Document reZy6myqnLYJw84xbq61v1KOe

Data Package Contract Lab Program Data Package for DERS/DuPont Env TYPE IV INORGANICS DATA PACKAGE DuPont Fort Madison GW Monitoring-1996 Annual Water Samples collected on 09/19/96 - 09/20/96 Sample No. 2585276-2585279, 2585281-2585285 DATE RECEIVED j OCT 17 1996 ! SAM_____ BT CED BY PA Cert. # 36-037 NY Cert. # 10670 NJ Cert. # 77011 Prepared by. Quality Assurance Review. Date ta/t^fafe Delivery Date /p-n-qu N36821 Lancaster Laboratories 2425 New Holland Pike, P0 Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681  Lancaster Laboratories A division of Thermo Analytical Inc._____ IfVnSIr- Joil' Sample Reference List foe SD6 # FMD03 with a Package Type of IV-X Lab Sample Number 2585276 2585277 2585278 2585279 2585281 2585282 2585283 2585284 2585285 Sample Code KRAIS MRA1D MRR2D MRA2S KRA48 MRA3S MRA3D MR3DD MRAFB Client Sample Description FMN-MRA-1S water Sample FMN-MRA-lD Water sample FMN-MRA-2D water Sample FMN-MRA-2S tmspiked Water sample FMN-MR&-4S water sample FMN-MR&-3S water sample FMN-MRA-3D Water Sample FMN-MRA-3D-DUP water Sample FMN-MRA-FBLK-2 Field Blank Water Sample Lcu'car-le' Laooratonto >42`> Nir.v Holland Pit.-.- I:'0 ->v. 124.?' lanv<Ster, PH I760L1-j-J-H'V:: rn> 717-066-26S' Shipping Address. Lariciisier Lat>orainnt*^ 24?? I\*-`A HOlirintl Pirt LriOCAS'ev. :jA "760' ? :"-f^6-23C0 Fa:.: ? * Environmental - Foods Pharmaceuticals A subsidiary oi Tnermo TerraTech im.., a Thermo Eiocrroi; cornncim.' DUP050307765 TABLE OF CONTENTS A. Case Narrative-Conformance/Nonconformance Summary................................l B. Sample Data................ 4 C. Quality Control Data..............................................................................................................14 D. Verification of instrument Parameters...............................................................38 E. Preparation and Run Logs...................................................................................................49 F. Raw Data.............................................................................................................................................73 1. ICP Data..........................................................................................................................74 2. Furnace Data............................................................................................................110 3. Mercury Data............................................................................................................182 4. Extraction/Distillation/Digestion Logs...................................194 G. Chain-of-Custody Record................ 198 DUP050307766 Case Narrative Conformance/Nonconformance Summary i DUP050307767 Lancaster LaboratoriesA Thermo Analytical Laboratory Where quality is a science.. CASE NARRATIVE FOR INORGANICS Laboratory Name: Lancaster Laboratories SDG Number: FMDOl Date Received: 09/19/96 nal ihr-ation Standards: Instrument calibration standards are prepared monthly from stock solutions purchased from Spex Industries Inc., JT Baker, Aldrich Chemical, VWR Scientific, EM Science, or VHG Laboratories. Case Narrative reviewed and approved by: ILA. Date y 0 Diane L. Lo'cka Specialist I Coordinator Inorganic Data PacVkaargreose 1-- -- Lancaster Laboratories 2425 New Holland Pike, P0 Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company DUP050307768 U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: LANCASTER_LABORATORIES_____ Lab Code: __________ Case No.: _______________ SOW No.: ILM04.0 EPA SAMPLE No. MR3DD_______ _MRA1D_______ _MRA1S_______ _MRA2D_______ JMRA2S_______ _MRA3D_______ _MRA3S_______ _MRA4S_______ MRAFB_______ Contract: SAS No.: __________ SDG No.: FMD03 Lab Sample ID. _2585284___ _2585277___ _2585276___ _2585278___ _2585279___ _2585283___ _2585282___ _2585281 2585285 Were ICP interelement corrections applied ? Were ICP background corrections applied ? If yes - were raw data generated before application of background corrections ? Comments: A Yes/No Yes/No Yes/No YES YES N0_ I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer-readable data submitted on diskette has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature. Signature: Date: U>\ \ 3 ^_________________ Name: Title: COVER PAGE - IN Diane L. Lockard Specialist I Coordinator inorganic Data Packages ILM04.0 48 DUP050307769 Page: 14 LANCASTER.LABORATORIES Run Name: 9627404T61 Tube: 13. CRI 09/30/96 13:37 INSTRUMENT ID: 05478 ELEM. AVG (ppm) %RSD #1 INTEGRATIONS #2 43 REREAD REDIG ___Ag ___Al 0.020401.997 0.03678 6.646 0.02038 0.0378i 0.02082 0.03853 0.02001 0.03398 ___As '' 0.02052 4.308 0.02148 '0.02037 0.01973 . Sa 0.00022 29.61 0.00024 0.00026 0.00014 ___Be 0.01014 2.450 0.01001. 0.00999 0.01043 ___Ca 0.10035 4.927 0.10469 ' 0.10138 0.09497 ___Cd 0.00976 0.459 O.00971 0.00978 0.00979 '__Co 0.09906 0.4S9 0.09917 0.09949 .0.09854 J_Cr 0.02040 1.430 0.02071 0.02014 0.02035 ___Cu 0.04950 0.171 0.04947- O.04943 0.04959 ___Fe 0.04062 24.34 0.05187 ; 0.03328 . 0.03673 ___K 0.06131 0.810 . 0.06109- 0.06096 0.06188 __ Mg ___Mn 0.03943. 4.722 0.03006 0.027 0.040^3 0103006. . 0104025 0.03005 0.03729 O.03007 Mo 0.00029 373.0 0.00055 0.00125 -0.00091 ___Na 0.16858 22.03 0.13544 0.16157 0.20874 ___Ni ___Pb 0.08089 1.305 0.00644 10.76 0.08126 0.00608 0.08172 0.00724 O.'07970 0.00600. ___Sb 0.12061 0.708 0.11980 0.12053 0.12150 ___Se 0.01011 4.345 0.00977 0.01060 0.00995 ___Sn -0.00075 164.9 -0.00186 0.00058 -0.00098 ___Ti 0.00015 95.85 0.000.27 -0.00018 0.00000 ___Tl 0.02060 10.04 0.02071 0.01848 0.02262 A ___V __ Y 0.10535 0.234 171904.00000 0.115 0.10508 0.10540 ' 0.10557 127.00000 171755.00000 172130.00000 0.04059 0.033 0.04058 0.04060 0.04061 148 DUP050307670 page: 15 LANCASTER LABORATORIES Run Name: 9627404T61 ^ Tuba: 14 ICSA. 09/30/96 13:41 INSTRUMENT ID: 0547S ELEM ___Ag ___A1 __ AS ___8a ___Be __ Ca -s Cd l CO ' . Cr . __ Cu.. __ Fa___K ___Mg ___Mn '___Mo _ ___Hi ___Pb __Sb ___Se ___Sn ___Tx ___T1 ___V __ Y Zn AVG (ppm) %RSD 0.00033 40.42 478.94635 0.317 -0.00254 59.59 O.00789 0.108 0.00076 15.77 463.73730 6.411 0.01032 1.140 0.00002 1792. ' 0.00592 6.544 -0.00218 13.25 187.80107 0.262: 0.05965 13.74 489.27246 0.246 0.00390 1.693 -0.00006 1946. 0.20265 26.89 0.00473 2.737 0.00609 25.96 -0.00192 58.87 -0.00606 37.07 0.00016 684.5 -0.00088 4.098 -0.00181 289.6 -0.01483 2.407 160381.67187 0.091 0.00982 0.342 ttl 0.00017 477.91204 -0.00101 0.00790 O.00063 461.54449 0.01046 0.00025 0.00613 -O. .00226 187.27685 .0,05966 488,23983 0.00395 0.00138 0.20792' 0.00463 0.00720 -0.00303 -0.00852 0.00006 -0.00086 0.00283 -0.01467 160468.00000 0.00984 INTEGRATIONS #2 0.00043 478.23693 - -0.00405 0.00790 O.00086 464.66278 0.01024 -0.00043 0.00616 ' -0,00186 187.86883 O.06785 488.98254 ' 0.00393 -0.00031 0.25433 0.00470 0.00428 -0.00197 "0.00411 0.00131 -0.00092 -0.00751 -0.01457 160464.00000 0.00978 #3 REREAD REDIG 0.00039 480.69006 -0.00257 0.00788 0.00080 465.00466 0.01026 0.0002-4 0.00547 -0.00242 18S.25753 - 0.05145 490.59497 0.00382 -0.00127 0.14570 0.00488 0.00679 --0.00076 -0.00556 -0.00089 -0.00086 -0.00076 -0.01523 160213.00000 O.00983 149 DUP050307671 Page: 16 LANCASTER LABORATORIES Run Name: 9627404T61 v INSTRUMENT ID: 05478 Tube: 15 ICSAB ELEli 4 AVG (ppm) %RSD 09/30/96 13:46 ., INTEGRATIONS #1 #2 . 43 REREAD REDIG - Aq :___Al As Ba Be Ca Cd "> Co V Cr Cu Fe K Mg Mn Mo Na Ni Pb Sb Se Sn ___Ti T1 V Y .Zn . - . 0.20628 1.199 0.20342 0.20761 466.42150 1.429 458.78042 469.41033 0.09650 2.968 0.09484 0.09485 0.50324 1.153 0.49668 0.50534 0.46731 1.263 0.46051 0.47114 451.99804 1.462 444.45434 456.77902 0.91704 1.179 0.90459 0.92420 0.45771 1.478 0.44992 0.46218 - 0.48501 1.176 0.47853 . 0.48926 0.52715 1.331 0.51933 0.52920 182.71130 1.674 * 179.18077 184.57627 0.05086 6.444 0.05005 0.05447 477.28186 1.486 469.12884 480.66183 . 0.47230 1.185 ' 0.46584 0.47575 0:00055 95.12 - 0.00074 0.00094 0.17470 2.039 0.17852 0.17410 0.92069 1.327 0.90671 0.92935' 0.05338 1.922 0.05249 0.05450 0.60465 0.948 0.59847 0.60981 0.04346 2.074 0.04244 0.104381 -0.00048 83.82 -0.00026 -0.00023 -0.00103 1.559 -0.00101 -0.00103 0.09101 8.436 0.08595 0.09984 0.48606 1.320 0.47865 0.48996 163133.00000 0.761 164559.00000 162547.00000 0.96563 1.297 0.95117 O'. 97260 0.20779 471.07373 0.09981 0.50771 0.47028 454.76077 0.92232 0.46103 .0.48725 0.53291 184.37687 0.04807 482.05487 ' 0.47532 -0.00004 0.17147 0.92601 0.05314 0.60567 0.04414 -0.00095 -0.00104 ' 0.08722 0.48957 162293.00000 0.97313 150 DUP050307672 Page: 17 LANCASTER LABORATORIES Run Name: 9627404T61 Tube: 16 CCV 09/30/96 13:50 INSTRUMENT ID: 05478 ELEM AVG (ppm) %RSD I INTEGRATIONS ttl- 82 #3 REREAD REDIG A 'i ___Ag ___A1 . __ As Ba. ___Be Ca . ' Cd \__Co ' _Cr ' ___Cu ___Fe ___K " MO . ___Mn __ Mo ___Na Nl ___Pb Sb ___Se ___Sn ___Ti . ___Tl ___V ___Y Zn 0.51628 4.336 24.10473 4.053 0;51862 4'.397 0.50310 4.596 0.51S37 4.460 24.44085 4.230 0.51001 4.593 0.49901 4.342 . 0.52233 4.664 0.50869 4.340 23.43742 4.496 25.08101 3.728 24.14282 4.103 0.51064 4.523 0.52987 4.710 24.62598 3.821 0.51286 4.701 0.49955 3.834 0.51550 4.017 0.50621 3.688 0.52684 4.176 0.53398 4.579 0.51040 4.563 0.52755 4.561 167864.67187 3.688 0.51505 4.323 0.50312 23.59986- 0.50845 0.48942 0.50209 23.91460 0.49748 0.48644 0.50777 0.49531 22.34784 24.56129 23.60389 0.49732 0.51198 24.04052 0.49860 0.48959 0.50158 0.49494 0.51561 0.51966 0.49826 0.51291 171626.00000 0.50239 0.50358 23.48336 0.50267 0.49008 0.50212 23.77580 0.49551 0.48656 0.50876 0.49658 ' 22.81022 24.52130 23.53836 0.49729 0.51925 24.12574 0.49927 0.48743 0.50561 0.49594 0.51271 0.52005 0.49568 0.51442 171249.00000 0.50200 0.54213 . 25.23096 0.54475 0.52980 0.54192 25.63216 0.53704 0.52403 0.55046 0.53418 24.65421 26-. 16044. 25.28622 0.5373.2 0.55838' 25.71166 0.54070 0.52163 0.53930 0.52776 0.55219 0.56221 0.53725 -0.55533 160719.00000 O.54077 151 DUP050307673 Page: 18' LANCASTER LABORATORIES Run Name: 9627404T61 Tube: 17 CCB 09/30/96 13:55 INSTRUMENT ID: 05478 ELEM __ Ag ___A1 __ As Ba Be ___Ca -- Cd :__Co __ Cr ___Cu Fe ___K __ Mg ___Mn __ Mo ___Na ___Ni Pb __ Sb ___Se ___Sn ___T i ___T1 ___V ___Y ___Zn . AVG INTEGRATIONS (ppm) %RSD #1 82 #3 REREAD REDIG 0.00079 50.04 0.10997 18.01 0.00177 26.97 0.00051 31.39 , 0.00065 23.82 0.17404 15.16 0.00040' 43.08 0.00107 34.33 0.00078 25.41 -0.00059 55.65 0.09262 18; 04 0.07428 13.38 .0.11816 22.51 0.00025 46. 13 0.00197 51.68 6.18591 19.80 -0.00017 142.0 0.00095 100.0 0.00322 59.66 -0.00030 262.7 0.00206 43.83 0.00073 23.65 0.00435 71.19 0.00038 44.62 171205.32812 0.179 0.00093 10.58 0.00100 0.12973 0.00226 0.00066 0.00079 0.20008 0.00036 0.00148 0.00083 -0.00033 0.10623 0.08524 ' 0.14344 0.00037 0.00302 0.14543 0.00004 0.00164 0.00484 0.00061 0.00285 0.00089 0.00405 0.00056 170850.00000 0.00098 . 0.00104 0.11007 0.00173 0.00054 0.00068 0.17473 0.00059 0.00095 0.00096 -0.00049 0.09766 0.07179 0.12063 0;00024 0.00191 0.19486 -0.00011 0.00134 0.00372 -0.00067 0.00107 0.00074 0.00758 0.00021 171384.00000 0.00099 0.00033 0.09011 0.00131 0.00034 0.00048 0.14732 0.00025 0.00077 0.00056 -0.00097 0.07397 0.06582 0.09040 0.00014 0.00098 0.21742 -0.00043 -0.00013 0.00109 -0.00086 O.00225 0.00055 0.00141 0.00038 171382.00000 0.00081 15 DUP050307674 Furnace Data 15S DU P050307675 LANCASTER L A B (3 RA T Q R I E 5 GRAPHITE FURNACE ATONIC ABSORPTION BATA REVIEWED BY: DATA VERIFIED BY DATA I'JUi NAME;. AC0&B3 CCRAT RON NAI'lEs . 962(3'301F04 ANALYST;:. 114 -INSTRUMENT NO: &47B4 BKO CORRBZ ELEMENT: AS 154 Conee*n Vrra*b ion is uvs&d "bo a 1 uabj. I *>o i. => < *\\ j. b ? cl-f calX tor-a*fcicm r-ane. w i 'Ll"! i n DUP050307676 RUN NAMES 96869011-4 PAGES :i ANALYST: 114 TUBE: SAMPLE S0 1 09/84/96 21 s09 Cl. ASS I MOL. /WT 0 AUG<DDb> jefcpp AMG sbs 1.16.00 11.6 -0.001 LANCASTER LABORATORIES INSTRUMENT ID: 4784 GT AA ELEMENT ; AS FMOL.. DF BATCH NUMBER 01 BURN 1 BURN 2 -0.868 "-0.001 TUBE:: SAMPLE 310 2 09/84/96 213 13 Cl. ASS I MCU.../WT 8 AUG < ppb> *RPP AMG abs 9.7900 5.4 0.027 FMOL. F BATCH NUMBER 01 BURN 1 BURN 2 0. 026 0.029 TUBE: SAMPLE sae 3 09/24/96 21 s 17 Cl. ASS TMOL/WT 8 AUGtppbT XRPP ft V (3 &. s 81.0800 7.3 0.057 FMDL DF BATCH NUMBER '0 1 BURN 1 BURN 2 0.054 0. 060 TUBE: SAMPLE S40 4. 89/24/96 21:21 Cl. AS*; IMOL/WT 0 AUG<ppb) JtRPD AMG aba 43.2608 5.6 0. 124 FMOL DF BATCH NUMBER 01 BURN 1 BURN 8 0. 129 0. 119 TUBE: SAMPLE S60 5 09/24/96 21:25 Cl. ASS TMOL/WT 0 AMG<ppb) I*RPD AMG aba 59.7100 8.3 0.164 FMOL DF BATCH NUMBER 01 BURN 1 BURN 8 . 8.Ifl8 ~8.167 TUBE: SAMPLE S60 6 09/24/96 2129 CLASS TMOL/WT 8 M b> JiRPP AMG abe 60.6700 0.9 0.246 FMOL. `1>F BATCH NUMBER 01 BURN 1 BURN 2 0.850 0.847 TUBE s 7 89/24/96 21 i: 3 4 A SAMPLE CL ASS TMOL/WT FMOL. DF BATCH..NUMBER ICV 0 &1 ) AMG <ppb> flRI-'D AMG a b s ' 53.4700 1.0 0. 164 BURN I. 8. 163 BURN 8 8. 166 ' , j. ^RECOVERY = 106.9 J. v> DUP050307677 RUH NAME s .9626901F04 PAGE s ANALYSTS 114 TUBE s SAMPLE 1CB 6 09/24/96 21s 36 Cl ASS !" a AVG<pb> *RP AMG abs 1.6008 76.6 8.002 LANCASTER LABORATORIES INSTRUMENT IDs 04724 OF AA ELEMENT.; AS FVOL DF BATCH NUMBER 8 1 . BURN 1 BURN 2 0. 005 -0.000 TUBE s SAMPLE CRA 9 09/24/96 Els4? Cl ASS IVOL/WT 0 FVOL DF BATCH NUMBER 8 1' AVGOsobJ ZRPD AVG abs 12.4100 1.0 0.036 TUBES 10 SAM PL. E CCV 1 09/24/96 ai4& Cl ACC #$ % 8 BURN 1 BURN a 0. 036 8. 036 ........... .............. ... ,.j ~ .. -- ~ FVOL DF BATCH NUMBER 8' 1 AMD <pob> ZRPD AVG'abs 42.3900 1.7 0. 130 BURN 1 0. 131 BURN 2 8. 120 /RECOVERY = 106 .0 ' TUBES 11 SAMPLE C.CB. 1 . 09/24/96 21s 58 Cl. ASS I VOL./WT 0 ..... . . . .. .......* *' ~ " - . -- -- -* -- FVOL ]>F BATCH NUMBER 8 ' 1 AVG(ppb) ZRPD AVG abs 1.0600 17. 6 0.081 BURN 1 BURN 2 0.001 0. 000 TUBES 12 SAMPLE PBWA 09/24/96 Cl ASC x ax a Is 5 4 JVOL/WT 180 * ; *' * *........ FVOL 100 * ........................ -------------- DF BATCH NUMBER 1 962661056801 / | . AVG <ppb) ZRPD AUG abs BURN 1. BURN > Sf-^ 1.3000 129.6 0.001 "07006. ~0.002 RR D _'I " TUBE;; 13 SAMPLE PBW Pr 09/24/96 21;;59 Cl ACS 3 VOL/WT 100 AVG (ppb) y-RPID A MG abs 21.4400 0.3 8.064 /.RECOVERY = 180.7 FVOL DF BATCH HUMBER' 100 1 962661056007 BURN 1 0.864 BURN 2 ~0.064 .............................................. '........................... " 15 tf DUP050307678 RUN NftllE's 9626901F84 PABE; 3 ANALYSTS 114 TUBE a S()*+,-. /5 01) 14 09/24/96 22 s 03 Ci. ASS rvoi./WT iMUHHcr. 1 AVG (ppb) 42.120 /RPD 8. 4 AMD '<& O*:i 0.129 LANCASTER LABORATORIE S M !"# $%&'% OF Aft ELEMENT AO FVOL 1 DF BATCH HUMBER 1 968661056001 BURN 1. . BURN 8 0. 127 8. 131 RE. RD TUBEs IS SAMPLE LOSW h 09/24/96 22s07 234 k5 666 HVPL/Mf -in:-Ax- 1 789:B ; <=> 60.77(30 StRPD 1.3 AVG abs 0.187 /RECOVERY 93. 2 FVpl. 1 ' Dl- BATCH HUMBER 1 968661056001 BURN 1. 0. 169 BURN...8 0. 166 TUBES. 16 09/24/96 22s 12 SAMPLE * 256X205 Dnh ?? CLASS 1WL/UT 100" AVG < ppb) *RPD AVG abv> 1.2700 100.7 0.001 FOOL DF BATCH HUMBER 100 1 962661056001 BURN 1 BURN EE RD 0. 004 0. 001 17 09/24/96 22i; 16 SAMPLE CLASS TVDL/MT 2563205 'feRPtSSp* A 100 ftWLlBJEteJL #RPP AVG afas 19. 1300 ~ 0 . 6 5~. 0S7 /RECOVERY' - JH&rZT <3>H*S>M iOa 1'^ TUBES. 16 _E 06 09/24/96 22320 Cl. ASS IV01../U1T ** 100 AVOCopb) /RPD AVG a Os 0.6700' 99.7 --0.001 FVOL PF BPITCH NUMBER 100 ' I 962661056001 BURN 1 07(957 BURN 8 0.057" ' FVOL 100 _ BATCH HUMBER 1 962661056001 BURN I. BURN 8 RE R 0.001 -0.002 U'UBEs. 19 Sk@ACD 2563886 Cl. ASS JV01./MT 6 . 3 00 AVG < ppb) JtRPD. AVG aba 10.9600 8.0 0.057 /-RECOVERY 94. 6 FVOL DF HATCH HUMBER 100 1 962661056081 BURN I. 0.057 BUSS J? (7(356 DUP050307679 RUN NAMES 9626901F04 PAGEs /. ANALYST: 114 TUBE*. 30 SAMPLE assies? .. 09/84/96 22 s 9 ' C:i. ACC 3 VOL /WT **.*** EF; AUG (opb) I4RPD AUG a ha 0~.' 3300 858. S' -8.80S LANCASTER 1I..ABORATOR 1ES INSTRUMENT IB: 04724 OFA A ELEi'l: ENf.: AS FUOL DF BATCH HUMBER "l00 i 968631856001 BURN I. BURN 8 SR RB ~ 0.880 -8.003 iTUBE: 81 SAMPLE 8533807 , 09/84/96 82 s33 Cl. ASS 3 UPt /U)T A>: 100 AUG <ppb) *RPP AUG alas "19.1300 0.1 0.057 FUOL I>F BATCH NUMBER 100 1 968631056001 BURN I. 0.857 BURN 8 0.057 ^RECOVERY 95.9 TUBE# 8 SAMPLE CCU 2 89/84/96 8:;33 Cl. ACC 3UOL./WT 0 AUG(isob) JSRPD ' AUG abs 41.9000 8.3 0. 183 tfRECOUERY = 104.3 FUOL BF BATCH NUMBER 81 BURN 1 0.186 BURN a 8. 130 TUBE s 83 SAMPLE . CCB a -09/84/96 88s48 Cl. ASS 3UDL/WT FUOL PF BATCH NUMBER 8 01. AUG < oob) yCRPP AUG aba 1.8880 31.4 0.80.1 BURN 1 BURN 8 -8.000 "5.001 TUBES 84 SAMPLE 8533803 89/84/96 82s46 - Cl. ACC 3VOL/WT . .tsM^KK-*; 108 "Sv / \ AUG < i-job) . y.RPD AUG ain 8.4808 163.9 -0.001 FU.QL. 1)F BATCH HUMBER 18 1 968631856057 BURN I. BURN -Q RR RD 0.008 -5.003 TM" TUBE s 85 09/84/96 SSiiSfl SAMPLE Ct. ACC 3 UDL/WT 8533803 CrS^Sp, *A 100 FUOL PF BATCH NUMBER 100 1 968631056001 AUG (pub) %RPI> AUS3_abs 80.4308 1.8 0.061 BURM_1 0.061 BURM__8 87068 ^RECOVERY = 108.4 . 158 DUP050307680 RUN NAME! 9626901F04 PAGE J ANALYST s 134 i..k m c ks Gf . k t.. k ; o r k H o r i e s INSTRUMENT ID! 64724 OFAA ELEMENT: AS TUBE t 86' SAMPLE X* 25dKjj>B9 09/24/96 22 s54 Cl ASS !l VOL/WT u** 3.00 FVOL DF BATCH NUMBER 100 i 962661056001 V/\ AVGLttPb) JiRPD AVG cii>-i ' BURN. 1. BURN ? ' RR Rj> /\ 1.5300 24.2 0.002 0.001 0.003 ___ ___ TUBES 27 SAMPLE 2563209 09/24/96 22s56 i. ACC 3 Uf.iL/MT UA- 100 AVG <ppb) #RPD AVG abs 20.0900 0-7" 0.860 JCRECOVERY = 92.6 FVOL. DF BATCH NUMBER 100 1 9626610560& 1 BURN I. ' BURN A 0.060 0., 060 TUBfcs aa SAmA-IJ ` 09/24/96 23 :0.1 Cl. ASS' TVOL/UT . 2563ap9 lbfC>3l>i> D-it*3 00 FVOL 100 DF BATCH NUMBER 1 962661056001 U/ \ AVGLp&b) -StfRPP AVG ai>-* y \ o.se 25.6 . 0.000 BURN 1 BURN - 2 RR RD 0.001 -0.000 TUBE s 29 SAMPLE ' 09/24/96 23 8 07,' Cl. ACS I VOL/NT 2583209 ftft'VSbtjfl ' P-x*; 100 ' FVOL. 100 1>F BATCH NUMBER 1 962661036001 AVG < nob) ffRI-'D 'AVG abs BURN I. 19". 5000 2.2 : 0.056 "0.057 BURN 2 0.059 ^RECOVERY = 97.5 TUBE! 30 09/24/96 23s I I. SAMPLE ^ ,, 163206' t}ftS'3DS Cl. ACC 1 JVOL/WT 10 AVG < ppb> SiRPD AVG alts 40.9100 0.5 0. 1 FVOL DF BATCH NUMBER 100 1 962661056003 BURN 1. BURN 2 RR R 0. 126 0. 125 TUBE 31 SAMPLE Z27.2ZZ 09/24/96 23s15 ci ks s :i voL/uiT -0 f Ko L DF BATCH HUMBER 01 ~ AVG <ppb> KKPP AVG afas 59.0900 50.4 " " . 162 BURN 1 0.161 BURN 0. 163 ^RECOVERY HOT APPLICABLE 159 DUP050307681 RUN NAMEi 9686901F04 PAGEs 6 ANALYSTS 114 LANCASTER LAOORATORIES INSTRUMENT IDs 84724 OFAA ELEMENT.; AS TUBE s 32 09/24/96 23 s 19 SAMPLf/i CL ASS If VOL/WT 258320* JV APG<ppt>) 100 XRPD . APG &b:> 4.6908 42. 1 0.013 MNu ; e s 33 . ' SAMPLE 2563218 09/24/96 8 32 4 Cl. ASS If VOL/WT 180 FPOL DF BATCH NUMBER 180 1 962661056001 BURN f. 0.017 BURN n 0.006 .. .. RR RD ___ ___ --------- -- FPOL DF BATCH NUMBER 180 1 962661056881 APG < pub) AHi-H) AV (3 cifcj.s- 2.2900 .6 8.067 BURN 1. 0.066 BURN 2 0. 866 ^RECOVERY = 67.0 TUBE s 34 SAMPLE CCP 3 09784/96 33 86 CL ASS IP01/NT 0 APS < ppb> SRPD APG abs 4.1.7700 0.3 0. l'6 ^RECOVERY =104.4 FOOL DF BATCH NUMBER O1 BURN 1 0. 126 BURN J> 0.186. TUBE s 35 SAMPLE CCB 3 09/24/96 23 s32 CL ASS If POL/WT 8 r APG(pBb) /RPD APG abs . 1.6688 33.4 0.803 FPOL DF BATCH NUMBER 01 BURN 1 BURN 2 0. 004 8.081 TUBEs 36 SjlfeLE. _ 09/24/96 23s36 Cl. AOS :i VOL/WT 2S636C3 Dnn^. **** 100 APG (pub? flRPD ftPO ab-,s 0.5500 90.1 -0.001 FPOL. DF BATCH NUMBER 100 1 968661056001' BURN 1 BURN 2 RR RJj) 0.000 -0.002 09/24/96 23s4 CL ASS IIPPL/UT P'Pi'o'.w'ft .1.00 FPOL DF BATCH NUMBER 100 1 962681056001 APG-(ppb) flRPD APG abs . BURN 1 80.3000 0.6 0.861 8,,061 BURN a . ~0.61 ^RECOVERY = 101.5 A DUP050307682 RUM NAME: 9626901F84 PAGE: 7 ANALYST: 114 TUBS a 36. SAMPLE P?^f384 09/24/96 23s44 f:|. ASS IVOL/UT 3 f:HFi AVG(ppb> /RPD' A VC A Ij ;> 1.9000 37.0 8. 003* LANCASTER' LABORATORIES INSTRUMENT IDs 04724 GE Aft ELEMENT.'. AS FVOL DP BATCH NUMBER 100 1 9626618S6001 BURN i. BURN fj RR RD ' *0.005 0.002 TUBE: 39 SAMPLE 2563624 89/24/96' 23:46 Cl. ASS IVOL/WT Pi 18 AVG < Op b) /RPD AVG aba 19.7680 1.1 0.059 FVOL DF BATCH NUMBER ~188 . 1 962661856001 BURN I. 0.059 BURN H 0.060 /.RECOVERY * '69-3 AA 'TUBE: 40 09/24/96 23s52 SAMPLE ,, Cl. ASS 3 VOL/NT FOOL DF BATCH NUMBER ^ 2563BC5 " **** 180 100 1 962661056001 AVG (p&b) /RPD AVC ab-> BURN L BURN r> RR RJD ~ 1.57(30 55. 7 0-002 0.084 0-000 ____ ___ TUBE: 41 09/24/96- 23s5 SAMPLE Cl. ASS IVOL/UT 2563625 ftTSfMWH ft* 108 FVOL DF BATCH NUMBER 100 1 962631056083. AVG < ppb) /RPD, AVG abs 20.0300- 2.4. -0.062 BURN I. ' 0.061. BURN 2 0.064 /RECOVERY 96.3 TUBE s 42 SAMPLE 2533686 09/24/96 88:: 08 CLASS IVOL/NT' . ***** 108 FVOL 100 DF BATCH NUMBER 1 962631056001 AVG <ppb) /RPD AVG abs BURN I. BURN 8 RR RD A 0. 7388* 116.9' 0.000 8.002 -0.808 43 09/25/96 00s84 SAMPLE 01. ASS I VOL/NT 2563026 T!)PA\SfN A- 180 AVG (ppb) /RPD AVG abs 81.4500 2.5 ,8.064 /RECOVERY = 107.2. FVOL DF BATCH HUMBER 108 1 968681056001 BORN I. 0.863 BURN 8 0.066 DU PO50307683 PAGE: ANALYST : 9626901F04 6 1.14 mtuL 2583627 i 09/35/96 80:061 Sftfifl MASS 3VfiLZMT *** 100 AVG<BDb> J4RPD AOQ. tfea. 2.0680 12.6 8.084 LANCASTER LABORATORIES INSTRUMENT IDs 84724 OFA A ELF MEN l' : AS F VOL 100 I> F...... BATCH ..n u m; e r 1 962661856801 PVJlJH t BURN.2 LB. BJ>. 0.004 0. 083 09/25/96 08 3 13 OKHCimFC| sM. I.VOL/WT A 180 A VG.ifi.fi b> JSfayS. am at.s 22.6680 4.9 8.069 /RECOVERY = 104 .0 108 ' ~1 ^62661056081 BURN 1. 0.066 BURN 2 0. 071 IPPMQR S6 mmsM, CCV 4 09/25/96 00:: 1.7 c.i. A IVOL/WT 8 FOOL F BATCH NUMBER 81 AVG < Di3b> /RP 0VG_abs BURN _i BURN 2. 'I 42.6300 2.4 0.131 8. 133 , 0.126 /.RECOVERY 186 .6 iyi&i. 47 09/25/96 00 * 2 |. A TkUVWX Cl AOS TVOL/0T FVOL I>F BATCH NUMBER CCB 4 8 81 AVGlPJB_b> BPD AVG &bs 1.9908- 10.6- 0.804 BURN 1 . BURN 2 0.083 0. 884 jum' 4,a. 0.9/25/96 00:: 5 g j -ASo TVQL/MT . 3 88 Effi; ...ML. ; ki5 h .n u m; e r 180 1 962601056002 A AVC3U3.RbJL SBPfii AVO &!.!:> 1.9300 3.0 0. 003 aysfcMi MMN..J1 s b m 0.004 0.003 A IMBJLl 49 09/25/96 00a29 gffl&kl. PBW s l q s ii lymvwi A-;; 100 FOOL i>F BATCH NUMBER 100 1 962601056882 ay.siR.BM,. asE.fi. ave ab* 22.6400 1.6 0.869 ; u r n i. 8.06:3 ; or n n 0.070 /RECOVERY 104.6 T6 TT i<J DUP050307684 LANCASTER LABORATORIES GRAPHITE FURNACE ATONIC ABSORPTION JC. BATA REVIEWED BY j$>(rW tli*KBATA VERIFIED BY: BATA F3 LIT HAMEs f*BP SB 13 RUN NAME: 9S26901F03 ANALYSTS -Cft INSTRUMENT NO: 63312 BKC> DORR: BZ ELEMENT: PB Concent-ration is used to evaluabu if s.am >? I. ealibr-atiori vango. kYZ within 16o DUP050307685 RUM HAUL-:!: 9626901F03 PAGE s 3 ANALYST: 60 U-lMCftG rii LAOORATUR11 INSTRUMENT IBs 0301! Gi-AA ELEMENT:; !?B TUBE: 1 SAMPLE S0 '09/24/96 20:40 Cl. ASS IU0L/UT 0 FUfU.' BE -BATCH NUMBER 01 AUG < DDb) 5SRPD AVG abs BURN 1 BURN 2 0.0000 0.0 0.010 . 0.012 0.009 TUBES SAMPLE S3 2 09/24/96 80s 153 Cl. ASS :r v o l /u t 0 FUGL PF BATCH HUMBER 01 TUBE: SAMPLE S9 AVG<ppb> 3.0000 *RP 4.4 AVG abs 0.025 " BURN 1 0.025 `I BURN 2 0.026 \ 3 09/24/96 20 a 50 r CLASS IVOL/WT FUOL PF BATCH NUMBER B 0 \1 AVGCoobJ SiRPD AVG abs - BURN- 1 BURN 2 9.0000 .5.6 0. 005. 0.000 0.001 TUBE : SAMPLE SIS . 4 09/24/96 21s03 ' Cl. ASS TVOL/WT B FVOL PF BATCH NUMBER 01 AVGtppb) XRPP AVG abs BURN 1 BURN 2 15.0000 1.0 0.149' , 0.147 0.151 TUBE: SAMPLE S30 5 09/24/96 21r.0O CL ASS TVGL/UT. * FVOL 0 D.F BATCH NUMBER 1 AVG (nob) . JiRPB AVG abs 'BURN 1 BURN 2 30.-0000 0.7 0.270 ' 0.869 0.271 ' TUBES SAMPLE S60 6 09/24/96 21s 13 Cl. ASS .1 VClL/WT 0 AUG < uob) JiRPD AVG abs 60.0000 0.5 0.462 FVDL PF BATCH NUMBER 0-1 BURN t BURN 2 0.46L 0.464 t TUBEs SAMPLE icy 7 09/84/96. 21 a 17 ' Cl. ASi:: iv o l /u it 0 f vo l pf [ \; k 5 ]^_; e r 01 AVG<ppb) gRPD AVG abs 'BURfl 1 19.9300- 0.2 0.191 0.198 BURN 2 .0.191, ^RECOVERY 99.6 RUN NAMEs 968690IF03 PAGES t? ANALYSTS ' 68 TUBE s SAMPLE I CD 8 09/84/96. 81s 88 CLASS IVCiL/WT 0 flW(DBb) SURF'D AVG abs 0.480S 99.9 0.004 l..ANCAOTGR LABORATORIELi INSTRUMENT IDs 03618 OFAA ELEMENT;; PB FVOL DF BATCH NUMBER. 01 BURN 1 BURN 8 0.007 0.000 TUBES i~AHPLE CRA 9 09/84/96 81s 26 CL ABC IVOL/UT .0 AVG < DDb>' ySRF'D AVG abs 4.8900 5.8 0.037 FVOL DF BATCH NUMBER 01 BURN 1 BURN 8 0.036 0.038 TUBEs 10 SAMPLE 7.22Z2Z 09/84/96 81u31 CL ABC JVOL/WT 0 AVG<Db> JiRPD AVG abs 83.8800 3.7 0.819 FVOL DF .BATCH NUMBER 01 BURN 1 BURN 8 0.813 0-884 TUBEs 11 SAMPLE CCV 1 09/84/96 81s 36 CL ABC IVOL/WT 8 AVG <ppb) %RPD AVG abs 83.9800 1.7 0.884 FVOL DF BATCH NUMBER 01 BURN 1. 0.881 BURN 8 0.886 sSRECOVERY 95. 7 TUBEs 18 SAMPLE CCB 1 09/84/96 21:; 41 CL. ACC :i VOL/WT 0 * .................. - *---------------- ----------1--- FVOL DF BATCH NUMBER 01 AUG (Mb) SSRPD AVG abs 0.5900 50.8 0.005 BURN 1 BURN 8 0.007 8.003 --------- '...............................-------v ....... ..... .. ....... . . .. . ... ... .. . ........ ... ,, . . TUBEs 13 SAMPLE 09/84/96 81 s4S CL ACL; JVCiL/WT 856316fg^Z2Z2 . Uk ih ; 50 FVOL DF 50 1 _________ BATCH NUMBER 9686-35715001 V _ ............ .. AUG < DDb) XRPK AUO ain'a 8.8900- 0.5 0. 075 ............. ............... .. ..... ....... . .... `........- . . . BURN L 0-875 X BURN 8 0.875 HR RD ~VA - 165 DUP050307687 RUN NAME: 9626901F03 PAGE: 3 ANALYSTS 66 TUBE: 14 SAMPLE 258316 09/24/96 21:5 - Cl. ASS i VOL/WT ^u -.-k -mk Am s AVG<p&b> XRPD AVG abs 19.3906 4.4 0.167 /RECOVERY = 56.5 1.. A NO A :n r< 1.. H at f< A T U K .1 E INSTRUMENT IP: 03812 OFAA ELEMENT : PB FVOL DF BATCH NUMBER 50 1 962635715001 BURN I. 0. 193 BURN n 0.161 TUBE: 15 09/24/96 21 sS'i SAMPLE CLASS JVPL/WT 2563166 t_ ; f'XZZ, *** 50 V AVG < ppb) /RPP AVG aba H. 4700 5.1 -0.021 FVOL ]>F BATCH NUMBER 5 T 962635715061 BURN l BURN 2 RR RD 0.022 0.020 ___ TUBE; 16 09/E4/96 21aS9 SAMPLE Cl. ASS 1'UGL/WT 2583166 ZI2ZZ2, , VHHKX-tw . 50. AUG t ppb> /RPP AUG abs 14.4300 3.1 3.143 /RECOVERY = 59.& FVOL 50 DF BATCH NUMBER 1 962635715001 BURN 1 0.14$. - BURN 2 0. 140 TUBE; -17 SAMPLE ' 25B3166 ... 09/24/96 22:0'( . . CL ASS TVPL/NT R*** .50 . FVOL 50 DF BATCH NUMBER 1 962635715001 V AUG (ppb) /RPP AUG ab* BURN i. BURN 2 F<ft RD 14.3000 0.3 0.142 0. 141 0.142 W| ___ TUBE; 18 09/24/96 22s09 SAMPLE ^ CL ASC IVOL/WT 2563166 Z22ZZ2 Rot 50 ' FVOL DF BATCH NUMBER 50 l 962635715081 AVG (ppb) /RPP AVG bs 26.8600 0.7 0.247 BURN L 0. 245 BURN 2 0.248 /.RECOVERY = 62.9 TUBE: 19' SAMPLE , 2583623^ 09/24/96' 22:13 CL ASi:: 1 VOL/NT ** 50 AVG(ppb) /RPP AVG &b- 26. .1160 6.1 0.241 FVOL 50 DF.. BATCH NUMBER 2 91.2635715001 BURN 1. BURN r> RR RD 0.23(i1 0.251 . ........... _ ....________________ DUP050307688 RUN NAME s ' 9626901F83 PAGE . / ANALYST s 60 TUBEs 28 89/24/96 22:10 SAMPLE CLASS - :iVOL/WT 2503623 3Z2L22' * A5 AVO < ppb> flRPP AVG abs 4470200 a. 3 0.371 ^RECOVERY == 93.6 LAN GAO'TER '..ABO R1-1T OR 1E INSTRUMENT IB: 83012 OF A A ELEMENT.: PB FVOL I)F BATCH NUMBER 50 ' 96635715001 BURN 1 0.365 BURN 0.377 TUBES 1 09/24/96 22s3 SAMPLE . CL AGS IVOt/WT 2533000 '7'%7,-^prr- *# 50 V ` AVG (ptab? /RPP A VC ai>s 2.5000 1.0 0.021 FVOL PF BATCH HUMBER 50 1 962635715001 BURN I. 8.021 BURN il Rf 0. 021* RD TUBE*. 22 SAMPLE 2533808 09/24/96 2:27 C:l. ACC IVQL/WT A* 50 AVG t ppfa? XRPD AUG abs ~"l5. 1100 "~0.1 8.158 FVOL 50 ,, 1>F BATCH NUMBER 1 962635715081 BURN 1 0.150 BURN 3 -0.150 ^RECOVERY = 63.0 TUBEj. 