Document rpRZX7XLZrYGQN7vKyM7vEK1v
STL Burlington Colchester, Vermont
Extended Data Package
SDG: 117591
Case Narrative Sample Report Summary - Geotechnical......................................................... Supportive Documentation - Geotechnical...................................................... Sample Handling................................................................................................. Last Page of this Document...............................................................................
1 5 27 33 36
Case Narrative
i
STLS E V E R N
TRENT
November 30, 2006
Mr. Charlie Young Weston Solutions 1400 Weston Way West Chester, PA 19380
STL Burlington 208 South Park Drive, Suite 1 Colchester, VT 05446
Tel: 802 655 1203 Fax: 802 655 1248 www.stl-inc.com
Re: Laboratory Project No. 26000 Case: 26000: SPG: 117591
Dear Mr. Young:
Enclosed are the analytical results for the samples that were received by STL Burlington on October 18th, 2006. Laboratory identification numbers were assigned, and designated as follows:
Lab ID
Client Samle ID
Sample Date
Sample Matrix
Received: 10/18/06 ETR No: 117591
692013 692014 692015 692016 692017 692018 692019 692020 692021 692021 DP 692022 692023 692024 692025 692026 692027 692028 692029 692030 692031 692032
DBCF01MSW0030041104 DBCF01MSW0040041104 DBCF01MSW0050041104 DBCF01MSF0010041104 DBCF01MSF0020041104 DBCF01IPF0040041104 DBCF01IPF0050041104 DBCF01IPW0040041104 DBCF01IPW0050041104 DBCF01IPW0050REP DOUF01IPW0030041104 DOLIF01IPW0040041104 DOUF01IPW0050041104 DL2F01IPW0020041104 DL1F01MSW0010041104 DL1F01MSW0020041104 DL1F01MSW0030041104 DL1F01MSW0040041104 DL1F01MSW0050041104 DL1F01MSF0010041104 DL1F01MSF0020041104
11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04
TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE
Documentation of the condition of the samples at the time of their receipt and any exception to the laboratory's Sample Acceptance Policy is documented in the Sample Handling section of this submittal.
Leaders in Environmental Testing
1.1
Severn Trent Laboratories, Inc.
STL
November 30, 2006 Mr. Charlie Young Page 2 of 2
In order to accommodate field length limitations in processing the data summary forms, the laboratory did, in certain instances, abbreviate the sample identifiers. Dashes have been removed from the client identifiers in this delivery group. The electronically formatted data provides the full sample identifier.
Lipids: There were no exceptions to the method quality control criteria during the analyses of these samples.
The analytical results associated with the samples presented in this test report were generated under a quality system that adheres to requirements specified in the NELAC standard. Release of the data in this test report and any associated electronic deliverables is authorized by the Laboratory Director's designee as verified by the following signature.
If there are any questions regarding this submittal, please contact me at 802 655-1203.
Sincerely,
Ron Pentkowski Project Manager
Enclosure
1. 2
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE _1_ of 6
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari ema il: i.KesarK3lwestonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
Charles Young
P.O. #: Quotation #:
Grab S a m p le
C om posite No. or C ontainers
PFOA Percent Lipids (STL)*
SAMPLE ANALYSIS
ExyLIMS #
Client Samilie Identification |
I C ollection | Date
DBC F01 MSW 001 0 041104 4-Nov-04
DBC F01 MSW002 fo 041104 4-Nov-04
DBC F01 MSW003 0 041104 4-Nov-04
DBC F01 MSW004 0 041104 4-Nov-04
DBC F01 MSW005 0 041104 4-N0V-Q4
DBC F01 MSF001 0 041104 4-Nov-04
DBC F01 MSF002 0 041104 4-Nov-04
DBC F01 IPF004 0 041104 4-Nov-04
DBC F01 IPF005 0 041104 4-Nov-04
DBC F01 IPW004 0 041104 4-NOV-04
C ollectio n
Tim e
19:15 19:20 19:23 19:25 19:27 19:40 19:45 20:00 20:05 20:00
X X X X X X ~Xi X X X
S am p le
M atrix
1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue
