The underslned purchaser hereby swears (under the penalties for perjury and false swearing) that all of the information shown in this Certificate Is true. cow&n-amctvr C*WANT A VINDC* SHOULD *5*0 AND COMPtY Wilts TNt INSY*UCT1OIS 04Y04 ON 50714 11041 04 AN mIlMP7lCW CIITWICAS1, Illgnofur Cf OWnerNadr,er Walter L, Bor&i4btt"4srtnient ,QiiM#.cS.Breet {Addr.es .4 Pb,t..4 Jerusy City, N. 3. 07302 QE-CPC00004I 52 SI 4 INSTRUCTIONS FOR USE OF EXEMPT USE CERTIFICATES I G..d Faith tn general. a vendor who occepts on exemplion certificate in "good faith" is relieved of liability for collection or payment oi tow upon transactions covered by the certificate The question of "good faith" is one offactarid d.pettds upon a consideration of all thi' condition, surrounding th. transaction. A vendor is presumed lobe familiar wills the law ondth. r4t. team, pertinent toihe business In which he deals. In order for "good foith" to be established, the following conditians.m'ust be mete (a) the certificate must conto}n no statement or entry which the vendor knows, or has reason to isnow. is false or' iSsleading (hi The certificate must be on officially promulgated certilicate form or a substantial ar,d proper repioductian thereof. (ci The certificate must be dated and executed in occordorica with Ihe published lnstrucfsohs, and must,b coniplete and regular in every respect. The vendor may, therefore, accept this "good f&th" Exempt Use Certificate art a basis for exampiluig soles to I he signatory Pu,' chase' provided thatr (4) The purchaser's Certificate of Authority number, indicating that the purchaser Is registered with the New Jersey Division of taxation, is entered an the facsof the CertifIcate. (e) The puichaser has entered all other information required on the farm, (1) The vc'ndor has no reason to bill eve that the property fob. purchased Is.! * type net ordinarily used in the purchaser's business fo the Durpose described In this Certificate. hap'ep.' CirlifIcateSolsi trqtrsacflons which are not supported by properly executed !utpott certificalee shall be derred to beta soble retail soles. The burden of proof that the tax was not required to be cahected Is upon the viSor. C erectiess a! Certificate "In general, vendors have"O days after date of late to obtain a corrected crlificate where the original certilicot. lacks material information i'equired tab. set forth in sold cettificate or where such information is'iricOrrectly stated. 4 Mditlenel Punhaas by Some PurchaserThis Certificate will serve to cover additional pjarchases by the some purchaser ol the tame general type dipropety. However, eoch smibeio'ont salo slip or'iir *'lnvblee'basidoWthig Crtifkoti must stsowihe purchaser's nome,oddrest and Certificate of Authority number forpUrpises ofyirificatlois. 5, letentien at Certificates Cersilicules must be retained by the wendor (us a period of not less than three ak from she dot, at the tast,.sate covered by Ike certificate. Certificates must be in the physical possession of the vendor and ovailubte for in specluon on or before Ihe 60th day !otbowing the dale alibi transact ion to which the certificate relates. 6. the niu.t ou,nsnn oxempt uses fo, which the Exempt Use Certificare (Form $1.4) is applicable are the foIlowing Soles of machinety. apparatus 61 equipment for usb or consumption directly and primarily iiithe production. generatton, ironimussion or distribution of got, electricity, refrigeration, steam or water for sale or in the operation of sew.raue systems. (N.J.S.A. .4:32B'8 (m) (2)j Soles of, tangible personal property purchased for use or consumplin directly and flclniyeJy in research and development. in-the .experimentalpr .lahorator sense. Such research nddev.lopnient shall not be deemed to include the ordinary testing or inspection of materials br poducts for uality cantrol. ifficiency surveys, managementitudiu, consumer surveys, advertising,. peomolions or e,.0Ch in connection with I1lerory, historical or similar projects. IH.i.S.A, 54,3214 ()I Sales or use of wrappIng paper, wrappIng twine, bags, cartons, tape, rape, labels, nonreturnable contaIners, reusable milk containers and a11 other wrapping supplies when such