23 SAMPLE CCV ~ 09/24/96 22s 32 till ACC 1 VOL/UiT FVOL DF BATCH NUMBER 001 AVG < ppb) *RPD AVG abs ~2479900 0.6 0.232 BURN 1 -0.231 BURN 2 8.233 ^RECOVERY = 100.0 TUBE s 24 SAMPLE CC; " 2 ' 09/24/96 22s 37 CL ACL: JVPL/WT 0. FVOL |>F BATCH NUMBER 01 AVG (ppb) #RPP 0.0900' 37.7 * AVG a fas 0.800. BURN 3 . BURN 2 0.010 07*006 TUBEs 25 SAMPLE PBW @9/24/96 22 s 41. CL AGO TVOL/UJT '*** 100 AVG (ppb) #RPD .AVG aba 0.6780 5.7 0.086 FVOL JDr.. BATCH HUMBER 100* 1 962601056001 BURN L UJRN 2 RR~ ED 8.005 3.806 DUP050307689 RUN NAME: 9626981F03 PAGE s 5 ANALYST: 68 TUBE s 26 SAMPLE PBW 09/24/96 ii : 4& CL ACC TVOL/WT ?: -i!'A .180 AUG < DDb) 21.4108 36RPP 1.4 AUG abs 8.204 ^RECOVERY = 107.(3 1..ANCAC f EA L A0iSA A TGRIE INSTRUMENT IPs 03618 GFAA ELEMENT;: PB FUOL F BATCH NUMBER 180 1 962681056001 BURN t 0.281 BURN r> 0.206 TUBE a 27 SAMPLE LCSW 09/24/96 22 s SB ' C:l ASS TUQL/WT :;w k *k k * l AUG<ppb> ffRPD AUG ab-:> 20.8300 1.1 0.193 FUOL i>F BATCH HUMBER 11 962661056001 BURN ). - BURN -7 RR RI) 0.197 8.200 TUBE a 28 SAMPLE LCSW f\ 09/24/96 22555 C(. ASS TUPL/WT 1 AUG Cppb> KRPP AUG aba 42.6500 3.5 0.357 /.RECOVERY = 109.1 FUOL. PF BATCH HUMBER 1 1 962681056001 BURN i. 0.366 BURN 2 0.349 TUBE 5 29 09/24/96 23 s08 SAMPLE r Cl. ASS JVOL/WT 2583285 DRA5S 100 AVG<ppb> StRPP AUG <sU>,: 1.8400 44.4 8.009 ' FUOL DF BATCH NUMBER 188 1 962681056001. BURN I. BURN 2 RR LA) 8.812 0.086 TUBES 38 09/24/96 23s04 . SAMPLE Cl. ACC TUOL/WT 2563285 T3?,h'o5fY <}KflK . 188 FUOL 1)F BATCH NUMBER 100 1 9432661856001 AUG < ppb> XRPP AUG abs . BURN t. 13.3880 0.3 8.132 8`.131 BURN 2 "0.132 /RECOVERY =61.7 TUBEs 31 09/24/96 23309 SAMPLE Cl. ACC TUOL/WT 2363206 fcftAAS) #*** 100 FUOL I)F BATCH HUMBER 108 1 968661056001 AUG < ppb) ZRPD AUG a bn BURN 1 PURH 2 RR Rp 0.9200 18.3 0.08a" 0^ 007 0T003 RUM NAMES 9626981F03 PAGEs 6 ANALYST s' 66 TUBES 32 SAMPLE 2563206 09/24/96 23s14 . CL ASS!: IWL/MT ' *KA* 106 AUG(ppb) /RPP AUG abs 14.5680 ' 1.3 8.144 sIRECQUERY = 6.. 2 LAN0ASTER LAB0!;ATUK iE3 INSTRUMENT 'IDs 03612 GFAA ' ELEMENTPS FUOL PF BATCH NUMBER 106 1 962661856001 BURN 1 0.1.43 BURN 8 8.146. TUBE; 33 89/24/96 23s16 SAM PL E CLASS 1UOL/WT 2563207 'tfrA bt> .** 188 AUG (ppb) XRPD AUG ab-* 1.4900 6.5 8.B13 FUOL PF BATCH NUMBER 180 1 96266105680.1 BURN I. BURN r; RR RP 0.013 0.012 TUBEs. 34 09/24/96 23 s23 SAMPLE _ CL ASS 1UOL/UJT FUOL 1>F BATCH NUMBER ` 2563287 BT'.A L>Dh ** ' 108 * 100 1 96'26ai056081 AUG(ppb) XRPD AUG abs BURN 1 .13". 7500 5.0 0.136 0.141 BURN 2 8.130 jCRECOUERY -- 61.3 TJJBEs 35 SAMPLE CCU 3 , 09/84/96 23 s 27 CLASS TUPL/WT ". " '0 FUOL PF BATCH NUMBER 0 1 ' AUG(ppb) IKRPP AUG abs "86.0200 1.0* 0.840 BURN 1 0.830 BURN 2 0.248 ^RECOVERY = 104.1 TUBE; 36 SAMPLE CCB 3 09/84/96 S3s38 CL ASS TUCH/UT 0 AUG (ppb) *RPP AUG abs 1.0500 1.4 0.009 FUOL -3>F BATCH NUMBER 01 BURN 1 BURN 2 0.089 8.089 TUBE! 37 09/84/96 83!36 s kmp l e : ct. k`` :j l v o l /u i 2563206 DH34-S *** 100 AUG(ppb) XRPP AUG a by, i.1180" 6.6 0.009 FUOL PF BATCH.NUMBER 180 1 968661056081 BURN l BURN 8 RR RP 0.010 0.009 161- DUP0503 07691 RUM HAMEs 9626901F03 PAGE a 7 ANALYST: 68 t.ANCAS TEA I..AB0RATOR IE INSTRUMENT IDs 03612 OFAA ELEMENTS PB TUBE: 36 SAMPLE 2583286 09/24/96 S3s41 . Cl. AUS T'VOL/WT !; ): *:A>: 100 AVG (ppb) /RPD. AMS abs ' IS. 2400* 0. i 0.151 FVOL DF BATCH NUMBER 100 1 962681856881 BURN I. 0. 151 BURN H 0.131 /.RECOVERY * 70.6 TUBE; 39 SAMPLE 2563209 89/24/96 23s46 Cl. ASS IVPL/UIT U*** 108 AVG (ppb) /RPD A VO ab-:> 8.0600 13.5 0.007 FVOL DF BATCH NUMBER 100* 1 962681056001 BURN t BURN 2 MR RD 0.000 0.007 TUBES '40 09/24/96 23a50 SAMPLE Cl A US': IVPL/WT 2503209 1&$v53T)Pi U*A* ~188 FVOL DF BATCH NUMBER 100 1 962601056001 Ave<ppb> /RPD AVG abs 15.2600 ' .0*6' 0.151 BURN 1 0.152 BURN P. 0.151 /RECOVERY 72.0 TUBES 41 SAMPLE 2503209 89/24/96 23a55 Cl ACC 1VOL/UT ** ' 100 AVG (nob? /RPD AVG ab* A 8.7400- 5.2 0.006 FVOL DF BATCH NUMBER 108 1 962681856881 BURN 1 BURN f> RR RD 0.006 8.006 _T TUBE s 42 SAMPLE 2583209 09/23/96 80s88 Cl. ACC 3'VPi/UT Dk k Ak 100 AVG(nub) /RPD AVG abs 18.9100 1.7 0.163 FVOL DF BATCH NUMBER 188 1 962681036001 BURN 1 0.165 BURN 2 "0.180 /RECOVERY - 94.6 TUBES 43 SAMPLE 2583209 BBSS 89/25/96 80s 8 4 C:l ACC !l VOL/UT R* *** 108 FVOL IF BATCH NUMBER 100 I 962681056801 AVG < ppb) /RPD AVG *<>:. 15.6588 1.9 "ii*. 153 BURN I BURN 2 ' 0. i57 0.153 RR RjD RUN HAHE s 9626901F03 PAGE s t\ ANALYST s . aa LANCASTER LABORATORIES INSTRUMENT ID: 03612 > GFAA ELEMENT; PB TUBES 44 SAMPLE ZZZZZZ 09/25/96- 00:09 CLASS JUCit/WT R***A* 0 AUGIonb) JiRF'P AUG &bs 30.9100 2.2 0.277 FUOL 0 PF BATCH NUMBER 1 BURN 1 0.272 BURN 2 .0.261 ^RECOVERY = MOT APPLICABLE TUBES 45 09/25/96 00:13 SAMPLE Cl. ACC It UOL/WT 563210 DBA'53 * it 3:41 *: * 100 FUOL . PF BATCH NUMBER 100 1 962661B560B1 XU > AUG < DDb) %RPD AUG A'o'i 1.9500 25.0 0.016. BURN 1. BURN 2 !'<R RP 0.019 0.014 ---- --------- , .... ................. . ....... ....... ...............*..... ... ..... . ... ..... ----- ;.......... . -- TUBE; 46 SAMPLE 2563210 09/25/96 00 a 16 Cl ACC :i UOL/WT 100 FUOL ,PF BATCH NUMBER 100 1 962661056001 AUG(ppb) *RPD AUG a bs ' BURN 1 BURN 2 15.0900 3.3 .0.150 0. 153 0. 146 ^RECOVERY' = 65. 7 -- ... --........ .. .. .............. . TUBES 47 SAMPLE CCU 4 ......... ... . . ...... . . . ....... ... 09/25/96 00;: 23 CL ACC :r u o l /w t 0 FUOL PI-' 01 -- BATCH NUMBER AUG < DDb) KRPD AUG abs 26.1600 0.0 0.241 BURN 1 0.241 BURN 2 0. 241 ^RECOVERY -104.6 TUBEs 46 SAMPLE CCB A 09/25/96 06s2? Cl. ASS JWL/MT 0 FVOL PF BATCH NUMBER 01 AUG < PDb) . KRPP AUG a bs BURN 1 BURN 2 0.6000 24.2' 0.007 . 0.006 0.000 TUBE ii 49 SAMPLE . asaaaas 09/25/96 00:: 32 Cl A Si:: I UOL/WT *** 100 FVOL PF BATCH NUMBER 100 i 962661056001 AUG <ppb> y.RPP AUG abs 1.0000 16-0 " 0.066 BURN 1, 0.007 BURK 2 RR RP 8. 009" ~ . -- .~1?1 i" ` ifllftffrtHK- 'r^J k* IX 4 14'- DUP050307693 RUN NAME: 9626901F03 akbc s 9 ANALYSTS 66 TUBE 5 SB. 09/25/96 00:37 SAMPLE ' Cl. ABU :fUOL/MT 2583823 BRpj'c*t>fis .100 L ft M C A(': L ft ft i f E A T O F: .1.1." INSTRUMEMT ID: 038x 2 GFAA !ILi .ME NT .! PB FUOL i?F BATCH NUMBER 100 1 962681836001 AUO (ppb)' 13.7408 StRPjD AUG a fas 1.9 ' 8.136 BURN I. 0.134 BURN r> 0.137 ; StRECOUERY = 63.7 TUBE:' SI 09/25/96 00*41 SAMPLE CL ACC IVGL/WT 2383024 BTSfi'SS #* 180 AVG<DDta) *RP AMG 0.9600 1-1 0. @08 FUOL DF BATCH NUMBER 100 1 962681056001 BURN 1. BURN 2 RE EI> 8.088 0. 008 ---- -.... TUBE s 52 09/25/96 00*46. SAMPLE Cl. ACC JVOL/WT 2503024 ^fi'SSpj ** 1.08 AVGCDDb) SttRPD AUG abs 13.4300 7.4 0. 132 StRECOUERY * 62. 4 TUBE s 53 09/25/96 80s 51. SAMPLE CL ACC 1UOL/WT 2563825 "feR A \ t> *** 180 Jr AUG <DDb) XRP AUG ab-:> 0.8500 10.2 0. 007 TUBE; 54 09/25/96 00 s 56 SAMPLE ' CL ACC If VOL /WT 2503025 ft IMP 'i t>pJ A 180 AUG (cmt>) WRPD AUG abs, 13.5800 0.2 0. 134 StRECOUERY 63. 6 TUBES 55 SAMPLE 2583026 09/25/96 01 J BB Cl ASS TVOL/WT ** 100 XV j AUG (ppb) JSRP.D AVG Ct f> 0.8600 14.7 0.807 FUOL ]>F BATCH NUMBER 180 1 962681056081 BURN L 0. 123 BURN 2 8.139 * ` * 1 ** " ** " .... * ** - " FUOL I>F BATCH NUMBER 100 1 962681056001 BURN l BURN 2 RR RD 0.008 0.807 , .......... ' *" * ..... ** *" ~ ~ -- FUOL 1>F BATCH NUMBER 188 1 962681856801 BURN 1 0. 134 BURN 0.134 ......... - - ~ .. ------------ FUOL JDF HATCH NUMBER 100 1 962681056001 BURN 1. BURN r> R R R1) 8- 086> 0.88a ---, RUN NAME : 96269B1F03 dkef :: : sc ANALYST: 66 gh; i: ; 56 SAMPLE _ 2533326 09/25/96 B18 0S PI. ABC i UCIL/UT ***A* 108 AUG < DPb) 12.6600 ?CRPD 1-7 AVG alas 0.124 ^RECOVERY = 59.0 I..MHC MUTER LABORATUKIE: INSTRUMENT ID; 03312 OP A A ELEMENT: PB FUOL. DF BATCH NUMBER 108 1 9626318560131 BURN t 0. 123 BURN 2 0. 125 TUBE 8 57'" 09/25/96 01s10 SAMPLE Cl. ASS JVOL/UIT 533327 D?^f\ 1C I * 100 AUG <-ppb> *RPP A VO *1>-a 0.7000 1.9 0.007 FUOL 1>F BATCH NUMBER 100 1 962631856881 BURN 1. BURN n RR RD 0.006 8.08? ---- ---- TUBE; 56 Skjklm 2S83fl27 09/25/96 01i:L4 5 l ks s iu o l /n t l A **A 100 AUG < ai3b) *RPP AUG abs 22.3980 2.9 0.215 SfiRECOUERY = 114.4 FUOL DF BATCH NUMBER 100 1 962631056001 BURN 1. 0.220- BURN n 0.211 TUBE; 59 SAMPLE CCU 5 09/25/96 01.: 19 CL AGS J UQL/WT 0 AUG < ppb) yiRPP AUG afas 26.0100 0.1 0.240 ^RECOVERY = 104.0 FUOL DF BATCH NUMBER 01 BURN 1 0. 24 BURN 2 8.240 TUBE; 60 SAMPLE CCB 3. 09/25/96 01;24 C:l ASS: TOOL. /NT 0 AUG < ppb? KRPP AUG 'abs 1.0500 5.3 0.009 FUOL DF BATCH NUMBER 0 '1 *i BURN 1 BURN 2 0.010 0.007 TUBE: 61 SAMPLE PBW 09/25/96 01s23 CL ACC IUQL/UIT :: K4r4i4<4Vo: 100 AUG <ppb) flRPP AUG abs 0.3500 23.5 0.007 FUOL IF BATCH HUMBER 180 1 962631056882 BURN !1 BURN RR RD 0.803 0.006 17- DU P050307695 LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION DATA RFVIEWED BY: DATA.VERIFIED BY Cflzffct DATA FILE NAME: 3E26811.RAT RUN NAME: 9626901F05 ANALYST: 68 INSTRUMENT NO: 04725 RKG C.ORR: B7 ELEMENT: SE Concentration Isr 'used to evaluate" 'If' earon'le resul ts are wT-FKin calibration range. 174- r.nv<95:lt!!.rp.:i:.--rfr^.K--Oft..y DUP0503 07696 RUN NAME: 9626901F05 PAGE: 1 ANALYST: 68 TUBE: SAMPLE SO 1 09/25/96 01 : 23 LASS 1YQL/WI 0 AVG(ebl. %RPD AVG abs -1.1600 24.9 -0.0.01 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 -0.000 -0.001 IUILLl SAMPLE S5 2 09/25/96 01:27 CLASS IVOL/WT *0 AVG/DDb') %RPD AVG abs 5.0700 5.4 0.015 FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 0.016 0.015 TUBE: SAMPLE. S15 3 09/25/96 01 :31 CLASS IVOL/WT 0 AVGfDDbl %RPD AVG abs 14.0800 0.1 0.043 FVOL DF BATCH NUMBER .0 1 BUrN__1 BURN 2 6.043 0.043 TUBE: SAMPLE. S25 4 09/25/96 01:35 CLASS IVOL/WT. 0 AVGToobl %RPD AVG-abs 22.7400 5 .4 0.065 f .v q l JD.F BATCH NUMBER 01 BURN 1 BURN 2 0.062 0.067 TUBE: SAMPLE S40 5 09/25/96 01:39 CLASS IVOL/WT 0 AVG %RPD AVG abs 38.8100 0.7 0.102 LV..Q.L. ...01 BATCH NUMBER 0 1< BURN 1 BURN ? 0.102 0.101 TUBE : SAMPLE S50 6 09/25/96 01:43 CLASS iYOL/WT 0 AVG/pobl %RPD AVG abs 49.2000 5.4 0.126 FVOL DF tJATCH NUMBER 01 BURN, 1 BURN 2 6.121. 0.131 TUBE: SAMPLE. ICV 7 09/25/96 01:47 CLASS I..YQL.iMI 0 AVG(DDbl %RPD AVG abs 19.2200 7.0 0.050 -- %RECOVERY =-96.. 1 FYOL ,,I)F BATCH NUMBER 0 '1 BURN 1 ` BURN 2 0.053 0.048 175 DUP050307697 RUN NAME : 9626901F05. PAGE: 2 ANALYST: 68 TUBE: SAMPLE ICB 8 09/25/96 01:51 ' CLASS IYOL/WT 0 AVGfoob') %RPD AVG abs -0.8200 45.2 0.000 1. ANCAS TER l. ARORATORI E INSTRUMENT ID: 04725 GFAA FtEMENT: SE FVOL OF... ; kx q h ...(J.Um; e .r 0 1 BURN 1 BURN 2 0.001 -0.000 TUBE: SAMPLE CRA ' 9 09/25/96 01:55 CLASS XYQLZWI .0 AVG(oobl %RPD AVG abs 4.1200 8.8 0.013 FVOL OF gATCH NUMBER 01 BURN 1 BURN 2 0.013 0.012 TUBE: 10 SAMPLE CCV 1 09/25/96 01:59 CLASS IVOL/WT o AVG(onbl %RPD AVG abs 24.2400 0.7 0.063 ^RECOVERY = '97..0 F.VOL OF BATCH NUMBER 01 BURN 1 6.063 BURN 2 0.06? TUBE: 11 SAMPLE CCB 1 09/25/96 02:03 CLASS IVOL/WT 0 ayg-CBabi i; h AVG abs -1.4100 16.4 -0.001 FVOl, DF BATCH NUMBER 01 BURN 1 . BURN 2 -0.001 -0.002 TUBEr 12 09/25/96 02:0.7 SAMPLE. P8W 2ZZZZZ CLASS IVOL/WT ******* 100 X\V AVG ( oobl 9SRPD AVG abs -1.4100 12.5 -0.001 FVOL OF BATCH NUMBER 100 1 962681056002 BURN 1 BURN 2 RR RD -0.001 -0.001 __ ___ TUBE: 13 SAMPLE ... PBW ft 09/25/96 02:11 CLASS im/wi 100 AVG ( gob ) %RPP AVG abs 70.4000 1 . 6 0.028 %RECOVERY 104.0 FVOl.. .OF BATCH NUMBER 100 1 962681056002 BURN 1, 0.029 BURN ? 0.028 17 ti DUP050307698 RUN NAME: 9626901F05 PAGE: 3 ANALYST: 68 TUBE.I 1.4 's k mp l e Lcsw 09/25/96 02:16 CLASS I VOL /LIT' AVG fcmbl %RPD AVG abs 8.6300 2.3 .0.024 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVOL ,,.P.F,,.' BATCH NUMBER 1 1 96268105.6002 BURN 1 BURN 2 RR RO 0.023 0.024 TUBE: 15 SAMPLE LCSW A 09/25/96 02:20 CLASS mu/wi 1 AVGfpobl XRPD AVG abs 20.1700 1.0 0.053 %RECOVERY =115 .4 FVOL ,,.QJL. BATCH NUMBER 1 1 962681056002 BURN _L 0.05? 0.053 TUBE: 16 09/25/96 0-2 :24 s kmp Le. ?-ZZ2ZZ 2583222"" CLASS imLzwi ^ 4fIfk Y 100 XvV AVGfoofo') SSRPD AVG abs -2.8900 12.2 -0.005 FVOL QF_ BATCH NUMBER 100 1 962681056002 BURN 2 EE RD -0.004 -0.005 TUBE: 17 SAMPLE 2583222 ", 09/25/96 02:28 CLASS JXQL./WI ****:*:* 100 AVGId obi 5KRPD AVG abs 7.6700 3.4 0.021. ^RECOVERY = 76. 7 FVOI. .Qf.. BATCH NUMBER 100 1 962681056002 BURN J. 0.6?? BURN 2 0.021 TUBE i. 18: SAMPLE 09/25/96 02:32 CLASS /fC^ ^ ^^ ^ ^ IVOk/WI 100 Jr AVG(oob1 5KRPD AVG abs 15.8200 5.5 0.0.42 FVOL . Q BATCH NUMBER 100 1 962681056662 BURN 1 BURN 2 BE BE 6.043 0.040" TUBE: 19 s kmp l e . 2 583 2 23 09/25/96 02:37 5 l ks s , iv o l /w t *****A* 100 AVG(pobl %RPD AVG abs 25.2100 0.7 "0.0 65 ^RECOVERY = 93.9 FVOL DF BATCH NUMBER 100 1 962681056002 3URNJL 0.065' BURN ? 0.065 DUP050307699 RUN NAME: 9626901F05 PAGE: 4 ANALYST: 68 IUBEj . 20 SAMPLE 2583224 09/25/96 02:41 CLASS IYQL/WT ******* ' 100 AVGfpbbI 2LRPJX AVG abs -2.5900 T.1 -0.004 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE E.V0L. _&_ BAXCiLbLUMBER 100 1 962681056002 BURN 1 BURN 2 RR RD -0.004 -0.00.4 ________ TUBE: 21 SAMPLE 2583224 09/25/96 02:45 CLASS IYQL/WT *****A* 100 FVOL J).F._ BATCH NUMBER '100 1 962681056002 AVGfppbl %RPD ' AVG abs 7.3700 5.5 0.021 BURN__1. 0.020 BURN ? 0.021 %RECOVERY - 73.7 TUBE: 2? SAMPLE CCV 2 ' 09/25/96 02:49 ' CLASS. IVQL/WT b AVGfppb! %RPD AVG abs 22.8200 0.4 0.059 ^RECOVERY 91.3 FVOL DF BATCH NUMBER 01 BURN 1 0.059 BURN 2 0.059 TUBE: 23 SAMPLE CCB 2 09/25/96 02:53 CLASS IVQL/WI 0 AVGfppbl 55RPD AVG abs -1.2000 3.5 -0.001 F..V.PL ..., DF BATCH NUMBER 01 BURN 1 BURN 2 -0.001 -0.001 TUBE: 24 SAMPLE 2583225 ftRPi 09/25/96 02:57 CLASS IVOL/WT ******* 100 AVGfppbl %RPD AVG abs 1.6700 10.4 ""o'. 007 FVOL _QJ BATCH NUMBER 100 i 962681056002 BURN 1 BURN ? o "bos 0.007 TUBE: 25- SAMPLE 2583225 09/25/96 03:01 CLASS I VOL /WT *****A* 100 FVOL QF BATCH NUMBER 100 96268105600? AVG(ppbl %RPP AVG abs BURN 1 11.8200 2.9 0.032 0.031 BURN 2 07032 %RECOVERY = 101.5 6 RUN NAME: 9676901 FOB PAGE : 5' ANALYST: 68 TUBS; 26 ' 09/25/96 03:05 SAMPLE CLASS. I VOL /WT 2583226 \5RP\\5 u****** 100 V AVGfppbl %RPD AVG abs -1.3300 12.2 -0.001 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE FV.0.1, ,.DF_,, &AICJ._N.U.WJ1LR 100 1 962681056002 BURN__1_ BURN 2 -0.001 -0.001 TUBE: ` 27 . 09/25/96 03:09 s kmp l e 5 l ks s j v o i/w i 2583226&RCM5& U****A* 100 AVGfpohl 2RPD AVG abs 9.7600 .1.5 0.027 %RECOVERY -- 97.6 FVOL PE BATCH Nl MBER 100 1 9626810' 6002 BURN 1 0.027 BURN 2 0,026 TUBE: 28 ' 09/25/96 03:13 SAMPLE CLASS. imAWT 2583226 ^(^^5^ D****** 100 V AVGfppbl %RPD AVG abs -0.9500 7.0 0.000 FVOL DF.... BATCH...Nl tjBF.R 100 1 9 626810" 16002 BURN 1 BURN 2 R i EEL -6.000 0.000 TUBE : 29 SAMPLE 2583226 09/25/96 03:17 CLASS IVOL/WT D****A* 100 FVOL DF BATCH t UMB.ER 100 1 96268l(i56002 AVG fppbl %RPD AVG abs BURN 1 BURN 2 A 9.8800 3.3 0.027 0.026 0.028 %RECOVERY = 98.8 TUBE: 30 09/25/96 03:21 SAMPLE CLASS LVpL/LJI. 2583226 tVRvilSS) f^****** ) go V AVGfppbl %RPD AVG abs 8.0700 0.3 0.02? FVOL J1F ... BATCH.. lyMBJjJB i rio 1 962681 56002 BJ,)RN 1 BURN 2 HR RD. 0.02 2 0.022" J TUBjLi. 31 SAMPLE Z7.Z7.27. 09/25/96 03:75 CLASS T.VOL/WT ' FVOL R****A* o0 DF BATCH NUMBER i AVGfppfo^ %RPD AVG abs B!(RN 1 19.2800 2.0 0.050' 0.050* BURN 2 0.051 ^RECOVERY = NOT APPLICABLE DU P0503 07701 RUN NAME: '9626901F05 PAGE; 6 ANALYST: 68' TUBE: 32 09/25/96 03:79 SAMPLE CAAS.S IYQL./.WI 2583227 CTWF) ******* 100 V AVG(pobl %RPD AVG abs - 19.9000 1.9 0.052 I ANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE FVOL BATCH. NUMBER 100 . 1 962681056602 RURN 1 BURN 2 ~ p0.053'. 0.051 4 TUpE: 33 s kmp l e 2583227 09/25/96 03:33 - L-AS5. IVOL/WT *****A* 100 AVGfonbl 5SRPD AVG abs 28.7000 1.8 0.074 %RECOVERY = 88. 0 FVOL OF BATCH NUMBER 100 . 1 962681056002 BURN 1 0.073 BURN 2' 0.075 TUBE: 34 SAMPLE CCV 3 09/25/96 03:37 CLASS 1YOL./W.I 0 AVGfpetal SKRPD AVG abs 22.3200 1.4 0.058 ^RECOVERY = 89. 3 FVOL DF BATCy .NUMBER 01 BURN 1 0.058 BURN 2 0.057 TUBE : 35 SAMPLE COB 3 09/25/96 03:41 CLASS I VOL/WT 0 AVGfoobV %RPD AVG abs -1.0900 83.9 0.000 ' FVOL 0 DF BATCH NUMBER 1 RURN 1 BURN 2 0.001 -0.002 TUBE: 36 09/25/96 03:45 SAMPLE 3?77777 CLASS IVOL/WT 2 583830 &**"&&* SC****** ^ 0Q V AVGfppbl 1KRPO AVG abs -0.8200 28.2 0.000 FVQ.L. 100 BURN 1 . 6.001 BATCH NUMBER 1 962681056002 BURN 2 -0.000 A TUBE: 37 09/25/96 03:49 SAMPLE , , 2 583830 ~d' CLASS im./JiI *****A* 100 FVOL ,,Q.F... RjAJCH NUMBER 100 1 962681056002 AVG/ppbl %RP0 AVG abs BURN J. 9.4200 3.1 0.026 6'.b?6 BURN 7 0.025 ^RECOVERY =94.2 18 h DUP050307702 RUN NAME: 9626901F05 PAGE: 7 ANALYST: 68 TUBE: 38 09/25/96 03:53 5AMLJ _ CLASS IVOL/WI 2 583831 XZJZ**1 ******* .100 V AVG/ppbl %RPP AVG abs 17.4600 5.4 0.046 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA ELEMENT: SE F VOL DF BATCHJfcJUMB.ER 100 1 962681056/302 pi)RN 1 BURN ? *0.047 0.044 TUBE: 39 SAfcSELE. 2583831,7.?. 09/25/96 03:57 CLASS IVOL/WT JK****A* -J 0 0 AVGfppbl &ELREL AVG abs 28.5200 0.4 0.073 %RECOVERY = 110.6 EVOL DF BATCH NUMBER 100 1 9626810E6002 BURN 1 0.073 BURN ? 0 . 073 TUBE: 40 SAMEkl 2583832 09/25/96 04:01 CLASS. IVOL/WT ******* -jog FVOL DF BATCH NUMBER 100 1 962681056002 A AVG/ppbl *RPO AVG abs BURN J BURN ? BL -1.0600 14.3 0.000 -cs.ool -0.000 TilBE: 41 09/25/96 04:05 SAMPLE CLASS .1Y.QL./MI 25838332222*2 *****A* 100 AVGfpphl %RPD AVG abs 11.8200 4.0 0.03? %RECOVERY = 118.2 FVOL. DF. BATCH NUMBER 100 1 962681" 56002 Rl.IRN 1 0.031 BURN 2 0.033 ISJBE. 42 09/25/96 04:09 5AMELL 2583 833 7-Z2ZIZ CLASS IVOL/NT 100 FV.01, ,_DF,, BATCH KjU MBER. 100 1 962681 056002 AVG fpp'bl %RPD AVG abs RURN._1 BURN 2 109.6400 1.9 0.275 0.279 0.271 OVER CALIBRATION RANGE TUBE: 43 . 09/25/96 04:13 SAMPLE . CLASS IVOL/WT 2583833 ,i *****A* 100 FVQL. JDF_ BATCH NUMBER 100 1 962681056002 AVGfppbl %RPD AVG abs BURN 1 126.3100 1.0 0.317 .6.319 BURN 7 *0.314 %RECOVERY = NOT APPLICABLE OVER- CALIBRATION RANGE 181 DU P050307703 RUN NAME : 9626901F05 PAGE: 8 ANALYST: 68 TUBE: 44 09/25/96 04:17 SAMPLE 2583834 .. 77^Y.T IYQLZMI ******* 100 V AVGfoobl *RPD AVG abs - -1.0000 4.1 0.000 * 1 nk 5 kopqr sktutkvo r t f INSTRUMENT ID : 04725 GFAA ELEMENT : SE FVOL ' JIE_ BATCH NUMBER 100 1 962681056002 BURN 1 BURN 2 *&/kr -o.ono -0.000 J vl TUBE: 45 09/25/96 04:21 SMIPJJL -,, , H 2583834 CLASS 1VOL/WT 100 AVGfDDbl %RPD AVG abs 12.4000 2.5 .6.033 ^RECOVERY * 124.0 f .v p l :.m. BATCH NUMBER 100 1 962681056002 BURN 1 0.034 BURN 2 0.033 TUBE : 46 SAMPl-E CCV 4 09/25/96 04:26 CLASS imyjii 0 AVGfDobl 5KRPD AVG abs 22.7700 2.9 0.059 %RECOVERY =.91..1 FVOL OF BATH n u m; e d 01 BURN 1 0.058 BURN 2 0..060 TUBE: 47 SAMPLE CCB 4 09/25/96 04:29 CLASS IVQL/WI, FVOL 00 OF BATCH NUMBER 1 AVG foobl %RPD AVG abs -0.5900 208.1 0.001 BURN 1 BURN 2 0.003 -0.001 TUPE: 48 SAMPLE pgVg 09/25/96 04:33 CLASS IVQL/WT ******* -] q o V AVGEpribl %R,PD AVG abs -1.1700 33.3 -0.001 F.Y.9.1. DP BATCH NUMBER 100 1 96268105600lu BURN 1 BURN 2 PR RD 0.000 -t s o t g(/z: TUBE: 49 SAMPLE PBW {\ 09/25/96 04:37 CLASS 1,VQL/LIT *****A* 100 %RPD AVG abs 1 1 .4700 5.5 0.031 %RECOVERY =0.0 r.VOI, DF gATQH NUMBER mo 1 962681056002 BURN J. 6.03.0 BURN ? 0.03.2 DUP050307704 RUN NAME: 9626901F05 PAGE: 9 ANALYST: 68 50 SAMPLE IX SW 09/25/96 04:42 GLASS IVOL/WT s*:*:**::**!*: 1 V %RPD AVG abs 8.5700 2 .7 0.02-4 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA FLEMENT: SF FVOL QE BATCH NUMB.ER 1 1 9 6268105 6 6 OlK i BURN 1 BURN ? Rfi/ RD 0.023 0.024 TSS/~H TUBE: 51 SAMPLE LCSW ft 09/25/96 04:46 CLASS IVOLZWT **:*:***: <\ %RPD AVG abs 20.6200 2.9 0.054 %RECOVERY 120.5 FVOL _DF BATCH NUMBER '1 1 962681056002 BURN 1 0'.~053 BURN ? 0.055 TUBLi. 5? 09/25/96 04:50 SMELL CLASS. imL/-WI 2583205 ^fSSS ******* 100 AVG(ppbT %RPD AVG abs 16.5400 1 .8 0.043 FVOL DF BATCH NUMBER 100 T 962681056OGftJ f BURN 1 BURN 2 0.044 0-043 TUBE: 53 SAMPLE 2583205 09/25/96 04:54 CLASS LVOL/MI *****A* 100 FVOL. JO F... BATCH NUMBER 100 1 962681056002 AVG ( piobl 95RPD AVG abs .BURN T 25.1800 0.3 0.065 0.065 BURN 2 0.065 . %REC.OVERY = 88. 4 / / \ \ TIJBE_: 54 SAMPLE 2583206 09/25/96 04:58 ' CLASS I VOL /WJ ******* TOO V AVGfppbl %RPD AVG abs -3.4500 4.5 -0.006 FVOL DF BATCH NUMBEF 100 1 962681056001 RtIRN 1 BURN 2 RR . RD. -0.007 -0.006 t u; e 55 SAMPLE 2 583 206 09/25/96 05:02 C__L_ASS IVOL/NT *****k * 100 AVGfppbl %RPD 6.9000 ' 2.9 %RECOVERY =69:0 FVOL D.F BATCH NUMBER 100 1 962681056002 BURN J n 7oi 9 BURN 2 0.020 X3: DUP050307705 r u n NAME: 9626901FD5 PAGE: 10 ANALYST: 68 TUBE: 56 09/25/96 05:07 SAMPLE. ^ GLASS IVOUWT 2583207 OBiA-PL> ******* 100 V AVGfpobV %RPD AVG abs -2.6500 10.6 -0.004 lANCASTER LABORATOP T ES INSTRUMENT I'D:' 04725 GFAA EtFMFNT: SE FVOL J?F_ BATCJH NUMBER 100 1 96268105600^ / BURN .1 BURN 2 -0.004 -0.005 TUBE: 57 gftMPt- E 2583207 09/25/96 05:11 . --CLASS jm.ZM.1 ****** 100 AVGfppbl %RPD AVG abs 6.4500 2.0 0.018 %RECOVERY 64.5 FVOL. ,QF._ BATCH NUMBER 100 1 962681056002 BURN 1 "0.019 BURN '2 0.018 TUBE: 58 SMELL CCV 5 09/25/96 05:15 CLASS - IVOL/WT 0 AVG/pobl %RP0 AVG abs 22.3200 3.3 0.058 %RECOVERY = 89.3 FVOL OF BATCH NUMBER 01 BURNLL ' 0."057 BURN 2 0.059 TUBE: 59 SAMPLE CCB 5 09/25/96 05:19 CLASS . IVOL/.WT 0 AVG/ppbl %r p q . AVG abs -1.1300 10.9 0 . ooo FVOL DF BATCH 01 BURN 1 BURN 2 -0.000 -0.001 TUBE 60 SMELL 2583208 09/25/96 05:23 CLASS IVOL/WT ******* 100 AVGfppbl %RP0 AVG abs 2.1700 15.4 0.008 Lyot DF BATCH NUMBER 100 . 1 96268105600^ , BURN J BURN 2 0.008 0.007 TURF: 61 09/25/96 05:27 SAMPLE _ CLASS 1V.QL/MI 2583208 PnS45 ft *****k * 100 AVGfpobi %RPD AVG abs 11,3300 3.9 0.031 ^RECOVERY = 91.6 FVCU. _0,F_... AATCH NUMBER 100 1 962681056002 BURN 1 BURN ? 0*030 0.031 184 Ik DUPO 503 07706 RUN NAME: 96Z69O1F05 PAGE: 11 ANALYST: 68 TJJ.BE.i- 62 SAMPLE 2583209 mum.09/25/96 05:3V CLASS y*:*2*c*** 100 V AVG(DDbl *RP0 AVG abs -T.5900 9.5 ' -0.002 LANCASTER LABORATORIES INSTRUMENT TO: 04725 GFAA ELEMENT: SE FVOL J 100 BURN 1 -6.001 Sk1 96268105=60TO^ BURN ? Rg/` RD -0.002 ______ ____ TUBE : 63 09/25/9605:35 SAMPL.E. C1-AS1 IY-Qk/WI .2583209 OnT>Oi>r\ y**:**^* <100 FVOL DF BATCH NUMBER 100 1 962681056002 AVGfopbl . %RPD AVG abs -BURN 1 11.9200 9,5 0.032 0.030 BURN ? 0.034 ^RECOVERY * 119.2 TUBE: 64 SAMPLE 09/25/96 05:40 CLASS IVOL/NT 2583209 I^jSDtV0 ****** 100 Y AVGfppbl %RPD AVG abs -0.9900 13.4- 0.000 F_VQk ,,P.L_ BATCH NUMBER 100 1 962681056001 / BURN 1 BURN 2' BM/RD 0.000 -0.000 fjf"___ TUBE: 65 . 09/25/96-05:44 MMELE CLASS . IVQL/Jil 2583209 OrwCTODS d **^x A* 100 AVGTppbl %RPD. AVG abs 12.5200* 5.4 0.033 ^RECOVERY = 125.2 FVOL _.PF_ BATCH NUMBER 100 1 962681056002 BURN 1 0.032 BURN 2 0.035 TUBE: 66 SAMPLE 25 83209 09/25/96 05:48 CLASS IVOL/NT R****** 100 Y AVGCppbl %RPD AVG abs 7.5600 14.5 0.021 F.V0L OF BATCH NUMBER 100 1 96268105600^ \ BURN 1 RURN 2 W RD 0.023 0.019 TUBE: 67 SAMPLE 2227.27. 09/25/96 05:52 CLASS IVOL/WT PJ****^* Q FVQL. DF BATCH NUMBER 01 AVGfppbl %RPD AVG %bs 21 .0200 1 .7 0 055 BURN 1 0.054 BURN 2 0.055 ^RECOVERY = NOT APPLICABLE 185 DUP050307707 RUN NAME: 9626901F05 PAGE: 12 ANALYST: 68 ' TUBE; 68 09/25/96 05:56 SAMPLE 2583210 DR63S GLASS. ivjQk/iJl ^ 100 AVG(ppbl %RPD AVG ahg 13.6100 1.9 ' 0;036 LANCASTER LABORATORIES INSTRUMENT TO: 04725 GFAA ELEMENT: SE FVOl ,,DF BATCH NUMBER 100 1 96268105600 fj BURN JL BURN ? ~ 0 03 6 0.037 TUBE_j_ 89 * 09/25/96 06:00 SAMPLE CLASS I.VQL/WT 2583210 \)ftP3Sft *****A* 100 AVGfppbl %RPD AVG abs 25.4400 12.6 0.066 %RC,OVERY 118.3 FVOL DF BATH NUMBER 100 1 9 6.2 6 810560 01 BURN 1 "oeo BURN 2 0.071 TUBE: 70 SAMPL.E CCV 6 09/25/96 06:04 CLASS IVOL/WT 0 AVG(pob) %RPD AVG abs 21.0200 5.6 0.055 %RECOVERY = 84.1 FVOL OF .BATCH 01 RURN 1 0.057 BURN 2 0.053 TUBE: 71 SAMPLE CCB 6 09/25/96 06:08 GLASS TVOL/WT 0 AVG(pob> %RP0 AVG abs -1 .2900 56.3 -0.001 FVQ.L DF BATCH 0 1 BURN 1 BURN 2 0 000 -0.002 TUBE: 72 09/25/96 06:12 .SAMPLE CLASS. IVp.L/W.1 2 583 8 23 DBb(7iIj ******* 100 V AVGfpobl %RPD AVG abs '-1.4700 28.5 ~-0.6o7 FVOL OF BATCH NUM_BEr 'V'-' 100 1 9 62 6810560 0^ BURN 1 BURN 2 RR /-RD -0.001 -0.002 TUBE: 73 09/25/96 06:16 SAMPLE CLASS I.VOL /LIT 2 583823 DWrtdLft *****k * iq q %-BED. AVG abs 9.0700 2 .1 0.025 ^RECOVERY 90.7 fVOl... DF__. BATCH NUMBER 100 i 982681056002 BURN 1 0.025 BURN 7 0.025 186 DUP050307708 RUN MAMET t 9626901F05 PAGE: 13 ANALYST: 68 TUBJE: 74 09/25/96 06:20 s kmp U ^ mum'5 l ks s 2583 824 p'RftSS ******* 100 V AVGfppbl %RPD AVG ebs 3.9000 10.0. 0.017 LANCASTER LABORATORIES INSTRUMENT ID: 04725 GFAA FIEMENT: SE FVOL PF 8ATCH__NUMBER 100 1 96268105600^ BURN.J BURN 2 R. "o'.ois 0.011 TUBE: 75 SAMPLE __ 2583824 09/25/96 06:24 CLASS IVQL/MT *****A* 100 AVGfPPbl %RPD AVG.. abs 12-9100 3.8 0.034 ^RECOVERY = 90.1 F V.pL J)F _ BATCH NUMBER 100 1 962681056002 BURN 1 6.035 BURN 2 0.034 TUBE: 76 09/25/96 06:28 SAMPLE ^ 2583825 ^.^10 **C*L*A*S*S* MI 1-00 v ' AVGfppbl %RPD AVG abs -1.6600 14.? -0.00? FVOL QF BATCH NUMBER 100 1 96268105600$j BURN_J_ BURN 2 RFV RD -o.oo?" -o.ool 77/__ TUBE: 77 SAMPLE 2583825 09/25/96 06:32 CLASS, HQLZiLT. *****A* 100 mm AVG sbs 8.6800 2.2 0.024 %RECOVERY 86.8 FVO),. PF BATCH NUMBER 100 1 962681056002 BURN_J 0.024 BURN 2 0.024 TUBE: 78 09/25/96 06:36 SAMPLE. CLASS. IVOL/WJ. 2583826 bPvft. 15 ******* 100 FVOL PF BATCH NUMBER 100 1 962 68105600^^ AVGfanhl %RPD AVG abs RURN 1 108.6000 2.9 0.273 0.7R7 OVER CALIBRATION RANGE BURN 2 0.77 8 lUBEx 79 09/25/96.06:40 SAMPLE CLASS im/MI. 2583826 pPn'0>s3 *****A* 100 EVQL 100 ; kt 5 h n u m; e r 1 962681056002 AVG(ppbl %RPP AVG abs RUPN 1 BURN 2 121.7800 0.6" 0.305 0.304 6.307 %RECOVERY = NOT APPLICABLE OVER CALIBRATION RANGE IS' DUP050307709 RUN NAME: 9676901F05 PAGE: 14 ANALYST r 68 TUBE: 80 09/25/96 06:44 SAMPLE . 'CLASS Ly,,Qi,/WI 2583827 pRftt \ *******. 100 V AVGfppbl %RPD AVG abs -1.5300 51.1 -0.001 i ANOASTFP LABORATORIES INSTRUMENT ID: 04725 GFAA FI..EMENT: SF FVOL 100 &ATCH_NUMBJR 1 9626810560 0 ^/ ^ ' BURN_1 .BURN 2 -0.003 -0.000 RD TUBE r 81 SAMPLE 2583827 ' 09/25/96 06:48 ^ CLASS MM rV *****A* 100 AVGCopbl *BE AVG abs. 10.2700 4.2 0.028 %REC0VERY o 102 .7 EVflL JD.JL. MISJUliM&SB 100 1 962681056002 BURN 1 0.027 BURN 2 0.029 TUBE: 82 SAMPLE CCV 7 09/25/96 06:52 CLASS IVOL/WT 0 AVG(oobl %RPD AVG abs 23.0100 1.4 0.060 ' %REC0VERY - 92. 0 FVOL. 0 F BATCH NUMBER 0 "i BURN 1 0.059 BURN 2 0.060 * TUBE: 83 SAMPLE CCB 7 . 09/25/96 06:56 5 l ks s im/wi 0 AVGfpobl *RPD 0.3700. 258.1 0.003. FVOi, 0J BATCH NUMBER 0 1 BURN 1 BURN ? 0.00? 0.005 DATA REVIEWED BY: DATA VERIFIED BY: %b'kl 138 DUP050307710 LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION DATA REVIEWED BYs DATA VERIFIED BY t DATA FILE MAl'iFi, f:EP700. RAT RUN NAMES 9627001F0S ANALYOTs: A03 INSTRUMENT MOs 047B5 BKG DORR a BZ ELEMENTS SE Concentration it ured to evaluate Li' :m.>I.o v:.*"mlL c a. I i b t a t. i o v* r a n r e- - 189 di-:j within DUP05030771 1 . RUN NAME s 962700IF05 PAGE: :i ANALYSTS 609 LANCASTER 1.A BORA I'GRIIL .INSTRUMENT IPs 04725 OFAA ELEMENT; SE 1 TUBE a 1 C9/2&/96 06 : 37 SAMPLE a. ASS TVOL/WT FVQL PF BATCH NUMBER S0 0 ......~0 ... 1 AVG < ppb) ZRPD AVG abs -0.3900 119.4 0.001 BURN 1 BURN 2 0.002 0.001- TUBE r. SAMPLE S5 2 09/26/96 06 8.41 Cl. ks s :; IVOL/NT i AVG<nob) ZRPB AVG abs 5.6700 7.0 0.015 FVOL PF BATCH NUMBER 01 BURN 1 BURN 2 0.016 0.015 TUBE; SAMPLE SIS 3 09/26/96- 06 s 45 Cl. ASS IVOL/W-T 0 A V G < p p b > ZR P D AVG a lv.s 13.3600 1.4 0. 