CHAIN OF CUSTODY
Cooler ID No.:
^--'RelinquishecpBy:
Date Time
Received By:
f< M o / HOO
Fed Ex
Cooler Temp. (C): Date Time
- f/> l --
r/
-- .-- -
--------- --T
i n/toAy //oo
\ o / , v / 0 __
* Subsample of macerated tissue to be sent to STL for Percent Lipid analyses
Comments
XX XX X ~>Ti X X! XX XX XX XX XX XX PROJECT REQUIREMENTS
*o Results Deadline: Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other:
COPY - ORIGINAL OPi M il SDG'# I \ 1
4 ;''y "ORIGINAL ON FILE ; ; ; # -------- _ _ _ ETR ;
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE 2 of 6
PROJECT INFORMATION
Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari em!3il: i.kesari@westonsolutions.conrI
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
G rab Sam ple C om posite No. of C ontainers
PFOA Percent Lipids. (STL)*
Sampler:
Charles Young
___________
SAMPLE ANALYSIS
P.O. it: Quotation #:
1
C ollection C ollectio n
w
ExyLIMS # [Client Samipie Identification | | D ate
Tim e
S am p le M atrix
Comments
DBC F01 IPW005 0 041104 4-NOV-04 20:05 X
1 Tissue
XX
DOU F01 IPW003 0 041104 4-Nov-04 20:20 X
1 Tissue
XX
DOU F01 IPW004 0 041104 4-NOV-04 20:25 X
1 Tissue
XX
DOU F01 IPW005 0 041104 4-Nov-04 20:28 X
1 Tissue
XX
DL2 F01 IPW002 0 041104 4-Nov-04 20:30 X
1 Tissue
XX
DL1 F01 MSW001 0 041104 4-Nov-04 20:45 X
1 Tissue
XX
DL1 F01 MSW002 0 041104 4-Nov-04 20:47 X
1 Tissue
XX
DL1 F01 MSW003 0 041104 4-Nov-04 20:52 X
1 Tissue I
XX
DL1 F01 MSW004 0 041104 4-NOV-04 20:54 X
1 Tissue
XX
DL1 F01 MSW005 0 041104 4-Nov-04 20:55 X
1 Tissue
XX
CHAIN OF CUS1 ODY
Cooler ID No.: e
Cooler Temp. (C): 0,Q
PROJECT REQUIREMENTS Results Deadline:
]
^-Tftnqulshed By:
Date Time
Received By:
Date Time
-
y P________
Fed Ex
L/
-- -- -- i ___
, -1
L. C tA J5-- \o}\ glob Ol^0
* Subsample of macerated tissue to be sent to STL for Percent Lipid analyses________
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other:
1
'.I
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE 3 Of 6
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jal Kesari em:til: i.kesarkStwestonsolutions.corr1
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
Charles Young
P.O. #: Quotation #:
Q rab Sam ple C om posite No. o f C ontainers
Percent Lipids (STL)*
SAMPLE ANALYSIS
ExyLIMS #
C ollectio n
|Client SamiFile Identification | ] D ate DL1 F01 MSF001 0 041104 4-Nov-04 DL1 F01 MSF002 0 041104 4-Nov-04 DL1 F01 MSF003 0 041104 4-Nov-04 DL1 F01 MSF004 0 041104 4-Nov-04 DL1 F01 MSF005 0 041104 4-Nov-04 DL1 F01 IPW001 0 041104 4-Nov-04 DL1 F01 IPW002 0 041104 4-Nov-04 DL1 F01 IPW003 0 041104 4-NOV-04 DL1 F01 IPW004 0 041104 4-Nov-04 DL1 F01 IPF002 0 041104 4-Nov-04
C ollectio n
Tim e
21:00 21:05 21:10 21:15 21:20 21:25 21:30 21:35 21:40 21:45
X X X X X X X X X X
S am p le
M atrix
1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue
CHAIN OF CUSTODY
^R elinquished By:
Date /i/r/u y
Cooler ID No.:
Time
Received By:
Fed Ex
Cooler Temp. (C): Date Time
_____/ ' / If y
________
~T T / / U / A ------------------- --
///roA/ /k t
* Subsample of macerated tissue to be sent to STL for Percent Lipid analyses
Comments
< Ou .
CL
XX
XX XX
XX XX XX XX XX XX XX
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other:
| 1
Sample Report Summary - Geotechnical
5
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSW0030041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692013 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL
1 0.1
Cone.
1.5
Qual.
Printed on: 11/28/0612:51 PM
6
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSW0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692014 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Liplds Determination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Qual.
1 0.1
1.8
Printed on: 11/28/06 12:51 PM
7
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSW0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692015 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL 1 0.1
Cone. 1.0
Quai.
