Document rpEO1xJNQVd7eqkL3EmBDeD2G

AR226-2496 .Analysis Report LancasterLaboratories f Wh&Gquaiitykasckrm a n a ly tic a l r e su l t s Prqrwed foP CRO-RLDuPomde Nemours & Co Barley Mill Plaza, Bldg. 27 Lancaster race & Route 141 WUrmogtoilLB 19805 302-992^76? Prepared by: Lancaste Laboratories 2425 New Holland Pike Lancaster, PA 17605-2425 SAMPt-E G R Q U P . , The m yi group for this submittal is 771719. Sandies arrived at the laboratory on Friday, July27,2001. The PO# for this group is LBIO-64237 and foe release number LE767. gieot Description. ----- .WWK-CHRBSMANJAP Water Sample limp-aster Inhs Number 3655318 ffliM a M The specific methodologies used m obtaming the enclosed `analytical result? are indicated on the laboratory chronicles. 1 COPY TO U RS-Diam onds Attn: ADQM AP Services Questions? Contact your Client Services Representative Nancy Bornholm at (717) 656-2300. Respectfully Submitted, ( _ . Christine M. Dulaney . Sr, Chemist ASH 0I 1728 \C \l tontaste,LaboratoriesIne. 2425 N ew Holland POte POBoxt242S lancartee PA 1760S-2423 TTTJrtS-rtOO fcn ?M* 1, 9/11/00 E ID L 43231 "i&lsls Rporf; * I ancasterLaboratories Where quaiityisasdenoe. lumenster fcaboratorios Sample Uo . SW 3655318 Collected!07/26/2001 09-15 by SO Submitted: 07/27/2001 09:55 Reported: 08/22/2001 at 13:27 Discard: 09/22/2001 MHK-CBR1SSMWJTAP Water Sample CHRISSMftN WSLIi 7/01 Page l o f i Account Kumber: 07032 CRG-B.I.DuPont de Nemours & Co Barley Hill Plaza, Bldg. 27 Lancaster Pike S Route 141 . Wilmington DB 19805 ,WKCHR OB 03334 AS Ssceivsd A S R e c e iv e d Itotud A nalysis C A S M um bsr X e a u lt D e te c tio n n ij.lt PC-143 3835-25-1 0.296 0-039 recovery of the mxregates P K * X and llH-PPm are outside the . QC limito - -* 00495 rcconresy is o u t s i t il 00 limit th^ H$/MSD. ife* RD between the HS/MSD is outside the QC criteria. The recovery was uithia the QC criteria for the associated iS- < */ H S Confirm of FC-143 3835-26-1 0.36 O.Xp the recovery of PC-143 was outside of QC limits in the MS associated with -a sample. The relative percent differ&ace .for PC-143 between the tts/HSD was also outside of QC limit. The recovery was within QC Units in the MSS. ' unite 9 /1 9/1 Dilution Factor 1 as a. 02324 A n a l y s is Marne PC-143 . 00495 02325 CC/HS confirm Of PC-143. pesticide Alternate Water Rxtr Laboratory C hronicle - Analysis Method PC-143 by GC/8CP Trial# Date and tine 1 09/66/3001 11:38 10/91PC-143 by CC/HS PC-143 10/91 08/15/3001 10:36 00/01/3001 08:00 Dilution Analyst . Factor Michelle <J. Kolodriejsfci timothy Trees D e h o r a h tt. Zim m erm an 1` l 1 ( . ASH 011729 UncSttrlaberatortes.8*. m e m b e r 33SHew HottomlMke PG Box 12425 UWMtet PA 17605-2425 B D 143232 Analysis Rporf LancasterLaboratories w , S ! & a S 6S & o i Stim m ary i Pagel of2 C lient Hanes CRG-B.I.Dupont de Honours &Co Group Humber 771719 Reported: 09/22/01 at 01:27 PM . Laboratory Compliance Q u a lity C ontrol 5 B32X5tLH25 2 Batch umber ; O12120003A PC-1 Blank KSttlt Blank MDI import Waits Salale number(a) : 3455318 0 -07S J -03 u g/l LC8 MSS 16 LC3 D ss JJCg/ueSD liiaitf ^ 3-55 m mm* Batch number: 01213HAX026 GC/MS C on fin i Of, PC-143 Staple number(a ): 3555318 M.P, .1 03/1 45 3-55 Batch number: 1220000A PC-143 Batch number: 01212BW026 GC/HS Confirm of PC-143 S a m p le M a tr ix Q u a lit y C o n tr o l ms Men r n f m a SP oca DOT a m . m s w a is m Swple number(n) : 3555319 15* ~ 21* ,50*100 32* m 30 Cone cone Sample number (>) 3555310 37* 57 50*100 4 5* 30 DOT MB Dtip ft* ta x Surrogate Q u ality Control A n a ly s ts Sawi; PC-1 4 3 l a H ater B atch number; 012120009A trm . . xin-KruA 3655310 Blank PCS MS HSD is 12 16 14 21 ..... , 3* 2* 3* 2* 0* idadta: 1-50 13-00 Analysis Kara: GOSS Confirm of PC-143 / Hater Batch number: 02 1 2 HMC02# pna 3655310 Blank PCS MS MSP 23 14 19 17 27 Iiisitg; l-SO ' ` pfdda 8* 11* 14* . 14* . . 20*. SO-150 \* ... Gi I 0H SV *- Outside o f specification (1) The result for one or both determinations was less than five times the LOQ. The background result was more than four times the spike added. ^QLm e m p e n U ntarti# taberatoriej, In c 2425 Ite w H lb n d Pika POBo* W*25 . tm ie u ta c M C S053425 I 1 I il E ID 1 4 3 2 3 3 i LancasterLaboratories W * 8 S S ^ a f S S Sr o l Smnaaxy ! C l i e n t Nam e; CRG-B, I .D u P o n t d e N em odre & CO R e p o r te d ; 0 8 /2 2 /0 1 a t 0 1 :2 7 PM - ngj^ Repor,t Page 2 o f2 G roup N um ber; 27171,9 '" A SH O im i *- Outside o fspecification . (1) The result for one Or both determinations was less than five times the LOQ. ' The background result was more than four times the spite added UnCffitirUtitom&feK Inc m m m u******^ \ ! E X D 143234