041 FVOL'- PF BATCH NUMBER 81 BURN 1 BURN 2 0,041 0.041 TUBES ?SAMPLE S25 4 @9/26/96 06 #49 Cl. ASS IVOL/UIT i FVOL PF BATCH HUMBER 0 .1 flVG<ppb> %RPP AVG &b& ~2A 12400 ' 0.4 07(367 BURN.....1 BURN 2 ' 0.066 0.067 TUBE; SAMPLE S40 5 09/26/96 06 s 53 tiLfiSili 1' VOL/UT E VOL PF BATCH HUMBER 0.01 AVG <ppb> XRPP AVG aba 36.2600 0.2 8.102 BURN 1 BURN 2 8.102 0.102 TUSEs. SAMPLE S50 6 09/26/96 06 s 57 . Cl ACC IVPL/WT 0 FVOL- PF BATCH HUMBER 01 ...... A AUG <ppb> ZRPD AUG aba. BURM ~ 1 BURN 2 50.9700 1.1 0.131 0.132 0.130 TUB.Es.. CAMPLE ICV 7 09/26/96 098 01 Cl. ACC IVOL/UIT 0 FVOL PF BATCH .NUMBER 0 1 A 190AUG (nob) ?.H PB. ATI.!_ajj.'r;. BURN 1 BURH } A 19.6500 6.6 0.053 0.049 0.'056 A /RECOVERY = 99.2 DUP050307712 RUN NAME s 96870011" 05 PAGE : r ANALYSTi 609 TUBE: SAMPLE SCB~~ 6 09/86/96 09 s 8S Cl. ASS JVOL/WT 8 AUG <ppb> ZRPO AUG abs -8.9108 37. 6 "0.001 LANCASTER LABORATORIES INSTRUMENT IDs 84785 OFAA ELEMENTs SC FUOL DF BATCH NUMBER 01 BURN..1 BURN.. S. -0.001 -8.000' TUBEs SAMPLE CRA 9 09/86/96 09 s 89 CL ASS TU0L/8T i AUG(ppb) 3tRP AUG abs 4.0708 4.6 0.818 FUOL DF BATCH NUMBER 0X BURN X BURN 8 0.018 0.018 TUBEs 18 SAMPLE CCU 1 89/86/96 89 ! 13 CLASS. XVOL/UJT 0 AUG (ppb> gRPJO A.UG._abs. 84.SS00 8.3 S . 06i: tfRECOUERY ~ 96.8 FVOL I>F BATCH NUMBER 81 BURN 1 (d. 06 4 BURN 8 0; 866 TUBE:. .1. X SAMPLE OCB 1 89/86/96 a*?* .17 Cl. ASS IVOL/NT FVOL I>F BATCH HUMBER 0i AUG (ppb) *RPP AUG abs BURN 1. BURN E -i. iaie ia.e -0.001 -8.001 -0.00a wIM&e -l is k mp Le PBW 09/86/96 09sSI CL ASS IVOL/WT . k *:-x k k 180 FVOL 188 F BATCH NUMBER 1 9&ci&BTafeftS.t' AVGCppb) RPD AUG ab';, BURN I. , BURN 8 RR RD -1.1 6 0 0 S 6 . 4 -0 - 001 0.801 - 0.00 8 TUBEs 13 SAMPLE PBM f\ 0*3/86/96 09.!S5 Cl. AGS IVOL/WT k *k '* 108 FVOL 3>F BATCH NUMBER 108 1 968661006001 AUG < ppb) /)>p:0 AUG abs BURN 1 BURNJ? I..iaim 0.9 .as '0.0S6 i'7ii? ^RECOVERY 101.S DUP050307713 RUN NAME* 968700 IF 81: PAGE it 3 ANALYST: 809 TUBE: 14 SAMPLE L.CSW 89/86/96 89:30 61 ASS IVGL/WT 1 V, X AVG (pp.b). *.Rp. 8.78(30 2,6 (3.(384 LANCASTERLABORATORIES INSTRUMENT IDs 04785 GFAA ELEMENT: SE FVOL JSF,, 0TCH .NUMBER 1. r1 968681056081 ; xyn i. mm n 0.084 e.085 m TUBE; 15 SAMPLE LCSWfi 09/86/96 03 s 34 Cl ASS IVOL/WT A>! 1 . FVOL i I>F' BATCH..HUMBER 1 96868105680.1 fty.PlB.Bkt #8P ftVG aba 19.6600 1.3 0.058 fiUfitLl 0.052 mmuL 0. (353 /.RECOVERY 108 .8 . ami. 16 SAMPLE! ^ 8583805 09/86/96 09:38 CLASS imvwx * tt m X AyG.lp.pby /RPjD. eyfi_jj!sL 16.9680 1,7 0.045 cyoLFV . 3Bft.lS.ti_N.UPJfiER, 180 1 968681056081 BURN 1 ; z{n ..* m m (3.845 8.046 TUBE: 17 SAMPLE _ 8583885 09/86/96 09 s 48 3. ftAS lyob/wx 10(3 AiisiaaBt. *f>E aye..*.*>*. 25.58(30 8.9 0. (367 /RECOVERY 86.8 em.... s l ..B.a.ipH ..|}~; 180 1 968661056881 BUR 11..1. . ; Ls . 0. 067 0.068 TUBE s 18 ieaELE 8563206 139/26/96 09:46 Lsii zmiux **** '180 A Gygjkpje&L *k p 6iijL6-.&k& 0. h 6(30 k x m x >: 0, (3(12 FV.O.L, PF ~im i 962681056001 SUBM...L SiUBlUl' r<R Rfe 0.005 -(3.001 TUBES 19 J&me. 2583206 . 09/26/96 09:50 IWL/UT I: Ax 100 am<jy?b>_ mEM. k g &b& 7,23(30 9.9 0.(320 /RECOVERY = 78.3 FVOL 1(30 BURN..-1 8.019 1 962681056001 BURN f> (3.(321 .ia W-- DUP050307714 RUN M A I'll:Is 9627001F85 PAGE s 4 ANALYST: 809 i.. AN CALITER LABORATORIES INSTRUMENT IDs 84725 orAA ELEMENTGE TUBE; ci& 09/26/96 09 S 55 SAMPLE CL ACC IVOL/WT 2583287 B>R4 ii)D * 106 FUOL. ...PF' BATCH NUMBER 108 1 962681056081 v> X' AUG < ppb) /RPD -1.0400 1.6 -0.(301 BURN 1 BURN 2 !' :!; . RD . 001 - 0.001 ..._ . ___ ' TUBE i; 21 SAMPLE __ 2583207 89/26/96 09 s 59 . CL.ACC IVOL/WT * A a 00 . . . ....... * - - * " ** " * ....... -- ~ FUOL DF BATCH NUMBER 100 1 962681856001 > AVGtpob) ZRPD AUG aba BURN 1 BURN r> 8.4700 5.5 0.023 0. 824 0. 022 /.RECOVERY ~ 64.7 TUBE; BE SAMPLE ecu a 09/86/96 .1.0 s 63 CL ACC IVOL/WT 0 AUG<ppb) /RPJD AUG abs 83.7000 4.1 6.063 FVQL ,,J>F... BATCH NUMBER 0 1 BURN 1 "5.061 BURN 2 ' 0~'064 /RECOVERY 95. 1 TUBE; 23 SAMPLE CCB 2 (39/26/96 10; 87 CL ACC IVOL/WT 8 FUOL PF BATCH NUMBER 81 AVG(ppb) /RPD AUG abs BURN 1 BURN 8 -1.1600 43.0 -5.08a -0.5 r "=07008 TUBE; 24 09/86/96 10.: 10. SAMPLE 2583808 B?)S4S Cl ACC IVOL/WT ffypL **** 1.00 . 100 PF BATCH HUMBER j 962681856001 AVG(ppb) ZRPD AUG abs 0.6800.146.8 '0.003 DUk N I. . ftURH (1 Rft Rif) 8.801 A.80S TUBE; 2S ' 09/26/96 10sl5 SAMPLE ^ Cl. ACC IVOL/WT 2583208 "E>PiS4Sf| A 1.08 AUG < ppb) /RPP AUG abs 9.9300- 5.S 0.(387 /RECOVERY =99.3 FUOL .PF.. BATCH.. NUMBER 100 1 962681056881 BURN 1. 8.826 BURN ? '8.026 n. DU P05 0307715 RUN NAMES 9627001F05 PAGE s ANALYST: 809 TUBE a 26 09/26/96 .18:19 S0NPL.E ^ GLSMi IVOL/WT as a 5a es "2<r\S3 D . 100 AVG<opb) *RPD- AUG aba "0. 9300 83.3 --0. 801 LANCAGTFR' LABORATOR XEB INSTRUMENT 13): 04725 GFAA ELEMENT-.! sr FVOL' DF BATCH -NUMBER 100 x 96a&6i85&5ai BURN 1 BURN A RE EI> --0.001 -0. (3033 TUBE: 27 SAMPLE 5583289 . 09/26/96 10823 . QLAlfe IVOL/WT UiTi>7KA . :l88 FVOL 3)3" BATCH NUMBER 100 . 1 962681056801 AVG<ppb) *RPD AVG abs BURN 1 ""5L&700 - 1.5 5.024 ` @.024 BURN 2 0-ias 3SRECOVERY =-*= 88.7 TUBE: 28 SAMPLE 5583209 @9/26/96 10:27 Cl. ASS IVOL/WT !)': 100 AVB (ppb) /.RED . AVG a Li " - i7i :i @5' 40. e -a. 00i FVOL PF BATCH NUMBER 180 1 962681056001 BURN I. `BURN 2 RR R_D -0.801 -*0.002 TUBE: 29 09/26/96 .10:31 SAMFS^. Cl. ASS IVOL/WT 2583209 BR`5`3DT>fV B*A T80 AVG < ppb) %RPD AVG abs ~ 9.1100 i.4 5.025 sl RECOVERY 91. L FVOL ,,... BATCH HUMBER ,100' I 962681856001 BURN 1 0.025 BURN n i".025 TUBE: 30 09/26/96 10:35 SAMPLE Cl. ASS IVOL/WT 2583209 \3iftS3 DS 100 AVG(ppb) JtRPD, '" 6000 7.9 @7021 FVOL DF BATCH NUMBER 100 1 962681056001 BURN I BijRN 2 RR R3) 5.020 0.022 TUBE a 31 SAMPLE 7.... j,,,... X. 1. 09/26/96 10:39 ' ` CLASS IVOL/WT Rk **A* 0 FVOL I>F BATCH NUMBER 5 i. AVG VP.Pbl. XRPJD AVG_,,abs. ""T&79500 0. 8 ...07045 BURN 1 0.. 845 llULM../ 0.57 ^RECOVERY NOT APPLICABLE 194 DUP050307716 RUN HAI'lEs 962780 IF05 k ; s 6 ANALYSTs 609 LANCASTER' LABORATORIES INSTRUMENT IDs 04725 OF ftA ELEMENT.: SC TUBE: 32 SAMPLE . 8563210 09/26/96 10:43 Gi. A33- IUOL/WT 3t> KKKKKK* 180 FUOL ..DF... BATCH NUMBER 100 ' 1 '9626^856001 AUG < opta) *RPD AUG Aba . BURN 1. BURN 2 RR Rj> 13.6900* 6.3 ~ 8.037 0.039 0.036 TUBE: 33 SAMPLE 25&32I 09/26/96 10:47 . Cl ASB IUOL/WT ,j ****k * 3 00 F.UQL 180 DF,, BAJCH NUMBER 1 968661856081 AUG (ppb) !>tRPD AUG abs BURN 1 . *23.2900 "3. 3 "~ 0.i&r 0.063 BURN R 0.*060 StRECOUERY - 94.0 TUBE : 34 SAMPLE CCV 3 09/26/96 10:5.1. Cl ASS lOtiL/WT FUOL DF- BATCH NUMBER 8.01 AUG (ppb> JURPD AUG abs23.2380 0.1.*" 8.061 BURN 1 0.061 BURN 2 0.061 /.RECOVERY = 98.9 TUBES 35 89/26/96 10855 A SAMPLE CCB 3 GLMiii. 3 UOL/WT 0 FUOL DF BATCH .NUMBER 8i AUG <PDb) flRI-'D AUG &bs 1.3300 5.5 -8.008 BURN 1 BURN 2 --0.002 "57(302 TUBE s 36 SAMPLE 2563633 (39/36/96 10 s59 Cl.ftSC IUOL/WT. 18 F.Upj. PF BATCH NUMBER 100. 1 962661056001 F|UQ <ppb> flRPD AUC Ab-4 BURN 1 BURN 3 RR RD -1.4700 15.6 -0.002 --0.002 --@.003 TUBES 37 09/26/96 11803 SAMPLE; y 'CL ACS IUOL/WT 2563623 'b&ftSPft >:-i:A 106 AU.G <ppb> jCf$PJ>. AUG abs 9.9500 6.4 0.027 tfRECOUERY = 99.3 . FUOL PF BATCH .NUMBER 108 1 968661856801 . BURN 1. 0.826 BURN 2 "iTSia, ( DUP050307717 RUN NAIIEe 9687001F05 PAGEs k k y s t s 7 609 TUBE;. 36 SAMPLE 2563624 09/36/96 1:1.507 OliililL liMI ' 188 AUQ (ppfa) XRPP AVG . abv: ~ &S0B ~7.S 0.814 I.. A MI.' A G T F.R t_A ft O R A T 0 RIE S INSTRUMENT XD: 84785 OFAA ELEMENT.: OC FVOL I)F BATCH NUMBER JSi 1 968661036001 ft ARM 'I. BURN 8 RR RJf) 0.0;1*4 0.013 __________ TUBES 39 09/86/96 11s11 SAMPLE CL AS JVOL/UT ' FVOL 2563614 frRPtaS^ J00 . 108 DF BATCH. NUMBER 1 968661056001 AVG-<japJ^ XRPD AVfi_ab> '1471800 4.4 0.036 BURN. 1. 0.037 BURN ~8 .0.039 JtRECOVERY 94.6 TUBES '40 .09/86/96 11 a 15 Sw'lPLE . Cl. AAA 'IUOL/WT . FVOL 8363683' ^RfM D' j :*" ' 7(310 . , 100 i)F BATCH HUH HER i 968661056001 flVGtPob) XRPB AUG a^v.. BURN : 1 BURN 3 JRl RD .... i7915 141.5. 0.087 0.058 0.001 TUBES- 41 SAMPLE 8563685 oftft 09/86/96 :L1; 19 Cl ASS IVOL/WT A-x iiii . AUG <ppb> XRPP AUG aba 18.8800 1*4.6 ".833 XRECOVERY =0.0 FUOL .. ]>_ BATCH HUMBER 100 1 968661056001. BURN t ftURH 8 5.038 51036' TUBE.S 48 -09/86/96 11 #83 SAMPLE ,, 8513686 WPiUi Cl AGS JVQL/WT j : 108 V, . AUG (ppfa) XRPD AVG *!):> 84.6800 1.7 8. 065 FVOL _j>F.... BATCH HUMBER ` 100 5 968661056001 ftl.iRH I. BJJ.iiW._3. FtR RB 0.066 8.065 TUBE s 43 SAMPLE . 8563686 09/86/96 11:: 8? A . ' Cl. ASS *1VOL/UT ::):>:A* 100 FVOL DF BATCH HUMBER 108 5 9686610565il ^ * AVG y?j?b> XIRPD AVG_ ab<=, BURN BURN 8 ' 35". 1600 *3.6 ' 0.1(98 .095" '.094 /RECOVERY 183.6 191 DUP050307718 RUN NAMES 9627001F05 PACES 6 ANALYSTS 609 TUBE: 44 09/26/96 11:31. SAMPLE C.l- ASS IVOL/WT `2563627 QRrYF^ 100 V /RPD AUG ad-i -1.2600 24. 1 . -0.002 TUBE: 45 8 ifiBEUSL oaflr,'A 2563627 DnfiFI t\ '26/96 11 a 35 CLASS :i VOL/WT : A 1 @8 JSRPP AUG abs 43. 9 (3.847 RECOVERY 175.6 L ANi; ACTCi'f *.. A 6 OR A T 0R X E INSTRUMENT IDs 84725 OFAA ELEMENT: SC FVOL I>F BATCH NUMBER 180 1 962661056801 BURN l BURN 2 BRi RD -0.002 . -0.001 - - ---- ----------- ----------- FUOL PF BATCH NUMBER 100 1 962661856001 BURN i. 0. 061 BURN. '2 0 ,, 033 TUBES 46 SAMPLE CCU 4 09/26/96 11:39 CLASS :i VOL/WT AVGCppb) J4R.PD AUG abs ' 23.8480 0.6 0.061 /.RECOVERY. 92. 2 FU0.L PF BATCH. .NUMBER 01 BURN 1 0.061 BURN 2 0.061 TUBE: 47 SAMPLE CCB A 09/26/96 11 a43 CLASS I VOL/WT "0 AUG(sab) KRPD AUG abs ~g. 2580 21.7- -0. 004 FVOL PF BATCH NUMBER 0I BURN 1 BURN 2 -0.003 , --0.0(35 TUBE: '46 SAMPLE PBW 89/26/96 11'.: 47 . Cl. ASS :i VOL/WT 1(30 AUG <ppb) %RPP AUG *b-~ - 1.5400 22. 1 -(3 ,, 0(32 rVOL PE BATCH NUMBER 1.00 1 96269105600 i BURN 1. BURN' 2 RR RD r0.003 -0.002 TUBE: 49 SAMPLE PBW~ 09/26/96 11351 . Cl ASS :i VOL/IJT 100 AUG(apb). /RPD AUG abs 11.2688 4.2 0.031 /RECOVERY. 112.fl E.UQ.L PF BATCH NUMBER 180 1 962691056001 BURN_I. "(3.030 BURN 2 ' 0.031 iaQV DUP050307719 LANCASTER LABORATORIES GRAPHITE FURNACE'ATOMIC ABSORPTION - DATA REVIEWED BY: DATA VERIFIED BY s 1^ <*/tilt* DATA Fill- NAME:; SEr?00D. RAT . .UN NAME! '36S700SF0S ANALYSTS GC INSTRUMENT1 MO: 047S5 - BKG CORR : B Z ELEMENT: SE Concentration :ui u&ed to evaluate i. f -vamolo calibration range. . a-t o -within DU P0503 07720 Sample Data DUP050307770 U.S. EPA - CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER_LABORATORIES_ Contract: MR3DD t,ab code: ________ Case No.: SAS No. SDG No.: FMD03 Matrix (soil/water): WATER Lab Sample ID: 2585284 Level (low/med): LOW Date Received: 09/21/96 5 % Solids: 0.0 concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 22.3 U P 7440-36-0 Antimony 12.3 U P 7440-38-2 Arsenic 1.3 U F 7440-39-3 Barium 147 B P 7440-41-7 Beryllium 1.6 U P 7440-43-9 Cadmium 3.3 U P 7440-70-2 Calcium 90800 P 7440-47-3 Chromium 4.3 U P 7440-48-4 Cobalt 4.2 U P 7440-50-8 Copper 5.1 U P 7439-89-6 Iron 167 P 7439-92-1 Lead 0.84 U WN F 7439-95-4 Magnesium 29000 P A 7439-96-5 Manganese 530 P 7439-97-6 Mercury 0.011 B CV 7440-02-0 Nickel 4.8 U P 7440-09-7 Potassium 3490 B P 7782-49-2 Selenium 0.70 U F 7440-22-4 Silver 1.7 U P 7440-23-5 Sodium 53900 P 7440-28-0 Thallium 1.1 u F 7440-62-2 Vanadium 5.2 u P 7440-66-6 Zinc 5.7 B P Color Before: COLORLESS Color After: COLORLESS. Comments: Clarity Before: CLEAR_ Clarity After: CLEAR. Texture: Artifacts: FORM I - IN ILM04.0 5 DUP050307771 U.S. EPA CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lata Name: LANCASTER_LABORATORIES_ Contract: MRA1D Lab Code: ________ Case No.: _ SAS No.: SDG NO.: FMD03 Matrix (soil/water): WATER Lata Sample ID: 2585277 Level (low/med): LOW Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M "I 7429-90-5 Aluminum 69.0 B P 7440-36-0 Antimony_ 12.3 U P 7440-38-2 Arsenic 1.3 U F 7440-39-3 Barium 61.9 B P 7440-41-7 Beryllium 1.6 U P 7440-43-9 Cadmium 3.3 U P 7440-70-2 Calcium 151000 P 7440-47-3 Chromium 4.3 u P 7440-48-4 Cobalt 6.8 B P 7440-50-8 Copper 5.1 U P 7439-89-6 Iron 235 P 7439-92-1 Lead 0.84 U WN F 7439-95-4 Magnesium 37900 P 7439-96-5 Manganese 1690 P 7439-97-6 Mercury 0.0090 U CV 7440-02-0 Nickel 5.7 B P 7440-09-7 Potassium 4590 B P 7782-49-2 Selenium 0.70 U F 7440-22-4. Silver 1.7 U P 7440-23-5 Sodium 79100 P 7440-28-0 Thallium 1.1 u F 7440-62-2 Vanadium 5.2 u P 7440-66-6 zinc 5.5 B P Color Before: COLORLESS_ Color After: COLORLESS_ Comments: Clarity Before: CLEAR_ Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 6 DUP050307772 D.S. EPA - CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES, Contract: MRA1S Lab Code: Case No.: _ SAS No. SDG No. FMD03 Matrix (soil/water): WATER Lab Sample ID: 2585276 Level (low/med): LOW Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429- -90--5_ Aluminum 627 P_ "7440- -36--0_ Antimony 12.3 U P_ "7440- -38--2_ Arsenic 1.3 u F_ "7440- -39--3_ Barium 93.7 B P_ "7440- -41-7 Beryllium 1.6 U P_ "7440- -43-91 cadmium 3.3 U P_ "7440- -70--2_ Calcium 104000 P_ `7440- -47--3_ Chromium 4.3 U P_ "7440- -48-4 Cobalt i 4.2 U P_ '7440' -50--8" Copper 8.2 B P_ "7439- -89-6" Iron 861 P_ "7439- -92-1" Lead 4.0 SN F_ '7439' -95-4" Magnesium 38500 P_ "7439- -96-5" Manganese 31.9 P_ "7439- -97-6" Mercury 0.0090 U CV _7440` -02-01 Nickel 4.8 U P_ _7440` -09-7 Potassium 975 B P_ 7782' -49-2 Selenium 1.4 B F_ "7440' -22-4" Silver 1.7 U P_ "7440' -23-5" Sodium 30100 P_ A "7440' -28-0" Thallium 1.1 U F_ ~7440' -62--2^ Vanadium 5.2 u P_ "7440' -66--6 Zinc 36.3 P Color Before: COLORLESS Color After: COLORLESS Comments: Clarity Before: CLEAR Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 A 7 DUP050307773 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: ___________ MRA2D Lab Code: ________ Case No.: _____________ SAS No.: SDG No.: FMD03 Matrix (soil/water): WATER Lab Sample ID: 2585278 Level (low/med): LOW Date Received: 09/21/96 % Solids 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 130 12.3 U 1.3 u 105 B 1.6 U 3.3 U 74600 4.3 u 5.3 B 5.1 U 205 0.84 U 27000 178 0.0090 U 4.8 U 3790 B 0.70 U 1.7 U 64800 1.1 u 5.2 u 6.8 B WN M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS. Color After: COLORLESS Comments: A Clarity Before: CLEAR, Clarity After: CLEAR FORM I - IN A Texture: Artifacts: ILM04.0 8 DUP050307774 U.S. EPA - CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO Lab Name: LANCASTER,, LABORATORIES,. Contract: MRA2S Lab Code: ______ __ Case No.: _ SAS No.: SDG No.: FMD03 .Matrix (soil/water): WATER Lab Sample ID: 2585279 Level (low/med): LOW Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS NO. Analyte Concentration C Q 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 54$ 12.3 u 1.3 u 66.8 B 1.6 U 3.3 U 144000 4.3 U 4.2 u 5.1 u 650 1.5 B 49200 37.3 0.0090 u 4.8 u 1620 B 123 1.7 u 52400 1.1 u 5.2 u 10.2 B WN S M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS. Color After: COLORLESS. Comments: Clarity Before: CLEAR, Clarity After: CLEAR Texture: Artifacts: FORM I - IN ILM04.0 9 DUP050307775 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: ___________ MRA3D Lab Code: ________ Case No.: _____________ SAS No.: SDG No.: FMD03 Matrix (soil/water): WATER Lab Sample ID: 2585283 Level (low/med): LOW Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight); UG/L CAS No. 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver 1 Sodium Thailima Vanadium Zinc 22.3 U 12.3 U 1.7 B 144 B 1.6 U 3.3 U 88300 4.3 U 4.2 u 5.1 u 160 0.84 u 28300 514 0.0090 u 4.8 u 3350 B 0.70 U 1.7 u 52800 1.1 u 5.2 u 6.8 B Q WN M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS Color After: COLORLESS, Comments: Clarity Before: CLEAR, Clarity After: CLEAR, Texture: Artifacts: FORM I - IN ILM04.0 A *.0 A DUP050307776 U.s. EPA - CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER_LABORATORIES_ Contract: MRA3S Lab Code: ____ Case No.: _ SAS No. SDG No. FMD03 Matrix (soil/water): WATER Level (low/med): LOW Lab Sample ID: 2585282 Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS NO. 7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 Analyte Concentration C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium-1 Zinc 29.8 B 12.3 U 1.3 U 244 1.6 U 3.3 U 134000 4.3 U 4.2 U 5.1 U 16.2 B 0.84 u 42400 3.6 u 0.0090 u 4.8 u 1590 B 164 1.7 u 27000 1.1 u 5.2 u 10.3 B Q WN * S M P P F P P P P P P P P F P P CV P P F P P F P P Color Before: COLORLESS. Color After: COLORLESS. Comments: Clarity Before: CLEAR. Clarity After: CLEAR. Texture: Artifacts: FORM I - IN ILM04.0 ii DUP050307777 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER LABORATORIES____ Contract: MRA4S Lab Code: ________ Case No. SAS No.: ________ SDG No.: FMD03 Matrix (soil/water) WATER Lab Sample ID: 2585281 Level (low/med): LOW Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429- 90-5 Aluminum 234 P_ "7440- 36-0" Antimony 12.3 U P_ "7440- 38-2" Arsenic 1.3 U F_ "7440- 39-3" Barium 44.6 B P_ "7440- 41-7" Beryllium 1.6 U P_ "7440- -43-9" Cadmium 3.3 U P__ "7440- 70-2" Calcium 330000 P_ "7440- 47-3" Chromium - 4.3 U P "7440- 48-4~ Cobalt 4.2 U P_ 7440- 50-8" Copper 5.1 U P_ "7439- 89-6" Iron 580 P_ "7439- 92-1" Lead 4.2 U WN F_ "7439- 95-4" Magnesium 106000 P_ A "7439- 96-5" Manganese 214 P_ "7439- 97-6" Mercury 0.0090 U CV "7440- 02-0" Nickel 4.8 u P_ "7440- 09-7" Potassium 4370 B P_ "7782- 49-2" Selenium 40.1 F_ "7440- 22-4" Silver 1.7 U P_ "7440- -2 3-5" Sodium 98000 P_ "7440- -28-0" Thallium 1.1 U F_ "7440- 62-2" Vanadium 5.2 U P_ "7440- 66-6" Zinc 16.7 B P Color Before: COLORLESS. Color After: COLORLESS Comments: Clarity Before: CLEAR_ Clarity After: CLEAR_ Texture: Artifacts: FORM I - IN ILM04.0 12 DU P050307778 U.s. EPA - CLP INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. Lab Name: LANCASTER__LABORATORIES_ Contract: MRAFB Lab Code: Case No.: _ SAS No.: SDG NO. FMD03 Matrix (soil/water) :: WATER Lab Sample ID: 2585285 Level (low/med): LOW Date Received: 09/21/96 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 7440-36-0 Antimony 22.3 U 12.3 u P_ P_ 7440-38-2 Arsenic 1.4 B F_ 7440-39-3 7440-41-7 7440-43-9 Barium Beryllium Cadmium 2.1 U 1.6 u 3.3 u P_ P_ P_ 7440-70-2 Calcium 61.0 B P_ 7440-47-3 Chromium 4.3 u P_ 7440-48-4 Cobalt 4.2 u P_ 7440-50-8 Copper 5.1 u P_ 7439-89-6 Iron 11.1 u P_ 7439-92-1 Lead 0.84 u N F_ 7439-95-4 Magnesium 24.0 u F_ 7439-96-5 Manganese 3.6 u P_ j 7439-97-6 Mercury 0.0090 u CV 7440-02-0 Nickel 4.8 u P_ 7440-09-7 Potassium 115 u P_ 7782-49-2 Selenium 0.70 u F_ 7440-22-4 Silver 1.7 u P_ 7440-23-5 Sodium 115 B P_ 7440-28-0 Thallium 1.1 u W F_ A 7440-62-2 Vanadium 5.2 u P_ 7440-66-6 Zinc 10.7 B P color Before: COLORLESS. Color After: COLORLESS. Comments: A Clarity Before: CLEAR Clarity After: CLEAR FORM I - IN Texture: Artifacts: ILM04.0 JL v DUP050307779 Quality Control Data 14 DUP050307780 U.S. EFA - CLP INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_ LABORATORIES___ Lab Code: ________ Case No.: _ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: _ SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) Aluminum 30000.0 Antimony 6000.0 Arsenic 50.0 Barium 6000.0 Beryllium 600.0 Cadmium 6000.0 Calcium 60000.0 Chromium 6000.0 Cobalt 1200.0 Copper 6000.0 Iron 6000.0 Lead 20.0 Magnesium 30000.0 Manganese 6000.0 Mercury 2.0 Nickel 12000.0 Potassium 60000.0 Selenium 20.0 Silver 600.0 Sodium ,60000.0 Thallium 50.0 Vanadium 2400.0 Zinc 6000.0 30328.11 5628.88 49. 38 5697.89 575.49 5707.85 59792.87 5802.17 1115.53 5763.13 5817.52 21.69 30327.64 5692.68 2.04 11362.51 60643.33 19.85 548.69 62217.87 50.19 2379.20 5699.41 101.1 93.8 98.8 95.0 95.9 95.1 99.7 96.7 93.0 96.1 97.0 108.4 101.1 94.9 102.0 94.7 101.1 99.2 91.4 103.7 100.4 99.1 95.0 True Continuing Calibration Found %R(1) Found %R(1) 25000.0 24431.18 97.7 25140.02 100.6 5000.0 4707.89 94.2 4730.77 94.6 40.0 41.54 103.8 43.83 109.6 5000.0 4774.24 95.5 4771.77 95.4 500.0 475.05 95.0 474.26 94.9 5000.0 ,4705.71 94.1 4704.77 94.1 50000.0 49070.69 98.1 49005.58 98.0 5000.0 4853.51 97.1 4831.61 96.6 1000.0 953.08 95.3 936.96 93.7 5000.0 ,4855.91 97.1 4855.79 97.1 5000.0 4849.17 97.0 4815.63 96.3 25.0 27.26 109.0 26.31 105.2 25000.0 24978.15 99.9 24898.22 99.6 5000.0 4721.60 94.4 4703.87 94.1 1.0 1.04 104.0 1.05 105.0 10000.0 9346.45 93.5 9329.10 93.3 50000.0 49502.84 99.0 49952.03 99.9 25.0 24.55 98.2 23.78 95.1 500.0 458.06 91.6 456.88 91.4 50000.0 50450.95 100.9 51278.33 102.6 40.0 41.55 103.9 42.93 107.3 2000.0 1959.17 98.0 1954.40 97.7 5000.0 4720.07 94.4 4691.66 93.8 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 DUP050307781 U. S. EPA * CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_JLABORATORIES____ Lab Code: ________ Case No.: _____________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: SDG No.: FMD03 Concentration Units: ug/L Analyte Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury___ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(1) 50.0 50.52 101.0 True Continuing Calibration Found %R(1) Found %R (1) 25000.0 5000.0 40.0 5000.0 500.0 5000.0 50000.0 5000.0 1000.0 5000.0 5000.0 25.0 25000.0 5000.0 1.0 10000.0 50000.0 25.0 500.0 50000.0 40.0 2000.0 5000.0 25777.18 103.1 4857.53 97.2 42.60 106.5 4898.88 98.0 491.10 98.2 4882.49 97.6 50867.64 101.7 5003.91 100.1 974.86 97.5 4980.24 99.6 5005.44 100.1 26.88 107.5 25368.12 101.5 4864.03 L_97.3 0.97 97.0 9657.98 __96.6 51198.66 102.4 23.23 92.9 469.50 93.9 52311.55 104.6 42.69 106.7 2012.71 100.6 4851.74 97.0 42.16 105.4 1.03 103.0 23.04 _92.2 42.31 105.8 M P P F P P P P P P P P F P P CV P P F P P F P P (1) Control Limits: Mercury 80-120; Other Metals 90-110? Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 16 DUP050307782 U.S. EPS - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No. : _____________ Initial calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No. : ________ SDG No. : FMD03 Concentration Units: ug/L Analyte Aluminum Antimony_ Arsenic Barium Beryllium cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(1) 20.0 19.90 99.5 True Continuing Calibration Found %R(1) Found %R(1) 40.0 41.65 104.1 25.0 1.0 25.0 26.11 104.4 1.03 103.0 22.86 91.4 26.29 105.2 1.02 102.0 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 17 DUP050307783 U.S. EPA - CLP 2A INITIAL AND CONTINUING.CALIBRATION VERIFICATION Lab Name: LANCASTER__LABORATORIES____ Lab Code: ________ Case No.: _____________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L Analyte Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(1) 20.0 20.69 103.4 20.0 19.58 ^_97.9 True Continuing Calibration Found %R(l) Found %R(1) M 25.0 25.0 25.95 103.8 24.85 99.4 25.69 102.8 24.76 99.0 NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR F NR NR NR NR NR (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 18 DUP050307784 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: IANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L gllg^S IS iiiS iiS S S gS il Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M NR 25.0 24.18 96.7 24.67 98.7 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 A FORM II (PART 1) - IN ILM04.0 18 DUP050307785 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTERJLABORATORIES____ T.ab Code: ________ Case No.: ___________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L MSSSSrSSSSSMSSMSSSSS Analyte Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calibration True Found %R(1) 20.0 19.08 95.4 True Continuing Calibration Found %R(1) Found %R(1) M NR NR NR 25.0 24.26 97.0 23.80 95.2 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 20 DUP050307786 U.s. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ Initial Calibration Source: LLI Continuing Calibration Source: LLI Contract: SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L g a a a a ^a a iB a g g g a a g a a g a g g s Analyte Initial calibration True Found %R(1) Continuing Calibration True Found %R(1) Found %R{1) Aluminum Antimony__ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel A Potassium Selenium 20.0 19.01 95.0 25.0 24.62 98.5 24.55 98.2 Silver Sodium Thallium Vanadium Zinc (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN ILM04.0 *O4 DUP050307787 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND TCP Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ AA CRDL Standard source: LLI_______' ICP CRDL Standard Source: LLI Contract: SAS No.: SDG No.: FMD03 Concentration Units: ug/L Analyte Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc CRDL Standard for AA True Found %R 10.0 10.72 107.2 3.0 0.2 5.0 10.0 3.12 104.0 0.19 95.0 4.07 81.4 14.09 140.9 True CRDL Standard for ICP Initial Final Found %R Found %R 120.0 125.87 104.9 130.48 108.7 10.0 10.0 20.0 100.0 50.0 9.81 98.1 9.38 93.8 17.60 88.0 99.30 99.3 53.77 107.5 9.81 98.1 8.89 88.9 17.58 ,87.9 107.98 108.0 51.23 102.5 30.0 80.0 20.0 100.0 40.0 31.31 104.4 79.25 99.1 20.35 101.8 99.96 100.0 39.46 98.6 32.67 108.9 78.66 98.3 21.14 105.7 101.42 101.4 39.49 98.7 FORM II (PART 2) - IN ILM04.Q n4 DUP050307788 U.s. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: IANCASTE_LABORATORIES____ t.ah code: ________ Case No.: ____________ AA CRDL Standard Source: LLI:__________ _ ICP CRDL Standard Source: LLI Contract: SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L Analyte Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc CRDL Standard for AA True Found %R 10.0 10.82 108.2 3.0 3.29 109.7 5.0 4.05 1 CD H b True CRDL Standard for ICP Initial Final Found %R Found %R FORM II (PART 2) - IN IIM04.0 DUP050307789 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ AA CRDL Standard Source: LLI ICP CRDL standard Source: LLI Contract: SAS No.: . SDG No.: FMD03 Concentration Units: ug/L Analyte CRDL Standard for AA True Found %R True CRDL Standard for ICP Initial Final Found %R Found %R Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead A Magnesium Manganese Mercury__ A Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 3.0 5.0 3.83 127.7 3.63 72.6 FORM II (PART 2) - IN ILM04.0 0 9 <k DUP050307790 U.s. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: LANCASTER LABORATORIES Lab Code: ___ _ Case No. : AA CRDL standard Source: LLI ICP CRDL Standard Source: LLI. Contract: SAS No.: ________ SDG No.: FMD03 Concentration Units: ug/L Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc i CRDL Standard for AA True Found %R 5.0 4.54 90.8 True CRDL Standard for ICP Initial Final Found %R Found %R FORM II (PART 2) - IN ILM04.0 DUP050307791 U.s. EPA - CLP 3 BLANKS Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ Preparation Blank Matrix (soil/water): WATER_ Preparation Blank Concentration Units (ug/L or mg/kg): UG/L_ SDG No.: FMD03 Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calib. Blank (ug/L) C 117 B 23.9 B 1.3 U 2.1 U 1.6 U 3.3 U 188 B 4.3 U 4.2 u 7.2 B 11.1 U 0.84 U 61.9 B 4.1 B -0.017 B -5.1 B 115 U -0.91 B 1.7 U 61.6 U 1.1 u 5.2 u 4.8 u _ Continuing Calibration Blank (ug/L) 1C2C3 C 22.3 U 20.9 B 1.3 U 2.1 u 1.6 u 3.3 u 25.0 u 4.3 u 4.2 u 7.0 B 15.8 B 0.84 u 24.0 u 3.6 u -0.020 B 4.8 u 115 u -1.1 B 1.7 U 61.6 U 1.1 U 5.2 U 4.8 U _ 22.3 U 24.0 B 1.3 U 2.1 U 1.6 U 3.3 U 25.0 U -4.4 B 4.2 U 5.1 U ^ 11.1 U 0.84 u 24.0 u 3.6 u -0.028 B 4.8 U 115 U -1.2 B 1.7 U 61.6 u 1.1 u 5.2 u 4.8 u 29.8 B 19.9 B 2.1 U 1.6 U 3.3 U 35.9 B 4.3 U 4.2 u 5.1 u 15.3 B 0.84 u 24.0 u 3.6 u -0.031 B 4.8 U 115 U -1.3 B 1.7 U 62.7 B 1.1 U 5.2 U 4.8 u Prepa ration Blank C 22.300 U 12.300 U 1.300 U 2.100 U 1.600 U 3.300 U 25.000 u 4.3 00 u 4.200 u 5.100 u 11.100 u 0.840 u 24.000 u 3.600 u 0.009 u. 4.800 u 115.000 u -1.540 B 1.700 u 61.600 u 1.100 u 5.200 u 6.500 B FORM III - IN ILM04.0 C A DUP050307792 3 BLANKS Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD03 Preparation Blank Matrix {soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): ______________ Analyte Initial Calib. Blank (ug/L) C Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 1.3 U 0.84 u _ continuing Calibration Blank (ug/L) 1C2 C 3 C 1.3 U 1.3 U 1.3 u 0.84 u -0.029 B -2.2 B 1.1 U 0.84 u -0.029 B -0.85 B -0.031 B Prepa ration Blank c M NR NR F NR NR NR NR NR NR NR NR F NR NR CV NR NR F NR NR F NR NR FORM III - IN ILM04.0 0>7 &i DUP050307793 U.S. EPA - CUP 3 BLANKS Lab Name: LANCASTER_LABORATORIES.