us. is incidental to th, delivery of personal property which has been sold. IN J.S.A. 5432O8 (a)j Soles of materials, such as chemicals 'and catalysts, used to, induce or cause a refining or chemical process, where such' materials are on integral or ussenti9l part of the processing operation, but do not become a component part of the finished product. IN.i.S.A. 5432I-8 (t)j ' The sale of advertising materiulsta be;published in a newspaper. IN.J.S.A. 544 (cc)) The use of prapenty far market sampling by th, purchaser. [N.J.S.A 54421.11(4)1 ft * ft REPRODUCIION O EXEMPT USE CERTifICATE POfiMSi Private reproduction of Exempt Use Certificates may be made without th, pdor permfssion ofthe of Taxation. STATI Of MW JERSEY, DEPARTMENT OP ThE IUASURY, DIVISION OP TAXATION Post Office lets 999, Trenten, 14.3.01423 QE-CPC000041 53 !VI VAV,Lri4l+II'eI Lm.-r I r' I Ir'-n' LnurL'ritrnI7rLrA100e%eJrLr';ILr-44ItZ+7rQc,' IIiflr' I CONSULTING: ULTRAMICROANALYSIS - MICROSCOPY - SMALL PARTICLE PROBLEMS - SOLID-STATE CHEMISTRY 13 February 1979 Dr. Joseph P. Sixrko, Jr. Colgate Palmolive Qompany 909 River Road Piscataway, New Jersey 08854 Dear Dr. Sinico: Using transmission electron microscopy and selected area electron diffraction we have analyzed three samples of talc. These taics were designated as H.S., P.L, and I.L. These samples of talc were dispersed in approxinately 10 ml of sopropyl alcohol and deposited onto a ThM grid. The grid was then analyzed at 200 kV and 20,000X. We found all three samples to be cprnpletely free fran asbestiform minerals The samples were extremely platy and there were indications of rolled talc shards, fragrance and coloration pigment, but we found no asbestiform minerals. Thank you for consulting McCrone Associates. If there are any further questions concerning this report or the data contained herein, please feel free to contact me. Very truly yours, GRG j d Ref. MA 7673 Gen R. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE 'CHICAGO. ILLINOIS 60616 312;642-7100 -CABLE: CHEMICRONE QE-CPC000041 54 (OLGA TB-PALMOLIVE COMPANY A Dc/a wart C.rpoation RESEARCH 4ND DEVELOPMENT DEPARTMENT 909 River Road . Piscatswq, New Jcrsey 08851 REC9VED i.': 1 2 ;3Th January 10, 1979 Mr. Ian Stewart Mccrone Associates 2820 South Michigan Avenue Chicago, IL 60616 Dear Ian, I have sent under separate cover three samples of Talc finished products for asbestos analysis. These are complex formulations with the exception of the Heaven Sent. I've attached the formulations for your information. We've applied optical microscopy and xray diffraction and have found no evidence of fibers or amphiboles. In the Peachbloom ama Illumination samples, however, there are interferences with the xray and particles coating to the talc making optical microscope study difficult. Please use the best techniques you can to determine pretnce of asbestos mithrals. The data are required for a potential legal case. I would appreciate ou giving them the best priority you can, A purchase order will follow separately. Sample I.D. 's are 11.8. for Heaven Sent P.B. for Peachbloom j., 't., p IL. for Illumination Sincerely yours, 1-' JPS:ls Attachment 5. P'Simko, Jr. I C 5137-S QE-CP0000041 55 FORMULAT loNg Peaclibloom Magnesium Silicate E/V Talc Ti02 Zinc Stearate Kaolin Cosmetic Ochra Red Oxide Illumination Korean Talc Zinc Stearate Red Oxide Concentrate Cosmetic Brown Conc&itrate Cosmetic Tan Concentrate Microcel Marcol 4o Heaven Sent Talc Magnesium Carbonate 35% 36 10 10 19 1 1 68 3 3 8 8 3 6 96 3 JPS1s 1/10/19 QE-CP0000041 56 VU;-Lr;A-;.: :.iY)Lli ION - ME1Th "3LTt.0 / ORIGINAL PURCHASE ORDER rt't:4.t*4;U't xt7&WO 4.i'Ek! Show Ibis thnnber dix! prefix om in- vo%,'es, packtng 630319 COLGATE-PALMOLIVE COMPAN A DELAWARE CORPORATION 105 HUDSON STREET, JERSEY CITY, N.J. 07302 A SHIP TO 56 GREENE ST. JERSEY CITY. N.J. 07302 Nccrons Assocates 9P0IS9CRAIVflEWRARYD, .N.J. at854 2820 South Michigan a.:enue Chicago, Illinois 20 GRAND ST. JERSEY CITY. N.J. 07302 RECEIVING STATION JEFFERSONVILLE. INDIANA 47130 RKAENCSEIAVStNCGITSYT,AKTAIONN66! 05 DISCOUNT TERMS i fJ2/io N/3D 2 EIN/30 S 1/10 N/3D 4 Net Cash Trade SHIPPING TERMS 1 FOB DestInation 2 D FOB Ship,.ing Ft. (Pre-Pay& 8ill)See Below 3 C] FOBShlppingPt. (Collect) City IF ABOVE .DDY NO BE MET NOTIFY 710 CARLTON ST. BERKELEY, CALIF. 