Document roZj4JdOOeEwrwRXyGbYN1yV
FORM N0.45A 201-10
--' TRICHLOR SHIPMENTS
TYPE 107 **
Color Specific Gravity 20/60 C Distillation Range
Low
apha
C
Water Content
High Cloud Point
C
NONVOLATILE Acid Acceptance
%
% as NaOH
pH Acidity/Alkalinity
1966
Avg .
(5 1.460
36.0 87.7 (-10 .0013 0.14
--
JAN
9 1-660
86.2 87.7 (-10 .0014 0.15 7.2 .0002
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION LAKE CHARLES, LOUISIANA
LABORATORY PRODUCT REPORT
FEB MAE APR MAY JUNE JULY
AUG
SEP
OCT
NOV
OEC
1967 Avg.
76
7 (5
(5 6
a (5 7 7
8
6
1.460 1-660 1 .A61 1.424 1.460 1.660 i ,/,An 1.46C 1.660 1.460 1.460 1.457
86.2 86.1 86.3 86.0 86.1 86.4 86.0
87.9 87.8 87.5 88.0 87.9 68.0 87.8
(-10 (-10 (-10 (-10 (-10
(-10
.0007 .0016 .0012 .0020 .0014 .0017 .0010
-W2-
0*20-
0.15 0.14 0.16
7.2 7.2 7.4 7.4 7.3 7.2 7.8
.0002 .0002 .0003 .0003 .0002 .0001 .0003
86.2 86.2 87.9 88.0 (-10 (-10 .0018 .0015 0.11 0.16 7.6 7.4
.0003 .0002
86.2 86.2 86.2
87.8 87.9 . 87.9 (-10 (-10 T-10 .0013 .0011 .0014 0.14 0.15 0.15 8.0 7.5 7.4 .0002 .0001 .0002
TYPE Ei110
Color
Specific Gravity 20/20 C
-apha (5*
11
1.460*
Distillation Range Low
C
High
Water Content Cloud Point
C
Non*Volatile Acio Acceptance
% %. as NaOH
86.3* 87.7*
-- --
T^IO* (-10
.0012* -
0.23* 0.41"
-- --
7 55
_ --
(-10 0.40
(---10
(-10
-
---
_ * -- -- --
7 -
(-10 -
-
(5 (-10
5
6
-
-
(-10 -
-
(-10._
--
-
-
--
--
86
--
-
-
(-10 --
0.18
(-10 --
0.33
TYPE 1 1 3
Color
apha
Specific Gravity 20/20 C Distillation Range
Low High Water Content Cloud Point Non-iVolati le
C
C %
15*
3
1.466* 1.466
o
86.7* 87.2*
(rlO*
86.6 87.2 (-10 '.0002
6
_
(-10
.0001
(5 (5
---- __
(-10 (-10 .0002 .0001
(5
(5
1.467
--5
5
(5 6 1.466
7--
--8
_15___
1.466
86.7
87.3 -16 -14
(.0001 .0002
87.0
87.4 -16 (.ooco
(-10 .0002
86a8
87.8 (-10 .0001
--
(-10 .0002
---- ----
-15 ^0001 (.0001
86.8
87.4
.(-IQ--
.0001
SL 013038
Months Avg. Effective May, Type
COMF1 5EHTT7 L: !ub jec r to P rotecl i ve 0 der of 14 th Judici 3l Dl: trict Court
No. 91-11*
122
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION
LAKE CHARLES, LOUISIANA
LABORATORY PRODUCT REPORT
TRICOLOR SHIPMENTS
Type Color
115
apha
Specific Gravity 20/0 C Distillation Range
C
Low
High
Water Content Cloud Point C
Non.-Volatile Acid Acceptance
* % as NaOH
196^ .Avg
JAN
FEB
MAR
(5 3
7
1.462 1.460
5
86.6
87.7 (-10 .0001 O.IO
86.7
87.5 (-10
.0003 0.13
_
(-10 (-10 .0002 .0003
APR
5
-- (-10 .0001
MAY
(5
(-10 .0002
JUNE JULY
AUG SEP
6 5 (5 5
(-10 .0001
-
(-10 (.ooca *
(-10 .0002
(-10 .0001
OCT
NOV
DEC
77 6
--
(-10 (-10 .0002 .0006 .0002
p-- e01
1967
Avg.
6 1.460
86.7 87.5 (-10 .0002 0.13
- cSmL 001,03039
* 4 Months Avg.
r f lif
rnu ?rnt*AiP rmr?---
ri-PtG jfc 1V Order
wXtll--fcl LSferic L Q1 1 \
Uv/iu
w
1
FORM N0.45A 201-12
PERCHLOR SHIPMENTS
1966 Avg..
TYPE 207
Color
APHA
Specific Gravity
20/20 C
Distillation Range
C
Low
Hi gh
Water Content Cloud Point
C
6* t -6?8*
120.5* 121.5* (0*
Non-Volatile PH Acid Acceptance
gm-100 ml .000/a* % as NaOH
Copper Corrosion Acidity Ml of 0.01 N NaOH Flask MG/30 CM
1.4* 7i*
SOXHLET MG/30 cm2 Condenser MG/30 CM2 Chlorides
ppm
2* 4* TE06*'