___ Contract: __________' Lab Code: ________ Case No.: ____________ SAS No.: . SDG No.: FMD03 Preparation Blank Matrix (soil/water): _____________ Preparation Blank concentration Units (ug/L or mg/kg): ______________ Analyte Initial Calib. Blank (ug/L) C Aluminum Antiraony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc CO 0 1 0.84 u B Continuing Calibration Blank (ug/L) 1C 2 C3 C 0.84 U 0.84 U -1.2 B -1.5 B 0.70 u Prepa ration Blank C M NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR F NR NR NR NR NR FORM III - IN ILM04.0 <<m%w DUP050307794 U.S. EPA - CLP 3 BLANKS Lab Name: LANCASTER_LABORATORIES_____ Contract: T.at-i Code: ________ Case No.: ___________ SAS No.: ________ SDG No.: FMD03 Preparation Blank Matrix (soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): ______________ Analyte Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Initial Calib. Blank (ug/L) c continuing calibration Blank (ug/L) 1C2 C 3 -1.2 B Prepa ration C Blank C M NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR FORM III - IN ILM04.0 920 w DUP050307795 U.S. EFA - CLP 3 BLANKS Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD03 Preparation Blank Matrix (soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): ______________ Analyte Initial Calib. Blank (ug/L) C Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc -1.4 B Continuing Calibration Blank (ug/L) 1C2 C3 -1.8 B -1.4 B Prepa ration C Blank C M FORM III - IN ILM04.0 SO DUP050307796 O.s. EPA - CLP 3 BLANKS Lab Name: LANCASTER_LABORATORIES____ Contract: Tah code: ________ Case No.: ____________ SAS No.: Preparation Blank Matrix (soil/water): _____________ Preparation Blank Concentration Units (ug/L or mg/kg): Analyte Initial calib. Blank (ug/L) C Alummum_ Antimony" Arsenic Barium Beryllium Cadmium__ Calcium Chromium_ Cobalt____ Copper____ Iron Lead Magneslum Manganese Mercury Nickel Potassium Selenium_ Silver____ Sodium Thallium_ Vanadium" Zinc -0.75 B Continuing calibration Blank (ug/L) 1c2C3 0.70 u 0.70 u SDG No.: FMD03 Prepa ration Blank C M NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR F_ NR NR NR NR NR FORM III - IN ILM04.0 3i DUP050307797 U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ ICP ID Number: 02360_________ ICS Source: LLI SDG No.: FMD03 Concentration Units: ug/L Analyte True Sol. Sol. A AB Initial Found Sol. Sol. A AB %R Final Found Sol. Sol. A AB %R Aluminum_ 500000 Antimony_ 0 Arsenic__ Barium 0 Beryllium 0 Cadmium 0 Calcium 500000 Chromium 0 Cobalt 0 Copper 0 Iron 200000 Lead Magnesium 500000 Manganese 0 Mercury Nickel 0 Potassium 0 Selenium_ Silver 0 Sodium 0 Thallium_ Vanadium_ 0 Zinc 0 1 m 500000 600 479747 483642.3 96.7 -27 581.7 _97.0 485924 488926.0 97.8 -9 577.5 ~96.2 500 500 1000 500000 500 500 500 200000 7 478.7 95.7 6 488.2 97.6 0 464.4 92.9 0 478.2 95.6 8 876.8 87.7 5 890.5 89.0 468825 471634.0 94.3 478095 483345.4 96.7 4 455.6 91.1 2 466.9 93.4 0 435.9 87.2 1 450.5 90.1 0 469.3 93.9 -4 474.9 95.0 __ 175903 177409,6 _88.7 __ 179313 181290.3 __90.6 ooooo 484312 488215.8 97.6 -18 424.7 _84.9 488664 492145.9 98.4 -21 431.6 86.3 oo in 1000 0 -9 858.8 _85.9 71 105.2 -10 28 880.3 88.0 51.4 200 4 189.6 _94.8 5 192.3 96.2 0 115 31.1 32 52.0 500 1000 2 463.7 92.7 16 ____886.5 _88.6 2 474.2 94.8 15 ____904.4 J90.4 FORM IV - IN ILM04.0 32 DUP050307798 u.s. k - 5 p 5A SPIKE SAMPLE RECOVERY EPA SAMPLE NO Lab Name: LANCASTER_LABORATORIES___ Contract: _____________ MRA2SS Lab Code: ________ Case No.: ____________ SAS No.: _______ SDG No.: FMD03 Matrix (soil/water) : WATER________ Level (low/med): LOW % Solids for Sample: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Analyte Limit %R Aluminum 75-125 Antimony_ 75-125 Arsenic 75-125 Barium 75-125 Beryllium 75-125 Cadmium 75-125 Calcium Chromium 75-125 Cobalt 75-125 Copper 75-125 Iron 75-125 Lead 75-125 Magnesium Manganese 75-125 Mercury 75-125 Nickel 75-125 Potassium Selenium Silver 75-125 Sodium Thallium 75-125 Vanadium 75-125 Zinc 75-125 Spiked Sample Result (SSR) C 2587.3800 528.6400 40.2000 2013.2000 49.9300 45.9600 199.2500 476.9800 246.5900 1602.0500 14.3000 513.5700 1.1100 478.7500 100.6500 46.3200 45.2300 488.8600 485.6700 Sample Spike Result (SR) C Added (SA) 542.0400 12.3000 U 1.3000 U 66.8500 B 1.6000 u 3.3000 u 2000.00 500.00 40.00 2000.00 50.00 50.00 4.3000 u 4.2000 u 5.1000 u 649.8700 1.5100 B 200.00 500.00 250.00 1000.00 20.00 37.3400 0.0090 U 4.8000 U 500.00 1.00 500.00 122.6562 1.7000 u 10.00 50.00 1.1000 u 5.2000 u 10.1800 B 50.00 500.00 500.00 %R Q M 102.3 P 105.7 P 100.5 F 97.3 P 99.9 P 91.9 P NR 99.6 P 95.4 P 98.6 P 95.2 P 64.0 N F NR 95.2 P 111.0 CV 95.8 P NR -220.1 F 92.6 P NR 90.5 F 97.8 P 95.1 P Comments: FORM V (PART 1) - IN ILM04.0 Zo DUP050307799 U.S. EPA - CLP 6 DUPLICATES EPA SAMPLE NO. Lab Name: LANCASTEK_LABORATORIES_____ Contract: _____ MRA2SD Lab Code: _______ Case No. : ____________ SAS No. : SDG No.: FMD03 Matrix (soil/water): WATER________ Level (low/med) : LOW % Solids for Sample: 0.0 % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L____ Control Analyte Limit Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc 200.0 15.0 25.0 sample (S) c 542.0400 12.3000 u 1.3000 u 66.8500 B 1.6000 u 3.3000 u 143917.6400 4.3000 u 4.2000 u 5.1000 u 649.8700 1.5100 B 49241.3500 37.3400 0.0090 U 4.8000 u 1623.3200 B 122.6562 1.7000 U 52443.6200 1.1000 u 5.2000 u 10.1800 B Duplicate (D) C 515.6700 12.3000 U 1.3800 B 66.8500 B 1.6000 U 3.3000 U 142817.0400 4.3000 U 4.2000 U 5.1000 U 610.4500 0.8400 u 48932.1700 37.3600 0.0140 1 4.8000 u 1578.1900 B 135.9551 1.7000 U 52255.2600 1.1000 U 5.2000 U 10.1700 B RPD 5.0 200.0 0.0 0.8 6.3 200.0 0.6 0.1 200.0 2.8 10.3 0.4 0.1 QM P P F P P P P P P P P F P P CV P P F P P F P P FORM VI - IN ILM04.0 3d DUP050307800 U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Lab Name: LANCASTER_LABORATORIES____ r.ai-i Code: ________ Case No.: ____________ solid LCS source: ________________ Aqueous LCS Source: LLI Contract: SAS No.: ________ SDG No.: FMD03 Analyte Aqueous (ug/L) True Found %R Aluminum_ Antimony_ Arsenic__ Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium_ Vanadium_ Zinc 2000.0 500.0 40.0 2000.0 50.0 50.0 4000.0 200.0 500.0 250.0 1000.0 20.0 2000.0 500.0 1.0 500.0 4000.0 10.0 50.0 4000.0 50.0 500.0 500.0 2000.02 100.0 542.27 108.5 37.64 94.1 1988.44 99.4 49.48 99.0 47.11 94.2 4056.94 101.4 200.20 100.1 495.29 99.1 252.71 101.1 1024.57 102.5 2 0.17 100.8 2035.18 101.8 487.77 97.6 1.05 105.0 495.90 99.2 3975.35 99.4 8.32 83.2 49.60 99.2 4101.31 102.5 50.93 101.9 500.51 100.1 498.04 99.6 True Solid (mg/kg) Found C Limits -- %R FORM VII - IN ILM04.0 iD DUP050307801 U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Lab Name: LANCASTER_LABORATORIES____ Lab Code: ________ Case No.: ____________ Contract: SAS No.: ________ Concentration Units: ug/L SDG No.: FMD03 EPA Sample 0 ADD No. An ABS MRA1S MRA2S MRA2SD MRA3S PB 0. 019 SE 0.047 SE 0.048 SE 0.057 1 ADD CON ABS 5.00 0.046 5.00 0.057 5.00 0.058 5.00 0.068 2 ADD CON ABS 10.00 0.072 10.00 0.066 10.00 0.066 10.00 0.075 3 ADD CON ABS Final Cone. r 15.00 0.094 4.0 0.9989 15.00 0.076 24.5 0.9998 15.00 0.075 27.2 0.9991 15.00 0.084 ____32.8 0.9964 1 : FORM VIII - IN ILM04.0 3 r. DUP050307802 U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Lab Name: LANCASTER LABORATORIES Lab Code: Case No.: Matrix (soil/water): WATER Contract: SAS No.: EPA SAMPLE NO. ______________ __ MRA2S L SDG No.: FMD03 Level (low/med): LOW Concentration Units: ug/L Analyte Initial Sample Result (I) C Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium_ Vanadium Zinc 542.04 12.30 U 66.85 B 1.60 U 3.30 u 143917.64 4.30 u 4.20 u 5.10 u 649.87 49241.35 37.34 4.80 u 1623.32 B 1.70 U 52443.62 5.20 U 10.18 B _ Serial Dilution Result (S) C 593.60 B 63.50 B 70.15 B 8.00 U 16.50 U 147672.60 21.50 u 21.00 u 25.50 u 694.65 50499.80 54.95 B 24.00 U 1826.20 B 8.50 U 53008.75 26.00 U 52.90 B % Differ ence 9.5 4.9 2.6 6.9 2.6 47.2 12.5 1.1 419.6 QM P P P P P P P P P P P ~ P ~ P " P P FORM IX - IN XLM04.0 37 DUP050307803 Verification of Instrument Parameters 38 DUP05 0307804 U.s. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES;___ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD03 ICP ID Number:, ____02360_____ Date: 07/15/96 Flame AA ID Number: ________________ Furnace AA ID Number: Analyte Wave length (nm) Aluminum 308.21 Antimony_ 206.83 Arsenic Barium 493.40 Beryllium 313.04 Cadmium 226.50 Calcium 317.93 Chromium 267.71 Cobalt 228.61 Cooper 324.75 Iron 259.94 Lead Magnesium 279.07 Manganese 257.61 Mercury Nickel 231.60 Potassium 766.49 Selenium Silver 328.06 Sodium 589.59 Thallium Vanadium 292.40 Zinc 213.85 Back ground CRDL (ug/L) 200 60 200 5 5 5000 10 50 25 100 5000 15 40 5000 10 5000 50 20 IDL (ug/L) M 22.3 P 12.3 P NR 2.1 P 1.6 P 3.3 P 25.0 P 4.3 P 4.2 P 5.1 P 11.1 P NR 24.0 P 3.6 P NR 4.8 P 115 P NR 1.7 P 61.6 P NR 5.2 P 4.8 P Comments: FORM X - IN ILM04.0 39 DUP050307805 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER__LABORATORIES____ Contract: Lab Code: ________ Case No. : ____________ SAS No. : _____ SDG No. : FMD03 ICP ID Number: ________________ Date: 07/15/96 Flame AA ID Number: Furnace AA ID Number: ____02803 Analyte Wave length Back CRDL (nm) ground (ug/L) Aluminum_ Antimony_ Arsenic__ Barium Beryllium Cadmium Calcium Chromium_ Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium_ Silver Sodium Thallium 276.80__ BD Vanadium_ Zinc 10 IDL (ug/L) M NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 1.1 F NR NR Comments: FORM X - IN ILM04.Q 40 DUP050307806 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES____ Contract: T.aT-i code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD03 ICP ID Number: ________________ Date: 07/15/96 Flame AA ID Number: ________________ Furnace AA ID Number: __ 03812 Analyte wave length Back CRDL (nm) ground (ug/L) IDL (ug/L) M Aluminum_ NR Antimony_ NR Arsenic__ NR Barium NR Beryllium NR Cadmium NR Calcium NR Chromium_ NR Cobalt NR Copper NR Iron NR Lead 283.30__ BZ 3 0.84 F_ Magnesium NR Manganese NR Mercury__ NR Nickel NR Potassium A Selenium_ NR NR Silver NR Sodium NR Thallium NR Vanadium_ NR Zinc NR Comments: FORM X - IN ILM04.0 41 DUP050 307807 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: ____________ SAS No.: ________ SDG No.: FMD03 ICP ID Number: ________________ Date: 07/15/96 Flame AA ID Number: ____________ Furnace AA ID Number: ____04724 Analyte Wave length Back (nm) ground Alummum_ Antimony" Arsenic_] 193.70__ BZ Barium Beryllium Cadmium Calcium Chromium_ Cobalt____ Copper____ Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium__ silver Sodium" Thallium_ Vanadium" Zinc CRDL (ug/L) 10 IDL (ug/L) M NR NR 1.3 F_ NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR Comments: FORM X - IN ILM04.0 42 DUP050307808 U.s. EFA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTERJLABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: _________ SDG No.: FMD03 ICP ID Number: _________________ Date: 07/15/96 Flame AA ID Number: _________________ Furnace AA ID Number: ____ 04725______ Analyte Wave length Back (nm) ground Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium 196.00 Silver Sodium Thallium Vanadium Zinc BZ CRDL (ug/L) 5 IDL (ug/L) M NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 0.70 F NR NR NR NR NR Comments: FORM X - IN ILM04.0 4v DUP050307809 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: LANCASTER_LABORATORIES_____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ SDG No.: FMD03 ICP ID Number: _________________ Date: 07/15/96 Flame AA ID Number: ____ 05220 Furnace AA ID Number: Analyte Wave length Back (nm) ground Aluminum_ Antimony_ Arsenic__ Barium Beryllium Cadmium__ Calcium__ Chromium_ Cobalt____ Copper____ Iron Lead Magnesium Manganese Mercury 254.00__ Nickel Potassium Selenium_ Silver____ Sodium Thallium Vanadium" Zinc CRDL IDL (ug/L) (ug/L) M NR NR NR NR NR NR NR NR NR NR NR NR NR NR 0.2 _0.0090 CV NR NR NR NR NR NR NR NR Comments: FORM X - IN ILM04.0 44 DU P0 50307810 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ SDG No.: FMD03 ICP ID Number: ____ 02360 ____ Date: 09/12/96 Analyte Wave length (nm) Interelement Correction Factors for: A1 Ca Fe Mg BA Aluminum_ 308.21 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Antimony_ ___206.83 _0.0000000 _0.0000000 _0.0001660 _0.0000000 _0.0000000 Arsenic___ Barium 493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Cadmium 226.50 -0.0000230 0.0000000 0.0003090 0.0000000 0.0000000 Calcium 317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Chromium_ 267.71 0.0000000 0.0000000 -0.0000960 -0.0000200 0.0000000 Cobalt____ 228.61 0.0000000 0.0000000 0.0000000 0.0000000 0.0007050 Copper____ 324.75 0.0000000 0.0000000 0.0000200 0.0000000 0.0000000 Iron ___259.94 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Lead Magnesium 279.07 0.0000000 0.0001830 -0.0001000 0.0000000 0.0000000 Manganese ___257.61 -0.0000100 _0.0000060 -0.0000530 _0.0000400 _0.0000000 Mercury Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Potassium ___766.49 _0.0000000 -0.0002000 _0.0000000 _0.0000000 _0.0000000 Selenium_ Silver 328.06 0.0000000 -0.0000190 -0.0003420 -0.0000100 0.0000000 Sodium ___589.59 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Thallium_ Vanadium 292.40 0.0000000 0.0000000 -0.0000200 0.0000000 0.0000000 Zinc __ 213.85 -0.0000180 _0.0000000 _0.0001370 _0.0000090 _0.0000000 Comments: FORM XI (PART 1) - IN ILM04.0 k5 DUP050307811 U.s. EPA - CLP 11B .ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: LANCASTER LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ______ SDG No.: FMD03 ICP ID Number: ____ 02360 ____ Date: 09/12/96 Analyte Wave length (nm) Interelement Correction Factors for: CD CO CR CU MN Aluminum_ 308.21 0.0000000 -0.0172320 0.0000000 0.0000000 0.0002970 Antimony_ ___206.83 _0.0000000 _0.0000000 _0.0071050 _0.0000000 _0.0000000 Arsenic__ Barium 493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Cadmium 226.50 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Calcium 317.93 0.0000000 0.0000000 0.0004200 0.0000000 0.0000000 Chromium Cobalt Copper Iron Lead 267.71 0.0002360 0.0000000 0.0000000 0.0000000 0.0000800 228.61 0.0007480 0.0000000 0.0001000 0.0000000 0.0000000 324.75 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 ___259.94 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0001000 Magnesium 279.07 0.0000000 -0.0015690 -0.0008500 0.0000000 -0.0085400 Manganese ___257.61 _0.0000000 _0.0000000 _0.0000000 -0.0003800 _0.0000000 Mercury Nickel 231.60 0.0000000 0.0013660 0.0000000 0.0000000 0.0000000 Potassium ___766.49 _0.0000000 _0.0000000 _0.0011180 _0.0000000 -0.0002000 Selenium Silver Sodium 328.06 0.0000000 0.0000000 0.0000000 0.0000000 0.0000900 ___589.59 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Thallium Vanadium 292.40 0.0000000 0.0000000 -0.0023290 0.0000000 0.0000000 Zinc ___213.85 _0.0000000 _0.0000000 _0.0000000 _0.0038820 _0.0000000 Comments: FORM XI (PART 2) - IN ILM04.0 DUP050307812 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: LANCASTER,LABORATORIES____ Contract: Lab Code: ________ Case No. : _____________ SAS No.: ________ SDG No.: FMD03 ICP ID Number: ____ 02360 ____ Date: 09/12/96 Analyte Wave length (nm) Interelement Correction Factors for: MO NI SB SN TI Aluminum_ 308.21 0.0069690 0.0000000 0.0000000 0.0000000 0.0000000 Antimony_ ___206.83 JO.0014310 _0.0004510 _0.0000000 -0.0019600 _0.0013270 Arsenic___ Barium 493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Cadmium__ 226.50 0.0001140 0.0000460 0.0000000 0.0000000 0.0002900 Calcium 317.93 0.0000000 "*0.0000000 0.0000000 0.0000000 0.0023260 Chromium 267.71 -0.0026620 0.0000000 0.0000000 0.0000000 0.0001400 Cobalt____ 228.61 0.0000000 0.0002320 0.0000000 0.0000000 0.0018800 Copper 324.75 0.0005340 0.0000000 0.0000000 0.0000000 0.0004750 Iron ___259.94 _0.0000000 _0.0000000 _0.0000000 _0.0000000 -0.0032890 Lead Magnesium 279.07 -0.0185040 0.0000000 0.0000000 0.0000000 -0.0044080 Manganese ___257.61 -0.0002990 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Mercury Nickel 231.60 -0.0022180 0.0000000 0.0000000 0.0000000 0.0000000 Potassium ___766.49 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0005230 Selenium_ Silver 328.06 0.0000000 0.0000000 0.0000000 0.0000000 -0.0001600 Sodium ___589.59 _0.0031250 _0.0000000 _0.0000000 _0.0000000 _0.0050000 Thallium_ Vanadium 292.40 -0.0059350 0.0000000 0.0000000 0.0000000 0.0001790 Zinc ___213.85 _0.0000000 _0.0033870 _0.0000000 _0.0000000 _0.0000000 A Comments: FORM XI (PART 2) - IN ILM04.0 4 n i DUP050307813 U.s. EPA - CLP 12 ICP LINEAR RANGES (QUARTERLY) Lab Name: LANCAS TER__LABORATORIES Lab Code: ________ Case No.: ICP ID Number: 02360 Contract: SAS No.: ________ SDG No.: FMD03 Date: 07/15/96 Analyte Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Conner Iron Lead Magnesium Manganese Mercury__ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Integ. Time (Sec.) 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 Concentration (ug/L) M 600000.0 p 200000.0 p NR 100000.0 P 10000.0 P 100000.0 P 600000.0 P 100000.0 P 100000.0 P 100000.0 P 250000.0 P NR 600000.0 P 100000.0 P NR 100000.0 P 900000.0 P NR 50000.0 P 900000.0 P NR 100000.0 P 100000.0 P Comments: A FORM XII - IN ILM04.0 48 DUP050307814 Preparation and Run Logs DUP050307815 tl.S. EPA - CLP 13 PREPARATION LOG Lab Name: LANCASTER_LABORATORIES____ Contract: ________________ Lab Code: ________ Case No.: _____________ SAS No.: ________ SDG. No.: FMD03 Method: P EPA Sample No. LCSW MR3DD MRA1D MRA1S MRA2D MRA2S MRA2SD MRA2SS MRA3D MRA3S MRA4S MRAFB PBW Preparation Date. 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 Weight (gram) Volume (ml) 100 100 100 100 100 100 100 100 100 100 100 100 100 FORM XIII - IN ILM04.0 50 DUP050307816 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: LANCASTER_LABORATORIES____ Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ Method: F SDG No.: FMD03 EPA Sample No. LCSW MR3DD MRA1D MRA1S MRA2D MRA2S MRA2SD MRA2SS MRA3D MRA3S MRA4S MRAFB PBW Preparation Date 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 Weight (gram) Volume (ml) 100 100 100 100 100 100 100 100 100 100 100 100 100 FORM XIII - IN ILM04.0 51 DUP050307817 u.s. EPA - CLP 13 PREPARATION LOG Lab Name: LANCASTER LABORATORIES ' Contract: Lab Code: ________ Case No.: _____________ SAS No.: ________ Method: CV SDG No.: FMD03 EPA Sample No. LCSW MR3DD MRA1D MRA1S MRA2D MRA2S MRA2SD MRA2SS MRA3D MRA3S MRA4S MRAFB PBW Preparation Date 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 09/24/96 Weight (gram) Volume (ml) 8 8 8 8 8 8 8 8 8 8 8 8 8 FORM XIII - IN ILM04.0 5o DUP050307818 U.s. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: Lab Code: ________ Case No. : SAS No.: ________ SDG No. FMD03 Instrument ID Number: 02360_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes As ABB Cc c c c FpMMHN Ks ANTV z LB s AEDARouE BGNG I E GA L N SO S S s s ICV ICB CRI ICSA ICSAB CCV CCB PBW LCSW MRA2S MRA2SA MRA2SD MRA2SS MRA2SL MRA1S MRA1D MRA2D CCV CCB MRA4S MRA3S MRA3D MR3DD A MRAFB CRI ICSA ICSAB 1.00 2106 1.00 2109 1.00 2113 1.00 2116 1.00 2119 1.00 2122 1.00 2126 1.00 2130 1.00 2134 1.00 2138 1.00 2142 1.00 2146 1.00 2150 1.00 2154 1.00 2158 1.00 2202 1.00 2206 1.00 2210 5.00 2214 1.00 2218 1.00 2222 1.00 2226 1.00 2230 1.00 2234 1.00 2238 1.00 2242 1.00 2246 1.00 2250 1.00 2254 1.00 2258 1.00 2302 1.00 2306 XX X X XX XX X XX XX XX XX XX XX XX XX X XX X XX X X X XX XX X XXXXXXXX XXXXXXXX XX XXX XXXXXXXX XXXXXXXX XXXXXXXX XXXXXXXX XXXXXXXX X XX X X X XX XXXXXXXX XX X X Xx XX X XX XX XX XX XX XX XX XX XX XX XX X X XX XX XX X X--XX XX XX X XX XX X XX XX XX_ X X X X """ XX XX -- XX XX XX XX XX XX -- XX XX XX XX XX XX XX XX XX XXXXXXXX XXX XXXX XX X XX X _ X X--XX-- X XX XX XX XX XXXXXXXX XXXXXXXX XXXXXXXX XX XX XX XX"X X -- XX--X X XX XX X X X X ---- XX XX XX XX XX XXXXXXXX XXXXXXXX XXXXXXXX XXXXXXXX XX XX XX XX XX--X X XX XX XX X X X X mmm X X X X -- XX XX XX XX XX XXXXXXXX XX X X X X X X X X "" X X XX XX X X X X --- X X X X XX XX X XX XXXXXXXX XX XXXXXXXX XX XX XXX X -- XXXXXXXX XX XX XX X XX X X X X X X X --- X X x X X X X X --* -- -- XX--XXXXXXXX--XX--X X--X X-XX- FORM XIV - IN A ILM04.0 0 DUP050307819 U.s. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER__LABORATORIES Contract: Lab Code: Case No.: SAS No. : ________ SDG No. : FMD03 Instrument ID Number: 02360 Method: P Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes AsABBc ccC CF PMMHNKsANTVz LBsAE DAROuE B GNG I E GAL N CCV CCB 1.00 2310 1.00 2314 XX XX XXXXXX XX XXXXXX XX XX XX XX XX XX XX XX XX FORM XIV - IN ILM04.0 54 DUP050307820 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER__LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No. FMD03 Instrument ID Number: Q4724_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes ASABBCCc c CF PMMHNKS ANTVz LB S AE DAR0UE B GN G I E GAL N SO S10 S20 S40 S60 S80 ICV ICB CRA CCV CCB PBW PBWA LCSW LCSWA MRA2S MRA2SA MRA2SD MRA2SDA MRA2SS ZZZZZZ CCV CCB 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1620 1624 1629 1633 1637 1641 1646 1650 1654 1658 1702 1706 1710 1715 1719 1724 1728 1732 1737 1741 1745 1749 1753 96.6 106.3 __ 111.0 100.2 X X X X X X X X X X X X X X X X X X X X X ... . .m ___ __ -- wmm ***" * *" ******* *""* "* ***** "* ***** -- ~ ""* "" FORM XIV - IN ILM04.0 5txj DUP050307821 XI.So EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER__LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD03 Instrument ID Number: 04724_ Method: F_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes A S AB BC C C C c F PMMHN K S AN T VZ LB S A E DARO uE BGNG I E G A L N SO S10 S20 S40 S60 S80 ICV ICB CRA CCV CCB MRA1S MRA1SA MRA1D MRA1DA MRA2D MRA2DA MRA4S MRA4SA MRA3S MRA3SA CCV CCB MRA3D MRA3DA MR3DD MR3DDA MRAFB MRAFBA ZZZZZZ ZZZZZZ ZZZZZZ 1.00 0415 1.00 0419 1.00 0424 1.00 0428 1.00 0432 1.00 043 6 1.00 044 0 1.00 0445 1.00 0449 1.00 0453 1.00 0457 1.00 0501 1.00 0505 1.00 0510 1.00 0514 1.00 0519 1.00 0523 1.00 0527 1.00 0532 1.00 0536 1.00 0540 1.00 0544 1.00 0548 1.00 0552 1.00 0557 1.00 0601 1.00 0605 1.00 0609 1.00 0614 1.00 0618 1.00 0622 1.00 0626 106.4 93.6 106.4 90.2 102.6 98.4 98.2 85.8 X X X X X X X X X X X X X X X X X X X X X X X X X X X X X FORM XIV - IN ILM04.0 56 A DUP050307822 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES_ Contract: Lab Code: ________ Case No. : SAS NO.: ________ SDG No.: FMD03 Instrument ID Number: 04724 Method: F Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. zzzzzz ccv CCB D/F Time 1.00 0630 1.00 0634 1.00 0638 %R Analytes A S AB BC CC CC FPMMHNKSANTVZ LB SA E DARoU E BGN G I E GAL N X X __ _ __ FORM XIV - IN ILM04.0 A A 57 DUP050307823 U.S. EP& - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJLABORATORIES. Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD03 Instrument ID Number: 03812_ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes ASABBCCC C C FPMMHNKS ANTV z LB SAE DAROUE B GNG I E GA L N SO S3 S9 S15 S3 0 S60 ICV ICB CRA CRAA CCV CCB PBW PBWA LCSW LCSWA MRA2S MRA2SA MRA2SD MRA2SDA MRA2SS ZZZZZZ CCV CCB MRA1S MRA1SA MRA1D MRA1DA MRA2D MRA2DA MRA4S MRA4SA 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1. 00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1625 1630 1635 1640 1645 1650 1654 1659 1704 1708 1713 1718 1722 1727 1732 1736 1741 1746 1750 1755 1800 1805 1809 1814 1818 1823 1827 1832 1837 1842 1846 1851 92.6 81.4 54.5 53.3 64.4 54.8 67.0 32.6 __ _ -- __ __ X X X X X X X X X X X X X X X X X X X X X X X X X X . __ -- ---- "" ------ ~~ "" *--* ~ ~~ ~ ---- "-- FORM XIV - IN ILM04.0 5S Mimm DUP050307824 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCAS TER__LABORATORIES Contract: Lab Code: ________ Case No. : SAS No.: ________ SDG No. FMD03 Instrument ID Number*: 03812 Method: F Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. D/F Time %R Analytes A S A B B C C C C C E PMMH NK S AN T V Z L B S A E D A R 0 U E B G N G I. E G A L N MRA3S MRA3SA CCV CCB 1.00 1855 1.00 1900 1.00 1905 1.00 1909 64.4 X X X X FORM XIV - IN ILM04.0 59 DUP050307825 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: _______________ Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD03 Instrument ID Number: 03812_ Method: F_ Start Date: 09/25/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes A S AB BCC C C C F PMMHNKS ANTVZ LB SAE DAR0uE BGN G I E GAL N SO S3 S9 S15 S30 S60 ICV ICB CRA CRAA CCV CCB MRA4S MRA4SA MRA3D MRA3DA MR3DD MR3DDA MRAFB MRAFBA ZZZZZZ zzzzzz CCV CCB 1.00 2334 1.00 2339 1.00 2344 1.00 2348 1.00 2353 1.00 2358 1.00 0003 1.00 0007 1.00 0012 1.00 0017 1.00 0021 1.00 0026 5.00 0031 5.00 0035 1.00 0040 1.00 0045 - 1.00 0049 1.00 0054 1.00 0059 1.00 0104 1.00 0108 1.00 0113 1.00 0117 1.00 0122 84.9 65.5 70.0 96.4 X X X X X X X X X X X X X X X X X X X X X FORM XIV - IN ILM04.0 60 DUP050307826 U.s. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER__LABORATORIES Contract: Lab Code: ________ Case No.: SAS No.: SDG No FMD03 Instrument ID Number: 03812_ Method: F_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes AS A B BC C C C C F PMMHN K S AN T V Z LBS AE DAR0uE BGN G I E GAL N SO S3 S9 S15 S30 S60 ICV ICB CRA CCV CCB MRA1S0 MRA1S1 MRA1S2 MRA1S3 CCV CCB A 1.00 0454 1.00 0456 1.00 0459 1.00 0502 1.00 0504 1.00 0507 1.00 0510 1.00 0512 1.00 0515 1.00 0517 1.00 0520 1.00 0522 1.00 0525 1.00 0527 1.00 0530 1.00 0532 1.00 0535 X X X X X X X X X X X X X X X X X A FORM XIV - IN ILM04.0 6 DUP050307827 u.s. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Contract: ________________ Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD03 Instrument ID Number: 04725_ Method: F_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes A S AB B C C C C C F PMMHN KS ANTV z LB SAE DAR0uE BGNG I E GAL N SO S5 S15 S25 S40 S50 ICV ICB CRA CCV CCB ZZZZZZ zzzzzz ZZZZZZ ZZZZZZ zzzzzz zzzzzz zzzzzz A zzzzzz zzzzzz zzzzzz CCV CCB zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz 1.00 0837 1.00 0841 1.00 0845 1.00 0849 1.00 0853 1.00 0857 1.00 0901 1.00 0905 1.00 0909 1.00 0913 1.00 0917 1. 