Document rxwynVVeO1bNp53wy3MypGD2r
to: x. R. Torkelson
72
THI DOW CH1MICAL COMPANY
MIPLAND MICHIGAN
ANALYTICAL LABORATORIES
REPORT SHEET
DATE March 4, 1959
MAIN LAB. NUMBER
SSR 275-883
YOUR NUMBER
Aa Hated.______
DESCRIPTION.
Rabbit Blood Oxalated
CHARGE .1219-26.
Sample 965A"
965B 966b I/, 967B >( 968b_
iffc
Mllligrama of Bromide per 100 ml.
IM a*-*#'*?
0.53 0.53 3725
2.75 2.78 _
__^3*O0_
-- 5.00
A
8.30 ^
1-J5 _SUI7,,
3.17
2 / }-+
C- t'i
to: T. R. Torkelson
THE DOW CHEMICAL COMPANY
MIDLAND NICNIOAN
ANALYTICAL LABORATORIES
REPORT SHEET
DAT! March 20, 1959
MAIN LAt. NUMBER_______AXfS 2026
YOUR NUMBER DESCRIPTION
As listed. Oxalated Rabbit Blood
1219-2
I
Sample No.
965 F 966 F 967 F 970 F
Milligrams of Bromide per 100 ml.
13*3 12.6 10.8 13.0
*
'V
r. ~
//,<r
2 hrs. 4 det.
y E. T. Wagoner
can
mw
Mirrtfi it .t.A tt-tt
00 130605
OONFTOFNTTAI
SIGNED
74 Sldg
trials
MX.
K HOv_ /7/r- ^
MATIXUkL.
BIOCHEMICAL RESEARCH LABORATORY
WEIGHT RECORD
<L*-
T -X S'* t^TV^2--PN.INO.
__ LtXPT. MO.
SUM MO.
moOLIM MO^_
ACCT. MO..
/ *I
to: T. R. Torkelaon
THI DOW CHEMICAL COMPANY
MIDLAND MICHIOAM
ANALYTICAL LABORATORIES
REPORT SHEET
DATE March 12. 1959
MAIN LAB. NUMBER
SSR 275-964
YOUR NUMBER _______ Afi_llBted.
DESCRIPTION
Oxalated Rabbit Blood
CHARGE___ ?-219-26
4
Sample No.
965E 966E 967E 970E
Milligrams of Bromide Per 100 ml.
4 hrs. 4 det.
.v E. T. Wagoner can
PMN wm PJBTt is B.I.A. BB-SI
MGNED
1
ii
^ 330607
CONF TOFNT TAl
Phone 6-5900 S. A. Shrader
mA
574 Bldg.
to.- T. R. Tork laon
THl DOW CHEMICAL COMPANY
MIDLAND MICHIGAN
ANALYTICAL LABORATORIES
REPORT SHEET
DATE April 23, 1959 _MAIN LAP. HUMBER ALS 2X25
YOUR HUMBER__________ AS Hated,
DESCRIPTION
Rabbit Blood
CHAROE 1219"26
Sample No.
965 0 966 0 967 G 970 G
Milligrams of Bromide per 100 ml.
ri-
C/ tfjt
8 hra. 5 det.
ey E.
Wagoner
can
MM MM Mlme II I.S.A. M-M
SIGNED
oo -\30k08 CONF
Phone 6-^qqq ader
m T. R. Torkelson
THE DOW CHEMICAL COMPANY
MIDLAND MICHIGAN
ANALYTICAL LABORATORIES
REPORT SHEET
_DATE April 10. 1959
OtAKCE ____1219-26
AT*? 17 5MAIN LAE. NUMEER_____
YOUR HUMBERAS listed.
description______Rabbit Blood__________________________________________
Sample No.
965 H 966 H 967 H 970 H 965 I 966 I 967 I 970 I
Milligrams of Bromide per 100 ml.
9 hrs. 8 det.
y E. T. Wagoner can
FBM BBN ftlITtB IB B.S.A. M-l
HONED.
no
Tr>FNTT Al
Phone 6-5900 S. A. Shrader
574 Bldg.
to: T. R. Torkelson
THE DOW CHEMICAL COMPANY
MIDLAND MICHIGAN
ANALYTICAL LABORATORIES
REPORT SHEET
DATE April 17. 1959
MAIM LAI. HUMBER ALS 2277___
YOUR HUMBER_____A3 listed.
DESCRIPTION.
Rabbit Blood
charge Igl9-g6
Sample No.
965 J 966 J ' 967 J I' 970 965 K 966 K J 970 K /
_y
Milligrams of Bromide per 100 ml. (By Reflux Method with
ethanolamlne)______
16.1 15.8 14.8 18.0 tJUdJ-
8.7 ' i'C'. "
9.5 10.4
x4
f. 3
Milligrams of Bromide per 100 ml.