JAN
** __
-- -- -- -
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION
LAKE CHARLES, LOUISIANA laboratory product report
FEB
MAR
APR
MAY
JUNE JULY
ADO
10 10*
12 9
M
(0
8.2 --
(0
8.2
-- -- -- -
_r
(0 8./i
--
(0 8-2
mm
_
--
_ -- '--
8
_
-4 -- 8.5 -
_
--- --- --
SEP
9
(0 --
8.5
-- -- -
OCT
NOV
DEC
1967 Avg .
8
9 10
9
-6?L
--
1.624
-4 -- 8.5
120.8 --
120.8
121.7 -
121.7
-8 Jo______ ~To
(.0010 8.6
(.0010 8,4 :
- --
--
--
--
--
--
--
---
--
-
0.12"
-- 0.12
TYPE 208
Color Specific gravity
APHA 20/20 C
Distillation Range
C
Low
HI GH Water Content Cloud Point
C
Non-Volatile PH
Gm/100 ML
Copper Corrosion
Acidity ML of 0.01 N NaOH Flask MG/30 Cm2
Soxhlet MG/30 CM2 Condenser MG/30 CM2
CHLOR1DES
ppm
7 1.624
120.6 121.6 (0 .0003 6.8
3
1
7 7
0.06
10
1.626
9 10 1.624 1.624
10 8 1.624 1.624
120.5 121.5 (0 (.001
6.5
120.6 121.6
(0
6.5
120.4 121.6
(0
6.5
120.4 120.8 121.7 121.7
(0 (0 (.001 .001
6.6
2
1
7 7
(0.06
3
1 7
8
0.12
2
2
8
9
*
2 (1
6
6 0.06
2 17 5
8 1.624
85
9
1.624 1.624 1.624
9 1.624
88 1.624 1.624
9 1.624
120.8 121.4 (0
.002
6.8
121.1 121.0
121.8 121.7
(0 (
(.001 (.001
6.9
7.1
120.8 121.7
(0
.001 6.9
120.9 121.6 (-10 (.001 6.8
120.5 120.9
121.5 121.7
(-10
(-10
(.001 (.001
6.9
7.0
120.7 121.6"
(0 (.001
2 1
8 (0.06
2 1
6
0.06
1
TI
5 4 0.06
2
1
6
4
0.06
1 (1
6
7 0.06
2
1
_2______
8
0.18
2
(1
6 6 6.03"
2 1
6
7
0.07
SL 013040
* 3 Months Avg
CON 'IDENT AT.: Sub"i< ct to Prote :t i ve Order c F 141! Jud i rial EJ .stric t Cou
No. 91-1145
t
FORM N0.45A 201 -13
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION
LAKE CHARLES, LOUISIANA
LABORATORY PRODUCT REPORT
PERCHLOR SHIPMENTS
1966 Avg.
JAN
TYPE 203 Color
apha
Specific Gravity
20/20 C
Distillation Range
Low
C
Water Content Non-Volatile
Hi gh
Cloud Point
C
GM-100 ML
PH Acid Acceptance
% as NaOH
8* 1-625*
120.6* 121.3* (0* (.0010 i 8.5*
Copper Corrosion
Acidity ML of 0.01 N NaOH Flask MG/30 CM2
SoxhleT MG/30 CM2
Condenser MG/30 CM*1
Chlorides
PPM
2* 2* 8* 5*-----------0.18*
--
-- _ -- -
-
FEB 10
MAR
* 8 ,
-- ~To"
-
-
(0 8.5
--- -_ --- ----
APR
MAY
10
7
_
(0
8.6 --
-- --
--
(0
8.6
--
-- --
JUNE
JULY
11
9
(0 8.7
(0 8.6
---- --
-----
` CONFIDENTIAL: Subject to Protective Order of 14th Judicial District Court
AUG
SEP
OCT
NOV
OEC
1967 Avg .
7
(0 8.6
--
8 --'
7 _
(0 (0
8.7
8.4
--_ -- ---- ---
87 __
8
(0 _ 8.6
_ (0
AQ_______
8.6 -
8.6 -
-- --- -- -- -- --
TYPE 209 Color Specific Gravity
APHA 20/20 C
Distillation Range Low
C
Water Content
High Clouo Point
C
Non-volatile PH Acio Acceptancr
Gm-IOO ML % as NaOH
Copper Corrosion .Acidity ML of 0..01 N NaOH Flask MG/30 CM2 Soxhlet MG/30 CM2 Condenser MG/30 CM2
Chlorides
ppm
8** 1.62
10 _
120**
122** (o**
-- (0
.004** 6.8** 6.4
---
--- -_ ---- -----
SL 013041
n mm
mm -- (0
7.0 -
-- -- -- -
8 10 -
-- -- (0
6.9
mm
(0
7.1 -
_
V -- --_ ---- -- ---- ---
-- - - 9 --
-- - -
-
- 10 --
--
-
- ---
--
-- - -
- --
--
-
- (0 --
- (0
-- - -
- --
--
-
--
6.9
-
- 6.9
-- - - -- - - -
- - - -- - ---
-_ - -- -- - - -
--- - - -- - - -
--
-
- --
---
---
- - --
---
for^F,X 45A202.13
HEAVIES STILL BOTTOMS
Trichloroethylfne 1, 1,2Trichloroetkane Pfrchloroethylene u.Tethachloroethane S-TETRACHLOROETHANE
Pentachloroethane
Hexachloroethane
ft ft ft ft *
ft
ft
1966
Avg.
fo.oi (0.01 Ik. 6k 3.45 30.59 34.94 3.81
JAN
(0.01 0 17.89 3.35 29.19 29.86 4.33
V"""
PITTSBURGH PL^.c GLASS COMPANY
CHEMICAL DIVISION LAKE CHARLES, LOUISIANA
laboratory operations report
FEB MAR APR MAY JUNE JULY AUG
0 .0.01 0 (0.01 15.89 19.54 3.95 3.33
31.18 36.93 30.61 29.93
4.34 3.30
0.04
0.08 35.07 2.88
27.69
22.39 2.21
0 (0.01 0.04 0.01 0 (0.01 (0.01 (0.01 18.10 18.75' 25.02 19.95
3.38 3.17 2.75 3.40 39.49 36.14 35.62 36.49 27.42 30.00 26.02 29.93
1.73 178(7 1.63 1.62
SEP OCT NOV DEC 1967
Avg.
0 (0.01 (0.01 (0.01 (0.01
(0.01 (0.01 (0.01 (0.01 (0.01
23.39 21.00 Lb.bV 32.91 22.02
3.11 3.04 2.86 2.5Z- _2*iL 36.36 36.80 40.76 36.82 35.29
29.41 30.70 33.
21.76 28.43
T^r~ l.6o 1.52 | 1.72 2.21
Heavy Unknowns
* 2.48 3.32
0 1.93 2.00 1.38 1.80 1.47 1.40 1.24 1.13 0.97 1.2$ 1.49
FeCl? Non-Volatile
ppm 68
130 6L 127----- 679
--
- 72 -
126 -
222
ft 0.72 1.43 T.Sii 2.53 1.30 - -
-
U.41 -
0.52 -
0.56 1.18
HEAVIES STILL REFLUX
(PER STILL FEED)
Trichloroethylene
ft
1,1.2 Trichloroethane
ft
Perchloroethylene
ft
U.Tetrackloroethane
*
S.Tetrackloroethane
ft
3.04 i.43 36.42 3.01 --
-
_
*---
- _
-_ -
---
_--
--
*-
- ---
-
-- ----
--
--
--
-- --- -
---
-- ----
--r -- -- * *
DRIED UNSTAB. PERCHLOR
Trichloroethylene
*
1.1.2 Trichloroethane
ft
Perchloroethylene U-Tetrachloroethane
s
S
H,0
pH
1 . ' 'NaI Test
Oxides
PPM
ppm
;o.oi 0.01 39.92 3.04
:23 i.9 ieg.