00 0921 1.00 0925 1.00 0930 1.00 0934 1.00 0938 1.00 0942 1.00 0946 . 1.00 0950 1.00 0955 1.00 0959 1.00 1003 1.00 1007 1.00 1010 1.00 1015 1.00 1019 1.00 1023 1.00 1027 1.00 1031 1.00 1035 1.00 1039 1.00 1043 X X X X X X X X X X X X X FORM XIV - IN --v 03 ILM04.0 DUP050307828 U.s. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: L&NCASTER_LABORATORIES, Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD03 Instrument ID Number: 04725_ Method: F_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes ASABBC C C CCF PMMH NKS ANTV z LB S AE DAR0UE BGNG I E GAL N ZZZZZZ CCV CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV CCB PBW PBWA LCSW LCSWA MRA2S MRA2SA MRA2SD MRA2SDA MRA2SS ZZZZZZ CCV CCB 1.00 1047 1.00 1051 1.00 1055 1.00 1059 1.00 1103 1.00 1107 1.00 1111 1.00 1115 1.00 1119 5.00 1123 5.00 1127 1.00 1131 1.00 1135 1.00 1139 1.00 1143 1.00 1147 1.00 1151 112.8 1.00 1155 1.00 1159 162.8 1.00 1204 1.00 1208 -9999.9 1.00 1212 1.00 1216 -9999.9 1.00 1220 1.00 1224 1.00 1229 1.00 1233 ____ X X ~ -- -- " """ X X X X X X MM "" -- MM M"M. MMP MM. MM. MM. MM MM MM X X FORM XIV - IN ILM04.0 6 ,r\ DUP050307829 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERJIABORATORIES. Contract: Lab Code: ________ Case No.: SAS No.: ________ SDG No.: FMD03 Instrument ID Number: 04725_ Method: F_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes ASAB BC C CC C F PMMHNKS ANTVz LB S AE DAROuE B GNG I E GA L N SO S5 S15 S25 S40 S50 ICV ICB CRA CCV CCB ZZZZZZ zzzzzz ZZZZZZ zzzzzz MRA2S MRA2SA MRA2SD MRA2SDA MRA2SS ZZZZZZ CCV CCB MRA1S MRA1SA MRA1D MRA1DA MRA2D MRA2DA MRA4S MRA4SA MRA3S 1.00 1546 1.00 1550 1.00 1554 1.00 1558 1.00 1602 1.00 1606 1.00 1610 1.00 1614 1.00 1618 1.00 1622 1. 00 1626 1.00 1630 1.00 1635 1.00 1639 1.00 1643 5.00 1647 5.00 1651 118.2 5.00 1656 5.00 1700 122.0 5.00 1704 5.00 1708 1.00 1712 1.00 1716 1.00 1720 1.00 1724 95.2 1.00 1728 1. 00 1732 91.5 1. 00 1736 1. 00 1740 113.4 1.00 1745 1.00 1749 -9999.9 5.00 1753 X X X X X X X X X X X X X-- X X X X-- X X X FORM XIV - IN ILM04.0 64 DUP050307830 ? U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES. Contract: Lab Code: ________ Case No. : SAS No.: ________ SDG No. FMD03 Instrument ID Number: 04725_ Method: F_ Start Date: 09/26/96 End Date: 09/26/96 EPA Sample No. D/F Time %R Analytes ASABBCCCCCF PMMHNK SAN TV z LB S AE DARouE B GNG I E G A L N MRA3SA CCV CCB MRA3D MRA3DA MR3DD MR3DDA MRAFB MRAFBA ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV CCB 5.00 1757 __ 139.5 1.00 1801 1.00 1805 -- X X 1.00 1808 1.00 1812 99.4 X X --- 1.00 1817 1.00 1820 1.00 1825 99.0 -- - - -- -- -- -- -- -- X X X -- -- - -- -- -- 1.00 1829 __ 110.6 X 1.00 1833 1.00 1837 -- 1.00 1841 1.00 1845 1.00 1849 X- 1.00 1853 -------------------------------- X------------ FORM XIV - IN ILM04.0 'M. DU P050307831 U.S. EPA - CLP 14 ANALYSIS REN LOG Lab Name: LANCASTER_ LABORATORIES Contract: Lab Code Case No.: SAS No.: SDG NO.: FMD03 Instrument ID Number': 04725 Method: P start Date: 09/26/96 End Date: 09/26/96 EPA Sample . NO. ' D/F Time %R Analytes ASA C C e cC F PMMHN KS ANTV z LBSAEDAR0u E BGNG I E GAL N SO 55 S15 S25 S40 S50 ICV ICB CRA CCV CCB MRA4S MRA4SA zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz CCV A CCB 1.00 2213 1.00 2217 1.00 2221 1.00 2225 1.00 2229 1.00 2233 1.00 2237 1.00 2241 1.00 2245 1.00 2249 1.00 2253 2.00 2257 2.00 2301 5.00 2306 5.00 2310 5.00 2314 5.00 2318 5.00 2322 5.00 2326 5.00 2331 5.00 2335 1.00 2339 1.00 2343 95.1 . ___ , - X X X X X X X X -- X X X -- ~-- X X ---- -- mmm ---- mmm -- ~""~ mmm mtmm mmm X "_ X --** FORM XIV - IN ILM04.0 66 DUP050307832 U.S. Sift. - CLP 14 ANALYSIS RTJN LOG Lab Name: LANCASTERJLAB.ORATORIES____ Contract:; Lab Code: ________case No..: . _______ SAS No.: ' SDG No.: FMD03 Instrument ID Number: 04725^ Method: F_ Start Date: 09/27/96 End Date: 09/27/96 EPA Sample No. SO S5 sis S25 S40 S50 ICV ICB CRA CCV CCB ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 MRA2S0 MRA2S1 MRA2S2 MRA2S3 MRA2SD0 MRA2SD1 MRA2SD2 MRA2SD3 MRA3S0 MRA3S1 MRA3S2 MRA3S3 ZZZZZZO ZZZZZZ1_ CCV D/F Time 1.00 0112 1.00 ,oii41.00 0116 1.00 0118 1.00 0120 1.00 0122 1.00 0125 1.00 0127 1.00 0129 1.00 0131 1.00 0133 10.00 0135 10.00 0137 10.00 0139 10.00 0141 5.00 0143 5.00 0145 5.00 0147 5.00 0149 5.00 0151 5.00 0153 5.00 0155 5.00 0157 5.00 0159 5.00 0200 5.00 0202 5.00 0204 10.00 0206 10.00 0208 10.00 0211 10.00 0213 1.00 0215 %R Analytes ' iA S A B B c c c c F .M. M- H 1 K; s A N T V z is:L ;i| ;s A D ;A: 'Ri' y :e s: N I E G A L N X "-- MM M. -- MM MM MM MM MM X MM MM MM- MM X -- X MM MM MM M. "" X "" * "MM MM MM MM " " XX " ""MM MM. M. MM M. " X MM M. -M MM MM -- MM M_ MM X MM M. MM MM M. MM -- X X "** "" MM MM MM M. ~ -- _ M. MM MM -- "" "***MM MM MM MM MM ~ MM. MM. MM MM MM "" " X X MM MM MM -- r-- " MB MM MM MM X MM MM. MMT MM MM ---- X MM MM. MM. MM. MM -- MM. X X *" "* MM M. MM ~ X M. MM MM MM MM. " -- "" ~~ X MMi M. MM MM MM MM X X -M MM MM -M. MM. MM MM MM MM X X MM. MM MM MM MM MM ___ _ __ _ _ _ X FORM XIV - IN ILM04.0 67 DUP050307833 U.s. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES Lab Code: ________ Case No.: Instrument ID Number: 04725_ Start Date: 09/27/96 Contract: ___________ ' SAS No.: ________ SDG No.: FMD03 Method: F_ End Date: 09/27/96 FORM XIV - IN ILM04.0 66 DUP050307834  u.S. ERA - CLP ' 14 ANALYSIS RUN LOG Lab Name: LANCASTER_LABORATORIES____ Contract: LlfejiiV'Gbdfefr... ' ' ;:! SAS No. : ; ' ' SDG No . : FMDG3 Instrument ID Number: 02803__ Method: F_ Start Date: 09/25/96 End Date: 09/25/96 Analytes Sample No. D/F Time %R M L: A B B :C `8: m E C A C R C 0 c u F E PM G M N H N I K S t A G N A T L V z N SO S10 S20 S40 ' SOUS80 ICV ICB CRA CRAA CCV CCB PBW PBWA LCSW LCSWA MRA2S MRA2SA MRA2SD MRA2SDA MRA2SS ZZZZZZ CCV CCB MRA1S MRA1SA MRA1D MRA1DA MRA2D MRA2DA MRA4S MRA4SA__ 1.00 4;i!0;L 1.00 2105 2108 '...vLiiDO;: 2112 1.00 2116 1.00 2119 1.00 2123 1.00 2126 1.00 2129 1.00 2133 1.00 2136 1.00 2140 1.00 2143 1.00 2146 1.00 2150 1.00 2153 1.00 2156 1.00 2200 1.00 220.3 1.00 2207 1.00 2210 1.00 2214 1.00 2217 1.00 2220 1.00 2223 1.00 2227 1.00 2230 1.00 2234 1.00 2237 1.00 2240 1.00 2243 1.00 2247 101.1 97.8 96.4 95.6 105.4 106.2 91.8 97.2 --m mmm MM __ X -M X X X X X X X X X -- -- MM X X X" MM X MM X X~~~ X -- X ~X-- " X M. MM ~ ~ X MM MM. "" X X X X --~X MM MM X -- """ X --X MM X FORM XIV - IN ILM04.0 DUP050307835 U.S. EPA - CLP 14 ANALYSIS RON LOO Lab Name: LANCASTER_.LABORATORlfiS. Contract: __ Lab Code: Case No'.: SAS No.: ________ SDG No.: FMDG3 Instrument ID Number: 02803 Method: F Start Date: 09/25/96 EndDate: 09/25/96 Analytes EPA Sample NO. Time A ii :Si! B A S m B E m g|; C A ;'C iff C 0 m0\ F E W ii M G MH N % N K S E A N A T L V % M 1 MRA3S MRA3SA cev 1.00 2250 1.00 2254 1.00 2257' 109.4 X X" X CCB MRA3D MRA3DA MR3DD MR3BDA 1.00 2300 '::I^OOS 2303 1.00 2307 1.00 2310 1.00 2314 96.6 94.2 X X-- X ---- X X" MRAFB 1.00 X MRAFBA zzzzzz zzzzzz zzzzzz 1.00 2321 1.00 2324 1.00 2327 1.00 2331 119.2 X -- ---- zzzzzz 1.00 2334 CCV CCB 1.00 2338 1.00 2341 X "" X mm* . FORM XIV - IN ILM04.0 70 DUP050307836 U.s. EPA - CLP 14 ANALYSIS RUN DOG Lab Name: LANCASTER LABORATORIES Contract: _ Lab Code: ________ Case No. : SAS No. : _____ SDG No. : FMD03 Instrument ID Number: 0522 o__ Method: CV Start Date: 09/25/96 End Date: 09/25/96 EPA ' Sample No. D/F Time %R Analytes A S A BB C C C C C F PMMH N K S ANTVZ L B S A E D A R 0 U : B B G N;: I E G A L N SO SO. 2 SO .5 S1.0 S2.5 S5.0 ICV ICB CRA CCV CCB zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz CCV CCB zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz 1.00 1714 1.00 1716 1.00 1718 1.00 ;1721 1.00 1723 1.00 1726 1.00 1728 1.00 1731 1.00 1733 1.00 1735 1.00 1738 1.00 1740 1.00 1742 1.00 1745 1.00 1747 1.00 1749 1.00 1751 1.00 1754 1.00 1756 1-00 1758 1.00 1800 1.00 1803 1.00 1805 1.00 1807 1.00 1809 1.00 1812 1.00 1814 1.00 1816 1.00 1818 1.00 1821 1.00 1823 1.00 1825 _ X X X X X X X X X X X X X FORM XIV - IN ILM04.0 71 DUP050307837 n.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: LANCASTERLABORATORIES Contract: Lab Code: Case No SAS No SDG No,: FMD03 Instrument ID Number*: 05220_ Method: CV Start Date: 09/25/96 End Date: 09/25/96 EPA Sample No. zzzzzz ccv CCB zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz ccv CCB PBW LCSW MRA1S MRA1D MRA2D MRA2S MRA2SD MRA2SS MRA4S MRA3S CCV CCB MRA3D MR3DD MRAFB CCV CCB D/F Time 1.00 1827 1.00 1830 1.00 1832 1.00 1834 1.00 1837 1.00 1839 1.00 1841 1.00 1844 1.00 1846 1.00 1848 1.00 1850 1.00 1853 1.00 1855 1.00 1857 1.00 1859 1.00 1902 1.00 1904 1.00 1906 1.00 1909 1.00 1911 1.00 1913 1.00 1915 1.00 1918 1.00 1920 1.00 1922 1.00 1925 1.00 1927 1.00 1929 1.00 1932 1.00 1934 1.00 1936 1,00 1938 %R Analytes A S AB B C C C C C F P MMH N K s AN TV z LB SAE DAR0u EBGNG I E GAL N X X ~ ---- X X X X X X X X X -- X X --~ ~-~ X X X X X X X X -- -- """ **** --* _ ~-" FORM XIV - IN ILM04.0 7 hf . DUP050307838 I 1 7o DUP050307839 ICP Data 7 DUP050307840 ! srssr Reviewed -By: / Lancaster Laboratories -ssrta Verified By Airgalyst: 811 Data File Name: 26903I11.DAT Run Name: 9626903111 instrument Parameters: Rinse Time: Individual Integration Time: Total Integration Time: 60 sec 7 sec- 21 sec . ement Symbol Element Name A4S , ` Silver Ai Aluminum AS Arsenic st Boron 32 Barium 3e Beryllium Cg Calcium CO! Cadmium Co Cobalt er Chromium cu Copper fe Iron K Potassium Li Lithium n Magnesium nr* Manganese no Molybdenum Na Sodium N1 Nickel P Phosphorous pt> Lead st> Antimony 5e Selenium Si Silicon Sn Tin Sr , , Strontium Ti Titanium T.l Thallium V Vanadium Wavelengtht 32S.06 308.21 193.69 249.77 493.40 313.04' 317.93 226.SO 228.61 267.71 324.75 259.94 766.49 670.7S 279.07 257.61 202.03 589.59 231.60. 214.90 220.35 206.S3 196.02 288.20 189.90 4.21. S5 337.30 377.57 292.40 76 DUP050307841 Ti Thallium 377. 5-7 V Vanadium 292.40 Zn Zinc 213.85 Page: 2 LANCASTER LABORATORIES Run Name: 96269P3I11 . INSTRUMENT ID: 023< Tube: ELEM 1 50 CONC l ppm 1 > AV6 , INTENSITY ECOUNTS) 09/25/96 * mso ' #1. 21:06 INTEGRATIONS #2 #3 ' Afl __ A1 As __J5 __ Ba Be __ Ca __ CcE __ .Co __ Cr __ Cu ___F* __ K __ j_i __ Mg __ Mn ;__ mo __ Na __ Ni __ P6 ___Sb __ Se ___Si __ Sn __ Sr ___Ti ___TI __ V ___Zn . 0.000 0. ooo 0.000 0.000 0. ooo 0.000 0.000 . 0.000 : 0. ooo 0.000 0. ooo o.doo 0.000o.'oao 0.000 0.000 0.000 0.000 0. ooo 0.000 0. ooo 0.000 0. ooo 0.1000 0.000 a.ooo. 0. ooo 0.000 o. ooo io.ooooo .21.66666 0.33333 4.00000 o.OOOOO 2.33333 6.33333 1.ooooo -0.66666 '5.33333 6.00000 0.33333 ?- 33333 a.OOOOO 16.66666 0.OOOOO 0.66666 O.33333 2.OOOOO -0.33333 -3.OOOOO 12.00000 24.33333 -1.33333 -1.33333 35* * --9.66666 0.OOOOO 2.OOOOO 0; 16. 20 173.2 0 0 24.74 32. 36. ; 10D 624.4 57.28 O 173.2 31. 49 0 24. 97 0 173. 2 458.2 ICO 964.3 33. 33 16. 66 24.07 173.2 86.60 1.618 48. 88 0 0 IO.OOOOO 22.00000 O.OOOOO 4.000000.00000 3.00000 "8.00000 0.00000' -4.OQDOO S.OOOOO 6.OOOOO 0.00000 10.00000 o.ooooa 20.00000 .ooooo 2.00000 2.00000 4.OOOOO -4.OOOOO -3.00000 12.00000 22.OOOOO 0.ooooo -2.00000 35.OOOOO -6.OOOOO 0.00000 2.00000 io.00000 18.00000 0.00000 4.00000 0.00000 2.00000 4.OOOOO 2.OOOOO - -2. OOOOO 2.00000 6.OOOOO 1.OOOOO 6.OOOOO O.OOOOO 18.OOOOO o.ooooo 0.00000 -l.QOQDO 0.OOOOO 1.OOOOO -2.00000 14.OOOOO 20.00000 -4.00000 -2.00000 36.OOOOO -8.00000 o.ooaoo 2.00000 ID.OOOOO 25.00000 1.OOOOO 4.OOOOO O. OOOOO 2.00000 7.00000 1.OOOOO 4.OOOOO 6.00000 6.OOOOO 0.00000 6. OC'OOO o.OOOOO 12.00000 a.ooooo 0.OOOOO o.aapao 2.00000 2.00000 -4.OOOOO 10.00000 31.00000 o.oooop 0.00000 36.00000 15.00000 0.ooooo 2.00000 76 DU P05 0307 842 LANCASTER LABORATORIES Run Nan; 96269031X1 INSTRUMENT ID: 02560 Tue: .2 ' SI ' S> 09/25/96 21:09 AVG CONC INTENSITY INTEGRATIONS ELEN (' pom) (COUNTS'? %RSD ttl #2 #3 ___Ea ID.OOO __ Cd 10.000 . Cr 10. OOO ___cu 10.000 . 10.000 ___fin. 10.000 Mo ' 50.000 _Ni 20.000 __Pb ___Zn 50.000 10.000 SO76.66650 D. 222 6747.00000 0. 526 11350.33300 0.243 15749.33300 0.436 . 6766.33349 0.261 4399.66650 0.241 33523.6679* 0. 305 11763.33300 0.349 13329.66699 0.406 5625.66650 a.-6ii 3056.00000 6706.00000 11320.00000 15670.00000 6746.00000 4836.00000 33204.00000 11716.OOOQO 13273.00000 5537.00000 8039.00000 6769.00000 11374.OOOOO 157SS.00000 6773.00000 4906.OOOOO 33324.00000 11790.00000 13336.00000 '5653.00000 8035.OOOOO 6766.00000 11357.00000 IS790.00000 6775.00000 4907.00000 36543.00000. 11784.OPQOO 13325.00000 5637.00000 7( DUP050307843 Page: 4 LANCASTER LABORATORIES ' Run Name: 9626903114 INSTRUMENT ID: 02-560 TuUei 3 .. S2 09/25/96 21:13 ELEM ' CONC t DDm I _A Be 5.000 1.000 __ Co 2. ODD __ Li 50.000 __ Sb . io.ooo - Se . 5.000 __ .Si Sn 5.000 10.000 __ Sr i .'g o g ___Ti T1 5/000 10.000 __ y 5.000 AVG INTENSITY ( COUNTS r . %RSD 847.OOOOO . 0.312 824.33331 0.350 2227.66674 0. 475 19895.33398 0.192 6550.00000 0. 389 2687.33325 1.153 '5380.33349 0.362 1607.66662 0.414 8024.33349 0. 144 16222.66699 0.181 1315.66662 0. 494 2236.00000 : 0.089 #1 849.00000 826.OOOOO . 2226.00000 19936'. OOOOO 6569.00000 2713.00000 5394.OOOOO 1606.00000 8032.OOOOO 16235.OOOOO . 1322.OOOOO 2238.00000 INTEGRATIONS #2 844.00000 826.00000 2239.OOOOO 19860.OOOOO 6560.OOOOO 2688.00000 '5358.00000 1615.00000 8030.OOOOO 16244.00000 1309.OOOOO 2236.00000 S3 848.OOOOO 321.OOOOO 221S.OOOOO 19890.00000 6521.00000 2656.00000 5389.OOOOO 1602.00000 8011.00000 16189.00000 1316.OOOOO 2234.00000 78 DUP050307844 page: -9- LANCASTER LABORATORIES Run Name: 9926903111 INSTRUMENT ID: 02360 Tute: A S3 --* 09/25796 21:16 AVG . CONC INTENSITY INTEGRATIONS ELEM ! t'pprnJ iCOUNTS! SiRSD #1 #2 #3 Ag ___B 1.000 2.DP0 S62.6666S 0.267 1169.66662 0.177 B60.0D000 1168.00000 B64.0QOD0 1169.00000 S64.OOOOO 1172.00000 DUP050307845 - S\-> LANCASTER LABORATORIES Run Names. 9626903X11 , INSTRUMENT ID: 02360 Tube: 5 . > 64 Ln CQNC . f pom i ,, ' : - 1 AVG INTENSITY (COUNTS) . 09/25/96 > . 56RSD . 1 21:19 INTEGRATIONS #2 #3 ___fill ___pa ___K ___ns ___Na 50.ODD 100.000 .500.000 100.000 500.000 . 24033.66601 80841.66606 i4849.00000 80105.66406 15925.. 33300 i.oe? 0.814 1.006 1. 152 1.022 24109.00000 80986.00000 14891.00000 80430.00000 15954.00000 24249.00000 81416.00000 14973.00000 80823.00000 16072.00000 23743.00000 80123.00000 14683.00000 79064.00000 15750.00000 80 DUP050307846 :7 LANCASTER LABORATORIES nun Name: 9626903X11 Tube: 6 ICV 09/25/96 21:22 INSTRUMENT ID: 2360 &LEM A ,,,,J3 --J3a ' '._2e __ ca- . ' ..._Cd __Co .cr Cu --F* ,,_J< -J-L -Jin. .-no ___Na __Ni ,,Se ___Si ___Sn .Sr ___Ti ___T i ___V ___Zn AVG I'd d h i'J %RSD O.S4869 0.539 30 .'32811 0.544' 2.30432 1.234 2..04.025 0. 635 5.69789 0.505 0.57549 0.438 59.79287 O. 553 5.70785 0.634 1.11553 1. 178 5.30217 0.411 5.76313 0.429 5.81752 0. 534 60.64333 0.678 30.41332 O. 384 30.32764 0.29 3 5.69268 0. 448 29.29029 0.353 62.21787 0. 579 11.36251 0.538 28.82855 0,. 799 5.62888 0.390 2.30234 0.677 9.19900 1.453 5.67684 0.758 ' 1.17207 0.565 2.36924 0.470 5.74379 O.-902 2-37920 O. 159 5.69941 0.484 ' #1 0.54593 30.16287 2.29138 2. 02540 5.66694 O.57347 59.41271 5.67625 1.10753 5.77661 5.73736 5.78743 60.19412 30-29333 30.23666 5.66747 29.17780 61.86244 11.29709 28.56596 5.60428 2.30723 9.07525 5.65193 1.16517 2.35790 5.70069 2.37773 5.66831 INTEGRATIONS #2 0.55182 30.32851 2.28465 2.04599 5.70284 0.57469 59.94956` 5.69994 1.10835 5.80605 5.76523 5.81555 60.73319 30.41919 30.33049 5.69201 29.31149 62.20734 11.37220 28.92224 5.64654 2. 28487 9.18094 5.65204 . 1.17265 2.36965 5.80382 2.37635 . 5.70883 #3 R O.S4S32 30.49295 2.33694 2.04936 5.72389 O.57832 60.01634 5.74736 1.13070 5.82385 5.78678 5.84958 61.00269 30.52725 30.41577 5.71857 29.38158 62.58383 11.41824 28.99746 5.63581 2.31491 9.34082 5.72656 1.17838 2.38016 5.74186 2. 3-8351 5.72109 REDIG 81 DUP050307847 Page: S LANCASTER LABORATORIES Run Name: 9626903111 T ube: 7 ICB 09/25/90 21:26 INSTRUMENT ID: 02360 AVG INTEGRATIONS ELEM fOSMB) %RSD 81 2 83 REREAD REDIG ___A9 0.00039 449.4 -0.00116 .. 0.00000 0.00235 ___A1 0.11657 8.441 O.10894 0.11310 0.12768 ___AS 0.00533 127. 4 0.00928 -0.00251 O.00922 ___j3' 0.00224 88. 32 0.00338 -0.00004 Q.00339 ___Ba O.OOOOO 0 0.00000 . 0.OOOOO 0.OOOOO :__ Be O.OOOOO 14 469 -0.00042 -0.00040 O.00081 ___p.a O.18762 1.319 0.19010 O. 18762 O.18514 ___cd -0.00148 O. 084 -0.00148 -0.00148 -O.00148 __ po O.00329 27.19 0.00239 ' 0.00329 0. 00416- Cr -O.00143 248.9 0.00239 -0.00202 -0,00465 __ pu ' 0.00719 27.00 0.00761 0.00888 0.00507 ___Fe O.00936 .36.48 0.01132 0.00541 O.'01133 - fc O.05618 103.8 0.02249 0.02249 0.12356 A ___Li ___MS O.OOOOO 0 0.06187 17.54 0.OOOOO 0.05688 0.OOOOO 0.07432 0.00000 0.05440 ___Mn 0.00408 0. 015 0.00408 0.00408 0.00408 ___Mo O.01384 10.82 0.01470 0.01211 0.01470 ___Ns O.05228 0. 019 0.05228 0.05229 0.05227 __ Ni -0.00507 58.02 -0.00337 -6.. 00337 -0.00847 ___TD 0.00875 85. 66 0.00125 O.01626 O.00875 ___Sb 0.02394 4 4.65 - 0.03512 0.02290 D.01381 __Se .-0.00-748 173. 0 0.OOOOO . 0. OOOOO. -O.02242 ___Si 0.01866 7. 6i7 0.01743 0.02022 0.01834 A ___5n 0.01665 86. OD 0.00840 O.00836 Q.03318 ___Sr O.00066 O 0.00066 0.00066 0.00066 ___Ti O. 000io 1624. -0.00113 -0.00051 O.00195 ___TI 0.03788 123.1 0.05793 -0.01749 0.07321 ___V ___Zn O.00156 165.2 0.00173 IDO. 7 0.00456 0.00179 0.00006 -0.00002 0.00007 0.00356 DUP050307848 9 LANCASTER LABORATORIES Run Ntam<s-. 9626903111 Tuee: ' 5. CRI 09/25/96 21:30 INSTRUMENT ID: 02360 ELEM AVG i' pom! %RSD ' #1 INTEGRATIONS #2 :#3 REREAD RSDIG ; __J*C __ a__ P _JB __ca cd:__ ___.Co ____ cr __cu f* <* 3-n o ___fin ___.Mo __}>f --N* Pt> __ 60 __jSe Si A ___Sn Sr 1 ___V __ 0.02035 6.653 0.01201 26.53 0.0191S 17.SI 0.00572 34.61 0.00000 O O.OD9S1 14.35 0.00041 341.7 0.00938 18.23 0.09930 .1.807 0.431760 5.787 0.05377 1.363 -0.00146 57.82 -0.02246 458.1 O. OOOOO 0 0.00139 275.1 0.03131 7.523 0.00692 O 0.03129 115.8 0.07925 4.955 Q.01901 11.39 0.125S7 3.182 -O.OOSIO 127.1 0.01378 0.061 -0.00994 348.0 0.00000 348.0 -0.00132 71.30 0.03957 66.38 0.09996 2. 580 0.03946 0.046 0.02114 0.01137 .0.02114 O. 00343 .ooooo 0.00899 0.00206 O.00740 O.10109 O.01642 0.`05335 -O.00196 -0.04491 O. OOOOO 0.00473 O. 03267 O.'00692 O.05221 O.03152 O. 01778 O.12132 -O.01869 0.01377 -O. 01617 -O.00020 -a.ooiii a. D2439 a.10294 0.03948 0.02114 O.00919 . 0.02117 O.00686 O.OOOOO O.01144 -0.00040 0.01037 0.09750 0.01818 0.05335 -O.00048 -O.11229 O.OOOOO 'a.00223 0.03267 0.0Q692 -0.01056 0.08152 0.01774 O.12384 0.00186 0.01379 ~D.041DO 0.00016 -0.00235 0.02442 0.09847 0.03944 0.01879 . 0.0154 7 . Q.01524 . 0.00687 0.00000 O.00901 -0.00040 . 0.01037 0.09930 O.01818 0.05462 -O.00195 0.08982 O. OOOOO -0.00278 O.* 02859 O. `00692 O. 05222 ' 0.074 72 O. 02151 O. 12745 ~0.00747 0.01379 0. 02735 0.00004 -O.00049 0.06991 O. 0984 7 O. 03946 85 DUP050307849 Page: ID LANCASTER LABORATORIES Run Name: 9626903111 Tube: 9 ICSA ,f 09/25/96 . INSTRUMENT ID: 02360 21:34 ELEM ___Ag _A1 ___AS __ e . Ba Be ' ___Ca ;___Cel .. ___.Co Cr ___Cu ___Fe ___K ___Li ___Mg ___Mn ___Mo ___Na __Ni ___Pb ___Sb ___Se ___SI ___Sn ___Sr. ___Ti ___T1 ___V ___Zn AV I bom J %RSD 0.00354 32.01 479.74703 0.343 . 0.25657 14.94 0.08573 2- 592 0.00742 0 -0.00040 0.4 80 46S.82516 0.246 0*00752 21.83 ' 0.00031 913.5 ,0.00391 46. 12 0.00030 416. 0 175.90252 0.239. Oi07130 54.58 0.00167 173. 2 484.31161 0.250 -O.01827 0. 089 -6.01427 13.88 . O.11523 n, q d i -0.00853 19.. 92 O.02700 14. 82 -0.02713 40.90 0.00881 119.5 ' 0.17582 0.815 O.00035 4051. 0.01968 0. 730 -0.01395 14.57 O. 11851 5S- 22 Q* OQ195> 133.0 O.01569 O. 130 INTEGRATIONS SI S2 0.00456 478.63433 0.28568 0.08797 0.00742 -0.00040 467.59960 0.00563 -0.00297 0.00327 0.00158 . 175.56112 0.04860 0.00502. 483.46005 -0.01826 -0.01644 O.11523 -0.00683 0.03013 -0.01999 0.02049 0.17426 -0.00783 0.01960 --O.01177 0.11847 -0.00104 0.01569 0.00373 481.64126 0.27090 O.D8352 0.00742 -0.00040 469.89566 0.00841 0.00151 0.00251 -0.00097 176.37252 0.04906 ' O . 0000-0 485.70269 -0.01829 -0.01384 0. 1152-? -0.01023 0.02839 -0.03991 0.00590 0.17613 -0.00806 0.01985 -0.01429 0.16383 0.003.45 0.01567 ' #3 REREAD REDIG 0.00232 478.96551 0.21314 0.08570 0.00742 -0.00040 468.98022 O.00853 0.00241 0.00594 0.00030 175.77394 O.11625 0.00000 433.77212 -0.01826 -0.01254 O. 11523 -0.00353 O.02249 -0.02148 0.00003 O.17708 0.01696 D.01960 -0.01579 0.07324 0. 0034.5 0.01571 ________ 8 DUP05 0307850 Ree5' li LANCASTER LABORATORIES. Run Name: 9626903111 Tubes 10 ICSAS 09/25/96 ,21:38 INSTRUMENT.ID: 02360 ELEN AS ' --P* __Cd __ .CO --pr cu Ilf* ,,3-i __/i "__jrn "If10 3s --N1 _,,5b _,.Se 131 __ 5n 3r__ Ti __ Tl _y Ijin AVG ToomJ ^:RSD O.18967 0.090 483.64230 0.317 0.37670 8.002 0.05965 3.032 0.47874 0.29S 0.464.44 0.303 471.63400 0.196 0. 87676 1,-209 0.43588 1.131 0.45558 0.123 0.46926 0.280 177.40960 0.229 0.10518 18.45 0.00167 229.1 488.21575 0.316 0.42473 0.007 -0.01730 17.32 0.03110 58.22 O.S5877 0.323 0.08127 4.550 0.58169 2.074 0.07654 62.50 0.09968 1.846 0.00199 722. 7 0.02001 1.437 -0.01417 8. 836 0.16517 32.25 0.46366 O.568 0.88647 0.109 - W1 O. 18974 485.10415. 0.35771 0.06144 O. 48039 0.46525 472.44265 0.88852 0.44096 0. 45623 0.46967 177. 81950 0. 11657 O.00502 489.78460 O.42470 -0.01903 O.02064 0.86669 O. 08549 O. 58619 0.07987 0.09755 -O.0Q636 O.02035 -0.01420 0.22275 O.46515 O.88760 INTEGRATIONS 2 O.18940 482.03890 0.36094 0.05782 0.47791 S . 0.46282 470.61920 - 0.86795 O.43559 O.45522 O.46778 177.00512 P.11621 Q.00251 486.69778 O.42476 -0.01384 O.05201 0.85651 O. 07968 O.56802 O.02712 0.09964 -0.00626 0.01985 -0.01290 O.15517 0. 46516 0.88595 #3 REREAD REDIS j O. 18957 483.78381 0.41146 0.05969 O. 47791 0.46526 471. '34017. O.87380 O.43110 . 0.45528 O. 4 7032 177.40419 O. 08276 -0.00251 438.16491 0.42473 -O.01903 0.02065 O.85310 O. 07862 O.59086 O.12263 O.10153 O.01860 0.01985 -0.01540 O.11759 O.46066 O.S85S7 A DUP0503 07851 paae: 12 LANCASTER' LABORATORIES Run Name: 9626903111 Tuber 11 CCV 09/25/96 INSTRUMENT ID: 02360 21:42 ELEM . Ag * ___A1 ____AS S ___Pa ___Be ,___Ca ___C9 ___co ___Cr ____Cu ___Fe ___k . ___ris ___fin ___.MO ___tNa ___NA ___PD .___Sb Se ___Si ?n ___Sr Ti ___Ti ___V Zn ' ' AVG fobm) %RSD 0.45806 O. 144 24.43118 0. 596 . 1.95987 2.469 1.24992 0. 842 4.77424 0.657 0.47505 0. 507 49.07069 0.449 , 4.70571 Q. 745 0.95308 1.040 4.85351 0.619 4.85591 0.654 4.84917 0. 397 49.50284 0.342 25.09214 0. 795 24.97815 0.520 4.72160 0. 350 24.44037 O. 801 50.45095 0.648 9.34645 O. 528 23.75544 O. 566 4.70789 0.606 1.92383 0. 476 5.00574 2.056 4.66581 0. 868 0.96345 O. 627 1.97821 O. 816 4.76758 0.629 1.95917 0.424 4.72007 0.612 INTEGRATIONS #1 2 0.45844 24.33214 1.92103 ' 1.24071 4.76062 0.47263 48.83940 4.68399 0.94237 ' 4.82253 4.83694 4.83731 49.68250 24.97821 24.91421 4.70658 24.27943 50.23174 9.30190 23.61156 4.69818 1.91941 4.91189 4.66788 0.96008 1.96502' 4.75905 1.95516 4.68825 0.45845 24.36285 1.944481.24766 4.75196 0.47507 - 49.09420 4.68694 0.95492 4.85542 4.83815 4.83881 49.34564, 24.97570 24.89254 4.71886 24.38326 50.29417 9.33782 23.77674 4.68546 1.93437 4.98950 4.62432 0.95983 1.97337 4.74276 1.95361 4.72724 #3 REREAD REDIG 0.45730 ; 24. 59853 _____________ 2.01410- 1.26140 4.81015 0.47746 49.27847 _________ ___:------4.74619 _______ 0.96195 ____________ 4.88258 _________ _________ ' 4.89262 . 4.87140 ________; ------------ 49.48039 _________ 25.32252 ________: 25.12770 _________ 4.73936 ___________________ 24.65842 50.82694 9.39964 ___________________ 23.87802 ______. ---------------- 4.74004 ________. ------------- 1.91771 5.11583 4.70524 0.97042 _________ 1.99624 4.80094 1.96872 ________ 4.74472 ________ 86 DUP050307852 LANCASTER LABORATORIES Run Name: 9626903111 Tube': 12 'CCS __ Ai A3 Ca >. Co ^Cr `"""cu __ LI fin "\po r>a _Pb " Sb ___5e ___Si __ 5n ~'j5r '31 "Tt i " __v U=* . AVO Ippmi 3sRS0 0.00039 450.7 0.0186? 25.71 0.0038.3 266.6 0.00226 87.59 0.00000 O -O.00041 3. 061 0.02433 17.60 --0.00148 0.066 0.00120 86. 17 -0.00172 117. 5 0.00698 24.03 0.01575 9.395 --O.04490 0.006 0.00167 173.2 0.01606 40.42 0.00000 30.14 0.01384 39.03 O.02089 260.1 0.00002 11479. 0.00877 308.2 0.02089 44-57 -0.00249 769.3 0.01274 31.93 0.01042 149.7 0.00024 57. 7.3 -0.00216 32.95 0.03771 180.6 0.00231 168.5 0.00117 177. 7 09/25/96 21:46 'INSTRUMENT ID: 02360 INTESRATIONS #1 . #2 0.00000 0.02143 -0.00210 0.00340 0.00000 -0.00042 . 0.02928 -0.00148 0.00060 -O.00288 0.00888 0.01723 -0.04490 O. 00502 O. 02325 0. ooooo 0.01990 O. 05226 -0.00335 -0.02123 0.02296 -0.01869 O.01554 O.00836 O.00016 -O.00175 0.10319 O.00682 0.00358 O.00235 O. 02147 0.D1564 O.00340 0.00000 -0.00040 0.02186 --O. 0014=8 . 6.00239 -0.00290 0,00634 0.01575 -0.04490 0.00000 0.01062 0.00000 0.01211 O. 05229 0.00002 O.03130 0.02899 O.01S68 0.00807 -0.00404 0.00016 -0.00175 0.04275 O.00006 -O.00002 #3 REREAD . REJQUM -0.00116 0.01313 -0.00203 -O.00002 0.00000 -o.100040 0.02186 -0.00148 0.00060 0.00061 0.00571 0.01427 -0.04491 o.OOOOO 0.01431 0.00000 0.00951 -0.04187 0.00342 O. 01626 0.01071 -0.00747 0.01462 0.02696 0.00041 ~0.00298 -O.03280 O.00005 -0.00003 87 DUPO 50307853 P89: 14 LANCASTER LABORATORIES . i?un Name: 9626903111 fut>e: 15 Pfeud PBW ------ a * * * * . > no-lOO. DF1.962695 /200015 S. 09/25/96 INSTRUMENT.ID: 02560 21: 50 EL-EM AVG (DDtn I %RSO 0.0Q07S 172.5 0.00901. 46.73 0.00586 116. 2 0.00683- 0.038 Q.00000 0 -0.00040 2.056 0.01691 29. 25 -0.00247 69 ; 19 0.00269 134. 3 -0.00232 190. 1 0.00380 33.39 .0.01033 16.50 0.DOOOO 55363 0.00167 173.2 0.01926 59. 68 0.00000 10.21 0.00692 49.60 0.05231 0. bis -0.00338 O. 317 0.00504 197.0 O.00767 105.3 -0.00623 295. 7 0.01149 32. 95 0.02695 61.01 0.00024 57. 73 -0.00226 55.08 0.02779 162.9 -0.00145 178.2 0.00650 15.56 INTEGRATIONS #2 O.QQOOO' 0.00906 -O.00201 0.00683 0.00000 -O.00040 0.01196 -0.00148 D. 00599 -O.00291 O.00380 0.01131 0.02246 0.00000 D-. 02178 O.OOOOD O.00822 0.OS232 -0.00339 0.00134 0.01686 -0.01495 0.01367 0.03320 0.00016 -0.00360 O.02778 0.D0D04 O.00710 O.OOOOD 0.01319 O.00979 0.00684 O.OOOOO -0.00039 O.01690 -0.00148 0.00329 0.00236 0.00508 0.01132 O.0224 5 O.00502 O.00671 d.ooooo 0.00302 0.05232 -0.00339 0.01629 0.00453 0.01494 O.01369 0.00830 0.00041 -O.00113 O.07307 -O.00444 0.00706 #3 REREAD REDIG 0.00234 ______ _______ 0.0047? . 0.00982 ,, 0.006S3 0.00000 -0.00040 0.02186 ________________ -0.00444 -0.00118 ____________ -0.00643 ________________ 0.00253 w Q.00836 -0.044 90 ' 0.00000 _______3 0.02929 O. OOOOD -- 0.00951 0.052.30 ____________ -0.00337 --O.002S1 0.00163 -0.01870 ________ 0.00712 0.03936 ______________ 0.00016 _____________' -0.00206 ______' -0.0174 8 _____ ' 0.00004 ______I _____ 0.00533 ________ ____ 8S DUP050307854 Pacwt 15 LANCASTER LABORATORIES Run N*es 9626903X11 TtiL'If! 1A 5 LC3u 3 * * * * f i,~ 1 * DPI,962695720001. S, . 09/25/96 21: 54 INSTRUMENT ID: . 02360 k INTEGRATIONS El 'M . fopraJ 58RSD 81 #2 #3 ' REREAD REDIG //VJ j j /j AI ___tfns :5j -JV2t pt * jZCd A Js.0 Zcr ___i- ^ A no pto ___kr 1 Sn 4r i .t . T1 7v A .Zzn 0.04960 1.371 2.00002 0.522 2.05108 0. 