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. ARR2G - 0720 MICROBIAL INHIBITION (DEHYDROGENASE ACTIVITY TEST) IESTSUBST~A ~~ NCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS# 2795-39-3). Remarks: The 3M production lot number was not noted. The test sample is FC-203. Current information indicates it is a mixture of 1.34% PFOS, 35% diethylene glycol butyl ether, 37.85% water, 20% ethylene glycol, 2.66 % Sultone foamer, 3% sodium octyl sulfate, 0.1% sodium lauryl sulfate, and 0.05% tolyltriazole. The following summary applies to a mixture with incompletely characterized concentrations of impurities. Data may not accurately reflect inhibition by the fluorochemical componentof thetestsample. METHOD: 00000 Method: Not noted. GLP: No Year completed: 1973-1974 Analytical monitoring: % Transmittance Statistical methods: Results were determined by calculation of the % transmittance and comparison with the blank. Test organism source: Not given Contact time: Not given. R0 ESO0 WTS 00000000000 Nominal concentrations: Blank control, 0.01, 0.1, 0.5, 1, 5, and 10% conc. Element values: Not given. CONCLUSIONS - No conclusions given. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 pataQuALY Reliability: Kiimisch ranking = 3. Study lacks description and recordsof the method followed. Sample purity was not properly characterized and the study lacks analytical confirmation of the amoo ffluucrocnhemitcal proportion in the solution. 000566 R0 EFERENCES 000 TSth.ePasutlu,diMeNs,weLraebcRoenqduuecsttedNubmybtehers320C34o,mp2a03n6y,,2E0n9v3i,ro1n9m7e3n-t1a9l74L.aboratory, o0 rWeR000000000 Last changed: 6/27/00 000567 ce: LA REQU800EK-S2T8 ____________ WaandtWase tewarter REQUEST FOR LABORATORY WORK Libero, __RO3G TO: ENVIRONMENTAL ENGINEERING LABORA--TBUOILRDINYG 536N rer wrt Name: Dale Bacon request vate S ProjectrNeo. e T5e74a0tm prob. kNoe, He ogGo,fn 1505 Date Rec'"d. Analyst: SamAple; 3 | mVcETaS Hold Sample For Boys Ea. Time. Hn 75 | hese Z px Sample Description Fezo3 |[vz]| "oTA otralyHarr dness, m/mT lCay sCaaoC0ss H T TIT t T TT ] T T p = ng nC HH --H--H H--F--" SCNiofraemteei,mmmogm/rolgaaa55sna0ss4 r t r rr rT t rr TT is Trt a E a a ar T H T --t--rrt r ------H b B Ea real Vingemg TET H r -- -- r r -- -- rr SSPuoreomanngma LAS E r lt E H l TVEo0ua0t:sSPusEpmeSpnsesSCoSoeor nomgyyix Toreymt Ligue{] 5,646 TrrTT 1+1 LTTooatraae ST Baca oT i r rT rTr ------ -- T FFeeaerd CCoC rlfaerpNsoRoeoRST r Hrrt r E Rams iron: maaes FTTeantT|mT|i% TfranagminHincce e| Oiland Gress,mg TTC Sea To ~~~---- 1"1-- TT TT -- 11 17 oT aje-- e LT 113rg1H1 1= 257% 499 73 1.0%, -- g3 75 c------ oo, gs {4 Me En So aSta ens Es, 2 Erman Eo.Gmt er000o56n80cnr BEST ICOTPY AVAILABL---- E " } --o----___________ WaWtaersatndewater 2034 REQUEST FOR LABORATORY WORK Lab RequestNo, __ZX OTF SrmeeDeBATOC:ronEwNVsIRrnOeNevMnEgNnTeAL ETN2 GINTEERTING LA|BprOenRenA--gTBmUoOIeLRDS IYNG 5p3o .a6nNa lIe DPesocrimptiion:N___ prob, No. 0% CodesA209 Tm Analyst: aap y_ON "5 26K ST iHoonmsos-- easmroi-- rono e--e n Te Tm [w2e25]TTZoenseGorooeT|me[sFrr ecoe2rde l1z~aa~zy ac] TPAlkalinmigt/lya,s CaCO3 TMT Alkalinity, mg/i as CaCO3. rrr oH Sulfuie, mg/l35SOs 0.01% TT 230TTT 7 8|B[eJ27a17] Arona 0S 