0 (0.01
99.90 0.06
0 (0.01
99.93 0.04
0 0' 0
0.03 - 0.01 . 0.02 99.92 99.92 99.95 0.04 0.03 0.01
6.5 Neg.
(-1 6.6 Neer.
--
6.4 T78 Neg. Neg.
575 Neg.
0 00
0'
(0.01 (0.01 (0.01 (0.01
99.92 ?9.94 99.94 99.94
0.04 0.04 0.03 0.02
--
6.7 Neg.
6.7 Neg.
8.2 Neg.
6.8 Neg.
00
0
(0.01 To^r (0.01
99.94 99.98 99.90
(0.01 (0.01 0.07
0 (0.01
99.93 0.03
-6.7 6.8 Neg. Neg.
4
- (-5 6.7 6.8 ' N g. Neg.
;L 013042
I
------- St of~
b jec t 4 Ln o
nMFl IT
tYi FT iiT i rr i ii
jhtial
jtecti 1 insfc
i ;e Oft
net <
kI' oux
..(itf- 5
PERCHLOR STABILIZATION
TYPE 208
WT. %
Perchloroethylene l ,J-OlCHLORO BROMOETHYLENE
1 ,2-DlCHLORO BROMOE TKYLENE K 1 ,2-TR1CHLOROETHANE
UlTETRACHLOROETHANE
EPE
Unknown. Total
1966
Avg _
JAN
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION LAKE CHARLES, LOUISIANA LABORATORY OPERATIONS REPORT
FEB MAR APR MAY JUNE JULY
AUG
SEP
OCT
NOV
DEC
1967
Avg.
-- 99.85 99.86 99.85 99.88 99.89 99.88 99.88 99.86 99.87 99.87 99.88 99.86 99.87
--* (0.01 (0.01 (0.01 (0.01 (0.01 (0,01 (0.01 ToToI (0.01 TSjor (0.01
(oToIi
(0.01 0.01 (0.01 (0.01 (n.m nno 0.02
0.02 (.01
0.01
(0.01 (0.01 0.02 (0.01 0.02 (0.01 0.01 (o.m (0.01 (0.01 0.01 (0.01 (0.01
-- 0.06 0.05 0.06 0.03 0.03 0.05 0.07 0.06 0.05 0.04 0.06 0.07 0.05
- 0.06 0.05 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04
_- -
--
_
-- - -
TYPE 207 Perchloroethylene
WT
1 , t-Dl CHLOROBROMOETHYLENE t.2-DlCHLOROBROMOETHYLENE 1. ,.l .2-.TR 1 CHLOROETHANE U-.TeTRACHLOROE THANE
EPE Unknown. Total
%
-
-
--
--.
..
-
_ 99.91 99.88 99.82 99.84 --
0 O' -
0.04
0
--
(0.01 0.02 (0.01 0.01
-
0.04 0.04 0.03 0.01
-
0.04 0.04 0.05 0.05
-
_ 00
0
0-
__
---- ----
-- -- -
---------- ---
99.77
0
0 0.61
6.07 6.05
0
99.84 0 0
6.61
6.04 6.05
0
SL 013043
COMF1 TENTH L:
Sub jec t to P roteci ive 0 rder of 14th Judici al Dii trict Court
Mo. 51-IT 5
--
FORM N0.45A 202-i1 5
TRICHLOR STABILIZATION
TYPE 115
BLM
THF
Carson Tetrachloride ADH
NPL
TfilCHLOROETHYLENE PEPCHLOROETHYLENE 1.1.Z-TR1CHLOROETHANE GDL
Unidentified, Total
WT.%
1966 Avgl.
--
-- -
-
-.
JAN
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION IAKE CHARLES, LOUISIANA
LABORATORY PRODUCT REPORT
FEB MAR APR MAY JUNE JULY
AUG SEP
-
--
n.?o o.o? 0.01 0.03 0.03 0.02
0.01 (0.01 99.50 99.50 99.62 (0.01 (0.01 (0.01 (0.01 0.01 (0.01
*-
---
(0.01 0.02
0
99.47 (0.01 (0.01
0
--
--
(0.01 0.03
0 99.51 (0.01 (0.01
0
-
*
(0.01 0.03 (0.01 99.48 0 (o.oi
-
(0.01
_
(n,m 0 0 99.98 0 0.01 0
-
(o.m
Or53 (0.01 99.52 (0.01 (0.01 0 (0.01
-- --
-- -
-
OCT
NOV
OEC
1967 Avg X
-
--
(0.01 0 0 O.Q3_ (0.01 (o.oi 99.48 99.57 (o.oi (0.01 (0.01 0.01 00 0 (O.Ol
--
-
(0.01 0.03 (0.01 99.64 (o.o: (0.01 0 0
3O.
--
0.02 0.02 (0.01
99.57 (0.01 (0.03 0
TYPE 107-
BLM THF Carbon Tetrachloride
ADH
NPL Tfl1CHLOROETHYLENE
Perchloroethylene K I.Z-Trichloroethane
GDL Unidentified.
Total
WT. %
-
-- T*
--_ --
-- -
--
_
0.07 0.01 0.01 0.04 0.03 0.01
-- 0.13 0.14 99.52 99.55 99.52 0.01 (0.01 (0.01 (0.01 (0.01 0.01 0.04 0.06 0.05
---
--
--
(0.01 0.12 0.12 99.57 (0.01 (0.01 0.05
--n---------
(0.01 0.03 0.13 99.50 (0.01 (0.01 0.06
- -
----
(0.01 (0.01 (0.01 (0.01 (0.01
0.03 0.03 0.03 0.03 0.03
0.14 0.14 0.14 0.14 0.15
99.50 99.51 99.49 99.48 99.47
(0.01 (0.01 (0.01 (0.01 (0.01
(0.01 (0.01 (0.01 (0.01 (0.01
(0.01 0.06
0.06 0.06 0.06
-- (0.01 (0.01 (0.01 J&01
---
---
(o.oi (0.01 0.03 0.03 0.14 0.15
99.47 99.51 (0.01 (0.01 0.02 0.01 0.06 0.05 (0.01 (0.01
--
--
0.01
o.o4 o.u:
99.51 (0.01 (0.01
"Tj;or
(0.01
__
SL 0w 11 3vl0U44H
+n Tvno 19?