603 2.02600 0. 635 1.98844 0.542 0.04948 .1.437 4.05694 0.276 0.04711 3.626 0.49529 1. 184 0.20020 0.535 O. 25*271 O. 520 1.02457 0. 726 3.97535 0.978 2.02560 0.656 2.03518 0.410 0.48777 0.484 2.01870 1.062 4.10131 0.882 0.49590 0.531 0.49509 1.531 . O.54227 0. 160 1.96343 1.052 3. 81718. 0. 859 3.82597 0.094 1.01179 0.442 0.99128 0.683 1.98284 2.637 0.50051 1.461 O.49804 0.415 0.04881 1.98395 2.01737 2.01285 1.98101 0.05030 4.D4868 0.04810 0.49439 0.19959 0.25124 1.01669 3. 99781 2.02057 2.03831 0.48641 2.00832 4.12226 O.49531 0.49509 0.54328 1.94412 3.77984 3.82390 1.00855 0.99354 2.04324 0.49746 0.49565 0.05D00 2.00973 . 2.03493 2.03858 2.00082. 0.04905 4.06971 0.04809 O.50155 0.20144 0.25376 1.03148 3.99781 2.04067 2.04152 0.49050 2.04336 4.12213 O.49878 O.50268 0.54179 1.96095 3.83026 3.82388 1.01690 0.99663 1.95251 0.50836 .0.49928 O. 04999 2.00138 2.04094 2,02656 1.98349 0.04910 4.05242 0.04514 0. 48992. .19958 0. 25315 1.025533.93044 2.01554 2.02570 0.48641 2.00443 4.05953 0.4.9361 0.48751 0. 541761.98523 3. 84145 3.83012 1.00992 0.93366 1.95279 0.49521 0.49919 31/ DUP050307855 ~i.; Page: 16 LANCASTER LABORATORIES Run Name: Tu&e: 15 U"**,: 96269031X1 m&A av 25B5279 . 1,DP1,962695720001, S t 9 09/25/96 21:58 INSTRUMENT ID:. 02360 - ELEM iS AVS ppm %RSD 0.00X10 1.776 0.54204 0.763 0.01493 45.43 0.05399 3.798 O.066S5 0 ' -0.00041 3.435 .43.91764 0.601 -0.00365 46.89 -0.00067 405. 1 --O.00158' 140.4 O.00103 93.85 0.64987 0,909 1.62332 2. 399 '0.03602 4.028 49.24135 0. 354 O.03734 6.34 1 D.00735 10.18 52.44362 0.241 -0.00111 175.8 0.00780 110.5 0.00856 73. 23 0.08499 16.50 11.99623 0. 494 0.00394 480.6 0.45603 0. 4 45 0.01837 7.012 0,,04272 70. 79 0.004 52 98 . 78 n,,01018 0.4 00 81 0.00108 0.54617 0.01885 0.05526 0.06685 -O.00042 142.94323 -0-00167 -0.00307 -0.00364. 0.00124 0.64396 1.60067 0.03769 4.9.04 04 8 0.04008 O.00692 52.32849 -0.00338 0.01776 O.D1062 0.07690 11.93026 0.008D9 0.45371 0.01941 0.07297 0.00451 0.01019 INTEGRATIONS 82 0.00111 O.54206 ' 0.01B&5 0.05162 O.06685 -0.00043 144.20877 -0.00464 -O.00127 -0.00187 -0.00002 0.65578 1.66830 0.03518 49.35492 0.03598 O.00692 52.57968 0.OOOOl 0.00278 O. 0D152 O.-10119 12.01334 0.02049 0.45695 0.01693 0. 0124.8 O.00S99 O.01021 83 REREAD 0.00111 0.53789 0.00710 0.05508 0.06685 -O.00040' 144.60092 .......... -0.00464 O. 00231 0.00077 0.00187 O. 64987 ............ 1.60100' O. 0-3513 4 9. 32866._________ 0.03593 0.00822 _________ 52.42269 O. OOOOl 0.00285 0.01355 0.07689 12. 04.509 -O.01675 O.45744 0.01378 0.04270 0.00006 O.01013 90 DUP050307856 Paffle 1? LANCASTER LABORATORIES Run Nam: 9626903111 2585279 K Tube: 16 UP*Kf100- iao"DFl. 962695720001,8M 09/25/96 22 : 02 INSTRUMENT ID: ELEM AVS fDDm'i *RSD ,n INTESRATIONS 2 #3 REREAD RED10 AS 0.01913 7.018 0.01758 0.01990 0.01990 ___ A-t 0.92340 1.877 0.91784 0.90952 0.94284 ___ A& 0.02837 0. 285 0.02838 0.02844 0.02828 ___ P ' 0.24728 X. 361 0.25060 ' 0.24387 0.24736 A .Bs* 0.44944 .0 0.44944 0.44944 - .44944 ___Be ca 0.00981 14.22 140.75131 0. 267 0.01142 141.17272 D.00900 . 140.63214 0.00900 140.44905 Cd,, 0.00909 18.81 0.01008 0.00711 0.01008 Co 0.09427 0.960 0.09337 0.09518 0.09427 ________; A cr 0.02059 IS. 67 0.02500 0.01795 0.01882 CU 0.05043 0. 724 0.05064 0.05000 ' . . Q.05064 0.82461 0. 717 0.83053 0.82459 0.81869 _______, _J< 3.62143 0.001 0.14157 2. 711 3.62151 0.. 14 576 3.62141 0.14073 3.62137 O.13322 ___MS 49.00344 O. 302 49.16742 48.96391 48.87900 ___ fin 0.06603 1.781 0.06670 0.06467 0.06672 _Jlo _Na . ___Ni 0.18776 0- 798 53.25880 0.180 . 0.07626 5. 145 0.18863 53.36344 0.07173 0. 18863 53.23789 0.07853 0.18603 53.17509 0.07852 A __Fb 5b 0.02397 18. 11 0.10802 8.654 0.01896 0.09727 0.02650 O.11259 0.02647 0. 11421 S'!? ' 0.08072 10. 09 0.08633 0.07137 0.08445 A ___si 12.01844 0.280 12.02095' 12 ,,05079 11.98359 Sn 0.51367 7.398 D.4SQ47 0.50540 0.55512 Sr 0.46405 0.316 0.46567 0.46367 0.46280 ___T i O.11652 3.182 0.12012 O.11271 0.11673 ___T1 0.08716 17. 89 0.06968 O.09213 0.09967 ___V 0.1010-3 2.568 O.10403 0.09954 O.09953 ___Zn Q.-05555 3.724 0.05677 O.05316 O.05672 .91 DUP0503 07857 LANCASTER LABORATORIES Run Name: 9626903111 Tube: 17 2585279 ^^SlS D D***. 100--100', DFlj 96269572OQ01fSs, 09/25/96 . 22:06 INSTRUMENT ID: ELEM 'fAs /k . ___As Tea /Be Jen -<4Cd Vco JrCr Jeu _je ; J.K ' ___Li Jfrrx Mo JJi i --fb Se ___Si ___.Sn __rSr _Ti V1 Jy Jj.r\ AV6 (Pmi %RSD -0.00167 41.08 0.51567 0.933 0.01114 61.22 0.05424 3.383 0.06685 n -0.00041 2.009 142.81704 0. 537 -0.00265 64.53 -0.00127 141.0 -0.00013 2610. O; 00167 87. 72 0.61045 0.280 1.57S19 6.168 O.03853 3. 765 48.93217 0. 710 .0.03736 3.120 0.00346 43. 30 52.25526 1.049 -O.00112 174. 8 0.01154 67.34 0.00451 67.85 O. 08323 24. 59 11.88577 0. 647 0.01637 43. 79 0. 45516 D. 870 0.01632 7.614 O.01507 32 5.6 '0.00301 85.83 O.01017 O. 217 INTEGRATIONS #1 #2 -0.00246 O.51289 0.01901 .05544 0.06685 -0.00041 142.27891 . -O.00462 -0.00306 0.00338 .0.00251 0.61144 1.46578 0.03769 48.84067 0.03805 0.00173 52.10874 -0. 0033.9 0. 01401 0.00145 0.06379 11.87239 0.02051 0.45346 0.01632 0.01262 0.00449 0.01019 : -0.00128 O. 51290 0.00721 0.05213' 0.06685 --0.00041 142.47685 -O.00166 -0.00127 -0.00013 a.00251 0.61144' 1.63426 0.04021 48.63960 0.03601 0.00432 51.79476 0.OOOOl 0.01779 0.00758 0.08249 11.81638 0.02053 0. 45234 0.01756 0.06532 0.00450 0.01018 #3 REREAD REDIG -0.003.26 ______! 0.52123 ______________ 0.00719 _______: 0.05516 _____________ 0.06685 -0.00040 ________________ 143,69536 -0.001.66 _________________ O. 00052 ________ ____L_ -0.00364 __ -O. 00002 _______ ________ 0.6084S' 1.63451 _________________ 0.03769 49.31626 1 0.03802 ______; 0.00432 _ 52.86228 _ 0.00000 ________________ 0.00283 o: 00449 __ 0. 10492 11.96854 ________ 0.00809 0.45969 0.01508 -0.03273 0.00002 ________ 0.01015 9 <r> & DUP050307858 (=>! 19 .LANCASTER LABORATORIES ftun Name: 9626905111 HlfcMfi IB 2585279 '^CLfNS^ 3 R*x ,100-100,DF1,962695 720001, 8, , 09/25/96 22:10 INSTRUMENT ID: 02360 AV ( Dom'f. *RSD 0.04632 0.009 2.53738 0.309 0.04194 28. 06 2.03081 0.000 2.01320 0.184 , 0.04993 1.390 :145.35977 0.136 Q.04596 3.722 O. 47698. 0.947 0.19925 1.843 0.24659 0.298 .1.60205 0.243 5.62060 1.248 2.09178 0.541 50.40988 O. 022 o:51357,0.453 1.93996 0.336 55.93817 0.212 0.47875 0.412 0.03621 11.97 0.52864 2.856 0.09912 9.496 15.58812 O. 143 3.93550 1.264 1.45807 0.116 1.01780 0.184 0.11218 35.57 0.48886 0.520 0.48567,0. 757 #1 , INTEGRATIONS #2 0.04631 2. 59298 0. 04191 2.03081 2. 01692 0.05033 145.13545 0.04497 0.47637 0.20041 O.24744 1.60057 5.54195 2.10350 50.41520 0.51221 1.93304 55.99051 0.47646 0.03120 O. 53578 0.09787 15.57038 3.93553 1.45985 1.01904 0.09716 0.49032 0.48272 O.04632 . 2.59093 O.05374 .2.03080 2.01320 0.05033 145.51524 0.04794 0.48177 0.19514 O.24617 1.60647 5.64310 2.09094 50.41780 .O.51629 1.94083 56.02190 O.47987 0.03876 O.51129 0.10909 15.61332 3.88573 1.45786 1.01564 0.08196 O.49035 0.48449 #3 ' REREAD REDIG 0.04632 -------------------- 2.57822 . 0.03019 _____-- _--------- 2.03083 ______________-- 2.00949 _ . 0.04913 I--~ 145.42863 ....:--------------- 0.04497 ------------ ----------- 0. 4 7279 0.20221. ___________ 0.24616 -------------------------- 1.59909 ________ ______ 5.67676 _______1--------- 2.08088 --------- 50.39664 __________ 0.51221 ________ _ 1.94602 ,, 55.80210 ________ ______ 0.47990 __________ 0.03866 -------- --------- 0. 53886 _____ _-------- 0.09039 ___________ .15.58065 ________________ 3.98526 _______ _ 1.45649 _________ 1.01873 --------------------- 0.15743 _ 0.48593 0.48979 ________ _____ 93 DUPO50307859 'I Pase; 20 , LANCASTER LABORATORIES Run Name: 9626903111 Tube: 19 2585279 Of\tL'Pv&3 tl ULItJ% 100--100. DF5, 962695720001-18, . - - ,, 09/25/96 22:14 INSTRUMENT ID: ELEM ___A<3 __AI ___As __ S 6a ___.Be Ca __ Cd Co __ Cr __Cu __f __.K ___Li . Mg ___Mn no __ Na .___Ni ___Pto ___Sb Se __61 ___Sn ___Sr ___T i ___TI __ V ___Zn AVG i'lkxn'l ' %RSD 0.00110 61.32 ,0.11872 5.696 0.00135'504.4 0.01772 0.148 O.01403 10.18 0.00040 351.6 29.53452 0.371 -0.00152 0.D70 0.00297 125-. 4. -0.00022 1212. 0.00126 0.072 0.13893 1.625 0.36524 18.44 0.00837 34.64 10.09996 0.390 0.01099 10.71 0.00302 42.85 10.60175 0.592 -0.00339 100.1 -0.00338 338.8 0.01270 27.51 O.00566 206.1 2.45177 O.506 0.00413 173.0 Q.09378 0.668 0.00296 20.80 *0.02776 143.9 0.00151 171.1 0.01058 0.305 #1 ' O.00070 0.12573 -0.00262 0.01774 0.01238 -0.00041 29.46689 -0.00152 0. 00597 .0.00257 0.00126 0. 13344 0.43260 0.01005 10. 06960 O. 01167 0. 00302 10.60174 ~0. 00680 -0.01334 D.01069 ~Q. 00742 2.44555 0.00827 O.09386 O.00358 0. 01276 0.00449 0.01061 INTEGRATIONS #2 0.00188. 0.11726 -O.00256 0.01773 O.01485 O.00202 29.47555 -0.00152 -O.00120 0.00080 O.00126 D.13696 O.36522 0.00502 10.08677 O.00963 O. 00173 10.53896 -O.00339 ' -0.00593 0.01674 O'. 00939 2. 44368 -0.00413 O. 09311 O.00235 0.07304 0.00001 O. 01056 #3 , REREAD REDIG O. 00071 O.11317 O. 00926 O. 01769 O. 01485 -0.00040 29.66111 -O.00152 0.00417 -0.00271 0. 00126 0.14140 0. 29789 0.01005 10. 14451 0.01167 ' 0. 00432 ID.66454 0.00000 0. 00914 0,01068 0.01500 2.46608 0.00827 O. 09436 ' 0.00296 ~Q.00252 O. 00002 O. 01055 9 DUP050307860 RaO'ff 21 LANCASTER LABORATORIES Run Natter 962690-3111 TLiDff! 20 2585276 ' rt\<lA \ JiOD--100 DF1f 962695720001 * 8. , 09/25/96 ' ' 22:18 INSTRUMENT ID: 02360 ELEtt M 5. XP* :*ca %cr X.CU %y yr*' _Mo 5f __ Sff Si A VO foomi SSRSD #i -0.00086' 133.9 0.00029 0.62747 2. 718 0.6316S -0.00520 1.590 -Q.. 00522 0.05204 3.570 0.05102 ;0.09368 0.763 0.09286 0.00039 .359.2 -0.00042 103.98912 0.845 . 103.22914 -0.00174 0.095 -0.00174 O'. 00108 251'; 6 'D.00407 0.00173 105.2 0.00320 0. 00822' 7.736 ,,00759 0.86075 0. 792 0.85681 0.97527 5.285 .0.98634 0.01005 24.99' 0.01256 38.54438 O. 533 38.35139 0.03190 7.390 O.03055 0.00346 43. 30 0.00432 30.05742 0.629 29.87949 -0.00282 34. 81- -0.00339 0.01856 42.06 0.02109 -O.00165 186. 4 -0.00472 -0.02953 88.58 7.87407 q h 999 -0.01832 7.80966 0.01212 59,,25 Q.00797 O.29106 0.620 0.28923 O.02334 7.0X7 0.02520 O. 03270 70.39 O. 01260 O.00450 0.189 0. 00451 0.03631 5 * 554- 0.03513 INTEGRATIONS #2 -0.00086 0.60870 -0.00511 O.05091 o:09409 0.00201 103.78584 -0.00174 -0.00130 0.00231 0.00886 0.85680 0.91908 .0.01005 38. 52109 0.03462 0.00173 30.03650 -O.00339 0.02478 -0.00165 -0.05944 7.85074 0.00798 0.29110 0.02273 0.02769 0.00450 Q.D386S #3 REREAD -O.00201 0.64203 -O.00527 0.05418 0.09409 -0.00041 104.95240 -0.00174 ________ D. 00049 -0.00031 ' 0.00822 0.86863 1.02038 0.00753 38.76067 O.03053 O.00432 30.25627 -0.DO169 0.00980 0.00143 -0.01084 ' 7.96181 0.0204 2 ` Q 29285 0.02210 ________ D.05782 Q.00451 O.03511 9b DUP050307861 Pas 22 LANCASTER LABORATORIES Run Name: 9626903111. .> Tube:- 21 - 258527? >)' lOO-lOOfDPI;96269572OD01,S,f 09'/25/96 INSTRUMENT ID: 02360 INTEGRATIONS . ELEN AVG (Dm> . 'SRSO 82 83 , REREAD REDIG R A -0.00073 183.9 0.06897 5.230 0.00551326.S '0.56479 0.921 "0.06190 0 0.00121 115.4 150.69319 0.176 -0.00254 67.35 0.00684 13.13 0.00360 74.72 0.00168 43.'53 0.234S2 1.921 4.58952 2.243 0.0351S O 37.90802 0.197 -1.69294 0.278 O.00778 25.45 79.06852 0.300 0.00567 69.13 0.00654 249.6 0.00757 39.36 -Q.00362 274.3 5.60896 0.250 0.01238 208.8 D.8306> 0.131 -0.00155 100.1 0.04760 73.35 0.00005 26.63 0.00552 18.73 -0.00152 0.07105 0.02125 ' 0.56027 O.06190 -0.00040 150.50309 -0.00155 O.00773 0.00654 0.00126O.22989 4.56702 0.0351S 37.82229 1.68751 . O.00951 78.79640 O.00341 -0.01219 0.01055 -0.02980 5.59558 -0.0166D O.82975 -0.00134 0. 02755 0.00007 O.00672 -0.00152 0.064SO 0.00947 0.56361 0.06190 0.00202 150.57978 -0.00451 0.00594 0.00301 ' O.00126 0.23581 4.49967 D.03518 37.95964 1.69566 0.00562 79.23598 O.01020 0.01778 0.00759 ' -0.01299 5. 62358 0.02066 O. 83037 -O.ODOll O. 02732 0.00004 CK 00492 0.00083 0.07104__________________ -0.01417 _______ ________ 0.57048 __________________ 0.06190 ______: 0.00202 _ 150.99668 - -0.00155 ____ 0.00684 0.00125 0.00253..______ 0.23875 _______ _____ 4.70188 _________________ 0.03518 __ 37.94212 _________________ 1.69566 ________________ 0.00822 79.17319 0. 00-340 ________________ 0.01404 _______I ' 0.00458 ________ _____; 0..01691________]______` 5.60771 I 0.03309 0.83187 " -Q.00320 ________________ O.08792 _____ 0.00005 ' 1____________~ 0.00494 ________I_____ 96 DUP050307862 pac* 23 LANCASTER LABORATORIES RUn Name: 9626903111 Tu&<.: 22 .2635278 'fVvQ-'Cv 3.0 09/25796 **** r 100-100, DF1, 962695720001,8, , 22:26 INSTRUMENT ID: 02360 | j ELM ____A* & VSo ; X3* ... XP \ccf ` 'L.Co w. XJ< --.J"'*- S^n STn q X/S*i X'^ s .51 6n Sr* T1 Xv X20 . AVG Id d ih T %RSD -0.00060 1.876. 0.12979 5.534 0.00129 1051. 0.53193 0.649 0-10482 1.363 '0.00040 350.1 74.63196 0. 560 -0.00154 0.065 0.00530 39. 02 -0.00296 90.96 0,00126 0. il4. O.20543 2. 195 3.7S797 1.028 0.02345 12.37 26.97459 O. 854 0.17309 0.006 0.00692 37. 49 64.81419 0.937 0.ODOOO 78. 78 0.01230 70.45 0.00866 53.23 0.00008 39401 6.22799 0.299 0.01446 74.4 1 0.56065 0.776 0.00290 46.45 O.04274 105.9 0.00152 223. 7 O.00685 0.420 INTEGRATIONS 81 . 82 -0.00061 0.12569 0.00917 . 0.53092 0.10400 -0.00041 74.24187 . -0.00154 . 0.00769 -O.00590 0.00126 0.20051 3.74298 0.02513 26.77736 0.17810 0.00692 64.447SS O.OOOOO 0.01733 0.00462 -0.01113 5.20993 0.00823 0.55737 ' 0.00445 O.04272 0.00450 0.00687 -0.00060 0.12560 -0.01442' 0.52911 O.10400 -0.00039 74.58083 -0.00154 0.00411 -O.00061 0.00126 0.20641 3.81041 O.02010 26.91836 0.17809 O.00432 64.4 7930 0.OOOOO O.00229 0.01369 0.03746 5.23796 0.00826 O.55899 0.00229 0.08803 "0.00220 0.00682 I 83 REREAD REDIG !' -0.00059 0.13809 0.00912 0.53578 O. 10647 0.00202 75.07318 -0.00154 0.00411. -0.00236 0.00126 0.20937 3.81052 0.02513 27.22807 0.17803 0.00951 65.51539 0.00001 O.01729 0.00766 -0.02607 5.23608 0.02639 O.56560 a.00197 -0.00253 0.00229 O.00685 ` ~ {I ii i DU P050307863 Pasae: 24 LANCASTER LABORATORIES Run Name: 9626903I11 Tube: 23 CCV 09/25/96 INSTRUMENT ID: 02360 j 22:30 ELEM AV foom} " %RSD =B1 INTEGRATIONS 82 #3, REREAD. REDIG A A __Aa __ A1 .--As ; S --Jla. . Ca cd ; 'f Co '___Cr ___Cu _J< ___Li __MO ___Mn __ no- ___Na --Jti. __Pb ___Sb ___Se ___Si ___5n ~ Sr Ti ___T i _.V 2n 0.45688 0.296 25.14.002 0.25.9 1.94S61 0.907 1.90303 1.DBA 4.77177 0.144 0.47426'0.292 49.00558 '6.228 4.70477 0.108 " 0.93696 1.064 4.83161 0.231 4.85579 0.213 4.81563 0.200 49.95203 3e-05 24.94135 O.315 24.89822 0.381 '4.70387 0.218 24.27294 0.670 51.27833 0.126 9.32910 0.366 23.37973 0.241 4.73077 0.488 1.88706 1.016 9.51524 1.604 4.72602 0.607 0.96133 6.214 1.96596 0.479 4.76319 0.672 1.95440 0.307 . 4.69166 0.323 0.45609 25.-06802 1.92931 1.8S240 4. 76434 0.47266 48. 89014 4.69886 O'. 92802 4.81945 4.84402 4.80624 49.95202 24.87.517 .24.81114 4.69430 24.11849 51.20561 9.29135 23.31463 4.72590 1.88206 9.36207 4.69288 0.95896 1.95668 4.77456 1.94749 4.67399 0.45844 25.15699 1.95245 1.90303 4.77300 0,4-7506 49.11403 4.70774 O.'94772 4.83392 4.85982 4.81514 49.95204 24.92041 24.88387 4.71475 24.25736 51.29931 9.35796 23.41611 4.71048' 1.90825 9.51620 4.74253 0.96232 1.96565 4.72700 1.95729 4.70224 .45610'__________ 25. 19505 _______ ____!------ 1.96406 ________ 1.92367 ...________________ 4.77796 _i------------------------ 0 . 47506 ;. 49.01256 _ 4.70771 0.93513. 4.84147 ------------------------ 4.86353 _ 4.82552 _______!--:------- 49.-95201 25.0284 8 ______ 24.99964 ___! 4.70256 24.44297 51.33008 ____________--. 9.33798 _____________!----- 23.40846 _______ 4.75595 _ 1.87087 _________________ 9.6674 4 _ -- 4.74266 0.96270 1.97553 ________________ 4.78800 1.95841 ____;___________ 4.69874 98 DUPO 50307 864 pasje: 25 LANCASTER LABORATORIES ! Run Name: 9626903111 r Tube: 24: COB ELEN ....M --A3 _J3 _J3S' ,,ca Cd CO jCr. CU __ K __ no ___Mn ___Jlo Na 3i ___Pb. ___Sb ""si `__Sn _J5r ___Ti Jt i '__V l_2n AVG' foom)- SsRSD -0.00117 100.2 0.00619 3B.53 -0.00594 114.7 . 0.00687 0.09D :ooooo o O.OOODO 9576. 0.01526 9.336 -D.00148 0.039 D.OOISO 57.65 -0.00436 90. B9 0.00465. 15.73 0.00196 43.45 0.01123 365.2 0.00000 O -0.00306 161.2 0.00000 18.93 0.01470 17.64 0.05228 0.020 -O.-00337 100.9 0.00629 68.63 0.02395 44.57 -0.00436 449.5 0.01460 6.431 0.00336 296.6 0.00012 2QS.1 -0.00154 61.12 0.00261 383.3 0.00231 96.71 0.00001 29090 09/25/96 22:34- INSTRUMENT ID: 02360. INTEGRATIONS #1 . ' #2 -0.00234 0-00394 -0.01381 0.00687 O.OOODO -0.00040. 0.01644 -6.00148 0.00239 -0.00318 0.00507 0.00097 -0.04490 0.00000 ' -0.00801 0.00000 0.01730 o.05228 -0.00336 0.00130 ' 0.02294 -0.02430 0.01459 0.00836 0.00041 -O.00175 -0.01749 O.00003 -0.00356 0.00000 0.004 82 -0.00201 0.00637 0.00000- -0.00062,0.01690- , --Ol0014 8 0.00239 -0.00025 0.00507 0.00246 0.12352 . O.OOOOO -0.00305 , 0.QOOOO 0.01670' 0. 05228 O.00003 0.00879 0.01382 -O.00374 0.01555 0.03319 -0.00008 -o.ado5i -0.00254 0.00455 0.00357 3 . REREAD REDIG j -0.00117 ________ _______ ! 0.00479 ________.1 j -0.00199"________________ ! 0.00636 | 0.00000 0.00080 ________ ; i j 0.01464 ;__________________ ! -0.00148 0.00060 ~ -0.00466 ________ _______ 0.00330 ;3 0.00245 _______ -0.04490 ________ 0.00000 __________________ 0.00137________ ; 0,00000 0.01211 0.05230 -0.00677 __________________. 0.00879 ________________ 0.03510 ;_________________~ 0.014 94 _____ 0.01367 ___L___ -0.01645 ________ ______ '- 0.00004 ________________1" -0.00236 ________ 0.0278S_________________ 0.00229 ~ D. 00002 ________________ 9v DUP050307865 Page: 26 LANCASTER LABORATORIES Run Name: 9626903111 INSTRUMENT ID: 02360 Tube: 25 2585281 09/25/96 100-100, DFI,962695?2OQ01fS.!, f . 22:38 'I AVG , INTEGRATIONS ELEN (ppm).. . 56RSD ,#i- #2 #3 ' REREAD REDIG ___As ___Se ___Si __ sn Sr -0*00264 105.2 0*23386 1.817 ' -0.01110 61.35 0.10970 2.440 O'. 044.57 0 0.00040 462. 2_ 330.34439 1.334 .-0.00462 64. 12 0.00295 175.3 0.00041 881.4.. 0.00379 57. 96 ' ,0.57986 1.177 4.36689 1.354 0.08544 0 106.24562 0. 304 0.21354 0. 548 0,00648 50. 55 97,,99052 0. 705 0.00341 99. 82 -0.00218 910.0 0/00046 997. 8 0.02764 54.64 8.83552 0.821 0.03083 11. 56 1-16255 0. 303 0.00379 28. 16 0.07783 73. 36 0.00154 168.6 0.01673 0.04 2 ` O.00056 0.23392 -0.01505 0.11006 0.04457 0.00201 334.51419 , -0.00462 O. 00594* 0.00454 0.00633 0.58775 4.40140 0.08544 106.57959 0.21419 O.00822 97.94864 0.00681 0.02037 0.00147 0.045D9 8.90492 O.03295 1.16829 0.00702 0.11794 0.004 54 0.01673 -0.00420 O.23808 -0.00323 0.11218 0.04457 -0.00162 330.78808 . -0.00165 O.00594 -0.00253' 0.00252 0.57592 4.40066 0.08544 103'. 93453 0.21219 0.004 32 97.32071 o.doooo '-0.00966 t 0.00460 0.01893 8:84143 O.03294 1.15658 0.00642 0.10310 0.00003 0. 01674 -0.00429 0.22958 ~n.01500 0.10686 0.04457 O'. 00081 325.73092 -0.00758 -O.00302 -0.00075 0.00252 0.57591 4.29859 0.08544 106.22274 0.21425 0.00692 93.70220 O.00342 -D.01727 0.00452 0.01891 8.76020 0.02676 1.16218 0.00394 O.. 01245 0.00005 0.01672 ;________ _____ ___.____ ;________ ________ ioo DU P050307866 Pai5 27 LANCASTER LABORATORIES Run Wme: 9626903111 , . TuM* 26 ' 25S52B2 fcsQLiSxSS fl JK W * f, :too- 100.DF1,962695720001* 09/25/96 * 22:42 INSTRUMENT ID: 02-360 el eM 'ji --A* N XCUi '^C4 XP* Y.CI" Xcu xW Yk j..i \Ow ^N m<ft1 JLN'1 _j PD Sc Si sn .Sr ;r.t __Ti Xy AVG Cd p id J ' %RS0 -CL. 00132 224.0 0.02962 14.08 ' O. 003.81 ,378.0 .06602 2. 691 0.24391 1. 343 ;. -0.00041 1. 759 134.14474 0. 857 -0.00247 69. 18 -0.00016. 1669. -0.00089 599.4 0.00148 65. 4 7 0.01624 10. 49 1.58769 6. Ill 0.03350 3.660 42.42814 0.812 0.00158 1.256 0.00519 86 27.0-3296 1.163 0.00001 37. 60 0.00917 131.7 0.00257 275- 3 0.09219 12.38 10.68893 0.839 0.00415 457.5 0.4.1421 0.966 -0.00299 17.62 O. 02766 54. 58 O.00226 99,, 5 7 0.01029 O. 170 Ikn s *2.- -0.00174 0.02986 -0.00212 0.06397 . 0.24019 -0.00041 . 132.88085 -0.00148 0.00223' -0.00208 . D.00063 0.01723 1.69973 0.03015 ` 4.2.03081 0.00160 O.00432 26.67713 0.00000 0.01795 0.01075 0.08223 ' 10.58967 0.02075 0.40960 -O.00360 0.04275 O.00225 O.01030 -0.00405 0.02559 0.00972 0.06703 0.24638 -0.00040 134.42472 -0.00445 -0.00315 -0.00559 0.00126 0.01723 1.53160 . 0.03518 42.64745 0.00157 O.00432' 27.27367 0.00001 -0.00461 -0.00147 0.10465 .10* 71287 0.00828 0.41682 -O.00268 O.02767 O.OOOOl 0.01027 - #3 REREAD REDIG 0.00182 0.03399 ________ -0.00216 0.06706 0.24515 -0.00042 135.12863 -0.00148 0.00043 0.00498 0. 00253 0.01427 1.53173 0.03518 42.60617 ' 0.00157 O.00692 27.14807 Q.OOOOl 0.01418 -0.00156 ________ 0.08970 10.76426 -0.01657 0.41620 -0.00268 0.01255 0.00452 0.01031 101 DUP050307867 LANCASTER LABORATORIES. Run Name: 9626903111 Tube: 27 * 2585233 xxxx"100-100,DPI,962695720001,8,, 09/25/96 22:46 INSTRUMENT ID: , ' ELEN AVS . foomT v %RSD -O.ODDS7 2.332 0.0130 54.61 0.005B0 234.4 d.34879 0.554 0.14362 O Ol00000 14552 '83.25633 0.333 -0.00004 3019. O.00349 156. 9 0.00055 482.0 0.00168 43.4 0.16005 1.066 3.352S2 2.527 0.03685 7.872 23.28123 0.419 0.51403 0.457 a. DD735 26. 95 . -52.79957 ll070 0.00114 170.7 0.00740 116.1 0.00254 279.1 -0.01612 13.39 9.05436 0.084 0.01032 193.7 0.54819 Q.337 -0.00340 27.75 0.07289 74.63 0.00153 16S.7 0.00683 0.367 INTESRATIONS #1 2 -O.00038 0.00482 -0.00202 0.34996 O.14352 -0.00040 88:14793 -0.0^004 0.00947 ' -0.00238- 0.00126 O.15906 3.27420 0.03518 28.23502 0.51267 0.00692 53.36472 0.00340 0.00249 0.01073 -0.01488 .9.04906 0. 03314 0: 54803 -0.00422 n.Q8792 ' O.00003 D.00682 -0.000360.01720 0.02151 0.34935 O.14362 -0.00042 88. '63534 - -0.00153 O..00229 0.00291 O.00126 O.16202 ' 3.34167 0.04021 23.41610 O.51674 O.00951 52.79956 O.ODOOl 0.00233 -0.00153 -0.01862 9.05095 0.00202 0. 5504 0 -0.00361 0.01255 0.00453 O.0068 #3, REREAD REDID -O. 00038 _____________i----0.01713 -0.00208 ________ 0.34655 __________________ O.14362 __1 0.00031 87.98587'--------------------------. 0.00143 ,, --0.00129 0.00114 o. 00253 ________--:---------0.15906 _________________ 3. 44260 _______________-- 0.03513 ______________ 28. 19256 ________ 0.51267 ______ ----------O. 00562 ________________ 52.23442 ________ _______ 0.00001 ' 0.01732 -0.00157 ________ -0.01487 9.06308 -0.00419 O.54616 -0.00237 ________ ______ 0.11821______ 0.00003 ,0.00682 ----------_---------- tJ DUP050307868  poflffi 29 ' LANCASTER LABORATORIES Run Name: 9626903112 TUt>*S 2S 2585284. 100-100, DPI, 96269572000X73,. 09/25/96 Vv* INSTRUMENT 10: 02360 22:50 . ELEM .&! __P ' ' a XCa X.w- IS w X* __1-1 ' xrin S$Na 5LN1 Fb . X&> ___51 3n Sr ""ji ' . *"_TI " .V n AVG 'CmT sRSD -0.00032 5.105 0.015S3 15.40 0.00185 735.4 0.33689 1.196 O. 14733-. 0. 840 0.00121 116.6` 90.80972 0.797 -0.00054 313.6 0.00409 43.86' -0.00030'824.3 . 0.00084 87.13 0.16695 2.045 3.48809 2.007 0.03853 3.765 29.03228 0.569 0.53031 0.886 0.00692 O 53.86707 O. 727 -0.00225 87.07 -0.00006 272380.00152 692.7 -0.03356 78.53 9. 28590 0. 711 0.00824 151.1 0,56489 0.697 -0.00238 56.20 0.08810 17.19 0.00153 168.4 0.00566 17.'80 INTEGRATIONS #1 - 82 -0.00030' 0.017-27 0.00970 0.33223 O.14857 . --Q;00042 91.23321 0.00142 0.00588 0.00116 0.00126 O.17089 3. 51063 0.03769 29.14879 0.53302 0.00692 54. 18103 -0.00339 0.00996 -O.00456 -0.02982 9. 32636. 0.00822 O.56809 -0.00177 0.08811 0.00451 0.00509 -0.00031 o-. 01302 -0.01387 0.33913 0.14733 0.00202 91.22207 -0.00153 0.00229 0.00116 O. 00126 O.16498 3.40956 0.03769 29.10508 0.5.3303 D.00692 53.99265 O.00GO1 0.00992 O.01373 -0.06160 9.32169 0.02071 0.56610 -0.00146 O.07293 0.00004 0.00682 83. REREAD RED-IG -0.00033 _____ _ .0.01721 --------- 0.00972 ______ 0.33929 ____ __ 0.14609 ______ 0.00202 ____ _ 89.97386 ----- -0.00153 _____ 0.00409 ______ -0.00324 _____ _ o.oaaoa -------- a.16497 ______ 3.54407 ______ 0.04021 .... 28.84297 ____ 0.52488 ______ 0.00692 -------- 53.42752 _____ -0.00339 _____ -0.02008 ___L_ -0.00459 ------ -0.00927 _____ 9.20964 ___ ... -0.00420 _____ O.56049 _____ -Q_00393 _____ O.10324 _____ 0.00003 _____ 0,00506 :____ 101'o' DUP050307869 Page:' 30 LANCASTER LABORATORIES Run Name": 962.6903111 INSTRUMENT ID: 02360 25S52B5 .. 09/25/96 22:54 DFI .962695720001, 3,, "1 ELEM. AVS ' ' DPBl)^ %RSD -0.00077 173. 8 O.00350 ISO. 4 - . 0. 00193 353.0 O.01142 17.33 ' 0.00000 0 -0.00041 1.993 0.06103 1.163 -0:-00345 95.95 O.00060 513. 5 -0.00055 455.4 - 0.00063 172.9 0.00344 49.62 -0.06736 152. 7 0.00000 0 0.00997 37.9B 0.00000 225.4 0.OODOO 0 0.11513 0.007 -0.00226 56.43 0.00626 65.53 0.0D359 128. S -0.01569 119.5 0.02114 4.400 0.00001 95246 0.00041 0 -0.00195 72.55 0.03778 100.6 0.00293 56.37 0.Q1D69 O. 150 . SI INTEGRATIONS #2 -0.00234 0.00900 -O.00203 0.01028 O.00000 -0.00041 0.06144 -0.00741 -0.0029S 0.00234 0.00190 0.00246 -0.04490 0.00000 0.00912 0.00000 -0.00056 O.11512 -0.00339 0.00871 0. Q0767 0.00371 0.02207 0.00831 0.00041 -0.00113 O.07302 0.004.4 7 0.01070 ' 0.00000 0.004SS -0.00199 0.01371 0.00000 . -0.00040 O.06144 -0,00148 0.00239 -0.00116 0.00000 0.00541 -0.1796^ 0.00000 0.00667 a.ooooo 0.00173 ' 0.11512 -0.00340 0.00575 0.004 55 -0.01869 0.02115 -0.01655 0.00041 -0.00113 0.04257 ' 0.00000 0.01068 S3 REREAD REDIG 0.00000 ................... -0.00339 _________ 0.00984 0.01025 O.OOOOO -0.00041 0.06021 -0.00145 0.00240 .......... * -0.00294 0.00000 0.00245 0.02247 O.OOOOO ......... 0.01411 0.00000 -O;00086 * 0.11513 ........ O. OOOOO 0.00128 -0.00144 -0.04111__________ 0.02021 0.00825 0.00041 ........ . mini------- -0.00360 -0.00253 0.00446 ` 0.01070 lO-i DU PO 50307 870 f'liit'jl'` -51 k5 k k; kie s Run Name:. 9626903111 rufc-e: 30.. C.R1 e l .e m __ A9 --A* .-As -- -- , Be. ': ""era --C<J ___Co __ Cr __Cu *3' --K __ I--*' jio tin __ Na ___ pb St> <>! 3i ____5n Sr _;ri T1 ___y "*._Zn .AVG . loom). . %RSD 0.02114 0.009 0.09064 7.914 0.02470 72.97 -0.00114 172.6 0.00000 .0 : 0.00951-14.40 0.00366 16.41 0.00889 16.66 ' O.10793 3.153 0.01758 11.55 0.05123 1.429 0.00197,42.53 0.02245 0.007 0.00000 O 0.00297 174.7 0.03267 0.000 0.00173 O 0.05224 0.032 0.07866 6.246 0.00754 109.S 0.13043 10.15 -0.00157 353.3 0.QQ445 53.57 -0.00370 531.6 .0.00008 346i 4 -0.00276 112.5 0.04965 97.33 0.10142 5.089 0.03949 0.099 09/25/96 22:58 INSTRUMENT ID: 02360 ; INTEGRATIONS #1 2 0.02114 0.05647 0.04-438 o.oqooo 0.OOOOO 0.00895 0.00949 0.00889 0.10558 0.01640 0.05031 0.00246 0.02246 0.00000 0.00464 0.03267 0.00173 0.05223 0.08150 0.01780 0.11524 0.01305 0.00444 -0.02561 -0.00008 -0.00235: 0.06964 0.10738 0.03953 . ,0.02114 n O.09892 0.02074 -0.00343 0.00000.' 0.01144 0.00948 0.01037 0.10647 0.01641 0.05205 O'.00099. 0.02245 0.OOOOO 0.00715 0.03267 0.00173 0.05223 0.05150 0.00252 0.13659 -O.01868 0.00818 O.00873 0.00041 0.00011 0.05477 0.0984 3 O.03945 #3 REREAD REDIG 0.02114 0-08652 0.00898 O. OOOOO O. OOOOQ 0.00901 0.00702 O.00741 ' 0.11187 Q.01993 0.05081 0.00245 0.02245 0.OOOOO -0.00285 0.03267 0.00173 0.05226 O.07299 O.00291 0.13963 0.00000 0.00072 0.00875 -0.00008 -0.00606 -0.00546 0.0954 4 O.03948 10 D DUP050307871 pcifle 32 LANCASTER LABORATORIES Run Name: 9626903111 . TuDe: 31 ICSA 09/25/96 INSTRUMENT ID: 02360 23:02 ELEM k .fppml %RSD' 1' # ' INTESRATIONS % #2 #3 REREAD REDIS A '__A _.JS -- _J3 __.Ca Cd ___po __Cr __Cu Lfe- _.J< ___.Li __ H9 __ Mn _>io __ .Ns ___I___PD ""~5e __~Si __jsn Sr ~Ti " T1 ___V zn 0.00531 53.91 485.92385 0.194 ' 0.24560 28.21 0.08416.1,150' 0.00619 19.99 -0.00040 0.460 478.09542.0.096 0.00513 18.04 0,00121 224.7 0.00167 62.43 -0.00357 35.61 179.31272 0.160 0.02824 137.9 0.00335 36.60 488.66406 0.141 -0.02098 11.20 -0.01730 22.91 0.03152 57.48 -0.01024 33.15 0.01658 55.98 -O00884 30.08 0.02275 95.73 0.17612 2.427 ' 0.00367 336.0 0.02010 0 -0.01456 12.34 O.09343 69.19 0.00199 130. 