94710 300 PARK AVE. NEW YORK. N.Y. 10022 ATTN; Receiving Clerk YOU ARE AUTHORIZ o TO FURNISH TH ARTICLES LISTED HEREON IN ACCORDANCE WITH THE TERMS AND CONDITIONS ON THE FACE AND BACK OF THIS DRUER QUANTITY AND UNIT SYMBOL NUMBER PRICE - Three talc srip1es for microscope analysis for asbestos ninerala coded P.B, IL, and B.S.9 cost arprox, $1000 Samples sent under separate cover .at--enion Mr Ian Stewart NOTE: This is a one tiMe reqnsst. "Co!o-?crnoHvo Coj... Please qend invoice to Helena Itubnstein ATTE;TIO cc? Pvr rd Piscitavray1 N. J. 02C54 Yr Herb Schneider, VENDOR TO PROTECT ALL METhIr-gARIS AGAINST CORBD.SJ-ON-B TABLE PROTECTIVE SEALING. ts4Jo1a rJu k n'4-. Q-) t.,,k4..LS. ).&AJ&. (S tW tkttS (&AjO. SELLERS INVOICES that include authorized tnsportation charges, must be supported by prepald freight bill or COPY of original bill of lading. MARK PACKAGES with purchase order number, symbol numher, contents and quontHy. Acceptance of this order Is to be deemed a certificatian that you have read and agreed to the terms and conditions on the back hereof. PAYMENT WILL NOT BE MADE AGAINST PRO PORMA INVOiCE. GATE - PALMOLIVE COMPAN OE-CPC000041 57 TERMS AND CONDITIONS WARRANTY - The Seller expressly warrants and agrees that there has been compliance with.and no violation of any trademark rights, patent tights, copyright, or of any rule, law or regulation of the Federal Government or of any State or arty of their respective agencies or political subdivisions, in the manufacture, production, sale and or shipment of the goods hereunder; and the Seller will indemnify and hold Purchaser harmless from any or all costs, damages, fines or expenses (including counsel fees and fees of expert witnesses) which may be menu-ed by the Purchaser by reason of any claim or suit arising out of the infringement of any trademark', patent right or copyright and/or by reason of any citation, claim or suit for damages and/or penalties brought' against the Purchaser based upon any injuries, damages or violations resullngor claimed to have resulted from anyalleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY --The Equal Employment Opportunity Clause Section 202 of Executive Order 11246 as amended related to Equal Employment Opportunities and Implementing Rules and Regulations f the Secretary of Labor are incorporated herein by specific reference. CHANGES IN ORDER - This order cannot be changed, modified or discharged in any manner except by agreement in writing signed by a duly authorized ropresentative of the Purchaser. The Parchaser reserves the right to (1) maIze: changes in the order (2) cancel all or any part of the order at any time by notice in writing. The Purdhaser shall not be responsible for costs incurred by the Seller in connection with this order, after the date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser an itemized statement of elaine against the Purchaser within twenty (20) days after the receipt of notice of such change or cancellation, the Seller shall be conclusively deemed to have vaived all claims against the Purchaser with respect thereto, CANCELLATION FOR SELLER'S DEFAULT - Should the Seller fail (1) to effect delivery on or before the specified delivery date(s) (2) to deliver goods in all respects conforming '.ith the requirements (3) to duly perform Seller's obligation under each and al] of thc ternes and conditions of this order, the Purchaser may cancel this order in whole or in part. Without prejudice to the foregoing, the Seller agrees to report promptly to the Purchaser any delays in performance or in shipment of the goods covered by this order. SPECIFICATIONS, DRAWINGS, ETC. - All specifications, drawings, plaits, designs, samples, or other documents referred to in this order shall be deemed an integral part of this order as fully as if set out in full herein and Seller warrants that all deliveries and/or performances hereunder shall conform thereto, each delivery and/or performance being subject to the inspection and approval of the Purchaser, whether or not any prior payment shall have