Document rpQRMZL5X0M4QNe8ZmgBk5g1J
CG 3 2 ('DATE >
0DE>.RT-6i8-D. PKG_____
F2H21
lLOT"NUMiii)~
EST, WT. 2567* LBS* STD/ HRS*
PREPARATION NOTES:.
PROCESSES ( 1RT-618-D (U)
APPRO* EWK 12-8-81
TIME
TYPED BY: KLW ___ M
COMTYP JOB NAME : .J32RT618DMU
NON-BLEEDING
EQUIP MENT
PREP 1
NAME: WATCHUNG RED Y I ^^i^RECORD '__BATCHES SINCE SPARKLER LAST
.USE I N-CODE | ACCT
LBS i i
l LBS*
-----------|---------- ----- |--------
i 1 CLEANED. AFTER 4 BATCHES, CLEAN, DRESS 1 J SPARKLER 2, PRE-COAT WITH 15* DICALITE
-JsSl
1 J^FILTER AID | OBTAIN FOR S11 2-CHL0R0-4-AMIN0T0LUENE-5-
I yC SULFONIC ACID I OBTAIN FOR S24 3-HYDR0XY-2-NAPHTH0IC ACID j>*r j INSTALL DV 6 CV RECORDER 2, CONTROLLER CHART
{ NOTE: NOTIFY PRESS ROOM AND ROPE OFF AREA
I UNDER V-922
l
! I
1 j
777-A i l*_
1 740-C j-
I 253-C I
RUN ID* (iDOG) WATER INTO
2. ADJ T-0
931 -f0 DEG F
'
iDD IN 1-2 MIN. DRESINATEX
. ^ . 'STIR 2 MIN *, RECORD: PH JcLlQ?* 5-1 * 5)
l^rtTIR 20 MIN OR LONGER FOR S27
58 I 530-A I 58
II jI
922 ` <65?G) WATER INTO V-922
3*~
IN V-926 SODIUM HYDROXIDE 2, RUN IN m--_5_____
I 7-D ! 188
TURN ON AGITATOR 2. STEAM 2, DUMP IN FROM S2
J 740-C i 963
J&L JMk. j&y2-CHLORO-
4-AMIN0T0LUENE-
.224.1
^SULFONIC
i IJ5-
,----,--,----
-- _____ i
i
P IN ACTIVATED CARBON
45 1 113-B | 45
IN DICALITE FILTER AID
.w
10 I 777-A | 10
HEAI TJ3.212-214 DEG F, RECORD HT,,MZL_* F,
I
I
_ _DEG F__ -WATCH FOAM
RECORD BY _-fcT< + >, IF NECESSARY ADJ TO +BY
SODIUM HYDROXIDE
ASSUME 50%
STIR 30 MIN AT 212-214 DEG F, THEN SHUT ' .
___: i
7-d
| OFF STEAM
WATCH FOAM
l NOTE: RECORD: SPARKLER PRESSURE
IF NOT ZERO, NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER ] UNTIL SOL1N*IS CLEAR. MAINTAIN AT 190-195 F
`WAY 28ip82
1 FOR SI 9 & RECORD^' HT__/^_$_,,DEG F AND
| 'RECORDER
DEG F
*a
| RECORD: START
TOTAL MIN_jSfcSL,------,
| CLARITY ______. NOTE: SAMPLE FROM HOSE -
| SHOW TO SUPERVISOR FOR O.K.
N38173
EQUIP KENT
L
904 10
E 2 OF 3 CG 32 CORE RT-618-D <U>
1* <500 WATER INTO V-904
WHEN 517 COMPLETE, PUMP IN V-922 THRU
SPARKLER, MAINTAIN V-922 AT 190-195 REG F,
RECORD: START
TOTAL MIN.
|
WEIGH IN PT FOR S35 SSQODDI l^i NITRIJjjl
__
MEASURE ^lJil*ONITS INN V-928 FOR SS 33
HYDROCHLORIC ACID
M,,___L____ , __SZZi
16" <15300 WATER INTO V-__J
W 'IN V-926 SODIUM HYDROOXXIDE 6 RU m__$:_____,
DUMP IN FROM S3 3-HYDR0XY-2-
NAPHTHOIC ACID'
rb'ir
BALE I Il'FBHMW
feWL___ _____ 70-90 DEG F & STIR TO DISSOLVE STEAM EJECT V-921/931 INTO CV
WHEN Si 9 COMPLETE;--SHUT OFF PUMP & INSERT- l
>22 FOOT PLUG
RUN IN 10* <2070 WATER it HEAT TO 190-195 FT
CIRCULATE 15 MIN THRU SPARKLER. .