1 O.01532 0,365 ` 0.00261 486.95318 0.18546 Oi08302 . 0.00742' -0.00040 477.66824 0.00463 0.00062 O.00288 -O.00484 179.41864, -0.01675 0.00502 439.30572 -n.01827 -0.01384 O.05244 -O.01363 0.00998 -0.01293 0.03338 O.17145 O. 00365 0.02010 -O.01660 O.10358 0.00351 O.01534 0.00501 485.71627 0.32138 O.08487 0.00619 -Q.00040 478.581.20 O.00456 -0.00117 0.00110 -O.00230 179. 5324.4 0.05080 O.00502 488.75341 -O.02234 -O.02163 O.02107 -0.01024 0.02564 -0.01294 0.03717 O.17705 0.01601 0.02010 -O'. 01559 O.16336 -0.00100 O.01525 0.00832 .--------------------------- '485.10208 _________________ 0.22996 _________________ 0.084.58 _ _____ ____-- 0.00495 __________________ -0.00040 ^----------- 478.03686 ' . .----------- 0.00620 -------------------------- 0.00420 --------------------------- 0.00104 _________ -0.00356 _________ ______ 178.98709 _ 0.05069 _:------------------------- 0.00000 _______________ 4 37.93307 ------------- ----------- -0.02234 -----:----- -0.01644 ________________ 0.02104 ____________ -0.00684 _____ 0.01113________________- -0.00066 -0.00230 ________ _______ O.17985 _________________ -0.00865 ________________ 0.02010 _____ .. -0.0124 8 1 0.02790 _________________ 0.00348 ________ ______ 0.01535 ________ ______ 106 DUP050307872 'Mril&l.. paw# t 33 LANCASTER. LABORATORIES Run Nwfl,e: 9626903111 Tut'# f 32 ICSAB 09/25/96 23:06 INSTRUMENT ID: 02360 el eM . --A* J\to __JJ --p* -J* ' J2 .,,_Cd .cw Her __j;u Zm fW Hrin __ N _r* __,st? ~ ".(S' __S i __yn _ 5r rJ j1 y AVG (Dom) %RSD ' ttl INTEGRATIONS 2 0.19233 0.367 488.92605 0.628 0.40338 18.91 0.06325 3. 716 0.48823 0.638 .0.47820 O. 774 483.34545 0.551 0i89050 0.652 0.45052 0.830 0.46690 1.187 0.47439 a; 552 181.29028 0. 617 0.05137 132.1 0.00083- 458.2 492.14593 0.636 0.43157 O. 537' -0.01297 23.09 0.05202 0. 016 0.88030 0. 773 0.06294 11.56 0.57754 1: 059 0.08637 46. 05 0.10194- 2 - 280 0.02577 226* 7 0 *02016 0. -556 -O.01579 9.970 0 * 16440 11.50 0.47422 0.94 7 O.90437 D > 692- ' . 0.19303 . 486.00796 ' O.38236 0.06468 0.48534 0.4 74 97480.63214 . 0.89078 0.44633 O.46086 O.47280 180.15618 -0.01654 0;00502 489.19033 O. 42889 -0.01124 D.05201 0.88711 0.05462 0.57073 O.08089 0.10441 O.09231 Ok 02022 -O.01418 O.16168 0.46972 O.S9970 0.19234 488.64010 0.33980 0/06455 0.48732: 0.47739 48.3-44030 .0.88456 0:45352 O. 46808 0.47405 181.31933 0.05139 0.00000 491.82000 0.43294 -0.01124 0.05202 0.88030 O.06814 Q.58257 0.04961 O.10161 O.00506 ' 0.02010 -0.01753 0. 184 53 0.4 7424 O. 90.318 #3 .REREAD 0.19162 492.13009 0.48798 D.06054 _________ ' 0.49153 G 4*8224485.96395 0.89616 0.45171 0.47176 0.47784 182.39532 0.11926 -0.00251 4 95. 4274 5 0.43287 ;________ -0.01644 O-05202 0.37349 0.06606 0.57932 0.12860 0.09980 -0.02004 n.Q2022 -0.01587 0. 14 700 O. 4 7871 O. 91022 107 DUP050307873 34 LANCASTER LABORATORIES Run Name: 9626903111 Tube: 33 CCV __ A9 . __A1 ' As ' __B . ___Ba ___B __ Ca CQ .Co Sr __Cu __ Pe __[< ___Li '__ Ms ___Mn ___Mo ,;_Na ___Ni ___Pb ___Sb Si ___Sn ' ___Sr __Ti __Ti __ V ___Zn AVG (potnl asRSD 0.46950 0,330 25.77718 0.446 2.01986 1.721 2.06892 0.724 4.89888 O.S63 . 0.491-10 0.746 50.86764 0.668 ' V. 88269' 0.699 0.97486 1.160 5-00391 0.910 4.98024 0.605 5.00566 0.674 51.19866 0.431 25.01005 0. 907 25.36812 0.570 4.86403 0.676 25.11400 0.838 52,31155 0.65? 9.63793 0.693 24.07511 0.713 4.85753 .1.107 1.93805 0.309 10.56582 0.799 4.8174 7 1.127 0.98741 0.727 2.00720 1.081 4.78204 1.590 2.01271 0.838 4.85174 0.619 09/25/96 INSTRUMENT ID: 02360 23:10 INTEGRATIONS #1 #2 0.46795 25. 799.53 2.01970 2.07289 4.91291 0.49188 50.78019 4-87952 0.97512 5.00623 4.99273 5.01187 51.23233 25.16419 25.38301 4.86812 25.10361 52.58364 9.68290 24-. 05381 4.83667 1.93119 10.53035 4.78009 O.99011 2.01667 4.86665 2.02308 4.33984 " 0.46791 25.65266 1.98517 2. 05233 4.86710 ' 0.48711 50.57988 4/84992 . 0.96360 4.95726 4.94585 .4.96890, 50.96285 24.74952 25.21655 4.8292? 24.9OS92 . 51.92510 9.38215 23. 914 96 4.81730 1.94232 10.50486 4.79253 O.97927 1.9S237 4. 71934 1.99275 4.82945 #3 REREAD REDIG 0.47265 ___ 25. 87934 ___ 2.05471 ____ 2. 08153 ___ 3 4.91663 ___ O. 4 94 32 ___ 51.24283 ..__ 4. 91802- __ 0.98584 _ 5.04826 __ 5.00213 __ 5.03554 _ 51.40081 _ 25.11644 25. 5048X 4.89471 ,, 25.32945 __ 52.42592 _ 9.70890 _ 24.25655 4.91862 3 1.94065 _ 10.66226 _ 4.S7978 _ 0.99285 I 2. 02.23'4 4.76014 2.02229 4.88594 I 108 DUP050307874  f r Page: 35 LANCASTER'LABORATORIES Run Name: 962690311-1 Tube: 34 CCS 09/25/96 23:14 INSTRUMENT ID: 02360 ^ AV<5 INTE6RATIONS ' " EL EM . .. loom') SsRSD #1. 82 83 REREAD REOI 1 ' Ag -0.00038 635. 1 . -Ov00116 ' -0.00233 0.00235 Ai 0.D2977 0.257 ' D.02968 0.-02983 0.02980 ___As -0.00999 68.29 .-0.01392 -0.01394 -0.00211 B 0.00283 34. 99 0.00340 0.00339 - 0.00168 Ba - : 0.00000 0 . '0.00000 0.00000 0.00000 Be 0.00040 351.6 -0.00040 -0.00042 0.00202 A Co . 0.03587 3.982 0.03669 0.03422 0.03670 Cd -0.00247 69.17 -0.00445 -0.00148- eO.00148 Co : 0.00119 172.9 -0.00119 0.00239 0.00239 ___Cr -0.00260 173. 3 -0.00640 0.00238 -0.00378 ___Cu 0.00486.32.83 0.00634 0.00507 0.00316 . 0.01527 11.19 O.01724 0.01428 O.01428 K 0.01123 173. 0 0.02247 -0.01122 0.02247 ___.Li 0.00502 0 0.00502 0.00502 0.00502 Mg 0.02149 37.46 0.01326 0.02936 0.02186 ___Mn 0.00000 35.24 O.OOOOO 0- DD0OD OiOOOOO ___Mo 0.014 7,0 30.56 0.01990 0.01211 0.01211 ___Na - 0.06274 28,,90 n,05225 0.05228 '0.08369 A ___Ni 0.00003 10867 0.00004 0.00342 -O.00337 ___Pb - n.oia.27 101.8 0.00124 0.02378 0.00878 ' Sb 0.01987 40- 62 0.02902 0.01683 0.01376 ___Se ___Si ___Sn ___Sr ___Ti ___Ti ___V ___Zn 0.00871 Q.Q2207 D. 0124.9 0.00033 O.pooID O.03771 0.00157 0.00000 173. 2 11.17 57. 39 43.30 1.044. 115.5 164 - 0 204 - 9 0.02241 0.02392 0-00837 0.00041 O.00133 0.08802 0*00010 --O.00002 0.01121 0.02302 0.02076 0.00016 -0.00051 0.01243 0-00455 0-OOOOO -0.00747 0.01927 0.00832 0.00041 -0.00051 0* 01263 0.00006 0.OOOOO ' _________ -- Data Reviewed by: Data Verified by jUvJl f-ai-ft loe DUP050307875 Furnace Data no DUP050307876 . LANCASTER LABORATORIES GRAPHITE FURNACE -ATOMIC ABSORPTION DATA REVIEWED BY : DATA VERIFIED BY: ' DATA FILE MAMFv ASr '5 OS. RAT RUN NAME: S6Sft'3eaF04 ANALYSTS f-G ` INSTRUMENT NO: 847E4 ' OKO CORR,5 BZ - ' ELEMENT: AS Concentration is used to evaluate! IT -icvrar:?-.u 1. <; :> ara' within calibration range. 111 / DUP050307877 RUN MUJ'lLs 96269021' U 4 PAGE s .'i ANALYST: 6, a TUBE: SAMPLE SB I . 09/25/96 16:20 CLASH I'VOL/WT 0 AVG(cob) JCRPD AVG abs 0.6400 167.4 0.003 l. AMCAO ri.ii -LADORA LORIES INSTRUMENT ID: 04724 orAA e l f me h t .! AO FVGL DF BATCH NUMBER 0i BURN 1 BURN g 0-005 -0,000 TUBE: '2 SAMPLE S10 09/25/96 16:24 Cl ASH. IVOL/WT 8 AVG(opb? JRP AVG aba 11.3700 6. 1 0. 032 FVOL i)F BATCH NUMBER 0 1~ BURN l BURN 2 '0.03.1 "0.034 TUBE: SAMPLE BH0 3 09/25/96 1.6:29 Cl. ASS IVOL/UIT 8 AVG < Dob) 23.0900 *RPP 1.8 AVG abs 0.075 FVOL DF BATCH HUMBER 01 BURN .1. BURN 0.076 - 0.074 ... TUBE: SAMPLE S40 .4 89/25/96 16:33 CL ASS IVCiL/WT 0 AVG<ppb> JiRPD AVG abs 38.6500 2. 7 0.1.43 FVOL DF BATCH NUMBER & 1. BURN 1 BURN 2 0.140 0.146 TUBE: SAMPLE S6@ 5 09/25/96 16:37 CL ASS JVOL/WT 0 AVG <ppb> I*RPD AVG abs 56.5908 1.6 0.211 FVQL DF BATCH NUMBER 0 J. BURN 1 . BURN 2 0.214 0.209 ': TUBE: SAMPLE 360 6 89/25/96 16:41 CL ASS XVOL/WT 0 AVG(cob) 62.0200 54RPD 1.0 AVG abe 0.291 FVOL _.DF__ BATCH NUMBER ;r BURN 1 BURN 2 0.293 "5.269 TUBE: SAMPLE ICV 7 09/25/96 16:46 Cl. ASS .TVOL/WT 8 AVG(nob> 49.3600 #RPt> : AVG a bib 0. 6 0. 177 ^RECOVERY = 96. 8 FVOL DF BATCH NUMBER 0 BURN 1 . 0.176 BURN 2 0. 176 1X3 DUP050307878 k o h t-tni'ii-: PAGE: h Nh LYST: '. oc'.oy 021- t.14 f' &a TUBEs SAMPLE XCB ~ a 09/25/96. 16 s 50 Cl. AS!.-' IVOL/NT 0 AVG <DPb) StfRPl) (3-2400 4-10-2 AM 13 abs LAN'-AC1 *..i'-itei.*i :n i uti.it.;. INSTRUMENT' IDs QA72A OF AA O.ilrtCWTa AG FVGL BE BATCH NUMBER 0 ,1 BURN 1 BURN 2 0.003 -0.003 ' TUBE Sfli1PLE CKft 909/25/96 16s5'> CLACC IVQL/UT 0 AUG(ocb) 10.7200 XRPD AUG abra 5.0 0.03Q FVGL * .0 DF BATCH NUMBER 1 BURN 1 BURN 2 8.036 0.039 TUBE; 10 SAMPLE CCV 1 09/25/96 16s50 CL_ACS rVQL/MT 0 AVG <ppb> flRPD AUG afas : 41.5400 0.4 0.149 .^RECOVERY = 103.8 IUSSi 11 SAMPLE COB 1 09/25/96 1? S03 01 ACC TVOL/UT 0 AVGtppb) XRPD AUG abs 0.0900 ***** -0.001 FVGL DF BATCH NUMBER 0 1' BURN 1 0.149 BURN 2 0.149 -- *9 FVOL DF BATCH NUMBER 01 BURN 1 BURN 2 0;002 -0.004- TUBEs 12 SAMPLE 09/25/96 17a06 CL A SC . IVOL/NT 100 AVG(ppb) 7SRPD AVIS abvi 0.9000 17.8 0.002 FVGL DF BATCH NUMBER 100 1 962691056801 BURN 1. BURN 2 RR RD 8.003 0.002 CUBE; 13 IS k p l e p*w 9&oOA 09/25/96 17s10 CL ACC TVOL/UT k w k **A* 100' AVG <ppb> 7CRPP AVG abs 19.3300 2-3 0.069 ^RECOVERY 96. 6 FVOL 108 DF BATCH NUMBER 1 962691856801 BURN 1. 0.060 BURN 2 8.070 RUM NAME: 9626902F04 PAGE: 3 ANALYST: 6S 17:15 IUOL/UT 1 AUG aiiv; 0.135 l.. AHCAO T! Ift LA BORA Y 0RIES INSTRUMENT ID: 04724 QFAA ELEMENT.! AS FOOL 1 DF BATCH NUMBER 1 962691056001 BURN i. 0.134 BURN 2 RR 0.136 _J_ RD TUBEj;. 15 SAMPLE LCSW UCbvv) .09/25/96' 17* 10 . CLASS lUQL/UT - FVQt. K-xtfitK-A* 11 DF BATCH NUMBER 1 962691056001 AUG (nob) ySRPD . AUG abs ' BURN l BURN 0 "56.9000 1.3 0.212 0.210 0.214 ^RECOVER* = 106.3 TUBE: 16 SiWF'LE/ asSei/s 09/25/96 17:24 Cl ASS 1VDL/WT u *'**w* 100 . FVOL 100 DF BATCH NUMBER 1 9&269105&&01 y /\ AVG<ppb) JtRPD AUG ab-* BURN t BURN 2 RR RD ~(S \ 1.1500 41.9 0.003 0.004 0.00S TUBE: 17 ^ 09/25/96 17:2s "0 SAMPLE ` Cl ASS IVOL/tJT FVOL DF BATCH HUMBER . 2565279-p^^^ ^U***A* 100 180 1 962691056001 AUG < ppb> *RPD AUG abfe 22.1900 4.0 0.079 BURN 1. . BURN `2 . 6.077 8.061 '' stRECQVERY = 111.0 ` TUBE! IS SAMPLE . 25S 09/25/96- 17:32 Ci. ASS IVOL/UT 100 FVOL 100 DF BATCH NUMBER 1 .962691056081 V / \ AUG<ppb> ?:RPP AUG atw BURN l BURN r> RR RD A - \ 1.3S08 3.9 0.004*' 0.004 0.004 _ LUJKj l 19 (39/25/96 17137 SAMPLE Cl. ACC IVOL/WT FVOL DF BATCH NUMBER A 585279 - 18 100 1 962691056081 AUG ( nob) Y.RPO AUG abs 21.4108 '4.4 0.~076" BURN 1. 0. 074 BURN 2 0.079 ^RECOVERY = 100.2 114 DUP050307880 KUM NHrlt. x 9626902K04 PAGE : h Hh LYST : 63 l mNl w :; j LHtiuiiHi ui-iiu INSTRUMENT .ID: 04724 DF AA ELEMENT. AS TUBE : 28 aateUL 2535279 . 09/25/96 17:41 Cl. ACC JUCiL/WT ?> s******* .1.86 \J AVG <m>b> JCRPD AUG abv, 40.2800 0.6 0. 144 FVOL- DF BATCH NUMBER 108 1 962691056001 BURN BURN 2 0.145 8.144 RR RD --, -- ruBag e'l SAMPLE Z2ZZ2Z 09/25/96 17:45 CL ASf: TVPL/MT Rw k k k Am 0 -- FUQL DF BATCH NUMBER 81 AUG < onb) KRPD AUG ,,abs 60.6300 0.9 0.213 BURN 1 0.217 BURN 2 0.220. /RECOVERY. = MOT APPLICABLE TUBE: 22 SAMPLE CCV 2 09/25/96 17 s 49 CL AGS IVPL/WT 0 * ** r FVOL DF BATCH NUMBER 3 . 1. 1' AUG < Dob) JiRPD 'AUG abs 43.3360 . 1.3 0.157 BURN 1 0.159 BURN 2 0.156 /RECOVERY =109 .6 ; TUBE: 23 SAMPLE' CCB 2 09/25/96 17:53 . CL ACG IVPL/WT 0 *v - * *** - . FVOL DF BATCH' NUMBER 0 .1 ` AUG<PPb> %RPP AUG ab<s , BURN 1 BURN 5 0.3500 30.a 0.80a . 0.003 ~ 0.001 TUBE g . 24 kl e ' 2535276 09/25/96 17s57 CL AGE: IUOL/MT * 160 '7 AUG <anb) siRPD AVO ab* 0.5100 193,4 0.001 FVOL DF 'BATCH NUMBER 186 j. 962691056081 BURN ' I. BURN a RFfc; RD -0.00a 0.603 __ TUBE : as SAMPLE 2535376 09/25/96 13:02 CL AGS IVPL/HT A* 106* FVOL DF BATCH HUMBER 168 . 1 963691056001 AUG < ppb) XRPD AUG aba 20.6600 1.5 8.074 BURN 1, 0.074 BURN n 07*073 ^RECOVERY 103. 3 LANOASTER LABORATORIES GRAPHITE FURNACE ATONIC ABSORPTION REVIEWED ; 7 VERIFIED BY: r:UF WANE; ASP70O.1 . RAT HATIE s 9fcfi7088Fe4 YST: INSTRUMENT NO: 847S4 BKG CORA.; B2 ELEMENT: AS 116 DUP050307882 RUN NAMES PAGE s ANALYSTS 9627002F04 .1 059 I..AHCA8 rr.i'i LABORATORIES INSTRUMENT ID: 64724 OFflA .'II-FMEN rAS TUBE*. SAMPLE 88 1 89/26/96 84 s 115 OLAM imzMi . -0.6500 m as*.* ' "8.002 LViLk ..BF... BAICH.J4W!BE 0.1 ; ...i -0.001 iai -0.00a (3 SfiftPLE 310 09/26/36 (3'isio Qkmi mourn. cm* j &e _ ; .; ...H.y.r*; 0 0 : 1 mLLmsa. a avaL-ata.. 9.4600 7.9 0.030 mmJL mL& 0.031 0.02 TUBES. mmji 320 3 09/26/96 84s24 5 ivoLZwi 0- ' ej^Bk 1m-- Paituaiiai^ A e.y.G.il?.t>b>.. '*&>: Ai3,,afe& '' &}&*..A BURM..E. 19.4708 (3.6 0.0591 0.056 0.056 rUBEs SAMPLE 34 4' 09/36/96 04*26 fckfi&i msuklS&tk !> . 8 . 0 . BATCH......HUMBER 1 6VG.ifi.pbi: x_Rm ` avG.^bs imjL suRH-g. -' . 41.4900 2.3 . 0.120 8.11a 0.122 LUBCJ-. SttjpPkfi. 368 09/26/96 84:32 C!=ftl.i.U 1.VOL/W1 8 m)L JB_ ? 5 .HimfilR 81 6y6.lfi.pb>. *RPO 6y.G...ab&. 61.4480 '0.6 0.134 BUM 1 BURH....2. 0.163 0.165 ryjBEL Mmp l e 900 6 03/26/96 0 4 s 36 GLftM. IVQL/W1 0 fiVCiERfel. *J3P_ ayG_.M. 77.4900 8.2 8.237 EVOk ..Jit... B6XCH,.HUMBER 0t BUM..A. ; ...8 0.236 0.237 mk*. 7 8ffifcLL j :5 09/26/96 04 s 4 CilAGU IVDL/WT 8 FVUL 1>F BATCH NUMBER 81 11V A 6V.6 < 2Pb>. *BP aVG. abs BUM ...1 BUM...2 58.52U0 3.7 8 . 15.1 0. 147 B; 155 DUP050307883 ..H NAME s 9627002F04 f* !,a..YST : 859 LANCAG t'Fft LA BO F< A TOR IE8 INSTRUMEN! IBs 84724 OF ft A ELEMENT ; A(3 '! llBE a SAMPLE U;B & 09/26/96 04 s 45 Cl ACC ;r.w.L/u;f FVOL 1)F BftT.CH... NUMBER 0 01 AVG Cools) JSRPO AVG, ,, &bs,_ BURN 1 BURN 2 8.3600 604.6 0.001 . 0.806 -0.084 .'Bi; * j ir*Pl-E 8 08/26/06 04 s 49 Cl. ACC IVOL/WT 0 - *...... ..... *' ..........-- -m im. ~ - FVOL I>F BATCH NUMBER 0- 1 * AVG Cools) JtRPD 10.8200 0.2 cib& 0.032 BURN 1 BURN . 0.032 0-032 s .10 ' h 'mr LE :;C~r 09/26/^6 04 s S3 IJ3C.C IVQL/WT 0 AVG <j?i?bJ)_ 3C.8.P. WG abs 42-6008 0.6 0.128' /.RECOVERY - 106.5 FVO.L I)F BATCH NUMBER 0, i BURN JL Bj.JRM. _2 0-12? . 0-128 J&J&JL 11 beis i 08/26/86 04 s 5? .OlABC IVOL/UM' ; s iFVOL ...BF._. BATCH. NUMBER ftp6 < onb) XRPD ~0.6600 '4.8 S.V6_atas '1002 BURN 1 BURN .2. 0.002 0-002 .).BE*. 12 88/26/86 05*01 SAMPLE 21-85276 ^v52.\tw l!. ACC IVOL/WT FVOL ..ML... BATCH HUMBER ::**** 100 . 100 1 862681056001 AUG (ppb) XRPP AVG Aim BURN I. BURN 2 RR ftp x' -0.4400 32.S -0.001 -0.001 -0.002 ..US&tJL 13 08/26/86 05:05 'MIHLE Cl. ACC IVOL/MT 2585276 ^q^ya; *: *A 180 AVG < r>pb> /RPO AVG attft 21.2900 1.7 0.064 /RECOVERY ~ 106.4 FVOL 180 . DF BA*1TCH HUMBER 1 962687856801 BURN t 7(365 BURN n ".-063 118 i < DUP050307884 RUN MflKEt 9627008F04 PAGE:: 3 ANALYSTt 859 XUBE*. 14 09/26/96 05sl0 !M m imzwT 585877 ^ ^ Q n r. ):}:)!):): 100 mmMfilBai , -0.491 aim. 7 -0.008 I..AMCA:TfLM LABOftATORXES INSTRLH'IEMT IDs 04784 OFAft ELEMENTS AS FVOl, _.DF_ BRlTH._MIJKBER 100 :L 9&8691B5-001 S.UEJUL 3MSM.J1 'BE Eli ' 0.001 -0. 004 TiJB&a 15 09/86/96 05 si 4 ifiiEJLE t'LLBSI* im./WT 58587? XX\QJXV. O *A* 180 ama&feL SEES. Qte6-.b 18.7308 3.8 0.056 ^RECOVERY == 93.6' FV.O.L ...PE.... BATCI1..JMMMBEJR. 180 1 96869105600.1 ML.i 0.057 PURH..fj 8.055 TUBE.: 16 gflBEUS. * 8585276 _ ^ 09/86/96 05:19 CLAS& UfflLAJl <:* 108 % wBMki mm mL*m 0.5980 99.1 8.808 E.YQL BF._ BATCH..MUMBER 180 1 968691856001 m~ 0.003 BE SSL 0.000 TUBE s 1-7 09/86/96 05s,23 samk q l b ml imusd EMfik BATC>;L_MIJKBE_R A 8585876 k k k k k A* 100 100 1 968691056001 A aaoiaabi s e e d . m&Jik* 81.8700 a.9 0.064 iiiEiLJL 0. 060 IMM. 0. 068 XRECUOERY 106. 4 LUBEs. 18 09/86/96 05sH7 k GLfi& IV>Q.LHX. 2585281 ^ ^ v ,.. 100 OcxOsh AS X filiSiaafei. SEES. - 1.8100 a?. 5 -0.004 FVOL. DF... B ATjCH__N U M BE ft 100 1 968691056001 siiEiut. sum. -0.001 -0.-0H6 RJi m. XUBEs. 19 09/86/96 05:38 SAMPLE L!=.AW; IUOL./WT 8585881 NV&PAS pN!:r:,:);!:A 100 avsiaabi. SEES. AyjL.ja.b.s. 18.0400 4.9 0.054 %ftECOVERY 90.8 FVOL .P._.. BATCI-LMUMBEft 100 1 968691058001 0. 058 SMftJi. 0. 056 119 DUP050307885 RUN NAMEs 9627002F84 PAGE s 4 ANALYST: 659 TUBE: 20 SAMPLE 2365262 09/26/96 05:36 Cl. ABO TVP1../UJT 180 AVG.ifi.E.fe>. XRPD -0. 3503. 43T. 3 AVC a'o-d -0.00:1 I.. AN CASTE R I.. A 0 OR A T Q RIE B INSTRUMENT IDs 04724 GFAA El .rj'ir.NTAS FVOL ' OF BATCH NUMBER 100 1 962691036801 BURN t BURN r> RR RD 0.082 -0.003 TUBES 21 SAMPLE. 3 as 232 _ _ . 09/26/96 05 s 48 ` Cl ASS IVQL/MT s m!k A 3.00 FVOL 100 . DF BATCH NUMBER 1 962691.8561301" AVG < pob) 20.5100 SCRPP .1.3 AUG Ahs 0.061 ' BURN I. 0.061 ' BURN 8" 0.062 ^RECOVERY 102.6 TUBES 22 SAMPLE CCV 2 .09/26/96-05 s 4-V ClAGU IVOL/WT 0 FVOL 1 .0 DF BATCH NUMBER 1 AVG<ppb? XRPP AVG abs BURN 1. BURN Z 42.1600. 2.3 0.126 8.,iaT ~e7iia ^RECOVERY a 105.4 * TUBE: 23 SAMPLE CCB 2 09/26/96 85:46 Cl Aliti IVOL/WT .0 FVOL 0 i)F BATCH NUMBER 1 AVG (nob) 1.0680 XRPP 60.3 AVG &b& ' 0.003 BURN 1. BURN 2' 0.002 '-0.004 TUBE : 24 09/26/96 SAMPLE Cl A&C 2585263 Vcvqjx^ O -i: *: >: : i 35 s SC . IVOL/NT 100 Ay'G<_Ei:iJ:)_>. SRPD. AVG 1.738 146.~4 0. 005 FVOL 100 DF BATCH NUMBER 3. 962691056001 BURN L BURN 2 RR RD .-0.000 0. 018 TUBE t 25 k mpLe 2341526 ^ 09/26/96 05::S7 Cl. A Si: .TVOL/WT A J 00 AVG <pr<b> 21.4300 SCRAP 3.0 AVG__sbs 8.064 ^RECOVERY = 9ft. 4. FVOL 180 DF BATCH NUMBER 1 962691036881 BURN 1 0.063 BURN C '07065 120 DUP050307886 RIJN NAME: PAGE s ANALYSTS 96870081"04. V> 859 86 gaimi. 2SASSS4 m/86/96 06*01 yjafiii i w l /mi r.r.iix .100 *EEL WU*M. 108.6 0.004 l..AH0ASTEA LAB0ftATORXl:"S INSTRUMENT ID: 84784 Gr.AA ELEMFMf.: AS Eifflk JBE_' 0 5 _ ; er 100 1 968691056881 MLi BteLa BE Bfi. 0. 80S 0.001 TUBE s : Sk p l e 879/6/96 06 :05 fiia&i JJiOkiMI : 4BB MU JD._ BATCbLNUMBER 100 1 96869105601 SVG<tul!>l. 0.9800 *Stt OVgi_abj> 5.0 0.063 BUBO. . 0-065 0.660 ^RECOVERY '96.8 TUBE: 88 9/86/96 06:69 SAMPLE GLaSii im/MI 8585885 ,, _ . (WLAPj 160 AUG <ppfo> -/RPD 1.390 186.4 AUG a`o* 0.04 FJsffik JB_. Bfiim..MyMBER 100 1 968691056001 syaiUL k -j i 0.008. 0. 000 '; m. ...... ...... TUBE: 89 k p l e 8585885 09/86/96 06 si') GAJiSii miL/wr s;*A 100 \n AUGiaaki. SBE- &.& 18.5400 3-0 0.0,55 % RECOVERY *= 65.8 Mk JBf_ e.ftTC.H....'.NUMBER 1-00 1 968691056001 SHEILA 0.857 SUfifiLS 0.054 TUlSgi SAMPLE PBU 30 09/86/96 06:16 QIJVOS IVifiLZUT ZZ2ZZZ *:*:* 100 W.61P.PM. WP. Ay.G_ab.i 0.1400 478.0 '0.000 ML ._D_ BAICH..,,WUMBER 100 1 96869.1056008 ; ; mj l oin<ji,.n m. m 0.608 -0.001 IM.SE*. 31 SAMPLE. PBW 09/86/96 06:88 LVUL/UX s A .100 f:.y.OL ...DF . BA TOH._ M U M B ER. 100 1 968691056008 &UG..(.&al?>.. XRPft aVS-afe*. 18.6400 6.4 0.056 SUBrLA 0.053 B.DRN ...8 0.058 ^RECOVERY = 93.8 121 DUP050307887 RUM NAMES 9627002F04 PAGE! 6 ANALYST: 859 LANCASTER LABORATORIES INSTRUMENT IDs 04724 OFAA ELEMENTAS TUBE: 32 09/26/96 06s26 SAMPLE C:.l kUQL/WT UCSW 277777 #**# 1 FVOL ...J?F_ 6IUJ*UJ4BE& ` .1 1 962691056002 AUG < ppb) RPP AUG aii- BURN t BURN f> RB RP 37.3200" ~4.-4' eTiia . 0.10a 0.1I5 ...... TUBE! SAMPLE LCSW 33 09/26/96 06; 30 CI_Aj3. jgQL/klT zzzzzz K-r.A 1 AVG <Pi3b> StBPD- AUG abs 57.1080 1.8 0.171 ^RECOVERY * 98.9 FVOL PE 2A.T CH. NUMBER 1 1 962691056002 BURN 1. 0. 169 BURN 2 0. 173 TUBE! 34 SAMPLE CCU 3 09/26/96 06a 34, Cl fir; J VOL/WT 0 FVOL 8 . PF BATCH NUMBER 1 AUG <ppfa> 5CRPD AUG abs BURH i " 41.6500 "5.U 0.125 0.125 BURN S " 0.~125 ^RECOVERY * 104.1 I.ye.Ci.' 33 k ; CCE< 3 ' 09/26/96 06a.>8 Cl ACS': JVOL/WT 0 AUG <DDb> SSRPO AUG afo* 0.9900. 57.6 0.003 FVOL PF BATCH NUMBER 01 BURN 1 BURN 2 0.004 0.002 TUBE! 36 SfUIPLE 2565290 09/26/96 06a 42 CLASS: TUOL/WX IU: 100 FVOL ,,J>F._ BAJC.HJiUMB-|< 100" 1 962691056082 .V/ ,S\ AUG < ppb) *RPD AUG ab-. -1.1100- 35.6 -0.003 BURH I. OIJRMJl RE RD -0.0*04 -5.003 ___ " TUBE.!. 37 sftnw^E 5535290 09/26/96- 06s 46 CLASS TVOL'/btT U* A* lie FVOL' DF BATCH HUMBER 108 1 962691056002 AUG Cppb> *RPP AUG aba 18.2300 4.7 *57 05*5* BURN 1 "5`. 056 BURN* 3 ""075s3 % RECQUERY * 91.2 DUP050307888 LANCASTER LAUimATDR-f ES BKAPMITE FURNACE ATOMIC ABSORPTION t>ATA REVIEWED BY UH 1 A VERIFIED BY; UfiTA mr 1'IAl'iFf RUN HA ME: 96S6903F03 ANALYST* Oft INSTRUMENT NOs 03S1E o k o cnrcRi ; ELEMENTS PB Concent-fat ion i s> used to evulua t:> i. f ,am;)!.o <:. a 1 :i. I.) r a t; i o n r a n cj e. i,u 11: : k v:; w .i t h i r. o .V DUP050307889 RUN NfiHL PAGE ; fiNftLY!>Ti 96269W3P 83 TUBES SAMPLE St) * 09/25/96 Cl ASS 16 s 25 J VGL/WT 0 AV6<DPb) *RM> . AVG aba 0.e&&. 8.0 0.884 I..MN0A: ST Eft l.. POOR AT DR 1 IT INSTRUMENT IB; 036If ORArt ELEMENT; PB FOOL OF BATCH NUMBER ~iit r BURN 1 0.-08S BURN 2 0.004' if USE a SAMPLE S3 S: 89/ 25/96 1630 Cl. AGS IVOL/WT 0 AVG <oir/b> 3.000 yT-RPP 17.4 AVG abs 0.023 FVOL PF BATCH NUMBER -.0 4 BURN 1 BURN 2 "i-iiai 0.025 TUBE; SAMPLE .89 1 09/25/96 16; 35 Cl ASS :r v o l /w t 0 AVGCnob) 9.0000 5CRPD 0. 1 AVG atas 0.053 FVOL PF BATCH NUMBER 01 BURN 1 0.0S3 BURN a 0.S53 TUBE; SAMPLE S:L5 09/25/96 Cl ACC 16;40 IVOL/WT 0 AVG <DDb> 15.0000 JiRPP & AVG ab& . 0.089 FVOL 1>F BATCH NUMBER 01 BURN 1 0.085 BURN 2 8.093 TUBE; SAMPLE S 30 1 09/25/96 J. fc> 2 & Cl. ACC IVOL/WT 0 AVG < d id b) 38.0800 %RP 2.3 AVG abr= ' 8.175 FVOL I)F BATCH NUMBER 0 1. BURN 1 0.172 BURN 2 "0.177*. TUBE ; SAMPLE S60 , 09/25/96 16 s 5 Cl. ARC !l VOL/WT '0 AVG <DPb) 68.0000 XRPB 2. 3 AVG aba 0. 380 FVOL 'PF BATCH NUMBER 81 BURN l BURN 2 0.295 "0.305 TUBE; SAMPLE :i: L V ' 09/'25/96 1 & s 5 Cl ACS IVOL/WT 0 AVG < nob) 21.6900 *RPO ' AVG aba 2- 0 0.128 ftRECOVERY 106. 4 FVOL.......1>F ... BATCH...NUMBER 0T BURN 1 0.128 BURN 2 "0.129 l-nub: nl-ivlL YS I : A 66 TUBE: SAMPLE ICB . 6 0U/85/96 lb:59 Ci ASH JVOL/.WT. 0 A'v'G ( ppb) 0.2500 S.E.PJS!. 93*5 AVG nb& 8.082 IH'd-'l RUMEN (, IDs WwitUi OF AA LLEHENTi PB FVOL .UK BATCH NUMBER 0i BURN 1_ BURN S 0,003 0.001 TUBE; i SAMPLE CkA 9 09/a 5/96 1?S0A. OlACH JVOt/UT *0 FVOL DP BATCH HUMBER. 01 AVG <ppb) r-ftl-'X) AVG a bib "3.1200 A. 7 0.023- BURN 1 0.823 BURN a 0. 24 CUBE s 10 SAMPLE /. /."jL".jL 21 09/25/96 17s 03 Cl. A lit; JVDL/WT XX-X - 0 FVOL 0 in- BATCH NUMBER 1 AVG < ppb? as. &40B gy^PD, AVG aba ""iTe "'0.139 BURN 1 BURN fi ""0.144 0.133 TUBE g. SAMPLE CUV 1 11 09/23/96 f:|. ALU 17*13 TVOL/UIT FVOL 1)1- 00.1 BATCH NUMBER AVG (ppb) ""87.8600 lRI-'0 " 1.3 AVG abs 0.159 BURN t 0.153 BURN 2 0.161 ^RECOVERY- * 109.0 TUBli:;SAMPLE CUB 1 12 89/25/96 17s 13 Cl1. ACC IVOL/WT 0 AVG<ppb) 0.S300 :/.Rl-i) 99.9 AVG -aba 0.002 FVOL 0 I>F BATCH NUMBER 1 BURN 1 8. 085 BURN g --0 . 002. TUBES 13 SAMPLE. l-'BW 09/25/96 17sCS Cl.. ACC 1WL/WT. s: xxx 100 FVOL PF BATCH NUMBER 100 1 96269155600? Av6 < ppb) ---0.0600 *RPi> AVG alls 99.9 -0.001 BURN I. -0.002 BURN A. 0.001 RR RP ____ __ DUP050307891 r;UN k h i... j ooccsosrec 'k :> ANALYST68 LftNCftGTLR LABORA! uRI Eb INSTRUMENT IDs 63612 0!" AA CL'F.MEN f i PD lUMLs. SAMPLE PliW 14 09/25/96 17 s 27 Cl ASS. TVOL/UIT K:*k V:A 1 00 AVO < nob) ARP I) AUG aba ""Ta.&isji' i.& 0.109 FVOL PF BATCH HUMBER 106 1 962691036001 BURN l 0.1 ii BURN IT 0.10a ^RECOVERY - M. 6 TUBES IS . SAMPLE ; llcpT VJCSV.0 09/25/96 l7t."$f Cl. ACS ' :r VOL/WT **** 1 FVOL ,,J)F BATCH NUMBER 1 I 962691056881' AVG<ppb> XRPP . ftVC :ab>>- 20.1700 3.-3 0.119 BURN I. 8. life BURN 2 IT IT Rji> 0.122______ TUBEs 16 SAMPLE LCSU LCSbOA 09/25/96 17*36 CLASS JVOL/WT :t FVOL PF BATCH NUMBER i i 962691856801 AVG<p.pb) ` #RPB AUG aba 36.4400 "0.1 .-8.207 BURN 1. 8.207 BURN 2 0.207 SC RECOVERY = ai.4 TUBE s .17 SAMPLE 2585279 -09/25/96 Cl. ASS 17 j 4 1. ' T VOL/NT 100 AVGtnnbl *RPP AVG ab* 1.5180 20.2 0.01.i FVOL 1>F BATCH NUMBER ' 108 . 1 962691056081 BURN I. BURN 2 RR Rj) 0.013 0.018* I Ul:< 5 18 k mp l e 09/23/96 17s 46 a Alls IVOL/Wi 2335279 fYvsuf\s^> Ar. 108 ftVG (tDb> j>-RPD 12.4100 4.4 AVG abn 0.073 ^RECOVERY 5J>. FVOL DF' BATCH NUMBER 100 i 962691856001 BURN t 0.876 BURN f> 0.871 TUBES 19 SBMALE 89/25/96 Cl. ASS n:w: .1.7 k 3fi ;i.vyL/NT 100 AVG (6Pb!. 0~. 1400 JSRP.1) 19*1 AVG__ LlJ.Ji.T t-aT 001 FVOL JDF__ BATCH NUMBER 100 i 962691056001 BURN I. BURN..2 RR RD 0.001 0.001 DUP050307892 RUN NAME m 96L'6905f 0,s I 'Hl'l- s ANAl YSTs fed t ; s . ea 585279 09/85/96 17s 55 &im ' lidfikiWI }> ): *A* OPi 100 m&Ssix&L &BES. eiULjtiai la.6600 1-0 a.066 XREC0UfcJfiV ' 53. 3- l.. rtNC fl:T C ft LA DO ft A T 0ft IE S INSTRUMENT IDs 03812 orft k e l f me m r p d Em, J8F_ 1'EICTL.NUdBEft 100 1 962691056001 BURN I. 0.063 BURN r; 0.063 TUBEs 21 SAHPL'E. 2585279 09/25/96 18*00 umi IVOL/WT 100 AVG < 0pb> 14. 3050 y-ftPD 0-2 ftVO AiiH '0-085 FV0L 100 BATCH NUMBER 1.962691056081 msu, s u mj i ; . m. 0.885 0.085 TUBE*- 22 ISSlS. zzzzzz 1 89/25/96 18*05 &imi iv o l /u i 0 POOL 0 1>F BATCH HUMBER 1 AVG 23.1600 ffRPO 2.5 AOG.,,bs 0. 136 BURN l 0.138 BURN 2 0. 134 JiRECOVERY - HOT APPLICABLE A IUMj l k le 23 09/25/96* 18 s 89 mACB IVpL/WT FVGL DF BATCH NUMBER CCO 2 0 01 . AV6 (.pj?_b). 26.31(30 5CRP:0 2.2 AVG..M5.g. BURN JL 0. 154 0. 151 BURN 2 8. 156 ^RECOVERY a*105 .2 24 saaeuK CCB 2 09/25/96 18".]/! eLQsu. iMOL../m . 0 FOOL ...??.._ BATCH NUMBER 01 fiyj.taab>. SEES. five...b -0.0900 99.9 -0.001 sy&nj, suEw_g. 0.001 -0.(302 TUBE * 25 .09/25/96 16*18 A s6PiUi. GLBi&L 1V.QL/MT EBfik J0E_ BATCIi..JiyilBEft. 2585276 :*:*:** ^0,'KVo 10 100 t 962691856001 y. Ay.&.i&akL *RP AUG_*i>* BJJRHJl. BOftfcLB SB. pj> 2.5700 5.1 v 0.019 0.020 0.019 ^ __ 1 Of t* < DUP050307893 RUN NAME: 962690SF03 PAGE s 5 ANALYST: 66 LANCASTER LABOf :h fOR .i t:: INSTRUMENT ID: 03812 OFAA ELEMENT: PB TUBES. 26 09/25/96 IBs S3 SAMPLE C:l AGG XVOt/WT 2S6527& '' = *** CtN^L^V^ ^ 100 AUG <ppb> ' i4RP]t) AUG abs. 15.4&0t3 10.0 0.090 FVQL . DF... BATCH. NUMBER 100 1 ' 96269li56081 BURN 1 0.085 BURN n 0.096 JS.RECOU.ERY = 64.4 TUBJEs S7 SAMPLE 2565277 . 09/25/96 10 s 27 01 AGG J VPL/MT ): >! vO 100 AVG ippb) JSRPP. AUG ab-a ""7574500" "fcTa "0.003 FUOL 100 DF ' BATCH HUMBER 1 96a&910S600i BURN 1. BURN H RR RD ~0.003 . "0.004 _7 TUBEs 26 SAMPLE 2*ase77 09/25/96 16:132 Cl. AGG. IVPL/MT v O ** 180 AUG < pgb) JSRPD ' AUG abs, 10.9700 12. 5 0."iis ^RECOVERY 54. 8 FUOL . DF BATCH NUMBER 10i 1 962691056001 BURN l 0.071 BURN P. .0.059 TUBE s 29 SAMPLE 2565276 . 09/25/96 16:37 ' Cl. AGG JV0L7UT *** : lie- -Q AUG <ppb) -JSRPJD AUG abs -0.4100 36.3 . -0.003 FUOL ....BF .. BATCH NUMBER 100 i 96S691056001 BURN. I. BURN 7 RR RD -0.004 -0.002 TU.BE.S. 30 09/25/96 16 s .40. SAMPLE ' Cl. AGG IVDL/UT 2505276 k *4JA'm mC-fts-o lx 100 FUOL ...I>F.._ BATCH NUMBER 100 1 962691056001 RUG <ppfa? 13". 4100 JSRPD .0.0 AVG ab& 0.079 BURN 1 0.064 BURN 2 0.075 A JSRECOUERY 67.0 TUBE: 31 09/25/96 16:46 SAMPLE . ClAGG IVOL/MT FVQL .....DF__ BATCH HUMBER A 2565261 , ,, (*\ i:k ***k * 5 ' " :i 80 108 i" 962691056001 V AVG <ppb) JtRPD AUG ab-F BURN I. BURN 2 RR RD 1 0.6400 71.6 ~0.005 -0.002 - 0.007 DUP050307894 i' UN MAl'IL l PAGE. a ANALYST: C 60 T UDEj. 3i.f 89/85/96 IB: 5.1. >AMPLE Cl ACC TVOL/tJT atiss'a&a {Y\eiW^> & :u k k ii ftVG < onb) mm Ay.G...abs 6.5285 1.9 0.048 JCRECOVERY 38. & l.ftNCA: 5 r ER LABORAT OR IE S INSTRUMENT ID: 03&1S OrAA ELEMENT; PS FVOL I)F BATCH NUMBER iee' ' 1 9&S&ii85&8i BURN. 1, ""0.043 TURN a 50.84 TUBE: 33 qk l e 09/r23/96 16:53 :rct fth p v o l Vu t asasaaa :* r'rsSJSVbS . 100 1f.1. 9 \ AvG (nob) -0.. 4700 9CRPD 1.7 AUG ctliw -0.004 FVOL 100 DF BATCH HUMBER .1 9&S69i0S&001 BURN 1. -0.004 BUiM E "'0.803 RR RD -- ----- TUBE: 34 SAMPLE cccsaac 89/25/96 19:00 ' Ci. k5 ; 3 VOL/WT ^ A* 100 AUG <nob) 12.6688 JSRPD ' AVG abs 4.5 0. 