Document rpEO1xJNQVd7eqkL3EmBDeD2G
AR226-2496
.Analysis Report
LancasterLaboratories
f Wh&Gquaiitykasckrm
a n a ly tic a l r e su l t s
Prqrwed foP
CRO-RLDuPomde Nemours & Co Barley Mill Plaza, Bldg. 27 Lancaster race & Route 141 WUrmogtoilLB 19805 302-992^76?
Prepared by:
Lancaste Laboratories 2425 New Holland Pike Lancaster, PA 17605-2425
SAMPt-E G R Q U P
.
,
The m yi group for this submittal is 771719. Sandies arrived at the laboratory on Friday, July27,2001. The PO# for this group is LBIO-64237 and foe release number LE767.
gieot Description. -----
.WWK-CHRBSMANJAP Water Sample
limp-aster Inhs Number 3655318
ffliM a M
The specific methodologies used m obtaming the enclosed `analytical result? are indicated on the laboratory chronicles.
1 COPY TO
U RS-Diam onds
Attn: ADQM AP Services
Questions? Contact your Client Services Representative Nancy Bornholm at (717) 656-2300.
Respectfully Submitted, ( _ .
Christine M. Dulaney . Sr, Chemist
ASH 0I 1728
\C \l
tontaste,LaboratoriesIne. 2425 N ew Holland POte POBoxt242S lancartee PA 1760S-2423 TTTJrtS-rtOO fcn
?M* 1, 9/11/00
E ID L 43231
"i&lsls Rporf;
* I ancasterLaboratories Where quaiityisasdenoe.
lumenster fcaboratorios Sample Uo . SW 3655318
Collected!07/26/2001 09-15 by SO
Submitted: 07/27/2001 09:55 Reported: 08/22/2001 at 13:27 Discard: 09/22/2001 MHK-CBR1SSMWJTAP Water Sample CHRISSMftN WSLIi 7/01
Page l o f i
Account Kumber: 07032 CRG-B.I.DuPont de Nemours & Co Barley Hill Plaza, Bldg. 27 Lancaster Pike S Route 141 . Wilmington DB 19805
,WKCHR OB
03334
AS Ssceivsd
A S R e c e iv e d
Itotud
A nalysis
C A S M um bsr
X e a u lt
D e te c tio n
n ij.lt
PC-143
3835-25-1
0.296
0-039
recovery of the mxregates P K * X and llH-PPm are outside the
.
QC limito -
-*
00495
rcconresy is o u t s i t il 00 limit
th^ H$/MSD. ife* RD
between the HS/MSD is outside the QC criteria. The recovery was uithia
the QC criteria for the associated iS-
< */ H S Confirm of FC-143
3835-26-1
0.36
O.Xp
the recovery of PC-143 was outside of QC limits in the MS associated
with -a sample. The relative percent differ&ace .for PC-143 between the
tts/HSD was also outside of QC limit. The recovery was within QC Units
in the MSS.
'
unite
9 /1
9/1
Dilution Factor
1
as
a.
02324
A n a l y s is Marne
PC-143
.
00495 02325
CC/HS confirm Of PC-143. pesticide Alternate Water Rxtr
Laboratory C hronicle
- Analysis
Method PC-143 by GC/8CP
Trial# Date and tine 1 09/66/3001 11:38
10/91PC-143 by CC/HS PC-143 10/91
08/15/3001 10:36 00/01/3001 08:00
Dilution
Analyst
. Factor
Michelle <J. Kolodriejsfci
timothy Trees
D e h o r a h tt. Zim m erm an
1`
l
1
(
. ASH 011729
UncSttrlaberatortes.8*.
m e m b e r 33SHew HottomlMke PG Box 12425 UWMtet PA 17605-2425
B D 143232
Analysis Rporf
LancasterLaboratories w , S ! & a S 6S & o i Stim m ary
i
Pagel of2
C lient Hanes CRG-B.I.Dupont de Honours &Co
Group Humber 771719
Reported: 09/22/01 at 01:27 PM
.
Laboratory Compliance Q u a lity C ontrol
5 B32X5tLH25 2
Batch umber ; O12120003A PC-1
Blank KSttlt
Blank MDI
import Waits
Salale number(a) : 3455318
0 -07S J
-03
u g/l
LC8 MSS
16
LC3 D ss
JJCg/ueSD liiaitf ^
3-55
m mm*
Batch number: 01213HAX026 GC/MS C on fin i Of, PC-143
Staple number(a ): 3555318
M.P,
.1 03/1
45
3-55
Batch number: 1220000A PC-143
Batch number: 01212BW026 GC/HS Confirm of PC-143
S a m p le M a tr ix Q u a lit y C o n tr o l
ms Men r n f m a
SP oca
DOT
a m . m s w a is
m
Swple number(n) : 3555319
15* ~ 21* ,50*100
32*
m 30
Cone
cone
Sample number (>) 3555310
37* 57
50*100
4 5* 30
DOT MB
Dtip ft* ta x
Surrogate Q u ality Control
A n a ly s ts Sawi; PC-1 4 3 l a H ater
B atch number; 012120009A
trm .
.
xin-KruA
3655310 Blank PCS MS HSD
is 12
16 14 21
..... ,
3* 2* 3*
2* 0*
idadta:
1-50
13-00
Analysis Kara: GOSS Confirm of PC-143 / Hater Batch number: 02 1 2 HMC02#
pna
3655310 Blank PCS MS MSP
23 14 19 17 27
Iiisitg;
l-SO
' `
pfdda
8* 11* 14* . 14* . . 20*.
SO-150
\*
...
Gi I 0H SV
*- Outside o f specification (1) The result for one or both determinations was less than five times the LOQ.
The background result was more than four times the spike added.
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U ntarti# taberatoriej, In c
2425 Ite w H lb n d Pika
POBo* W*25
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tm ie u ta c M C S053425
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I il
E ID 1 4 3 2 3 3
i
LancasterLaboratories
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C l i e n t Nam e; CRG-B, I .D u P o n t d e N em odre & CO R e p o r te d ; 0 8 /2 2 /0 1 a t 0 1 :2 7 PM
-
ngj^ Repor,t
Page 2 o f2
G roup N um ber; 27171,9 '"
A SH O im i
*- Outside o fspecification
.
(1) The result for one Or both determinations was less than five times the LOQ.
' The background result was more than four times the spite added
UnCffitirUtitom&feK Inc m m m u******^
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E X D 143234