been made thereon by the Purchaser. NONCONFORMING MATERIAL - If Seller delivers defective material or material not conforming to the agreeupon specifications, Purchaser may (I) hold such material at Seller's expense pending Instructions as to disposal, (2) rcturn it to Scller at SelIer's.expense, or (3) utilize it in the form received or uftci up-wading or other operations arc performed ole it, or utilize it in a different manner or in different proportions with other products than was intended, and Seller 'viii he liable for any dinlinution in the value to Purchaser of the material and tar any incidenlal or other damages suffered by Purchaser resulting from such defectiveness or nonconformity. No replacomcnt of defective or nonconforming material will be made by Seller unless authorized by Purcliar. -LIABILITY FOR DAMAGES - Whenever Seller shall, by virtue hreof, have property of the Purchaser in its possession, the Seller shall be deemed an insurer thereof and shall be responsible for its safe return to the Purchaser. ASSIGNMENTThis order shall not be assigned or transferred without prior' written consent of the Purchaser. WAIVER -- Purchaser shall not be. deemed to have 'vaivod any of its rights hereunder emleas such waiver shall have been signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated there. in, shall be effective as to any delivery or other transaction which may occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL With respedi frarticularly to orders covering labor and material, Seller agrees to start work immediately, to proceed with the utmost dispatch and to complete a)! of the vork tinder this order. All such work shall be.performed in strict accordance with Purchaser's "General Conditions for Contract Work" Specification Nd:oe2o-CE, nbi shall work be permitted to start on Purchaser's property until required Insurance Certificates have -been received by Purchaser. Ti1e is hereby declared to be the essence o1 this order. Prices shown are firm and not subject to adjustment because of increase or decrease in material prices and/or wage rates arid/or freight rates and/or other itemsof cost. The acceptance of the final payment by Seller shall be-held to be a waiver and discharge of any and all elainis.and demands against the Pjrchaser for compensation and damages on aeount of any matter arising out of or in connection with the Contract or the performance of the work. Any exfra S additional work perforntid by Seller shall be on a fixed price basis or cost plus fee basis arid thust be in each case, first authorized in writiag by Purchaser. Seller's rates for such purposes shall be as set forth in a quotation from Seller prior to starting-any such extra or additional work and confirmed by Purchaser's prior writtea authorization- - QE-CPC00004 158 414 (TO7$, lit I. I. ;.e.pin.4 by pw.*.n. ;..S r . ,.teh.S by nadr, lad k,ikvtH*., - l.b ii Wd C.. like S. 1141$ CUIII4CATI MAY HO? SI U$lO IN ONHICTION WITH THI PUICHAII Cf SNYIC4S MAY SE REPkODUCED tilt as! Nrw 3rrsrg 04V1$toN OP TAXATION MLII TAX lUMP? USI CIR?WCATh FORM ST4 S (H... if Yr.Ai) Pu.; PlAItS. L51511KAtt 0? AIlIlIPIlIlY NIIMStN 131-815-595/aol Vp The undersigned purchaser certifies that tie not required to pay the New Jersey kin oSlo, Us. ?ax on the purchase 0, purchase. covered by this Certificate because the tongibi. petsonni property putchased will b. used for an e.ertpt purpose. Sold tangible personal property will be used for tie. fIlowing exempt purpoeet ior uSe or con.tption dlnatly and exelu.ivay in rssssrob and dsve1onent in the e*p.tiSrMI 0*' lIbOfltOfl' lflhIt. Tie. exemption on she sale of said tangible personal property to be used for the above described 84exempt purpose is provided In subsection N.JSA. 54321.1 (5ee reverse ifs for lisiksg of principal exempt uses of tangible personal properly and fill In the Mock with pr.pee suh.ecfIon citation). I, th. undersigned purchaser, have read and complied with the Instructions and rules promulgated pur- suant to the New Jersey Sales and Use Tax Act with respect to the use of the Exempt i.e Certificate, and it is my belief that the vendor named herein is not required to collect the soles or use tax on the Ircinscic- lion or. transactions covered by this Certificate, The undersigned purchaser hereby swears (under the penalties for perjury and false swearing) that cii of she Information shown in this Certificate Is true. coixan-azsLxvE CtSNY A V5NDC* shOULD *5*0 AND COMPtY WITh TN! IN5TMJCTICI4S OIVhI ON 50* 541*5 OP AN UIMPI1CN CIIWICATI, AM! O P%I*CHAM* (q. ,,ehSr.tI GoMsls.i ci tg,wIIct) 'V (UnoIsr. it ov.mpsonner. waiter L. zu.. bartment .QiZMlq iAddreu it Pvrthes) ...BrJeeertisy City, N. 3. 