(By Usual Methodcaustic treatment)
15.9 13t7
16.4
10 hrs. 10 det.
>Y E. T. Wagoner can
FPffM mo NIITU II I.I.A. M-M
-0 I30fl l0 C0NFTr>FNTT,
Phone 6-5Q00 ader
74 Bldg
T0'T. R. Torkelson
THE DOW CHEMICAL COMPANY
MIDLAND MICHtOAN
ANALYTICAL LABORATORIES
REPORT SHEET
DATE_________
AL HUMBER
YOUR NUMBER DESCRIPTION
June 2. 1959 ALS 247*3 As Hated. Rabbit blood oxalated
CHARGE . 121Q-26 j -PROBLEM ______________
Sample No.
965L 57'fo 966L 967L 9701^ 965M sy'r 966m 967M 970M ,
/
Milligrams of Bromide per 100 ml.
20.9 15.6 10.6 18.1 _ _L*'
15.1 10.2
8.7 12.7
p
I
DO 130611 CONF TDFNTT At
t;
T. R. Torkelson
THE DOW CHEMICAL COMPANY
MIDLAND MICHIGAN
ANALYTICAL LABORATORIES
REPORT SHEET
DATE June 4, 1959 _
A L NUMBER
ALS 2604 .
YOUR NUMBER
As listed.
DESCRIPTION
Rabbit Blood.Oxalated
CHARGE PROBLEM
Milligrams of
The number on the sample bottle is 963N.
The samples of this series were analyzed by Analytical Method MLS. 5**. 6, May 13, 1954.
SPLE.
4
HRS.
BY E. T. Wagoner can
DET. 4
00 13001?
CONFTDFNTTAl
SIGNED
Shrader
PHONE me- pgpn
bldg. 374.
DATE -- TIME! STAR^.
STOP _ TOTAL TIME _
~7~
-Ami
J/JAt-./KL
RATE OF SAMPLE FLOW
.MINUTES
fr2-> LITERS/MINUTE
SCRUBBER NUMBER____
^ITON SCALE) 2-
COMB. (ANALYZER READING
OR IR
(ANALYZER ZERO
)
COMMENTS!
DATE
-
TIME: START------- A'
STOP -
TOTAL TIME .
TES
RATE OF SAMPLE FLOW .
' e ILITERS/MINUTE
SCRUBBER NUMBER
COMB.
'J S'(ANALYZER READING#^
ON SCALE)
OR IR
(ANALYZER ZERO
COMMENTS:
)
DATE _________ TIME: START.
?/fr(T7
ITT
STOP _ TOTAL TIME _
JjL
, MINUTES
RATE OF SAMPLE FLOW
4-X3JTERS/MINUTE
SCRUBBER NUMBER COMB. (ANALYZER READIN&J^JL^J^ON SCALE)
OR IR
(ANALYZER ZERO
)
/Ihm/
/ml. 0,8} N *fWO/> ml. ALIQUOT
SPEED
CHAMBER NO.6e-------------------- i--i
ANIMALS in chamber
LJ y..
ANALYSIS .
>!. 0.03 N Ag N03
f_ ------*1. 0.03N NH4 SCN
?r y*~ ml. NET
(SSR.
Report No., (SPEC..
)- X____FACTOR
/P.P.M.
^
-1-
j. *3--------LITER MINS.
5=^;
7^SPEED
7^
CHAMBER NO-------------------------------------------- .----------- -
--
ANIMALS IN CHAMBER
LJ V.^/CSJ-No
ANALYSIS0.03N Ag NO3
/.3r .oil. 0.02N NH4 SCN
_______ (L 6 / -Ml. NET
Report
(SSR
mi. x
FACTOR ^/'P.P.M.
__Min. X___Z..?~__
LITER MINS. ,
7SPEED
CHAMBER NO. . IIMALS IN CHAMBER
Y.. Hrs,
ANALYSIS .
{9*
/
ml. 0.03 N Ag NO3 ml. 0.02 N NH4 SCN
.ml. NET
(SSR . Ropon No. (jpg^
M. XJH1__ FACTOR
__X___ min. X
/ 3--______ LITER MINS.
P.P.M.
COMMENTS:
MATERIAL ,
/
ANALYTICAL
V/ (TyAA^!^_
FACTOR,
DATE . time: SttTaArPtT * _
STOP TOTAL TIME . RATE OF SAMPLE FLOW.
~TT minutes LITERS/MINUTE
SCRUBBER NUMBER .
COMB.