Printed on: 11/28/0612:51 PM
8
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSF0010041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692016 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Qual.
1 0.1
0.1
u
Printed on: 11/28/0612:51 PM
9
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSF0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692017 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Quai.
1 0.1
0.4
Printed on: 11/28/06 12:51 PM
10
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPF0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692018 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Llplds Determination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL
1 0.1
Cone.
6.5
Qual.
Printed on: 11/28/06 12:51 PM
11
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPF0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692019 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Qual.
1 0.1
2.1
Printed on: 11/28/06 12:51 PM
12
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPW0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692020 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Liplds Determ ination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/26/06
% 1 0.1
0.5
Printed on: 11/28/06 12:51 PM
13
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPW0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692021 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Liplds Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Quai.
1 0.1
4.0
Printed on: 11/28/06 12:51 PM
14
GEOTECHNICAL / GENERAL CHEMISTRY
Duplicate Sample Report Summary
Client Sample No. DBCF01IPW0050REP
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692021 DP Date Received: 10/18/06
Method
L IP ID S
Parameter
% Llpids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
Sample
Duplicate
Result
Sample Result
Cone. Qual. Cone. Qual. RPD*
4.0 3.4 16
* Control Limit for RPD is +/- 20%, unless otherwise specified. Printed on: 11/28/0612:51 PM
15
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPW0030041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692022 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL
1 0.1
Cone.
0.9
Qual.
Printed on: 11/28/06 12:51 PM
16
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPW0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692023 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Liplds Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Qual.
1 0.1
0.2
Printed on: 11/28/06 12:51 PM
17
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPW0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692024 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determination
Analytical Analytical Run Date Batch
11/26/06
Units
%
DF RL
1 0.1
Cone.
0.5
Qual.
Printed on: 11/28/06 12:51 PM
18
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPW0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692025 Date Received: 10/18/06
Method
L IP ID S
Parameter
%Lipids Determ ination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/26/06
% 1 0.1
2.6
Printed on: 11/28/0612:51 PM
19
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSW0010041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692026 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL
1 0.1
Cone.
1.4
Qual.
Printed on: 11/28/0612:51 PM
20
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSW0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692027 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Qual.
1 0.1
2.3
Printed on: 11/28/06 12:51 PM
21
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSW0030041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692028 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical Run Date Batch
Units
DF RL
Cone. Quai.
11/26/06
% 1 0.1
1.4
Printed on: 11/28/06 12:51 PM
22
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSW0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692029 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Liplds Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL
1 0.1
Cone.
1.3
Qual.
Printed on: 11/28/06 12:51 PM
23
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSW0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692030 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Lipids Determ ination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/26/06
% 1 0.1
0.7
Printed on: 11/28/06 12:51 PM
24
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSF0010041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692031 Date Received: 10/18/06
Method
L IP ID S
Parameter
% Liplds Determ ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL Cone. Quai.
1 0.1
1.3
Printed on: 11/28/0612:51 PM
25
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSF0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117591 Lab Sample ID: 692032 Date Received: 10/18/06
Method
L IP ID S
Parameter
VoLipids D eterm ination
Analytical Analytical Run Date Batch
11/26/06
Units %
DF RL
1 0.1
Cone.
0.6
Quai.