mHPlI F.NTIA .:
s TiEJ*^SC_T
- UL r 9 ufl--c
No -
nhect ve Or ler
1 Dis ict ^our t
1-114 >
FORM NO. 45 A 202-16
TRICHLOR STABILIZATION
TYPE 1 10E BLM
THF Carbon Tetrachloride ADH
NPL Trichloroethylene
Perchloroethylene t . 1 . Z-TR 1 CHLOROE THANE GDL
L) ;l BCENTt F 1 ED .1 TOTAL
WT.. %
1966 Avg.
--
-- -- -
JAN
--
-- -
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION LAKE CHARLES, LOUISIANA
LABORATORY PRODUCT REPORT
FEB MAR APR MAY JUNE JULY
AUG
SEP
OCT I NOV
OEC
1967 Avg ,
-- -
---
-------
-- __
(0.01 (0.01 otoi
-- 0.06
- 0.23
0.24 0.27 0.31
- 96.90 _ 99.11 99.30 96.96 _
-- O.OT -- (0.01 0 (0.01 --
-- n.m
0.01 (0.01 0.01
- 0.12 -- 0.17 6.13 0.09 --
- _ - (0.01 (0.01 0.12 -
- ---- -- ---- -- (0.01 (6.01 -- 0 0.03 - 0.28 0.27 - 99.50 99.15 - (0.01 (u.ui - 0.01 (o.oi, - 0.17 0.14 - (0.01 0.03
-
TYPE 113 BLM THF Carbon Tetrachloride
ADH NPL TR1CHLOROETHYLENE PerchLOROETHYLENE
1 , 1.2- TR 1 CHLOPOETHANE GDL UNIDENTIFIED. TOTAL
WT. %
-- --
-- -- -- -
-- - _* --
-- _ _ --
(o.oi (0.01 (0.01 (0.01 0.01 0.01 (0.01 (0.01 (0.01 0 . (0.01 (0.01
- .009 -- 0
----
_
0
0 00 0 00
00 00
0 (0.01
0 0
99.99 99.96 99.97 99.95 99.96 99.96 99.96 99.96 99.97 99.96 99.98 99.97
(0.01 0.C6 (0.01 (0.01 (0.01 0
(0.01 (0.01 (0.01 (0.01
(0.01 to.01 (0.01 (0.01 (0.01 0.01 (0.01 (0.01 (0.01 0.01 0.01 (0.01
_
-- 0.06
0 0 0 0 00 0 0
---
- ---
-- - -- (0.01 0 (0.01 (o.oi
nSiL nU1loUn4A 0K
1
--tUWr nDiim nr*
Subjec x--ce-- 'lOlUt
ot It 4Ati.nU
X v. LUX--trt
01-11 15
Pmirl 1
%
FORWW'0.45 A 202-1 7
DRIED UNSTAB. TR1CHLOR
Carbon Tetrachloride
Trichloroethylene
1.1.2 Trilhloroethane Perchloroethylene
'
%
%
% *
1966 Avg
(0.01 99.98 (0.01 (o.oi
JAN
(0.01 99.98 (0.01 (0.01
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION LAKE CHARLES, LOUISIANA
LABORATORY OPERATIONS REPORT
FEB MAR APR MAY JUNE JULY AUG SEP OCT
0
99.99 (0.01
0
(0.01
99-. 98 (0.01 0
(0.01 (o.oi (o.oi
99.98 99.99 99.98 (o.oi 70.01" C0.U1 (0.01 (0.01 (0.01
(0.01
99.96 (o.m n
(0.01 0.01
99.97 99.98 0.01 (0.01
00
0 99.98 (0.01 (0.01
NOV OEC
0 99.98 99.98 0 0.02 0 (OiOl
1967
Avg (0.01 99.98 757JT 0.01
H70 pH NaI Test - Oxides
ppm (50 6.6
ppm Neg,
(50 6.6 Nee.
(50 736
6.7 6.4 Nee. Neg.
--
6.8 Nee.
--
6.7 TTs Nee. Neg.
6.6 Neg.
----
6.8 6.9 Nee. Neg.
--
6.9 Neg.
-
6.9 Neg.
-
6.9 Neg.
(5o 6.8 Neg.
' `
-
SL 013046
L
_
,,
i
~'
f
aU jec 1 A l-U
CONFi
--to "F uci
TENTIA otect ri'Dls
j:
ive Oi :rict
der Court
NO*-- ('r-114
* --
>. 45 A 2
-c'V*-'- \>vs
3Av j\'V
W
'XX'
.9.PITTSBURGH PLXTl GLASS COMPANY CHEMICAL DIVISION LAKE CHARLES, LOUISIANA
SL 013047
r
-----------------------------------st----------------------------------
GENERAL DEPARTMENT
1966
Avg.
JAN
FEB
pERCHLOR (STAB.) PRODUCTION T/D Shipments T/D Inven mor rof<i
1 RJ CHLOH li IA H. ) PrOPUC 1 ION I7T3
Shipments T/D
Inventory Tons
78.5 57.2
67.9
81.7 55.8 45.0
1823.3 8099.0 1740.4
71. Jit 58.2
65.3
81.2 52.5 104.2 2047.7 2657.0 1567.6
MAR
APR
67.7
83.7
62.9
106.9
1889.C 1190.6
70.0
93.2
64.1
101.9
1753.3 1493.6
MAY
JUNE JULY
AUG
SEP
OCT
NOV
DEC
1967 avg.
98.7
99.8 89.4
33.1 109.7 142.8 3219.3 2920.1 1969.4
111.1 104.0 107.7
54.7
133.2 98. n
3286.8 2409.9 2866.8
95.7 43.6
2875.5
105.1 51.5
78a 69.1
80.3
55.9 144.6 36a 112.6 79.1
4349.c 1461.9 2793.0 U7CT 218114
111.7 120.6 59.5
84.5 82.2
89.0
53.1 97.4 130.3
70.3
73.8 85.7
4684.9 5382.1 3188.6 3628.0 3537^" 3067.2
Unstab. Pehchlor Production T/D
EDC
Cl 2
T/T T/T
79.4
0.766
0.480
Tri-Eth.Bot. T/T -
NHr,
Lbs./T 15.3
61.2
0.864 0.523 -
19.1
70.1 0.859 0.499
13.5
70.7 0.853 0.568
23.7
80.5 0.761 0.504
19.5
99.0 0.716 0.443
-- 7.7
104.4 86.3 0.701 0.689
0.454 O.46I
---
11.0 17.5
98.1 0.652 0.433
-
104.3 0.63? 0.444
-
54.1 0.653
0.415 --
5.5
8.6
77.8. 0.672 0.472
-
5.0
70.2 81.4 0.744 0.738 0.496 0.476
-10.8 T27B
Unstab. Trichlor Production T/D
EDC
t/T
Cl2
T/T
70.8 0.972 0.304
Tri-Etk.Bot T/T
NH,
Lbs./T 10.7
.