0Lg TT ssTTTs--T - gs Th T eo Chloride, mg/l as CF Silica, mg/l as SiOz eae Tuoride, mall 35 Ortho Phasphate, mg/i as P 0 To 1 Conbrol-MMI TT `Total Phosphate, m/l asP 1 qI5 ||5s| TI ods [45 | 58 azz1 1 2 | zg [24 To re tt = | `Hex. Chromium, mg/fasCr. Total Cyanide, mg/l as CN. TTT Ferrocyanide, mg/l as CN rr rT Tron, mg/t as Fe Manganese, mg/l 3s Min rT TTT Surfactant, mg/l 2s LAS. Phenol, mall rrr TTT BOD, mg/t rT COD, mg/1 (Short, Long, Dilute] Total Suspended Solids, mg rT TT TT TT T T Volatile Suspended Solids, mg/l Turbidity,mg Silica [g7q0 TT [I=886 [1 [TTTT T TotalSolids, mg/l Total VolatileSolids, mg/l rT rT rT TTT Conductivity, mhos Total Bacteria, No./100mi rT TT Total Coliform, No./100 mi rrr -- Fecal Coliform. No./100 mi Fecal Streptococcus, No./100mi rrr rrr TTT AmmoniaNitrogen,ma/l as N Kiedidahl Nitrogen, mg/l as N TT TT Oil'and Grease, ms rrr r rr Comments 1r 7r 1 r 1 -- Eafhom 77C Zed G=a 7 1 7 pC 7 pr eC os a as Emm So. 22 Err wt n00D 0569ereLuPR--_ Tle, Se F HE . r REQUESTOR Lob. Reged No. 09S<-- PRODUCT ECOLOGICAL ASSESSMENT A -- Lot wks REQUEST FOR LABORATORY WORK [a FC 203 T LABORATORY 43 (fe 32 NRAEMQEU:ESTSiDATE: PROJECT N0.: CSOADMEPLNEO.DATE: . DATE NEEDED: ~ PROB. NO.: ADNAATLEYSRTE:CEIJVErDaSsApMPrLE: 2 -2%-14DATE COMPLETED:' 3/22/74 HOURS SPENT: IShy Y_ @.o - psschirTIoN \ TURPOSE OF TESTS: En * - Wo = C 5 c ~ te18e73 EE = Tha F,% MF Earraisnheuster Fii sh' sh] 0 H- H WRalucsrtoiocrgaPnliasnatss r1 r 0 STaredFdaent Hormals T TT T T 1] TTT 17] cue . Parent Material fa" 0TX0 ultints : aSioasay Other S T S r SS ] S-- IIrT II Tr] IT 11 T Lean chatL i"ipia:es EO o ar TBoOrS of thaaee Si ` . WR RrG&:4 W7eGdin oani TII T IT T T 1 T IT r T Oltoahsesrar 1 --Ir -- -- - rr 17r 11IT ; BEST COPY AVAILABLE - ocof}o Shar i iy kd at fey A Lo BEST COPY AVAILABLE Cnnscommen monies I I icapt ur Comebussttieons A cally E(TULR , TH i -- Sere Lown ro || f=g eo ore ; Sxygen Uptuke ria T ---] 3 a -- _ 1 H----H ---- = 1 EC -- l in oH is [a= dig Siacowuiation . Fedos fpr our) fron [2a a hhyn ----H-- HT i J -------------- 11] IX] 4 Sdd dada Wi NT) 3 =. | |~ |Ii ||HE \ ras .. 1 000571 . " . C, TsTwe Govan pescanmior Mets at ENVIRONMENTAL ENGR. LAB - WORK BEST COPY AVAILABLE [iE eae ' File: page No._%0) SHEET Date: Hey7s Anal3y; h-- m FC-20% Coch _ Info tetfis Sf fw ef eeif es fe eG doflon tio GY Cl AT: 480m 6T 7% 8G ee67 Le ee MOEA NT ge fe . Cel ees EN ee 8S 6 TT CL MOY 80 C. sr alsern sn ieeeoss gen -- (LoRR43 Feel Cwisn ifeo es oy dwfrees choom 05 feUS _C de a gE ee - sit 4d e en ni SAE =. a RRRTET _ GT gm 2 OS HTS _ lo ih HE ---- 25> 24.0599 A 2% 0228 Ne gases SVS ML 740528. S5dz0 oo T420k 33294" ooosiz ty File: . ENVIRONMENTAL ENGR. LAB - WORK SHEET CFT MPLE DESCRIPTION cok BEST COPY AVAILABLE peDaeteee: Page No._ shyfi7`r Fezor Cole ETT ee tetfiy ly loc amfe GloLLolzs 0S 40 oo GoMafuo tthe ge Als TTT mee ireOT BE LR -- a RE Re LOA i Cl LEER dz eile i ay : 6.1% 36 i 3 0S a4 Co C. E- Woo $e Cobol _Lorzdn Fenee tn 45 (Chafoomifo a0 TEE 37 US mfoaespe 05 46% 57s CC betfe RS aes. ieee QL 368 2 aAE NRE vRg GN URn E REETTE _ dB 3 0s Ms : a tc - ow SisMe T-- osszA1a3n8 ycv" s Sz20a9p mTF, e MA0wll _ ToodscJe 103574 Reviewed bye T9004 C pikemfE ~ooosia