Printed on: 11/28/06 12:51 PM
26
Supportive Documentation - Geotechnical
27
STLS E V E R N
TRENT
PERCENT LIPIDS
28
Percent Lipids Calculations
D a te : T im e :
11/26/2006 2245
A n a ly st: E T R (s ):
C lie n t:
JFF 117591 WESTN2
S a m p le ID
MB112606C 692013 692014 692015 692016 692017 692018 692019 692020 692021
692021DP 692022 692023 692024 692025 692026 692027 692028 692029 692030 692031 692032
S a m p le
W e ig h t
(g )
10.00 9.97 10.03 10.00 10.02 10.01 10.01 10.03 10.00 10.04 10.01 10.02 10.04 10.01 10.04 10.04 10.03 10.04 10.02 10.02 10.00 10.00
D ish
(
g)
0.9916 1.0037 1.0210 0.9973 0.9955 0.9955 1.0074 1.0465 0.9987 1.0305 1.0150 0.9955 1.0245 0.9955 1.0037 0.9975 1.0141 0.9965 1.0020 1.0227 1.0015 0.9914
D ish /R e sid u e
(g )
0.9912 1.0189 1.0394 1.0070 0.9965 0.9995 1.0720 1.0680 1.0042 1.0705 1.0491 1.0041 1.0268 1.0002 1.0296 1.0114 1.0372 1.0109 1.0148 1.0298 1.0140 0.9969
E x tra c t F in a l
V o lu m e
(m L s )
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
A liq u o t U s e d in
D e te rm in a tio n
( m Ls )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% L ip id s
<0.1 1.5 1.8 1.0
<0.1 0.4 6.5 2.1 0.5 4.0 3.4 0.9 0.2 0.5 2.6 1.4 2.3 1.4 1.3 0.7 1.3 0.6 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117591MBLK112606C
29
11/28/2006
Percent Lipids Calculations
D a te : T im e :
11/26/06 2245
A n a ly st: E T R (s ):
C lie n t:
JFF 117591 WESTN2
S a m p le ID
MB112606C 692013 692014 692015 692016 692017 692018 692019 692020 692021
692021 DP 692022 692023 692024 692025 692026 692027 692028 692029 692030 692031 692032
S a m p le
W e ig h t
(g )
10.00 9.97 10.03 10.00 10.02 10.01 10.01 10.03 10.00 10.04 10.01 10.02 10.04 10.01 10.04 10.04 10.03 10.04 10.02 10.02 10.00 10.00
D ish
( D ish /R e sid u e
g)
0.9916 1.0037 1.0210 0.9973 0.9955 0.9955 1.0074 1.0465 0.9987 1.0305 1.0150 0.9955 1.0245 0.9955 1.0037 0.9975 1.0141 0.9965 1.0020 1.0227 1.0015 0.9914
(g )
0.9912 1.0189 1.0394 1.0070 0.9965 0.9995 1.0720 1.0680 1.0042 1.0705 1.0491 1.0041 1.0268 1.0002 1.0296 1.0114 1.0372 1.0109 1.0148 1.0298 1.0140 0.9969
E x tra c t F in a l
V o lu m e
(m L s )
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
A liq u o t U s e d in
D e te rm in a tio n
( m Ls )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% L ip id s
<0.1 1.5 1.8 1.0
<0.1 0.4 6.5 2.1 0.5 4.0 3.4 0.9 0.2 0.5 2.6 1.4 2.3 1.4 1.3 0.7 1.3 0.6 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117591MBLK112606C
30
11/26/06
Percent Lipids Calculations
Date: Time:
/
~^
1TM
f
Analyst:
ETR(s):
//7 ^ /
Client: L E ^T b X,
Sample
Weight Dish ( Dish/Residue
Sample ID ( g )
m iiu c c /O.oo
b9 Z Of b 9 - 9 7 69zo/9 6 0 -o? M I G / 5" /O-oo
<6 9 1 0 ( 6 6 9 zon 6 9 1 0 (5'
/tf.o t
/'Of
10*01
g) (g)
/0.99/6 >. <?? /.a,
f . 0 0 % 7 A 0 /5r<9
A Z iO A 0 6?9 9
0.991% / . 0 0 7 0
6 . 99*59 a a 9 9 A 9~
0 . 59 5 s A - 5 9 9 65
/ o o m A 1 Z
6 9 1 0 /9 ,0.06
~f. 0 0* &
0 9 7 'OO t - & O' 5 9 5 1 6 ' 6 ) 0 5 Z
697oi i
e n o 'o o f M ldZ -U
6 9 ioVb &9 i o i 9 6 flo i s'
69101(6
699017
id-09
/. i)i
/O .o t
6 0 -OZ f0 . 0 (
/-7 j-09'
6 0 .0 7,
/ O ld 5 A A 5
/ . 0/62D A <9 4^ 9 / . 955S A 0 0 * 6 / 6* 6)7*/*? A 2,S> 0 >5 5 9 b A A A A 7 . A0 3 ? A )Z 9<b 6 .9 9 7 *? A A n 5
I-O /'/l /. OS-72,
Co9l
60 . 0 9 6 - 5 9 0 5 f- O i ><?
6 9 7 0.79 fO.OZ, Z.OZ 0 A 0 / 5 ir
6 9 l 0 6 6 0,0 z. A d v t 1 / , 0 , 7 <99?