Unstab. Product o2
T/T 0.289
n2 t/T 0.325
Catalyst Lbs./T 2.70
400# Stm.(actual) Lbs./T 3122
kwh/t
63.1
MC Hvy. Still Bottoms
T/T 0.022
Unstab. Product Cl` Yield
% 78.9
C Yield
% 77.5
ft/AN HOH-j/t STAp. P^ODUC7-
r 5': cue r f -zt* Maintenance Salaried Total Contract Man Hrs. PnciuorT
MAN HOURS/T SHIPPED
Bulk Drum SALARIED
T-, c C8 c.617 0.241 1.466 0.034
0.C68 1.069
0.026
61.8 1.080 0.327
18.9
67.4 1.084 0.315
--
16.0
71.9
I1.056
a:35i'
-
92.0 0.961 0.318
11.4
111.6 0.904 0.280
-
4.5
107.5 106.7 "0:885 3.870 0.286 3.291
--
7a 7.3
111.8 122.0 0.823 0.370
0.273 0.281 ..
60.9 0.824 0,262
-
19.0 4.3
1.5
0.340 0.464 2.75 4406 *130.5 0.001 73.1 68.5
0.316 U7J07" 0.273 0.275
0.436 0.436 O.46F 0.322
1.10 3800 104.2
7.97
3698
108.5
3.82 . 3198
93.7
3.25 210ZT"
59.7
000
O
0.008 75.1 71.7
69.0 W3
0.030 78.6
76.0
5875" 83.2
0.274 0.274 0.250 0.255
1.89 i.52
2084 2460
60.8
O.O17
64.0
--
87.4 85.3
83.6 83.0
0.262 0.278
0.257 0.254 0.201 0.665
2.70 3.06 1652 2227 67.2 - 63-5
1.42 2229 76.2
----
89.4 87.3 91a 86.3 83 ,S~~ 36.5
0.715 0.792 0.273 1.780 0,0
O.n??
0.713 0.28,5 1.650 0.059
"f r""5 C 0.942 0.254 1.931 0.0
z> ^ y
0.659 0.197
1.365
0.033
N> .4i? 0.432 0.172
1.023 0.114
6.412 0.453 0.359 0.563 0.176 0.170 0.947 ia91 0.053 0.0
0.423 0.648 0.183 1.254 0.0
0.390 0.434 0.104 0.924 0.0
0.713 0.856
0.315 1.884 0.038
0.094 0.818 0.031
0.068 0.066
0.554, 0.992 0.023 0.026
0.038 0.852 0.019
0.090 0.895 0.027
0.050 0.032 1.108 1.164
0.015 0.010
0.081 0.855 0.028
0^54 0.538 0.018
0.039 0.782 D.012
90.5
88.2
0.851 0.939
0.299 0.313
--
1.3
7.8
91.0 0.929 0.300
-- 9.6
0.264 0.252 6.41 2673 76.2
86.8
85.7
0.263 0.280 0.342 0.364 2.14 3.34 3592 2844____ 66.8 80.9
--80.9 82.9 73.4"
0.499 0.570 0.202 1.271 0.012
*
0.562 0.542 0.568 0.628
0.208 0.210
1.338 1.380
0.057 0.030
0.077 0.602
OLtfi21
0.046 0.062 0.429 0.799 0.012 0.021
FORJ 0.45A 21C- 2
MATERIAL BALANCE CARBON - TONS
Total Carbon in Feed Carbon in Unstab. Product Process Loss by Difference
Accountable Process Losses Blowdown Reactor MlSCELL ANE0U5
Sue Total
Unaccountable Process Losses
Carbon Loading Loss
Total Carbon Losses
PITTSBURGH PE
GLASS COMPANY
CHEMICAL DIVISION
LAKE CHARLES, LOUISIANA
PERCHLORETHYLENE.TR I CHLORETHYLEN'E DEPARTMENT OPERATIONS REPORT
1966 Avr,.
JAN
FEB MAR
APR MAY JUNE JULY
AUG
SEP
OCT
NOV
OEC
1967
Avg .
971.3 740.1
231.2
911.6 911.7 1042.9 1124. 1295.1 1248.3 1195.1 1243.4 1342.6 680.1 6?4-7 629.1 724.7 654.4 1077.1 1043.5 992.0 1073.6 1122.4 588.2 2*6. Q 282.6 31 ft 12 270.4 218.0 PClL.fi 203.1 169.8 220.2 91.9
973.2 1039.9 1084.0 834.4 815. C 864.9
138.8 224.< 219.1
14.2 200.7 16.3 231.2
9.0
14.6
252.3 20.0
286.9 0.0
17.9 17.8
244.7 280.4 20.0 20.0 282.6 318.2 0.0 0.0
19.9 230.5 20.0
270.4 0.0
Id. 4 "
187.6 20.0 218.0 0.0
7.8 7.3
22.3
177.0 175.8 127.5
20.0 20.0 20.0
204.8 203.1 169.8
0.0 0.0 . 0.0
17.8 9.8 182.4 62.0 20.0 20.0
220.2 91.8
0.0 0.0
34.8 20.1 15.0 104.0 184.8 184.1 20.0 20.0 20.0 138.8 224.9 219.1 0.0 0.0 0.0
10.2 37.0 30.5 -18.5 -1.4 -20.2 49.2 4.9
23.9 5.0 15.7 44.0 40.0 16.7
241.4 323.9 313.1 299.7 269.0 197.8 254.0 208.0 193.7 215.1 10?.$ 182.8 264.9 235.8
CHLORINE-TONS
Total Chlorine in Feed Chlorine in Unstab. Product Process Loss by Difference
Accountable Process Losses Blowdown Reactor Miscellaneous Sub Total
Unaccountable Process Losses
Chlorine Loading Loss
Total Chlorine Loss
- SL 013048
4727.0 4336.2 4271.2 5132.2 5473.4 6154.2 6056.2 5817.5 6043.6 6457.9 3254.2 4834JO 5036.8 5238.9 3806.6 3172.4 3205.8 3676.6 4300.9 5426.9 5291.3 4965.1 5404.8 5640.0 2963.7 4194.? 4074.9 4359.9 920.4 1163.8 1065.4 1453.6 L172.5 727.3 764.9 852.4 638.8 817.9 290.5 639.4 961.9 879.0
78.8 762.1
79.5 920.4 0.0
81.2 93.8 7973 110.4 57.7 43.3 40.6
982.6 871.6 1253.8 962.1 569.6 621.6 711.8
100.0 100.0 100.0 100.0 100.0 100.0 100.0
1163.8 1065.4 14T? .6 i 1172.5 7277T 764.9 352.4
0.0 0.0 370
0.0 0.0
0.0 0.0
123.7
415.1 100.0 S38.8 0.0
98.8 54.4 . 619.1 136.1 100.0 100.0
817.9 290.5 0.0 0.0
82.5 111.8 83.2
456.9 750.1 695.9 100.0 100.0 100.0
639.4 961.9 879.0 0.0 0.0 0.0
50.9 187.3 164.3 -101.4 -1.9 1-20.0 252.4 14.6 127.3 -34.0 84.1 202.1 188.2 80.3
971.3 1351.1 1229.7 1352.2 1170.6 607.3 1017.3 867.2 766.1 783.9 374.6 841.5 1150.1 959.3
loHFTD uNTIM *
Si bject
to
i'r ytectd VB--CHf< tw trietn
of
4th
J
iciiciait lu.s>i
--- ttll__ 1. i. xs
210-3
9
CONFIDENTIAL;
PITTSBURGH PL7T_ GLASS COMPANY
CHEMICAL DIVISION LAKE CHARLES, LOUISIANA
of 1|l4j?thfCJi uWdt0oic, iPa9lr1j.-\t1el>1c14st5itvreictOrr'dvemr rffc
PERCHLORETHYLENE-TRICHLORETHYLENE DEPARTMENT OPERATIONS REPORT
REACTOR NO. 1
On Stream Time Disch. Press.