(ANALYZER READINflfi^5S`L- ON SCALE)<2____
OR IR
(ANALYZER ZERO
COMMENTS;
)
/7/
DATE__________
TIME: STARTSTOP _
/A ^ /
^7/ /inr
TOTAL TIME _
f/ ~^MINUTES
RATE OF SAMPLE FLOW
-liters/minute
SCRUBBER NUMBER
COMB.
(ANALYZER READINcJ-^^^ ON SCALE)
OR IR
(ANALYZER ZERO
COMMENTS:
)
-.J /7/s-y____________________________`___________________
/Utm/
/! 0.0}IH Af HO/5 t. ALIQUOT
SPEED ^ letjft******
CHAMBER NO. _t_____
,_______
/ESG..ANIMALS IN CHAMBER y'UOfM
fS
Ol-J No
ANALYSIS ml. 0.03 N A* NOj
ail. 0.02 N NH4 SCN
.ml. NET
0.CF__ ml. X
jRoporr N*.,, `(SPEC-------- -- ----------------------FACTOR
J"S" -i. X---TTITER MINS.
7SPEED
CHAMBER NO-- ANIMALS IN CHA:MBER
n. YY.o
ANALYSIS- _______ ml,. 0.02 N /> NO03j
________________ *1. 0.02 N ________________ ml. NET
NH4 SCN
.`ff
Report
_____________
4JLL .ml. x Uic-
1"^
.factor/^#/ P.P.M.
Air LITER MINS.
COMMENTS:
Hi
DATE _________
TIME: START.
STOP _ TOTAL TIME _
7
RATE OF SAMPLE FLOW_______
SCRUBBER NUMBER ____________
COMB. (ANALYZER READING
OR IR
(ANALYZER ZERO
COMMENTS:
minutes
LITERS/MINUTE
.ON SCALE) )
SPEED J
CHAMBER no. fr
ANIMALS IN CHAMBER
ANALYSIS .
_______________ ml. 0.02 N
ml. 0.02N
-MZ- ml. NET
.ml. X. . min. X .
To.
No
A* N03 NH4 SCN
(SSR Rnpert No. ,tBrr
. FACTOR is-T. pJPal
.LITER MINS.
I
COMMENTS:
CONF TDFNTTA!
BIOCHEMICAL RESEARCH LABORATORY
FUME CHAMBER EXPOSURE RECORD
ANIMALS:
HATS-----------LAOES
CAVIES- - --CASES
RABBIT#g3cAGES 3U?/- f JL-
PROBLEM NO. T_
_J__________________________
EXPERIMENT NO.
/__________________
RUN NO---------------
VAPOR CONC:___ ^_____ IBJ./1.
EXP. NO.
NO. DAYS
DATE
HOUR
HOUR
HOURS
IH BY OUT BY EXPOSED
r1/
-7-3~9
/$ fi?~ ' / /c (Z^ * 7. ^
11 -93? 9 c>3 R*r" i
?,>
n if -93? 7 /S
1 & ftv~` 7'&
3^ hS A~(oS4 Z OvC e fir 3 oS iff 7,d
9jS * 3/3-3? 7 ie R**~' ? /# R**" Z *
16 ?
9 >3 ftvr- ,1 dS
7-0
37 A * -fo-37 r oS R*t-'
03
7< o
3 S 3/ ~l(rz
n io pt** 7< O
ffu H-tl-ST # ]V
/X 7cr
4-0 S3
? /0
(o 7. dP
s& '~Usf? ? j3 RY-- 3 /3 ps" ?&
77
7 3,3
% ss R~~` 7.0
11 9 '*33? 7 30 R--- X $0 Rr-*- y,#
f? 7 33 \i<^' JS , 7-C
teTs -z7ST 7 93
% *ys Af*' 7-0
y-7 3*
7 30 &*r*- so Kr~" ?.<D
H? il l-WTf 7 &> K^~' 2. so kt- 7'
Hi US' -3bsy if H Rt-' 3 / /?r-' 7 *
S0 _ 4 6? S-f-39 7
7 93
70
jr/ 4 1 SYS? ? 3d
1 30
>~
sx 7'* SS-S9 7 St tK / e\ i$ si
5~3 74 3-43? 7 sro
-L* sTO /?!-- 7 tf>.
SI T> 6-7-5? S c*~ R-*~ *
/^cr'` 7- ^
S'S' 73 s'-srsy 7 K ft^ i. 9?
7 .<>
f4 U
S'7 17
1i 7
30 30
ff-T' K-r-
i 2
so sv fir**'
7c ?. a
M IS s-ft'61 7 '/S H*r- ?- L RJV' 7, &
59 79 S-m-S9 7
Iff X SL
IIwpb i
So
?3
f'ffvf r-igo?