07 QE-CP0000041 59 MI INSTRUCTIONS FOR USE OF EXEMPT USE CERTIFICATES I Good Faith In general, a vendor who accepts an exemption certificate in "good faith" is relieved of liability far collection or payment of tax upon transactions covered by the certificate The question of "good lois I," is one of fact and depends upon a conuderotiori of oIl ihe conditions surrounding The transaction. A vendor Is presumed to be familiar with the low and SIte regale' lions pertinent to the business in which he deals. In order br "good faith" to be ntabi'shed. she following conditions must be met: (a) The certificate must contain no statement or entry which she vendor knows, or has reason (a know, Is false or misleading (I,) The certificate must bean officially promulgated certilicate form or a substantial and proper reproduction thereof. () The certificate must be dated and executed in accordance with the published instructions, and must be complete and regular in every respect. the vendo, moy, therefore, accept This igood fafth Exempt Use Certificate on a basis for exempting sales to the signatory purchaser provided that: d) he purchaser's Certificate ci AuthorRy number, indicating that the purchaser Is registered wHit the Hew Jersey Dividon of Taxation, centered on the face of the CertIfIcate. (e) The ptkhoser has entered all other information requited on the farm. (I) Tue vendor ha; no reason to believe that the properly to be purchased Ito!. type not ordinarily used In the purchaser's business tar the purpose described In this Certf irate. 2. IMproper Crn'tlNcat.Salutronsactlotis which are not supported by properly executed nemptiots certffitctes shall be de.ned to be taxable retail sales. The burden of proof that the tax was not required to be collected Is upon the veisdor. L Correction ef CertifIcate "In general, vendors haveko days after date of sole to obtain a corrected certificate where site original certificate locks material information required tab. set forth in sold cettlflcote..or where such Information is Incorrectly slated. AdditIonal Purcheses by Same PurihaserTh,is certificate will serve to cover addfl irdtOseiby the a purchaser of the same general type oi property However each subsequent sales sup or pvrchaseinv&ce based on sins Certificat, must show the purchaser's name, address and Certificate of Authority number fOtpiposf4i$f1Edtion. Retention ef Certificates Cerlificotes must be retained by the vendor for a period of not less titan three years front the dote of thelcat. sale covered by the certificote.Certlflcates must be L sit, physical possession of th. vendor and ovailable for inspection on or before the 60th day following the date of tIt transaction so which ihe certificate reicstes. 11w nuns stiumon axempt uses lo, which she Exempt Use Certificaie (Form St'4) is applicable are the following: Sate' ol machineiy. apparatus r equipment for use or consumjiioh directly ovid jiilmarily inthe producio, eneration, ironimuition or disiribulion of gas, electricity, refrigeraiion, steam or water tar sale or In the operation of sewerage systems. INJ.SA. 54:328-8 (in) (2)1 Sales ottdngible personal property purchasedtor use or consuthptio directly.ond exclusively in research ond development in she experimental or laboratory tense. Suth research and development-shall not be deemed to include the ordinary testing or inspection a! miiels or produrt for t4ILsOtity catittal iflktency ryi sfsanagometititudin, consumer surveys. adnrtising, pronotioni or research in connection with literary, hIstorical or similar prolects. IN.i..5.A.54t32b-8 (n)J Soles or use of wrapping paper, wrapping twine, bags, cartdns, tape, Fope,' labels, nonreturnable