I
PUMP V-922 THRU SPARKLER INTO V-904
RUN IN 5* Cf03G>' WATER INTO V-922 t, HEAT TOT 190-195 F, CIRCULATE 15 MIN THRU SPARKLER |
P V-922 THRU SPARKLER INTO V-904
I
Y BLOW OUT SPARKLER INTO V-904
I
TO 165-170 F (SMPLTO SUPVR FOR G.K.) |
RUN-IN N-28-D FROM S21 IH 12-15 MIN & STIR !
MIN AT 165-170 DEG F
..........
I
ADJ-TO 129*C3409G>AT 28-30 DEG F AND .
fECORD: TEMP
____ j .-* ICE -140X330!
RliW-Ilf N-725-A FROM S20 AFAP <5-10 MIN)
\
& RINSE IN PT
i
STIR 30 MIN AT 28-35 DEG F MAINTAINING
}
+CR, +KI F0R.S41 jtAWD RECORD:
!
TIME START_J^j l MW7 CR_!fl__< + )
+> J
NOTE (1) IF CRr, KI-, ADD 20$ AS IS IN-
i
CREMENTS
HYDROCHLORIC ACID ASSUME 322 !__
i
RECORD: CR_i_._< + > , KI< + >
I
<2) IF CR+, KI-, ADD 20$ AS IS INCREMENTS I
SODIUM NITRITE.
ASSUME 332 I__
i
RECORD: CR______< + >, KI__ ______ < + >
i1
5 7-A
28-A 725-A
DUP050047892
EQUIP MENT
CV 11
CV
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| PAGE J3 OF 3 CG 32 CODE RT-618-D <U>
1 USE i N-CODE 1 LBS 1
ACCT LBS
\ j&GHP INTO CV BARIUM SULFATE
i 167 I
UA&TTq 37* (3496G) AT 28-32*F
If
132X3301
' ----------- TEMP_J^z_X^DEG F & VOLUME _______* \
\
IH FROM DRUM AMMONIUM CHLORIDE
1 222 ij
-3 MIN
'I
^MEDIATELY COUPLE DV THRU UNDERSURFACE
l
1 DISTRIBUTOR INTO CV IN 45-60 MIN. MAINTAIN} ____
1 CV AT 28-32 DEG
"RECORD: START..
MIN .
STIR 30 MIN & RECORD:-BASE
<+> ,
!
1
I DIAZQ ,,
< "), _C 9 *0-9.8 )
. I.
i
} ^NAL TEMP __3L&__DEG F
}I
IF NECESSARY, ADJ TO PH 9.0-9.8 AND RECORD I
'}
!
JSODIUM HYDROXIDE
ASSUME50% }
i
MfayDBPCHLORIC ACID .
ASSUME32% }________ ii
HEAT T0jffiHHKE& F IN 65-70 MIN AND
}
1
i. RECORD
& REC0RDER//_V__DEG F }
|
I'.NOTE: *ATFW4^W6 F, OPEN WATER
SPRAY
}
f
1 1/4. TURNS
I
6 5-A
167
:s?-A IfJ&P
165-A I 222
57-A I ____
7-D 28-D
24 * (61SG)WATER INTO V902
TURN ON AGITATOR t, STEAM 6 DUMP IN BARIUM
i^eHLORIDE .
T HEAT TP
.. ** STIR TO DISSOLVE
|
| 1506 I f
|Se N S44 COMPLETE, IMMEDIATELY"STRIKE ~V902 1
} THRU UNDERSURFACE DISTRIBUTOR INTO CV IN
MIN. MAINTAIN CV AT /#*H&6DEG F.
:ORD; START^td3?^fT0TAL MIN,,_/<2.-- CAT CV TO 198-202 DEG F IN 10-12 MIN
5 MIN AT 198-202 DEG F
fTCOD TO 18<+/-1 8,000GX,
RECORD: PHSS-<9v 0-9.4) t* STO> AGITATOR
I SHUT OFF WATER"SPRAYSy
V
!
}
START ^
Fi- Ij.Nn * OF'TR
I
.I j
1 [
| 1 }
1 1
16-B I 1506
I
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY} THRU PRESSING, DUMP IN, STIR 5 MIN & STOP } AGITATOR. RESUME PRESSING. I-GCTANOL ~ I
10
588-A
10
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