77 ,
I* H*
t ir
$ 7.0
}. <0
REMARKS
0.Xo.k._____________________________________
&K+ ___________________________________ a 4-
s.tf, 0.H OK. 0AC, QAf. art.
oft.
0/<` <rS, 4*t. a*.. &'(, &/<, #/9.
't-r 44*f o.K>
o.K.
c?A'
d,K* 00 130815 O',*. (.ONF TDFNT TAt ok' n(c<
BIOCHEMICAL RESEARCH LABORATORY
FUME CHAMBER EXPOSURE RECORD
ANIMALS: RATS------------ CAGES_________________________________________ CAVIES----------- CAGES_______________________________________
3 ARABBITS--------CAGES *T t-- 9^7
PROBLEM NO. T-------------------------------- --------- -- EXPERIMENT NO------------------------------------- -------RUN NO _________________________ _ VAPOR CONC:--------------------------------------
c1+ 4t& &
EXP. HO.
NO. DAYS
DATE
HOUR IN
BY
HOUR OUT
HOURS RY EXPOSED
/ <7 A-ASSf f
tfr-' f DP IX'T'' 7-o
X / A-*4-59 fT
3R*^* ID
7,0
h A-a. l-l^rsT?
/a ft~-* a-t
3 3
/%. R*~' 7 p ft--' 7/p
jiT 9 Z'17-S?
C 7 5--2.-CT9
XcT
C>S
7. 4to" fey-*
3 esT
7. 0
R7 5- 3 =>'9 r ? 3-y-o'^
/S ie^. ,3 /CP ft--- 3
(S R*i+* 7. 0 io R"^' 7. *?
9 j0 3 5-jT?
(P ft-r 3 /P
- 7.0
/> // Z-b-Sf
/S
((
/</ 63-7-0"?
cT
3 jo ft"* 7-o
5 65
7. <D
i% /? 3-16-of
it-
- 3 /l ft--- 7-0
/3 / 0 3~//S?
60 fl-r* 3 &e (l^ * 7. 0
M /?
CP# ft -- 3 0? Br-- ) t>
nr/ O 3 '7 of 7$
3 10 Z?*^' 7.0
/ 3/ 5-tle~9
f it $ l- if 7,0
17
3-n-9 7 .*P
A. P. If 7,0>
!</ 3-/^? * o 7 /? 3 >1 e^r 7,0
t9
3'1`f-Sf 7
Lf? .A_ M- JJL 7,0
2o
3 --3 ^5j 7
f
tft
7,1 _
z / l 7 Z-*3-S? ?
3 P0 /p?^' 7.0
i.2. 27 3^-sp 7 i> o' ir~~'
Co' PV6-. 7- 0.
3 2-T^7 7 a S fi <** 3 esT
7. 0
2# 3
S' l* ft**--- 3 n R*~` 7. 0
zf r#
$> lt> R^r _a_ [* I?-- 7./P
L- 3o 3-M?f r Do R^' 3
70
2-7 3 l
if 3 fir-* 3` *2--
7` 0
3 7 V-i--p'"?
/O' ft-*- _L,, t o' fil- 1 0
tf If V.-3 =T9 fp
RT'V ,? PC ft -- 7 0
y/
7 2.0
704 2,0 ft -- *
remarks
PK.
P.K._____________________________________ P./C, &*&//*&? fPb/
PCf,
cs. P.K, P.K,
&K, cp*'
eft.
p.k>
p> /< p/<. 0?A,
o/r 0 tf~
A/f' ck~
0 tc
0/7. o.K. 0.K,
P.K. O.K.
PS.
. ^".. a. ft.
DO 1. 3. 0_ 616 rONFTOFNTTAI
O.K-
Pile No, 3<- 5 k no. _l?SJTr^L.
SET UP FOE VAPOR EXPOSURE TO ppm-
Chamber #C-
MW --JM.
DENSITY r.
BP
n^
/_
ppm s/mg/llt
PPm = J&2&L mg/lit
ppm = 0.193- ns/lit
Assuming an airflov; oT /lit/min
'"rtf'**7
[IS?'?
3(oz. ,,
/r.y
lit/min x
ms/lit =
m/mi n
SjdT?" -"/min
2?rr nc/mi
/ ml Syringe
m^/niln
rs^-fs
Speed
vfA_L \
f 1
The delivery is -ty/ff ml/min
ni/nrin = _Jlit air/min
^^/rOJ-n-ii/min
/" lit air/min
V = lit air/min lit air/min r. 0.035315 ft3/llt = /?. jTft3/hln
Us ins Fiovrneeer /^(T
setting
ofthe required airflow.
DO 130017 CONF T DFNT T Al