containers, reusable milk containers and all other wrapping supplies when such use is incidental to the delivery of-personal property which has been scfd. IN iSA. 543214 (0)1 Sales of materials, such as chemicals and catalysts, sued to induce or cause a ref iriin or chemical process, where such materials are an integral or essential part of thepracessing operalian, but do not become a component part of the finished product. IN.i.S.A. 54:3288 (t)I The sale of advertising materials to be published inc newspaper. IN.J.S.A. 54-8 (eefl The use of property for market sampling by th, purchaser. IN.i.S.A 54328t I (4)) etc RIPROOUCT1ON OF EXEMPT USE cERTIFIcATe FO*MSi Private reproduction of Exempt Use Certificates may be made without the prior permIssion of the Division of Taxation. STATE OF 41W SERSIY, OIPARTMINT 0? THE TREASURY, DIVISION OP TAXATION Past Office Mx 999 Trenton, N.J. 01425 OE-CPC000041 60 Memo from BILL GREW () VP/mtO. 3 j/c6a. L?'cJ / /r///1C'-1..(t-) c.cfl .Y / r_ Co JJU t QE-CP000004I 61 cQcaQoct QE-CPC000041 62 - PROJECT COST RECORD talc PROJECT TITLE: SPONSOR: CYPRIJSLNDU I- $ ADDRESS: 651 Metuchen Rd OiJ %-.J.IJ..ia_LL-kLnJ.1a..4,.L41..-.c.C1J_A'L till (Il'U"Q' n HAS PROJECT NO.: D&TE RECEIVED: NO.: 9foi - $ Contact: NlD e V'Y1 A /I1t4S SUMMARY OF PROBLEM: Lab Notebook Refereiaces: No. pp. Initials No. pp. Initials No. pp. Initials Photomicrographic record no. 3 Telephone No. Sample disposal: returned filed (where) discarded DIRECT COSTS (Exclusive of oper. Individual time time on lust, below) Travel Charge Summ2 Date Name hR131 ( ftfl Hours /) if oOCharge Date Traveler Destination Cost 4 Individuals $ Instrument Travel . Outside Other Instrument time Date .SEM TEM XRD EMP IMP ESCA EMMA MOLE Hours Charge Date Company Photo Photo MateriaLs Supplies Total Charge Cost $ OIC for bUilt Pro) cot Ldr Group Ldr RIlE PROJECT LEADER: TOTAL CHARGE $cc BILLED TO CLIENT $ INVOICE NO. (5) 'Y'' wV't n-iqq t7TzYt3oe, 3qn. 2Th4g 35 QE-CPC000041 63 :c. AOc ,:\ / '/f?' ." cA(:e .4/vU'y L/CQ79 Jr /1 -r- (/(jI..5-/. .j-I p f, /4 1 p -'2 cIA .-L1-' /3 K. 1_. ) I. QE-CPC000041 64 KYAVA waiter , mccrone associates, inc. !AvA CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID$TATE CHEMISTRY 25 February 1983 Mr. Keith B. Lehman Cyprus Industrial Minerals Company 651 Metuchen Roal South Plainfield, New Jersey 07080 Dear Mr. Lehman: I have completed ny asbestos analysis on a talc sample labeled "Monoblend", Lot 1120965k P113833 an submitted under your purchase order #45079. The sample was ecamined with the transuri ssion eleetcon microscope. The sample contained no detectable asbestos. The Exult of detection for the nEthd is approxixuately 0.1% per weight of asbestos. Thank you for consulting McCrone Associates, please contact BE if you have any questions. Sincerely, Richard M. Ellis, Jr. Research Microscopist RNE: fe Ref: 9863 2820 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS 80615 312/842-7100 CABLE CHEMICRONE QE-CFC000041 65 yprus Industrial Minerals .Comp sflSo%.th Flow.t St..t La. Aaq*. CJROIT XC7I tSaobon. t2131 eZiW Vendor Walter Mccrone AssociaSs Inc. 2828 South Michigan Ave. .; Chicago, ILL 60607 Attn: Richard M. Ellis, Jr.. Purchase Order Ship To: Acknowledgement Requested F- Keith B. Lehman CYPRUS INDUSTRIJ\L MINERMS 651 Metuchen Road .... So. flainfield, N.J. 07080 To: Date 2/9/83 Quantity Ordered . ... .. . ......rpV . Quantity Received t - ...,'bescnption - for.. '.. please run yointceguJ.ar test asbestos fibers on enclosed -. sample 4 - Please ie th s'P.O4 for all invoi.c;kicngfl>f&orth- e..y. ear 1983 -. Date Required ASAP Unit PdCO - .-.-.-.. . Terms Net 30 Total . ... I/ TI.