Temp. F Vaporizer Liouor Dowtherm Out
Highest Tube
Lowest Tube
Sec. Cond. Disch
Catalyst Charged
Catalyst From Centrifix
Flow GPM
EDC
SCFH
Clj
Air
o*
1966 Avg.
Hr& 8434* psig 12.8
283 481 824 790 ^4 Lbs. 34703* Lbs. 3466C* 5.2 6666
1197 11142
JAN
710 10.5 ?4# si 4 818 783 88
2400 2620 5.2 5412 1535 9928
FEB MAR
672 612
10.7 iotn 223 272
535 O 1
817 tnn
" 764 69
1614 1062
6.0
770
59 16230 i/,iin 4.3
5898"' 6221 1545 1 5/, 3 7130" Q311
APR MAY JUNE JULY AUG SEP OCT NOV
695 742 720 12.2 13.0 13.1 294 294 793
512 514 677 819 813 838 782 -7S2 796 35 T5----- 23 2120 '3120 2600 2120 ~2I2tr 2600 5.0 5.0
5942 ' 6225"' 6773
1527 1526 1841 11218 11331 31819
744 744 12.1 13.1 "286 286 484 464
812 782 _
28 21 3000 2500 3000 2500
5.3 5.3 "5I5T" 671$ "I53I~
9984 10998
770 37.8
OHS.
213 13.0 278 457
588
8.7 261 424
--
22
2120 7170 4.8 7116 1511 11375
-
47 18 0 13240 0 13240 5.2 4.4 5550" 7179 1533 1543 10919 9628
DEC
1967 Avg.
744 7904* 5.7 11.2 251 272 530 491.
818
-- 780
20 2100 2100
3.9 5693
37 50644* 47592# 5.0 6332
1541. 1534 _ 8040 10282
Vent Analysis CO;
Ha
Per-Tri Ratio
iPer
Tri in Crude
% 37.8 37.1 17.3 29.2 % 13.2 14.6 11.1 34.3
1.23 1.49 1.08 1.31 % 85.23 85.03 79.12 79.11
53.0
3.9 1.35 83.42
50.3 50.5 2.0 4.1 1.06 0.96
78.25 82.41
40.9 47."05.6 3.0 1.09 o;w 82.37 3i:so
41.0 27.6
1.4 5,0 1.01 1.21 82.00 82.26
48.8 33.9 7.4 3.8
0,73 1.03 76.95 79.21
39.7 _ 7.9_ _ 1.10 80.99
REACTOR NO.
On Stream Time Disch. Press.
2
Temp. f Vaporizer Liouor Dowtherm Out Highest Tube Lowest Tube Sec. Cono. Oisch.
Catalyst Charged
Catalyst from Centrifix
Flow GPM
EDC
SCFH
Cl2
A) R
' o.
VENT ANALYSI S CO; HCL
Pf.r-Tri Ratio T- ' * --------
SL 013049
Hrs. psig.
8485* 12.6 257
708 9.5.
472 530
817
734 735 60 63 lbs. 31840 * 2750
lbs. 27675 * 2620
4.9 5.3
6818 5204
1836 1510
10266 9132
% 31.9 % 8.7
1.32 % 84.39
* Totals
16.3
7.3 1.37 78.36
672 636
690 739 720
11.1 9.4
12.2 12.6 12.5
549 818
749 71 1614
279------ 292 558--: 512 818------ 822 758------ 788 61-------- 44 11293 2120
286 "468
787 33 1590
288 437
--
-
34 2600
1062 12690
~5wr6,2 4.7 5805
2120
5.1 6600
1590 2600 ~5X~ 5.5
6411" 6713
1508 1609 9069 3618
1494 1504 1802 11220 14342 L0311
-
637 11.6
294 434 821
784 43 9574 9574 5.8
6252 1499 7430
12.8 11.4 -12.4. 28.4 1.23 1.27 78.32 75.39
32.6 4.6 l.`l6 "
81.93
23.8 2.6
0.96
79.26
18.8 31.1 4.5 3.4 1.02 1.18
76.88 81.03
744 12.9 293 432
720 12.8 287 440
----
25 2500
2500
26
2750 2750
5.3 4.8
6833 7116 1502 1511
11299 11375
398 12.7 291 455
-
-
28 1060 1060
4.9 6617 1500 11512
57.0 3.0 0.94 *1.63
54.4 59.1 2.1 2.7
0.99 1.00 81.38 82.32
627 12.0 269 457
-
-
2$ 2290 229(1 170 7098"
1506
10991
55.7 5.3 1.03 79.68
744 4.7 251 591
--
27 2100 2100 4.2 4851 1526 7559
8035# 11.2 283_______
489 820 767 40
42241* 42956* 5.2 6272 1505 10238
33.5 33.5L-- 8.0 7.0
1.11 l.ll
82.65 79.90
SL 013050
REACTOR NO. 3
On Stream Time Disch. Press.