6 9 ti) I 66). 0 # 0 0 6 /9 ' / . o 6 y<)
6*92 0 61- 6 0 , DO 6)'9 9 m 0 - 5 9 0 9
-- ______ .---- -
------ 17 h u M
-^ --------- ---- ----
Extract Final Volume (mLs)
10 10 10 10 10 10 10 10 10 10 10 . 10 10 10 ,10 10 10 10 10 10 10 10 10 10 10 10
Aliquot Used in Determination
( mLs)
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% Lipids
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #Drv/oi #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
OO CD
C^ A
LIPIDCAL UPLOAD 1
31
11/26/06
zz
STL BURLINGTON
% LIPIDS
Sample Handling
33
7208 SOUTH PARK DRIVE SUITE 1
[)> 01 0205446 840 11 7922243774250201 FDE 133455337 290 1/1 31LB N 208 South Park Drive Suite 1 Colchester VT Kirk Young 30544693110003217922243774252015
Client: T R: SDG:
W rS ? T /-'' 3 . TttW I n -H T ^ V
STL BURLINGTON SAMPLE RECEIPT & LOG IN CHECKLIST
(D ate R eceived: / Q - / v? - C X
` Tim e Received: O Q rn C T '
Received By: \
'S -
Log In Date: \ \ / ^ 3 / b
By:
S ig n a tu re :
(J
s?
.
Sam ples D elivered By: ^ S h ip p in g S ervice C o u rie r H and O th er (specify) List Air bill N um ber(s) o f Attach a photocoDy o f the A ir Bill:
Date:
/ X ~ / / & * * -* * ' '*
// / tr
COOLERSCREEN
`V "
T h ere is n o evidence to indicate tam pering
Custody seals are present and intact
Custody seal numbers are present
If yes, list custody seal num bers:
-
YES : X
NO X
NA ......
c o m m e n t s --'. '
y:
Therm al Preservation Type: W e t Ice o Blue Ice None p o t h e r (specify) r i f ' v i i C.fcL
-
IR Gun ID: ( ,, 2 -
C orrection F actor (C F ) = >
C
^
' >
C ooler 1:
~ IS .5
C Cooler 6
.
"C C ooler 11
"C C o o ler 16
C
Cooler 2:
~ 2 U . L > C Cooler 7
"C C o d e r 12
"C C o o ler 17
"C
C ooler 3:
'C Coder 8
"C C ooler 13
"C C o o le r 18
.
: "C
Cooler 4:
"C C o d e r 9
"C Cooler 14
"C C o o le r 19 '
"C
Cooler 5
"C C ooler 10
C Cooler 15
C Cooler 20
.
"C
Unless otherwise documented, the recorded temperature readings are adjusted readings to account for the CF of the IR Gun
EPA Criteria: 0-6C, except for air and geo samples which shouldbe at ambient temperature and tissue samples, which maybe frozen.
Some clients require thermal preservation catena of 2-4C or other such criteria. The PM must notify SM when alternate criteria is specified.
Sam ple containers were received intact Legible sam ple labels are affixed to each container
Y e s L` Nor- - N A .' i ^ ^ i i C O l V l j V f T S
X-
.X Tys-k ,-',NO N-'
C O C is present and Includes the following inform ation for each container: Sam ple ID / Sam ple Description
X
1*
D ate of Sam ple Collection Tim e of Sam ple Collection
X X1
Identification of the Sam pler ,,
Xf
Preservation Type
X
Requested Tests Method(s) Necessary Signatures Internal Chain of Custody (IC O C ) Required If yes to above, IC O C Record initiated for every W orksheet
X X
X
YES : I M
-N A
Th e sample container matches the C O C Appropriate sam ple containers were received for the tests requested S am ples were received within holding time Sufficient am o unt of sam ple Is provided for req uested analyses V O A vials do not have head s p a c e or a bubble > 6 m m (1/4" diam eter) Appropriate preservatives were used for the tests requested pH o f Inorganic sam ples checked and Is within m eth od specification If no, attach Inorganic Sam ple pH Adjustm ent Form
X X X
X
X
X
X y
T%
te ? 4 & C 1 -V O r
i]
-W #v4 i v " t
a r\
S c x /v v o V i? c c v -v -te X rf? T
/v v ?
'x y ti
^ C ,c tC . ` s
-fe r
V-Vv ' j V -kT / '* ST - 'C / 'v 'v
*
\ f x V h f \ <5 4 b c ~ c x \ \
to iv .A
c ? -4 rrx I V
T T 'A i 4 .S f S 4 ( X \ \
1
FSM002:10.26.05:2 3TL Burlington
35
Last Page of this Document
36