-cnt-t; 2. - A 45079 Abova order number must appear on all papers arid packages reladve to this Order. QE-CPC000041 66 fl waiter C. mccrone associates, inc. I CONSULTING ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 22 Septexnbei 1981 Mr. Vern Alibis Cyprus Industrial i4inerals Company 651 t4etuchen Road -South Plainfield, New Jersey 07080 Dear Mr. Ailtus: I have completed my asbestos analysis of a talc saip1e 1a1ele4MonQblen4, - lot number 812065. The sample was examinedwith.the transission electron microscope. No asbestos minerals were detected. The analysis ha a detection 1ijit ot approximately 0.1% by weight:. - Thank you for consulting NcCrone Associates; please ontact ie if O33 have any questions. Si cerely Richard N. Ellis, Jr. Research ticxoscopist MA 9863 2820 SOUTH MICHIGAN AVENUE CHICAGO, ILLINOIS 60616 3121842-7100 CABLE CHEMICRONE QE-CPC000041 67 Cyprus Industrial Minerals Company 651 Met ychen Road South Plainfield, N.J. 07080 Telephone (201) 754-4880 TWX 710-997-9528 August 21, 1981 p..L-O Mr. Rick Ellis Walter C. McCrone Associates, Inc. 2820 So. Michigan Ave. Chicago, Illinois 60616 Dear Mr. Ellis: Enclosed herewith please find one (1) sample of Monoblend, Lot No. 812065. Please perform the usual test for asbestos and retnn the results to our office. Very truly yours, CYPRUS INDUSTRIAL MINERALS KBL/hbt Enclosure Keith B. Lehman Asst. Plant Supt. ;: CYPRUS QE-CPC000041 68 waiter c. mccrone associates, inc. CONStJLTINO IJLTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 28 August 1981 Mr. Vern Alitus Cyprus Industrial Minerals Company 651 Metuchen Road South Plainfield, New Jersey 07080 Dear Mr. Alitus: I have completed my asbestos analysis of a sample of Cyprus Monoblend talc Lot #712165. The sample was analyzed by transmission electron microscopy and electron diffraction. The sample contained no detectable asbestos minerals. The limit of detection is approximately 0.1% by weight. - Thank you for consulting Nccrone Associates. If you should have any questions concerning this analysis, please contact me. - Sincerely, Richard M. Ellis, Jr. Research Microscopist RblE: fe Ref; 9863 2820 SOUTH MICHIGAN AVENUE cHICAGO, ILLINOIS 60616 312/842-7100 CABLE CHEMICRONE QE-CP0000041 69 raj%j waiter G mc crone associates, Inc.I CONSULTING: ULTRAMICROANALYSIS MICROSCOPY . SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 29 11pU .]SSI Mr, Vern AZitus Cyprus Industrial Rtnera.]a Company 651 l4etuchen Road South Plainfie],d, NJ 07080 Dear Mr. A1.ltus: I have compZsted 7y asbest.9S a,na,.J,yss of a, ane: b. is crCyprtis Monoblend Talc Lot #311865 receiyed by 20 March 1981, j4gq-The sample was analyzed by trns.rqsstpp. el.ectxqn. scopy and e1ectroi diffraction, The sample bonine n detectable asbestos minrw1. floeThank you tar consi1,ti,ng MCCXQne Associ.ates. contact us if yoi have ny questions, SinceZyr RME j r Ref. MA 9863 J,chrd M. 1],is .Iesearch. Bi9rQSCQpifl 2820 SOUTH MICHIGAN AVENUE. CHICAGO, ILLINOIS 60616 312/642-7100 CABLE: CHEMICRONE QE-cPc00004l 70 a waiter c. mc crone associates, inc1CONSULTING: ULTRAMiCR0ANALYSIS MICROSCOPY 'SMALL PARTICLE PROBLEMS . SOLID-STATE CHEMISTRY - 29 4prJJ. .1981 Xjr, Vern AZitus Cyprus Industrial Minez'@s. Company 651 Netuchen Road South Plainflej,d, NJ 07080 rear Mx, 3,ltus; I have compteted flw asbstps i.ysb. of a ap o Cyprus Monoblend T1c iot, #311865 eciyed by is on 20 March 1981W he sample was ana1yze by scopy and electron diffraction, detectable asbestos. xn&nen1s tgn :i4cq-' sample j2qntaine4 flQ Thank you for consifltinq McCqne As.goc&atec, contact us if yo ha,ve ny qpestipns 3,eae Siqceyqly, BME; :i r Ref. MA 9863 13d M. ZL\5 Ies4rch cqscopJt 2820 SOUTH MICHIGAN AVENUE. CHICAGO, ILLINOIS 60616 3121842.7100 CABLE: CI-IEMICRONE QE-CPC000041 71 3ou&4\fL c.Cyprus Industrial Minerals Company Interoffice Correspondence To From halter C. Mc Crone Vern All ti's Date March 20, 1981 Subject7 Colgate samP) I- Incloset are two different saniples of Meterial to be tested and the results returned here to me as per our recient conversation. LOT # 311865 is a new lot. I still have not recieved the retunn of the/previous sanwle LOT # 110865 which I requested retumQed to me. i1Aa em Alltus Plant Supt. CYPRUS QE-CPC00004I 72 kYAIA waiter c. mc crone associates, inc. TA,A1 CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS 'SOLID-STATE CHEMISTRY 25 March 1981 Mr. Vein Ailtus Cyprus Industrial Minerals Co. 651 Netuchen Road South flainfield, New Jersey 07080 oear Mr. Alitus: I have completed my asbestos analysis of a sample of Cyprus Monoblend Talc Lot #110865 received by us on 11 March 1981. The sample was analyzed with the transmission electron microscope (TEM) and electron diffraction. The