Temp.F Vaporizer Liouor Doh'Therm Out Hi ghest Tube
Lowest Tube
Sec. Cond. Disch. Catalyst Charged
Catalyst from Centrifix Flow GPM EDC
SCFH
Ct2 A| R
02
Subject C?NFIIDEN'J,I/'J^
PITTSBURGH PLATE GLASS COMPANY
CHEMICAL DIVISION
f l4th
LAKE CHARLES, LOUISIANA
PERCHLORETHYLENE. TR I CHLORETHYLENE DEPARTMENT
OPERATIONS
REPORT W*
9i~li45
UlC^
1966 AVG.
Hrs. psig.
8333*
12.3
277 476
823 781
61
lbs. 25820 * lbs. 26900*
5.2 7008
1023 10650
JAN
707 10.1 270 518 815 786 58 2550 2620 5.2 5857 1478 9661
FEB
666 12.2 .273 499 814 779 60 1076 1053
6.5 6377 1446 10626
MAR
664. 5.6 240 621 815 787 72 2785 3460
5.4 5547 1473 7468
APR MAY JUNE JULY
AUG SEP
621 744 790
6.6 13.1 13.0 256 279 977 599 466 J,83
806 819
753 779 79 "71-- 80 12330 1590 2100 12330 1590 2100
4.9 5.8 5.9 5419 "5785" 6709 1457 1452 1443
7423 11554 11903
744. 744 623
11.6 13.1 12.3 271 "271 272
461 452 451
817
745 78 3000 3000
-
"75------ 53 1500 11690 1500 11690
6.0 5.7 6128 6216
1401" 1442
4.9 7081
1449
9955 10377 11400
OCT
399 13.0 275 467
_
--
23 1190 1190 5.2 6653 1445 12171
NOV
600 11.5 267 489
--
-
21 2560 2560
4.8 7071 1475 11234
DEC
1967 AVG.
744 7976* 5.4 10.6
245 257 586 508
-- 814 - 772
22 55
2100 44471* 2100 45203*
4.1 5.4 5367 5368
"1499" 1455
7952 10144
Vent Analysis
Co2
HQ.
Per-Tri Ratio
tPer
Tri in Crude
% 24.2 39.6 39.3 21.2 27.2 53.9 53.2 35.6 T93~" 53.3 45.5 41.8 33.9 38.7
% 9.3
1A.1 7.9 17.8 19.7 4.4 2.3 1.5
2.V 5.5 2.6
9.8 8.3 8.1
1.33 1.08 1.38 0.93 1.57 1.01 1.09 1.12 ~rr&- 0.94 1.22 1.19 1.09 1.15 X 81.74 83.35 84.13 79.19 74.38 81.03 83.14 81.27 32.15 85.72 86.08 86.53 85.49 82.71
REACTOR NO.
On Stream Time Disch pbess.
4
Hrs. Ps,a
Temp, of
Vaporizer Liouor Dowtherm Out
Highest Tube Lowest Tube
Sec. Cono. Disch.
Catalyst Charged
lbs.
Catalyst from Centrifix
Flow GPM
EDC
SCFH
CL2
lbs.
A| R
8295* 731 12.0 10.0
279 275
459 .509 823 8j.3 783 782 66 64 43073* 10500 43570* 10480
4.9 .5,0
6653 1235
5587 1540
10527 10083
657 744
11.1 8.6
275 249
520 596
815 816
777 781 76 67
1076 3i i.n
1063 3460 6.0 5.4
6089 6605 1538 1560
10l6l 9229
693 5.3 249 . 687 811 788 40 1060 1060
5.4 6173 1552
5629
"584 720
10,8 12.1
275 279
430 443
"320 -
"753
-
24 "24
13830 2100
13830 2100
4.8 5.5
6145 6591
1571 1561
10890 11606
744 12.7 277 458
813 779 27 3000 1050"
6.0
6265 1396 11664
719 12.3 273 465 --
-
27 2500 2500 5.4 6305 1587 11286
720 13.0 270 442
--
-
25 2120 2120 4.9
7374
1558 11764
399 12.3 275 414
-
-
27 17S5 1766 478 7033 1530
10763
498 10.3 261 438
--
-
28 1760 1760 4*7 6629
-
11049
593 5.2 247 579.
--
28 2100 2100 3.8 5087
--
7711
7902*
12.0 267
499 815 783 38 44952*
45239* 5.1 6324 1541 10066
Vent Analysis
Co2 HCL
Per-Tri Ratio
Per i Tri in Crude
X 31.3
X 11.2
1.33 % 85.35
^Totals
46.3
7.9 1.60
86.97
42.5 25.8 16.2 19.0
1.28 1.45 85.73 84.01
21.4 2?;o~
1.13 77.13
53.4
12.6
0.76
83.26
59.1 49.7 5.5 2.8
1.02 1.12
84.93 88.92
58.9 3.2
W
37.81
59.7 37.2 5.9 4.3 1.04 0.79
87.21 87.31
47.9 14.8
0.88
84.89
30.9 44.4 4.7 10.5 0.95 1.07
84.56 85.23_
FO 0. 45 A 210 - 4A
REACTOR NO. 5
1966 AVG.
ON STREAM TIME DISCH PRESS TEMP. OP VAPORIZER LIQUOR
DOW THERM OUT HIGHEST TU BE
LOWEST TUBE
SEC. CONO. DISCH. CATALYST CHARGED CATALYST FROM CENTRfFIX FLOW GPM EOC
SC FH CI2 AIR
02
HRS PSIG
LBS. LBS.
-- -
-
-
-- --
-
VENT ANALYSIS CO2
H Cl
-PER TR1 RATIO
+PER
TRI IN CRUDE
%-
%-
%--
PITTSBURGH I
GLASS COMPANY
CHIMICAL DIVISION
l/.KF CHARLC5, LOUISIANA
PERCHLORETHYLENE-TRICHLORETHYLENE DEPARTMENT OPERATIONS REPORT
JAN
-- -
-
-
-
FEB
MAR
APR
MAY
JUNE
JULY
-- -- --
14000
0 -
-
-- -
744
-
-
1236
1500 -
-
720 -- 8i6
794
1120
2120 -
-
710 -- mm 815 785
-
2120
2120
-- --
702 -- --
-
2100
210CF
-
-
733 -- -- 802 765
2500
3000
-
AUG
SEP
OCT
619
_
*
-
8500
8500
-- -- -- --
720 -
399
-
-
-
-
---
2120 1060 2120 i060 ---
-
--
--
NOV
--
* -- 12540
12540
-
DEC
AVG.