sample contained no detectable asbestos minerals A few fibers of a clay mineral, sepiolite or attapulgite, were seen. t Thank you for consulting McCrone Associates. Please contact us if you have any questions. Sincerely, RIlE; gb Ref: 9863 Richard N. Ellis, Jr. Research NicroscoiSt 2820 SOUTH MICHIGAN AVENUE CHICAGO. tLLINOI$ 60616 312/542-7100 CABLE: CHEMICRONE 0 E-CP0000041 73 -a QE-CPC000041 74 QE-CPC000041 75 PROJECT COST RECORD PROJECT TITLE: tale sample for asbestos (TEM) SPONSOR: ADDRESS: ill t,uLI. A1uit Way - P.O. ox 341i ugLewuoU, ULu PROJECTNO.: Ilk 1119 DATE RECEIVED: 7 27 3: P.O. NO.: COMMITMENTS: $ .300 Contact: Dr. Kenneth W. Olson TelephoxieNo. SUMMARY OF PROBLEM: Lab Notebook References: No. pp. Initials No. pp. Initials No. pp. Initials Photomicrographic record no. Sample disposal: returned filed (where) discarded DIRECT COSTS (Exclusive of oper. Individual time time on inst. below) Date Name. Hours Charge / Instrument time Date SEM TEM XRD EMP IMP .ESCA EMMA MOLE Hours Charge Travel Charge Summary Date Traveler Destination Cost Individuals $ Instrument Travel Outside Other Date Company Photo Photo Materials Supplies . . Total . Charge Cost $ OK for billing Project Ldr Group Ldr *,1R.......... TOTAL CHARGE $ BILLEDTOCLIENT $ 3/b INVOICE NO. (8) St4&ct. / QE-CPC000041 76 1IA1 waiter c. mccrone associates, Inc. i CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 21 October 1982 Dr. Kenneth W. Olson Cyprus Industrial Minerals Company 7200 south AJ.ton Way Englewood, Colorado 80155 Dear Dr. Olson: Our laboratory has completed the asbestos analysis of talc sample 'TAltac 400, 052582" under your purchase order fl-0074-82. No asbestos was detected. ApproximRtely 0.1 to 0.15 grams of material was suspended in 10 mis of .01% methyl cellulose This was ultrasonerated for 15 minutes and a drop of the supernatant liquid was placed on a carbon coated transmission electron microscope grid. The sample was then examined by transmission electron microscopy. Enclosed with this report are electr n micrographs of the talc. If you have any questions regarding this analysis, please do not hesitate to call. Sincerely, DPI': fe End. Ref: 11196 Deborah P. Palenik Manager, Electron Optics Group 2a20 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS 60616 312/842-7100 CABLE CHEMICRONE QE-CP0000041 77 KVA!A waiter C. mccrone dssociates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STAtE CHEMISTRY 21 October 1982 Dr. Kenneth W. Olson Cyprus Industrial Minerals Company 7200 South Alton Way Engie.wood, Colorado 80155 Dear Dr. Olson: Our laboratory has completed the asbestos analysis of talc sample "Altac 400, 0525821 under your purchase order 9K-0074-82. No asbestos was detected Approrimitely 0.1 to 0.15 grams of material was suspended iii 10 mis of .01% methyl cellulose. This was ultrasonerated for 15 minutes and a drop of the sup ernatant liquid was placed on a carbon coated transmission electron microscope grid. The sample was then examined by transmission electron microscopy. Enclosed wtth this report are electron micrographs of the talc. If you have any questions regarding this analysis, please do not hesitate to call. Sincerely, DPP: fe End. Ref: 11196 Deborah P. Palenik Manager, Electron Optics Group 2820 SOUTH MICHIGAN AVENVE CHICAGO, ILLINOIS 60816 312/842-7100 CABLE CHEMICRONE OE-CPC00004178 Cyprus Industrial Minerals Company Tatc Division 7200 South Alton Way, P.O. Box 3419 Englewood, Colorado 80155 303-740-5444 July 20, 1982 Ms. Deborah Palenik Walter C. McCrone Associates 2820 South Michigan Avenue Chicago, Illinois 60616 Dear Ms. Palenik: Enclosed please find talc sample "Alta.lc 400, 052582" for analysis for asbestos and asbestiform minerals using the TEM-SAED method in your laboratory. As per our telephone conversation of July 20, 1982, this work is to be done using our P.O. #TK-0074-82 and is to cost $300.00. As we are eager to obtain the results of your analysis, we hope to obtain your report soon. Sincerely, Kenneth W. Olson, Ph.D. IWO/me Enclosure C. It. Moebus QE-CP0000041 79 a '1 'I y ) 13,500X waiter c. mc crone associates, inc. QE-CPC000041 80 waiter c. mc crone associates, Inc. OE-CPc000041 81