744 -- -- -- -
2100
2100
_ -
6549* --
811 782
50396*
37160*
-- --
- - - 49.8 47.9 39.5 38.3 43.5 50.1 48.4 41.8 26.9 42.9
--
-
-
9.7 7.7 5.9 4.7 5.7 6.9 5.4
5.6 6.2 6.4
-
-
--
1.27 1.07 1.06 1.30 0.99 1.08 1.20
0.97
1.00 1.10
-- - - 84.52 84.28 82.02 83.63 83.61 83.44 83.65 80.95 82.85 83.22
OqiL Un 11 JtoUOr 1| -
C(3f
Sub] set t< 3f 14t h Judi
FI OEM IftL prot< ictive
ci al listr 1
Order xt--tou
L
L
He , n-. 145--
^TOTALS
FORM NO.45A 210*5
REFRIGERATED BRINE
Temp. F
Warm (Out) Colo (in)
PITTSBURGH
GLASS COMPANY
CHE^P DIVISION
LAKE CHARLES. LOUISIANA
PERCHLORETHYLFNE - TR I CHLORE THYLENE DEPP RTMENT OPERATIONS REPO.RT
1966
Avg.
47 38
JAN
47 39
FEB MAR APR
61 41 50 37
25 18
MAY
6 5
JUNE JULY
8 11 46
AUG
11 4
SEP OCT
9 12 46
NOV
11 7
OEC
15 10
1967
Avg.
21 16
DRYING STILL
Temp. F
Bottom
Top
Bottom Pressure
psig
210 161
1.11
-200 158 1.16
205 148 0.92
210 3.60 1.08
206
164 1.32
203 204 20? 171 170 165 1.40 1.27 1.16
199 198 199 165 168 169 1.33 1.26 1.27
198 165 1.34
198 202 160 164 1.39 1.24
PER-TR1 STILL
Feed Reflux Bottom Temp. Overhead Temp.
gpm gpm
F F
19.9 34.1 288 192
19.3 39.4 291
194
18.7 34.1 288 192
21.9 " "2576 33.5 '3477 292 "29cr 189 191
27.2
26.4 285 186
24.2 24.2
283 185
23.0 3^.4 290 187
24.1 37.5 292
185
24.6 40.2 292 185
23.9 34.4 285
184
22.6
32.f> 280 180
20.4 32.6 281
180
23.0
33.7 288 187
HEAVIES STILL
Feed Reflux Bottom Temp.
Overhead Temp.
gpm gpm
F F
9.3 87.3
344 253
8.7 97.1
343 248
8.1 98.2
345 253
9.5
] Ey.tr
12.1 107.7
334 328
252----- 258
12.4 11.4
107.7 109-2
341 341 258 257
11.6 109.0
338 236
11.4 11.8 10.9 117.7 129.9 115.9 339 336 338
255 "255 255
10.2 97.4 339 233
10.3 67.2 318 236
10.7 105.0
337 250
Feed Reflux
PER STILL
Recycle To Wash Column Bottom Temp.
Overhead Temp.
Feed
TRI-STILL
Reflux Bottoms
Recycle Bottom Temp.
Overhead Temp.
_
SL 013052
gpm 9.54 9.32 8.41 9.72 11.50 11.81 10.66 10.39 10.57 10.97 10.88 9.36 8.51 10.18
gpm 17.93 18.40 18.39 13.80 21.74 18.16 20.76 16.13 22.23 22.90 23.45 18.38 15.41 19.98
gpm 0.144 0.258 0.196 0.227 0.186
0.035 0.064 0.061 0.041 0.035, 0.027 0.181 0.118
gpm 9.04
8.27 8.11 - 8.91 9.26
11.08 10.25 9.56 10.27 10.46 9.95
9.05 8.18 9.45
F 281
264 270 277 232
281 283 258
262 282 283
261 266 274
uF 246
233 239 2ZlO
229 "242 244 220
239 232 231
222 "225 233 t
gpm 8.65 8.58 8.25 9.72 10.88 11.90 10.89 11.26 11.97 12.65 12.56 11.57 9.95 10.85
gpm 5475f~ 60.08 60.22 54.82 52.74 56.08 63.62 56.03 60.97 64.05 57.73 63.25 64.10
gpm 37^5
8.13 7.72 9.8/, 11.61 12.96 10.13 9.32
9.66 10.34 10.14 8.95 7.18 9.67
gpm 1.304 1.625 1.732 1 -105 0.009 T7977 1.150 1.060 2.143 2.325 2.324 2.088 2.506 1.687
F ?36
234 236 232 234
230 231 229
229 231 230
227 230 231
F DS
145 145 152 143
139 139 139
139 "138 141
136 135 141
ON? ID INTI AL
----
of 14th Judicial District Court; No. 91-1145
F0RILN0-45A 2|0.6
TRl TOPPING STILL
Bottom Temp. Overhead Temp,
F F
PITTSBURGH F^B GLASS COMPANY
chem!5u divisi n
LAKE CHARLES, LOUISIANA
PERCHLORETHYLENE-TRICHLORETHYLENE DEPARTMENT OPERATIONS REPORT
1966 Avg.
199 195
JAN
195 194
FEB
195 198
MAR
194 194
APR
200 198
MAY JUNE JULY
195 194 192 193 191 192
AUG SEP
189 188 190 189
OCT
189 189
NOV
187 186
OEC
188 186
1967
Avg.
192 192
NEUTRAL 1ZATION
Perchlor NH3
Flo* To Stg,
psig gpm
11.5 8.62
Tri chlor
NH3
Flow To Stg.
PSIG 7o
gpm 8.21
9.8 10.2 13.0 *.97 6.13 6.74
10.9 11.4 13.1 6.95 5.26 6.55
13.0 7.39
12.3 3.72
Io77 10.0 9.0 8-70 8.67 7.73
8.2 8.82
A
8.3 8.82
9.3 6.36
6.7 6.0 9.5 _ 7.19. 6.91 7.62
11.7 10.6 11.6 7.70 7.55 7.90
l7l67.4 4.1 0.8 8.49 7.42
1.6 3.2 8.2 6,44 5.87 6.80
SL
013053
----- or*U..tt vt--ti
c ject
Wide
0 Pro
icial
TiAr.;
:ectiv Distr
1 0. 1145
r-----------