076 ^RECOVERY = 64 .'4 FVOL 188 DF BATCH NUMBER 1 962691056081 BURN L 0.879 BURN E 8.874 TUBE 5 SAMPLE CL V 3 35 09/25/96 Cl. ACC 19a05 IVOL/WT 8 flvG(ppb) 26.6600 ?iRPD 0. & AUG 8. 157 ' ^RECOVERY = 107 - 5 FVOL . DF BATCH NUMBER .1 BURN l 8. 1.5& BURN a 8.15a TUBE: SAMPLE CUB 3 35 09/35/96. 19:89 Cl ACC jvoL/wr 8 AUG < ppb) -0.4400 SRP.fi. 65.5 AVG ibf=' -0.003 FVOL 8 BF, BATCH NUMBER '1 BURN 1 "0.002 BURN a -0.005 . TUBE t 37 '..AMPLE aaasaas 09/85/96 CL ACC 19 a 14 IVQL/UT 180 11 A v' G \ p p h) % 1A1-* 0 AVG...ab-r. 0.5400 23.8 -0.004 FVOL IBB DF BATCH NUMBER 1 968691056001 BURN 1. BURN E RR RD se-0.003 -8.005 --- ---- *a rf/- DUP050307895 LANCASTER LABORATOR1ES GRAPHITE FURNACE ATONIC ABSORPTION DATA REVIEWED BY DATA Flu f NAl'iI"j. `PBPCSIS RUN NAMEt S6270&iF83 ANALYST! ASS- INSTRUMENT NOs 0301B Mi<G CORft i BZ - ELEMENT s PB Oow-eMratiov, u used to evaluate, i f toration range. to v.-uiLU- within 130 DUP050307896 i-. uw N A h i: s 9637001F03 PAGE s .1 ANALYST: 839 t ; s SAMPLE 30 ' I. > 09/25/96 23:34 CLASS Ivm/UT 6 AUG(ppb) 0.00W0 aSRPD 0,0 AUG aba 0.003 i.5 k n.-:r< k; k u r .u ::s INSTRUMENT IDs 0 3 0 t.: OF ftA ELEMENT I'B FUOL '0 I)F BATCH NUMBER 1 BURN 1 0.005 BURN 2 0.002 TUBE s SAMPLE : '09/fi$/96 23 #30 GiftWL lyOL/WT .................... FUDL ,,.BF,, BATCH NUMBER Augjjjjafei. 3-0800 W&EJB. 13.2 autii...afafe. 0.027' BURN 1 0.024 BURN 2 . 0.829 TUBES SAMPLE S9 . 09/ 25/9& 23s 41 Cl A.SB iyOL/WT 0 AUG< Pob> 9.0000 #Rpj|> AUG aba 4.7 0.W&6 FV0L 0 BATCH HUMBER 1 BURN 1 00&9 BURN 2 0.(364 , TUBES. SAMPLE Si 5 (39/ 25/96 23s40 CLASS IUOL/.WT 0 8.'/ii_^ELEj3.L *RPD " liTue' 4.4 AUG aba 0.105 FUOL 0 BF BATCH N.UMBER. 1 BURN 1 '8.106 BURN 2 ' 0.181- TUBES SAMPLE 330 i 09/25/96' 23:53 k :; j v o L/w t 0 AUG.<pj5 >.)_. 30."00 J5Rft 0.7 AUG aba 0.2U0 FUOL 0 BF BATCH NUMBER 1 BURN 1 ' 201 BURN. 2 * 0.199 | UBEs SAMPLE 360 , 09 / 25/96 23s5/3 k ;s ; IUOL/UIT 0 60.0000 *RPP 0.5 ftUG.._aba. 0.332 PUPL,......1>F._ BATCH ..NUMBER. 0 it BURN _1 0.331 BURN 2 0.334 TUBE; SAMPLE ICU W9/ 26/96 00:03 C'-t ASS: , IU0L_/WI i AUS <ppb> 1 s"."9000 Y.RPO 3.7 AUG aba 0.137 ^RECOVERY == 99.5 FUOL DF BJiTCH HUMBER 0' 1 BURN 1 0.133 BURN 2 8.140 131 DU P050307897 Ik 'Ui-I NAME ,, i 'A l-.tr. 5 ANALYST s 3 708 3.1-1)3 P 59 TUBE! SttffeLf. ICB a 09/B6/96 80107 -Glftltfi `IVDL/WT 8 0vB.y3p.bL . 5500 #&e & u* aye^M. 0.805 I .AN Oft: i rr.ft LftBAftftTORlES INSTRUMENT IDs 03ftIS nrAA ELEMENT : PB e u q l _iihT. MmLmms. i BURN .1. 07085 SMOiL-i. 0.005 meg.*.. BANPkE CRA 09/2&/TO ;00!lf> "Cl ASK -I-WL/tJT 0 m JB_. B(t .5 _ ; 0i ffiiSSLtttttftL- &mm. SiML-afes. 3.a98 a.a 8,889 6,UR.N..,,1. s j r h __2 8.02s 0.030 lUSIx 10 SAMPLE 7.222. ZZ 09/86/96 00s17 &&& imzai K * {} ftVfl<ppb> jKRPD a 1.9888 0.4- AVCS abs , 0.150 EJfflk _d f _ 01 BU.RN,,J, BURNJL 8.1S0 0.149 IUBi SAMPLE CCU 1 11 89/86/96 88sai QkfiHi IVOL/0T 0 EVfik __ BSISiJiiaifilB. B1 QVGCjiab). SSS.- AVG-^M. 6.1108 0,a 8.176 iyfiti-3, : WS8LM. 0.176 0.176 ^RECOVERY 1&4.4 TUBES. QdLE CCB 1 IS 09/26/96 80s 06 GlflS& TVOL/MT 0 ftVGlfefiJbJL mea am.*** 0.7900 59.6 0.007 EMQL 0 BATCH NUMBER 1 BURN 1 0.018 BURN .a 0.084 TUBE 8 .1.3 SAMPLE 89/26/96 0s.*Jt Cl- AUi: TvOL/WI WLSVAjS ** 180 AV B..< s j ?Jj .L 2?BJEUS. k VO 61)-. 0.6600 0.0 0.006 EAffik . _?)r-- ,BAiCH,__NIJMBER 188- 5 96869105600:1. ayfitf-i a!,sN_a m m 8.006 0.006 132 DUP050307898 RUN NAMEV62 /001FW.S PAGE 5 TiNALYS I' i 359 TUBEj 14 SftilE S5a5EB.I 09/26/96 00:35 CLAgO JVPL/WT s & * 10 AVG (pi:<b) is.9600 y-PPD ftVC abs a. i e.ua * RECOVERY ~ 64. 9 Lh NCA: ; fs'-.R LABORk I uK J. EE .INSTRUMENT ID: 03612 orrtft !T.I..GHENT PB FVOL ...DF... BATCH__MUf3BE.a 100 s 96269ies68i BURN I. 0.116 BURN G ' 0.119 TUBEi!.. 15 s MKj e 09/26/96 00 a40 ct Acs iv o l /mt asassB? 'pCs^.'Sv'2> vi XX 100 AVG <ppb) 0.7400 7tRPfl 5.3 AVG ab-i 0.007 FVQL DF BATCH NUMBER 100 " 1 962691056001 BURN I. BURN 2 RR gjO 0.006 0.00? TUBE;. 16 SAMPLE 2565263' , 09/26/96 00s-VS 'Cl I.V.OL/WX #*:* A* :i 00 ^ vv AVG<ppto> .1.3.1000 XRPP 0.2 AVG a.bs 8.093 FVCIL .. P.F., BATCH NUMBER 10 1 962691056001 BURN 1, 0.093 BURN 2 ' 0.093 ^RECOVERY == 65.5 TUBE: 17 09/26/96 00s49 SAMPLE &AS& IVOL/MT 2565664 ;>: revsL^.'CiO ' 100, AVG <p,pb> 0.5306 sr pd 33. 6 AVO ail- 0.001: FVQL ...J>e._ BATCH NUMBER 180 1 962691056001 BURN I. 0.007 BURN 2 0.003 RR. RD TUBEs, SAMPLE 2565264 09/26/96 -00s3-i CLASS: TVOL/WT k A C\ 100 AvG< ppfa> XRPP AVG aba 14.0000 3.1 0.099 ^RECOVERY - 70.0 FVOL _DF_ BATCH HUMBER 180 1 962691056001 BURN 1 0.096 BURN 2 0. nil TUBEs IS SAMPLE V15265 09/26/96 00*39 ci_ k i v o l /w t :-j : .100 AVG tppb> 0.5500 *RPO A /[-... 0. 003 FVOL . PF ... B AI'CH ..NUMBER 100 i 962691036081 BURN l. BURN A RR RD 0.083 0. 0.8/ 13 DUP050307899 RUN Nh I'II:.: ; PAGE s ANALYST: 902780.1F83 A 659 aw k p l e . e9/a&./96 01:04 Ot. AOS im/uj. asasaasi ^ ,, , !I !i V. )!&)( wmv-eA . 100 k 5 imLL ia. mm. rn&L &. 0v...a.fea 0.133 e * 5 o v e r y 96. 4 LANCAOTHR LABHRATOR1S INSTRUMENT Il>: 03018 OF AA CLEMENT : PS FVOL 100 I>F BATCH NUMBER I 962691856001 BURN I.. 8.139 OMAN 2 0. .1.26 TUBE i 21 89/26/96 SAMPLE CLASH NSW Z2Z22Z ? WG<fipb>. *RPft 'c /) 0.7200 22.4 el i m IVPL/WT 100 AVG Ab-: 0.006 gm. 100 mmumms. 1 962691056002 mmLA 0.007 OUR*! .2 0. 805 PR M .................. /USE: (3k ; 22 09/26/96 01:13 l.:L Alit: TVOL/WT ->: >: i: A )t 300 ZZZZZZ aytua&b). 2SBPSL AVG abss 20.6488 0.4 0. 141 / RECOVERY = 103 . 2 FVOL 100 BF BATCH HUMBER 1 962691056082 BURN JL 0.141 aim n. 0.142 rUBE : UA0PLE ccv a 23 09/26/96 01:17 ks amzHi 0 AVG !mib) 26.2900 %R\-'T> 0.9 a.y.G *. .8.177 ^RECOVERY * 105 . 2 Em ..J.)F BATCH NUMBER 01 MsH :L 8. 176 BURN- 2 . 0.176 XU BE: 24 sAimji cCB 2 09/26/96, 01:22 yuptiii imzai 0 ayG<aafe.> 0.760 * 39.9 Ay.G_ab6. 0.0(37 m J>J: BATCH NUMBER 81 atfLU, 0. (389 B.M.AN 2 (3. 80S iy.BE: 25 SfiJ3B-L I...C9W 09/26/96 01:27 (XL0.HU IWL/WI ;; >: *: j ; -j ; -j : -j : 1 U/-\ J QVO iaiibX. SSEfi. 21.96)00 3.4 0.. 150 FVOL _DFI... BATCH NUMBER 1 1 968691056002 8. 144 Bim_.ii r<& m 8.156 -1-37T DUP050307900 LANCASTER LABORATORIES ORAPHITE- FURNACE ATOMIC ABSORPTION WIT") REVIEWED BY; iATA VERIFIED-. BY i, ft DATA Fit F. NAFIEfc' PB87&03 " RUN 'NAME* '4687&S8FS3 ANALYST ; *09 INSTRUMENT NO-s 03612 OKG CORK ; to/ ELEMENTs PB 135 Concentration is used 'bo evaluate- i. f sarrtji I. o vssul t-s are w:i.'thin calibration-range. / DUP050307901 RUM NAME r. 9627008F83 PAGE s .1 ANALYSTS as 9 TUBES SAMPLE 30 1 - ' *9/86/96 04 s 54 CLASH J V0L/WT 0 AUG <ob) !*RPO AVG abfc 0.8808 0.8 0.801 w M ..... ....... ... TUBEs SAMPLE S3 : 8 ..... 09/26/96 84 s 56 Ci ASH IVOL/WT 0 AUG(cob) XRPO AVG 6B 3.0088 8.8 8.820 LANCASTER I..ABORI-)i'uk/t INSTRUMENT IBs 03iv.i.8 g f kk 'e l e me n t : p ; F yo i,.....D F _ .6 ftLC.H. h u m* h k e" i BURN 1 BURN 8.001 8.888 PUOL ._DF_ BATCH HUMBER ft 1 BURN.. 1 BURN - 2 020- 0.808 TUBES SAMPLE S9 3 89/26/96 04 5 59 CL ACC JVOL/UIT 0 AVG<ppb> /Rf?.I> AV(j 9.8008 8.8 0.860 FOOL PF BATCH NUMBER. 04 BURN 1 BURN 2 ei.a&e 8.808 TUBEs. SAMPLE SIS 4 09/86/96 053 08 CL ASS '.i'm/wj: 8 AUG (cob) 5SRPP WG cibs IS.8888 0.8 0.182 FVOt 1>F BATCH NUMBER &1 BURN' 1 BURN ...8 8., 102 0.808 TUBE s SAMPLE S30 S 09/86/96 eSaG'i CL ASS 1VOL/UT 0 AVGtppb)' /RPP ft VO abs 30.0808 0.8 8.204 5 1FUOL PF BATCH NUMBER BURN.. 1 BURN 2 0.28/t 8.880 TUBEs SAMPLE S60 6 09/26/96 (dS s 87 CL ASH TVGL/WT. 8 AVG<pob> 5SRP0 'ftVO aba 60.0000 0.0 0.347 FVOL T)F BATCH NUMBER i' ~ 1 BURN 1 BURN 2 8.347 0.088 :b .j b ~. SAMPLE JCV 7 89/26/96 85 s 18 . Cl ACC: TVOL/WT 8 AVG (ccb) /RP0 . AVG abs 88.6908 0.0 8.148 /.RECOVERY = 403.4 FWIL- PF BATCH NUMBER 0 4- BURN 3. ". I*i8 BURN'2 136 DUP050307902 RUN NAME a '968708SF03 PACEs P ANALYST - 659 TUBE s SAMPLE ICB 6 09/86/96 85a IS Cl. ASH IVOL/WT 0 AUG < piab) KCftPD AUG afa'g 0, 400 0.0 8.883 LANCASTER LABORATORIES INSTRUMENT IDs 036i8 OF AH ELEMENT.; PB FVOL OF, BATCH NUMBER ' r BURN 1 BURN 8 0-OO3 0-000 TUBES Sk Fip Ce CKA C H 9 09/86/96 05sIS 5 ks :tv o l /w t f oul of ;k 5 n u m; r 1 AVG < nob) 3-6300 XRPD AUG abr= BURN 3. BURN 0^8 0.085 . 0.085 8.000 TUBEs 10 SAMPLE CCu"l ' 09/86/96 85s17 CLASH IVOL/WT 0 FOOL 8 OF BATCH NUMBER 1 ' AUG < ppb> %RPD AUG abs . BURN 1 " asT'isQ . " 018 8.176 0.1 ?& BURN 8 .'0.000 ^RECOVERY = 183.6 TUBE! SAMPLE CCB 1 .11 09/86/96 5 a 8 Cl ASS 1 VOL/WT 8' FUDL. OF BATCH ' NUMBER 01 AUG <t>pb>' yiRPO AUG aba BURN 1 BURN 8 ^ " "i'l 8080 ~8.0 0^801 0.081 8.080 TUBEs 18 09/86/96 0Ss28 , SAMPLE Cl. ACC 3 UQL/WT 8565876 mJs^ ^ ^ **8* 188 F UOL 188. OF BATCH NUMBER . 1 968691056001 ` A COHC< p p b) ' . 8.6988 . BURN 1 8,.019 A TUBEs 13 09/26/96 05s85' ^ SAMPLE Cl. ACC I VOL/WT . F;V.OL DF BATCH NUMBER 8565876 '><v3v\l"!5 ^ n- >: >: 1 n 180 180 1 968691056001 A ' ^ -y CQHC<ppb> 6.9300 BURN -1 0.046 TUBEs 14 89/86/96 05s27 QAMPL.E ' Cl. ACC I UQL/WT '8565276 &*****'* 108 <wt-ie=fwi` wV*fty CONC < apb) BURN 1 18. 6408 0". 078 FUOL OF BATCH NUMBER 180 i 968691056081 j ot 1*5 i DUP050307903 RUN- NAMES 9G27802F03 PAGEs 3 ANALYSTS &59 T^BJi.s IS SAMPLE . - 09/ES/9G 8S * 38 CLASS XVPL/UT 250S276 <y s J2j C\\*=' 3*,t**'*'*-**1** . 188 vy CQHC <ppb) BURN 1 - 13.0980. ' -'0.094 ' LANCASTER LABORATGRI ES ! INSTRUMENT ID: 03012 "GFAA -ELEMENT! I-'B FVOL 180 DP BATCH NUMBER 1 96E&9185&0B1 X INT -* CORN COEF -= 4 ..80390 RR 0.99094 SJLGPE r - .08582 Y INT . * 8.02018 Rfi. ! TUBES 16 SAMPLE , CCU E. - . , 89/2G/96 05s35 ' v CLASS IVOL/WT ";L 8" ' FVOL B PF -BATCH NUMBER 1 AUG(DDb) VjKRPD ` AVS &bs .aS,G900'; 0.8 . 0 k 174 BURN 1 , BURN E '0.1.74 0.000 JSRECOVERY-10E.& . f TUBE: 17 SAMPLE ecu a - 09/E&/9G 85&3S ' . V^' CLASS lUOL/UT ' ' FUOL .;, a'. 0 DP BATCH NUMBER i AUG<ppb> . ffRPD AUG aba BURN 1 BURN S' -0.1000 '; 0.8 -.eel. -a.! .80s DATA REVIEWED BYs DATA UERIFIED BY ifZtyrM 138 DUP050307904 LANUAST ER LftftOKATOR X ES GRAPHITE. FURNACE ATOMIC ABSORPTION DATA REVIEWED StYs DATA VERIFIED BY 6 9^ DATA Flit NAMf i; SFr7B0S.. RAT RUN NAMES ^&S7;epJ.1.1"5 ANALYST; DAS INSTRUMENT M0s 04785 DKG CORK.! BZ ' El EMEMTs SE Concentr-ation it> us><wJ to evaluatis i. i' calibration ranne. 139 I.t-;> r-: within DUP0503 07905 r u n wanes 962/88if'5 PAGES i ANALYST s' <i9 ; . SaNPLE S i 09/26/96 &s37 BiM Tyotvwi fty6<ppM>. mE&. &VJLftk. -0.390 .119.4 8.001 l-.ANCAG (EH LABORA I'UR ILS INSTRUMENT IDs- 0472S nrf-iA e l e me n t s e E.y.Qk ..ML. BATCH HUMBER 1 BURN 1 BURN 2 -.ilia 8.881 TUBES SAMPLE S5 a : 09/26/96 08s4t L Cl. k 5 5 lUOi/UT 8 VQk JttE^. BMOBMBBa. 1 AUG < DDb> *RPD fty.6. asfeSL lUBfcLi BURN..S. 3.8700 '7.8' 0.IS 8.016 0.01S urns. SAMPLE SIS 89/H!6/9& 08 s 45 Cl., ACC im/ffil . Ry.GlfififeL &REB. AUG aba 13.3600 1.4 0.841 FVOL 0 BURH..1. BURN 2 0.041 0.041 I.UBJLL SAMPLE sss 4 09/26/96 06 a 49 Cl ACS' JVGL/WT 0 AVtSCimb) *BPk AVg__abi= 24.2400 8.4 ' 0.067 FVOL DF BATCH 81 BU&N...1 BURN a 0* @66 .067 k TUBE*. SAMPLE S4U 5 09/26/96 06 s S3 Cl ACC jVOL/WT 0 FVOL DF BATCH NUMBER 01 AVG<ppb:> *RPP AV *M. BUM i, BURN.il ,S!j.2800 0. 2 0. 102 . 0.182 0. 102 TUBES 6 2B.II!PL :;s 89/26/96 06a57 * ELMS* IVOL/NT 0 ay.G.<jmbi- mtn AyG ibi 50.9708 i. i 8.131 FVOk ...I1fifilCH . NUMBER 0l BUEN.J, ; a 0.132 0. 130 TUBE s SAMPLE :icv 7 89/26/96 09 s 01 Cl ACC IVDL/UT 0 Ay.<ijLaafeL SBPJBt AUJi^bg. i9.as00 a. a 8.053 ^RECOVERY 99. a FVOL DF BATCH NUMBER 0 1' BUM..JL 0. 049 BURN...a. 0. 0S6 140 DUP050307906 RUN NAMEs 9687061F05 PAGE S P ANAL YST t. 609 TUBEs idss k- PLC. 6 09/86/96 09 s 05 .... eCl. ACE:, IUOL/UT AUG <ppb) ftRPD AUG abs -~i.Sii .37. & '0.001 LANCASTER LABORATORIES INSTRUMENT ID: 04785 Ot'AA ELEMEN 1' a SE " ia iFOOL IIP BATCH NUMBER gjjgji I BURN.. .2. -0.001 . 000' TUBE: 9 SAMPLE ; CPA ' 09/26/96 09800 _5 k i9ik>:yx 0 AUG <oab> YRPP AUG abs A.0700 4.6 0.012. F. -U-OL~ ._..-.. BATCH NU MBE. R B"UaR. Nifis1 .BURN g 0 0.12 TUBE: 1-0 SAMPLE CCU 1 09/26/96 09s 13 ACS IUOL/WT 0 AUG(ppb) /.RPD AV6 abs 84.5500 8.3 0.065' ^RECOVERY =- 96. 2 FUOL OF BATCH NUMBER i :t BURN 1 0.06 4 BURN a 0.066 ; e:: 11 SAMPLE CUB 1 09/26/96 09s.1.7 Cl. ACC IUOL/MT "..... TM "i ~ AUG_<,iij2.bJ_ 2-J.TEjO AUG aba "~-"i."i200 leu ""-0.001 FOOL. OF BATCH NUMBER i. BURN....1 S.yj'XL_.l ' -0.001 0.002 TUBE: SAMPLE PBW 1 C- 09/26/96 09:21 Cl. ACC; TVOL/UT . ZZZZZZ ;:-j : :;>; 100 FUOL 100 OF BATCH NUMBER 1 962661056003. AUGtppbl XRPD AUG ab-A BURN i BURN 2 R,l;( RB "~r.irm 86.4 -0.iii -0.001 -.a TUBE: 13 09/26/96 09i25 SAMPLE Cl. AI.C TVOL./QT PBW 222222 sHn:i:A* 100 AUG < ppb) /.RPP AUG abs 10.1200 0.9 .026 FUOL OF BATCH NUMBER 100 1 96866 105600 1. BURN 1 0.086 BURN 2 5.027 Jt RECOVERY = 101.2 A A DUP050307907 RUN NAME::. 9627001FW5 PAUL s 3 ANALYST s 609 TUBES' 14 9/86/96 '09s 30 SAMPLE .OLBSli IMBLfltl ixsw ZZZZZZ xxr.xii-r.i: X flV6.<p.R.t>>- ms. a.7600 a.a 0.0a4 LANCA3TE R E ABORA"f UR..L E 6 'INSTRUMENT IBs 04725 OFAA ELEMENT: E FVOL JBE.. SftTtfifcUSUQSEB. 1 1 962661056001 t ffio -mmji ; & m. 0.024 0.025 ; .;. 15 09/26/96 09.Vs ifettiifck g l m&. iyoj=.^Mi I CSW mk A* 1 ZZZZZZ avsififtfeL ms, ay.e_.abs 19.6600 1-3 0.058 jCRECQUERY " 106.6. eiisk j e ._ 1 i 962661056001 ; u l 0.052 s.yf<N,,ji 0.053 CUBES. 16 09/26/96 09a.16 saM.ayi. asaaaes QkB'& imzwi ZZZZZZ 1t 00 fiysiRftfei mp. -avc ' **.. 16.9600 1.7 . 0., 045 BPk .JML. BAICH...NUMBER. 100 1 962661056001 B-Ur<N.-t BURN..*1 RR RB 0.045 ' 0.046 TUBES 17 ififiEUL 2563200 09/26/96 09a42 GLM& IMI *k A 100 ayeiEfiM. mm 25.5600 0.9 0.067 /.RE 0 QUERY = 66.2 FWL ...DF... BATC;H....M.yMBER 100 .1. 962661056001 IRRJUk 0.067 `URN r> 0.066 TUBES 16 09/26/96 09 a46 k ..'LE . 5 k"" , ivmvwx 2563206 2Z4.4-4.*- **. 3 08 ayciPfifeL mm. sm-jiM. 0.0600 0.002 f u o l .; #.. Ifflcyfflllia 100 1 962661056001 . SMRN..J, B.1IRM 2 BE Rj> 0.005 -0.001 TUBE: 19 09/26/96 09:58 3AMPLF- y,AEU 1WE/WJ1 2563806 2ZZ444 . .::A 100 ayG(p.pb). *RPJ>. ay.e....a.fa!L 7.8300 9.9 8.880 ^RECOVERY 72. 3 FWL .!".. BAICW .. NUMBER 100 1 968661056001 BUsH_.-X Bi>EW..2. 0.019 0.021 RUN NAME* 9627081F85 PAGE i ft ANAL VST i. <109 TUHEk 20 sasM. 2503207 ^"..d '9/56/96 9 : 55 r:i.as? TUPL/WT -k 108 Xf BUG <.Ei?b>. XRPB. aye "1.0400 1.6 -0.001 L AMOA: 5 TCEi LA B1 HRAT OR 1IV INSTRUMENT X 3> a 84785 OFAA ELEWltNTj SC FU.pL. 1>F BATCH NUMBER 188 1 962661056801 BURN...! -0.801 BURN., f*. RR. . RD -0.001 BJBEr,. 81 IMUL asasae? 09/56/96 09 s 59 i-imu im/wi ,yf A >; a 00 9VP<afcfeL **?? evp ft.bL 6.4700 a.5 0,023. ^RECOVERY * 64* 7 FVOL BF... B.AXfiH..WUQfiER. 180 1 968681856081 ; $%& _L 8. 824 auatt_ 0. 088 .ME* 2 SAWPLK. ecu s 09/86/96 10 a 83 Lfifc& t v o l /u x 8 AVglafib) %RPD AUG atas 83.7600 4.1 0.063 ^RECOVERY - 9S. ;1. EPk 8 ; '() 1 8.061 ifiTetLiiusMB. 1 BURN a 0/064 S3 *k,*; , ;. 55; a 09/S6/96 10: 87 lyQk/HT. 0 .. fwaiapfei. mm Ayfi..a.bs -1.1600 43.0 -0.00a FPftk -PF.... BATCH NUMBER 81 BURN 1 ; ./1.a "8.001 : 0.802 IJJBE.S. 84 89/86/96 10 <18 SAMPLE. C.LAJ5& B&U.WT asasaea ZZZZZZ i:5: * r' :l 80 X Aueiapb) %R AV6 'aba. 0.6600 146.6 0. 003 eypk d f .. BAmi.HUMBER 108 1 962661856001 B.URM..X. 88. R.A> 8. 801 0.885 A lUfflL*. as 09/26/96 18s 15 SAMPLE. GLA8& lyou/wi mu ..... m... BATCH.. NUMBER. asasaaa ZZ22 ^2 J v* ** *v ^ ^ :l 80 180 1 968681056081 AyBiBjJb) RRJ> WQ. %fesi ; '() J. BURN 8. A 9.9380 5.5 0. 08? 0.086 0.088 ^RECOVERY 99. 3 , '141o DUP050307909 RUN NAMEs 9687001FUS PAGE s ANALYST s - 609 TUBE; . 8 SAMPLE 8563889 09/86/96 10519 mp <*JV MjJ 5 *** 4*0&B feotisa, (us JL-. QL0Cii. U-s; v. -j : JVGL/WT . 100 AVG <ppb) StRPP- AVC dtas --0.930 83. 3 -0.001 LANCASTER- LABORATOR1ES INSTRUMENT IDs 04785 GFAA ELEMENT: SC FVOu' ..DF BATCH NUMBER ~108 I 968601056551 BURN 1 BURN 8 RR 'RD -0.001 -0.000" TUBES 87 SAMPLE 8563889 .09/86/96 108 0.1 -EU ftrfft IVOL/UT (.IK* A* 100 FVOL I)F BATCH NUMBER 100 1 968661056801 AVOtPtob) AVG aba BURN t ' 6.6700 - i.S 0.084 ' 0.084 BURN 8 0.085 /.RECOVERY * 00.7 TUBES 86 89/86/96 108.87 SAMPLE 8503809. zzzzzz Ct ACC JVOL/WT jfHI J;4>' 4i")t -K 100 FVOL DF BATCH NUMBER 108 1 962601056001 A AVG Cppbl /RPD AVG ~i.1100 4 0., 6 0.001 BURN 1. BURN 8 RR RD -0.@01 -.0.008 __ ___ TUBE s 8`9 09/86/96 18 s 31 SAMPLE Cl. ACC :r v o l /u t 8503889 r> )!)-. -k k -k 100 ZZZZZZ AVG(DDb) /RPf> AVG Aba 9.1100 i. 4 5.555 ' * * * *.......* *' ........... ......... . *?* "* *' * ** FVOL ' DF BATCH NUMBER 100 1 96866.1056001 BURN 1 0.085 BURN 8___________ 0.085 S'. RECOVERY = 91.1 TUBE s 30 09/86/96 10; 35 SAMPLE Cl ACC :i VOL/MT 8503889 ZZZZZZ **** 100 AVG(ppb) XRPD A VO ab'i 7.6000 7.9 0. 081 FVOL DF BATCH NUMBER 100 1 968601.056001 BURN t BURN 8 RR RD 0.080 0.088 TUBES 31 SAMPLE 1ZZ2Z2 09/86/96 103.19 Cl ACC I VOL/NT R*KA 0 FVOL. DF BATCH HUMBER 0 1, AVG<ppb> *RPD AVG abs BURN 1 16.9500 5.6 . 0.045 57045 BURN .,8 57045 /.RECOVERY = NOT APPLICABLE .v , <- ........ .... ' RUN NAMES 9627001F05 PAGES O ANALYSTS 609 . TUBES 32 09/26/96 10:43 SAMPLE ilMii- IV.OL/WI 2563210 gZZZZZ KICK**** .1.00 X mkSMMhl. 2SBEB. 13.6908 6.3 0.037 .' - ./ LAMCAU'f&i LAO ORATORIES INSTRUMENT IDs 04725 OFAft ELEIIIIN'I .! SC FVOL ..1>F ... BIHJN.tfJ3jBiR 100 1 '962661056001 syrnui mmLSL m m. 0., 039 0.036 TUBES 33 09/26/96 10s47 BAWWJL GLfl Bi!3k/Wl 2563210 TT7777 100 M, -.J>.F__ 23MI.SFL n u m; 100 1 962661056801 AVQ<p.P.frJL SEES. ttflfcjJML BM8JUL ayajiyi 23.2980 3.3 0.861 0.063 0.060 ^RECOVERY == 94.0 ism* 34 SAMPLE CCV 3- 09/26/96 10s51 Elm' 0 Em. _E_ Mm?... NUMBER. 01 amiaafeL *S em_&k. ; 456_j , 23.2300 .0.1 0.861 0.061 SUBfcL 0.861 ^RECOVERY - 92.9 TUBES. 35 SAMPLE CCB 3 09/26/96 10 s 55 GLfiiali IVOL/WX 0 AVGiftjaM. SB& ayO__ss.bB - .1.3200 5.5 "0.882 FyfiU ...f ..,,. MXSH.-yi!!lE . 0. 1 BURN 1. BURN 2 -8. 002 -0.002 m_S.Es. 36 09/26/96 1.0 s 59 SAMPLE mm ciasy imzwi 2563623 **--& 100 Ay<X<ja.ftM.. *BB& SMi -1.4700 15.6 -0.082 F.U0L .J>.F,, BATCH NUMBER 10 1 962661056001 &u m..s. r r -0.002 -0.003 m. TUBE: 37 SAMPLF 2563623 89/26/96 llsft.T ELAEU sK*A 100 (WGt&pbjL *BBS. 9.9500 6.4 8.027 jRECOVERY * 99.5 F.yQL ...m:;... 7; k 5 h .89:;; <r . 100 1 962661056001 BUiM-J, 0.826 amw..a 0.026 T4'5 DUP050307911 RUN NAME'S 9627001F05 PAOEs 7 ANALYST:; * 609 .. ' LANCASTER LABORATORIE INSTRUMENT IDs 04725 GEAA ELEMF.NT i -i'~ TUBE_s 36 09/26/96 11*07 SAMPLE Cl. 'iUOl /NT 2583624 - lfTTK^` #*** ` 188 FUOL PF BATCH NUMBER IBS 1 962681056001 AUG < sob) XRPft AUG ab-n 4~&600. : " 7, S 0.014 BURN- I. ; u r n 2 r k r<j) 0.0. 0.013 TUBE,! 39 9/26/96 11s II CAMPLE p-yy77 Cl ACC lJ.^nL/Wt 2563624 x-x A 10 AUG < prab) i.affiPJD AUG afofr 14.1200 -;4.4 - .036 tfRECOUERY * 94.6 FUOL PF BATCH NUMBER 100 i ifefi&8i05600i BURN 1 iTia? BURN 2 ".0.039 TUBES 40 .09/26/96 Hi: 15 ` SAMPLE Cl, ACS lUOL/WT 2563625 ZZ22ZZ I FUOL .. 100 - PF BATCH NUMBER 1 962681056061 V AVG<ppb> *RPP AUG C)v BURN .1 BURN 2 KRI RjD * "5~ 910 141.5 0.027 0.052 .0.001 ___ TUBEs- 41 ` 09/26/96 11s19 SAMPLE Ct ASS lUOtl/UT. 2563625 TTTZZZ ***A* 100 ':\yG_il?JS.feL iBEJ&. AUG a b.s "TaTsei 14" 6 ""0.033 FVOL PF BATCH NUMBER. 100 1 962661056001 By.RH_J._ 0.030 BURN P. 0.036- ^RECOVERY 0.0 TUBE?.. 42 09/26/96 11*23 SAMPLE Cl. AGS TUOL/UT 2563626 ZZZZZZ :::: 4;t: v. 100 AUG <opty) :WP AUG ab-i 24.020 1.7 5.065 FVOL PF BATCH NUMBER 100 5 962601056001 BURN t. BURN 2 RR Rj>. 5.066 0.065 TUBES 43 09/26/96 lls27 SAMPLE . Cl ACC 1UOL/MT 2563626 zzzzz' z K< A- 3 00 . AUG 1 Di:>b) 3*RPD AUG &bs> 35..1600 3.6 .092 alRECOUERY " 10 3. 6 FUOL. 1>F BATCH NUMBER 100 5 962661056001 BURN 1. 0. 09 BURN 2 . 94 RUM NAI1E s 9687001F0S PAGES (S ANALYSTS &0-s> LANCASTER LABORATORIES INSTRUMENT IDs 04785 OFAA El .GWENT i SC TUBES 44 09/86/96 11s 31 SAMPLE GL.0SB IVOL/WT 858368'7 zzzzzz ** 180 FUOL......DF BATCH NUMBER 100 1 968661856001 y_ AUG < p a b) /KPP AUC ab-a ~ -1.8800 84.1. -0.808 ......... .......' . ... ,... . ..... . . . .... .... . ....... TUBE s 45 .09/86/96 Si)! viL? SAMPLE CL AOS IVOL/WT 8583687 zzzzzz KK*:*wA* :I00 BURN l -..008 BURN 8 P -8.001 .. -------------. FVOL DF BATCH NUMBER 100 1 968601856001 AVG<ppb> 3CRPP AUG ab& . 17...S600 , 43.9 8.847 BURN 1. 0.061 BURN n 0. 033 /RECOVERY ~ 175 s TUBE s 46 SAMPLE CCU 4 09/86/96 CLASS .......* * *" ' ' *' * ' r ;i. l: 39 3VOL/WT FVOL DF .0 0 1 BATCH "**' ""**" NUMBER AUG<DDb) /RPD AUG aba . BURN 1. 83.0400 8.6 0.061 0.061 BURN 8 0.061 /RECOVERY = 98. a TUBE s 47 SAMPLE CCB 4 09/86/96 11:4.1 C.I. ASK IVOL/WT 0 AVQ(pob> /RPD AUG aba -8.8500' 81. ? -0.004 FVOL PF BATCH NUMBER 0I 'fiURM 1 BURN 2 -0.003 . -0.00S TUBE s 4 8 SAMPLE PBW 09/86/96 I1:47 . GLaSli -I VOL/WT 10 AUG <pd b) JS8PJB. AV&..alvj. -1.8408 88.1 -0.008 FVOL PF BATCH NUMBER 10 :l. 968691036001 BURN 1 BURN' f> RR RD -0. 003 -5.008 , ........; TUBE - 49 09/86/96 3. Is SI i A SAMPLE t:t AMS 3 VOL/WT FVOL, BjPO. C_H..MUMB KB. PBW k A* 100 . 100 l 968691056001 AUG < Gi?til JfiRPD AUG ,alis> BURN l. BURN a 11.8600 4.8 0.031 0.030 0. 031 A /.RECOVERY . ~ 113. 6 DUP050307913 l-H-il H... UWJ.I U PAGE; 9 ANALYSTS 009 ' -j I .1 > ...... INSTRUMENT ID: 04.725 GFAA ELENEM f ; SE TUBE: 58 's^iiLg. =5 >? 09/26/96 1.1 s 55 VftSC TWL/UT' t:3! 1 AVG < nob) . RPP AVO- abvi 6-iatsi 4.0 0.023 EyOL J&F,, BATCH NUMBER 1 1 962691856081 BURR 1 QIJRM n m RD ia.ljaa 0.024 TUBE'S 51 09/26/96 11:59 ' SAMPLE pi. 7WLJJM. LCSW Vci>vJ-> few- .- - 1 F&Pk ,J>... BATCH HUMBER 1 1 '862691056001 flllG(BBb) *RJ2J> AUG abs BURN l // "124.6000 "9.5- 0-065 6.861 BURN 2 . .0.069 ^RECOVERY- * 162-6 TUB.s 52 . SAMPLE ' 25652% 09/26/96 12:04 Cl. ASS iyOL/UO: U***# 100 FVQL _D._ BATCH MUMPER 10 1 962691050001. J ' . AV6 <ppfo> *RPP AUG -!) BURN I. BURN 2 RR/ RD "66.3700 2.3 0.177 "0.160 "i~ 175 "S OVER CAL I BRAT ION RANGE TUBE:.' S3 09/26/96 12:06 SAMPLE ' Cl ACC IVPt/UT 2565279 _5_r\02jCHc_Kb. U*A*' 10 AUG <ppb> %RP AUG abs 61.2400 0.5 -0.211 EVDL PF BATCH NUMBER 1, 00 1 96269105600.1. BURN ). 0.811 BURN P. 0.210 ft RECOVERY = NOT APPLICABLE OVER CALIBRATION RANGE TUBE: 54 SAMPLE 2565279 vTX\'^w^-\ 09/26/96 12 s 12 Cl. ACC IVOL/MT 3;-j : O 10 FVOL F BATCH NUMBER 100 1 962691056001 y. AUG < ppb) 9S.R.PD. AUG ab^ BURN 1. BURN n SR Ri) 74.1700 6.5 0. 192 0.201 0.164 T>% OVER CALIBRATION @kn g e : TUBE : 55 09/26/96 SAMPLE Cl. ACC 2565279 Th : (Vv^a-^ OS\ AUG(pb> *RP 64.7200 1.1 12:16 1VOL/WT 100 AUG abs, 0.219 r-UOL DF BATCH NUMBER 100 1 962691056081 BURN 1. 0. 216 BURN 2 0.221 ftRECOVERY == MOT APPLICABLE OVER CAL I'BRAT I ON RANGE 148 DUP050307914 RUN NAME a 9627001 Fid S PAGE s 18 ANALYST s 609 LANCASTER LAEiORATUR!Eb INSTRUMENT IBs 04725 ' GFAA ELEMENTS SE TUBEa 56 SAMPLE F' 5ft5279 @9/26/96 12 s 20 CL AUi; 1 VOL/UT s lie FVOL ...JDF... BATCH NUMBER iie ' i. ifeaisieseiii y AVG < DDb) XRPD. AVG alva BURN 1, BURN 2 RR_ RB 74. .1400 1.5- 8.192 0.190 0.194 "ic2 OVER CALIBRATION RANGE TUBEi. -5 7 09/26/96 1 2 s 24 SAMPLE CM: ASS 1VGL/WT - .y.OL _F,,. BATCH HUMBER '"l Z2Z2-ZZ R - )( K-A 0 8 1 AVGtobb) /RPD AVG abs 90. 6200 0.5 0.235 BURN 1. 0.235 BURN 2 8.234 /RECOVERY NOT APPI.,1CABLE OVER CALIBRATION RANGE TUBE s 56 SAMPLE CCV 5 09/26/96 12*29 CL ACU IVOL/WT 0 FVOL. BF BATCH HUMBER 01 AV6<Rp|3) XRPD AVG abs 22.6680 .1.-6 0. 068 BURN 1 0.068 BURN 0.061 /RECOVERY 91. A TUBE: 59 SAMPLE CCB 5 @9/26/96 12s33 CLASS 1 VOL/NT 0 FVOL !>F BATCH HUMBER 01 A AVG <Kpb> XRPD AVG abs -8.6500 65.8 ~0.00l BURN 1 BURN 2 8. 07*8 --(i.002 A - .......... A TUBE s 60 89/ 26/96 12a 36 SAMPLE CRASS IVOL/WT FVOL BF... BATCH NUMBER 2565276 180 100 i 962691056081 V AVG < Bb> XRPD AVG aii'i BURN 1. . BURN n go. RI) ... @.7600 .1.6.2 0.004 0.003 0.804 cy __ TUBE r. 61 89/ 26/96 12: 'i l. SAMPLE CM. ASS I VOL/NT 2505276 C^2J>At> 'fC A* 180 AVG ( p|:<b) XRP.0 AVG abs 10.9200 0.6 0.830 /RECOVERY a 101.4 ;----------------------------- FVOL DF ... BATCH NUMBER 100 i 968691056001 BURN 1. 0.0 0 BURN 2 8. @29 149 DUP050307915 RUN WANE: 968700IE 05 PAGE: -3 3 ANALYST: (.-*09 LAMOA'.S TER LABORATOEIES INSTRUMENT IDs 04785 OF AA ELEMENT.: rjr. BCDETUBE: 5k 65 09/56/96 18:45 Cl. ACC 1 yf.iL/WT ,-565877 5^^ x <> i: 180 V AUG<nob) 5SRPD AVG abs -1.2100 54 ,. a .-8.802 TUBES 63 SAMPLE 2565277 .: 9/26/96: 12 s 49/ ' Cl, ACC JV0L/WT >:A 130 . FVOL DF BATCH NUMBER 100 1 962691856801 BjJAN.J BURN r> [ . R D -8.001 0,008. jjt ...... * * .............. * *'*** " "*-** FVOL DF BATCH > UMBER 103 1 968691 { 56001 AUG<iSDb> KRPP AUG abs' BURN 1. 6.2508 i.. S 8. 023 0.083 BURN n 0. 083 ^RECOVERY ~ 62. 5 --............ .. TUBE i 64 SAMPLE 25527>. ... . . . . . . . ............... .... 1......... ............. ..... - -- ^ 09/26/96. 18 s S3 ci. k5 5 JVOL/WT u-i: >: i: :-. ): 180 FUOL OF BATCH NUMBER .1.00 1 962691iseSeT y AUG < ppb) JLRgfii 'AUG ab-H PUCK I. 01 JAM r> <R RD 0.710(1 88.6 " 07880 -8.001 -0.000 TUBEt 65 SAMPLE 8sasa76 89/86/96 ms 57 ClAs.S 3VPL/MT ;): ::Am :i (30 flV.il<.fi,R.b>. tfRPD. AVG abs 10.0900 1.3 0.827 ^RECOVERY 108.9 Fvtn. OF BATCH NUMBER 100 1 965631 056001 ; FeG.eHa?l" . a ; IJK r; 0 02 LTUBE 8 66 k mp l e : asaseai 09/86/96 13s81 ci ccc ;r ycu./uiT :i 06 AUG <ppb> #RPD_ AV0_jC?^ 35.9500 0.4 0.094 FVOL . DF BATCH NUMBER 180 1 968691856081 BURN_t_._ RjJE';hl <J:< R J) " 87894 ".94 JjT TUBE: 67 89/56/96 13.: 85 ^BQBCE Cl ACC I yOL/WT 5565561 m<LPKUSf\ 100 AVG <i.Pb> 2S.BPJ). AUG abs 44.6080 1.4 8. 116 ^RECOVERY sc.; FVOL .JDF_ BATCH, NUMBER 108 i 968691056001 BURN 't ~i7l7? BURN >. " TuS RUN NAME1. 968`?001F05. PAGE * iP ANALYSTi 609 I..AHCAG i'Lli LABORATORIES INSTRUMENT ID: 04785 OF AA ELEHLN 1 : 5!~ TUBES 66 SAMPLE asisaae 09/86/96 13 s10 CLASS IVOL/UT *> 5 :l 00 E.VOL PF BATCH. NUMBER 100 1 968691056001 V ftvo<pb> ZRPD AVG a by BURN 1 BURN 8 RJS RD .... 69.9100 0.4 0.833 0.838 0.834 ___ OVER CALIBRATION RANGE ^6 TUBE| 69 SAligLE : 8565868 09/86/96 13s14 <:|. ASS IVUL/WX .108 FVOL OF BATCH NUMBER 55 1 .96869.1056081 AVG<ppb> /RPP AVG Abs 10i". 9400 .' 8. 4 0.864 BURN 1' 0-263 BURN 8 0.863 /.RECOVERY * NOT APPLICABLE OVER. CALIBRATION RANGE TUBE s . 70 SAMPLE CCV 6 09/86/96 13 s 16 cr ASS IVOL/UT 0 FVOL BE BATCH... NUMBER 01 AVG <DDb) XRPI) AVG aba 88.4700 0.5 0.059 BURN 1. 0.059 BURN a -.0.060 /RECOVERY * 69. 9 TUBEs 7.1. SAMPLE CCB 6 09/86/96 13 s 83 Cl ASS IVQL/WT 0 AVG < isob) /RPI) AVG abs -0.3100 170.6 0.001 FVOL 1>F.. BATCH NUMBER 0 1 .. BURN.JL BURN 8 ~i .00S -S. 000 TUBEs 78 SAMPLE 856586 3 09/36/96 13:i35 CLASS 3VGl/WT s:?:*; k *:.**: .100 V AVG <lib) %Rt-*i> AVG .... -0.9100 U. 4 -0.001 mi....FVOL . BATCH NUMBER .100 1 9686910.56001 BURN L BJ.iRN..,,.0. R&> Rl) - 0.001 -0 .,001 5, .. lUBLr. 73 'AMPLE .'53586 3 09/86/96 13 s 39 i :[. ASS IVGL/WT i:s:*A# :l 00 AVG <DDb) JtRPD AVG k h^ 9.1700 5.4 O. 085 /RECOVERY - 91.7 FVOL. ...Pf..... BATCH NUMBER 100 i 968691056001 BURN 1 0.084 BURN 8 0.086 151 DU P 050307917 LANCASTER LABORATORIES . ' GRAPHITE FURNACE'ATOMIC ABSORPTION - DATA REVIEWED BYs DATA VERIFIED BYs DATA HI F NAMES SEP7003-RAT RON NAME: 96370031-05 ANALYST GO INSTRUMENT1 NO: 04785 8KG CORRj BZ- ELEMENTS SE Concent-ration is used to evaluate if earn;) Io -reeu'l. U-;; a-re within calibration -range. ,. ' ; IS DUP050307918 RUN NAME s PAGE s ANALYST: 9627U02F05 > TUBES SAMPLE' S0 1 09/86/96 15:46 CL ASS XVOL/WT '0 LANCASTER LABORATORIES INSTRUMENT IDs 04725 ' QFAA ELEMENT : SE FVOL 0 DF 1 BATCH MNn u m; . AVG<oob> 0.0000 XRPD 35.6 AVG aba --0.001 TUBE; SAMPLE 35 a : 9/86/96 15250 . CLASS TUOL/UT 0 BURN 1 -0.001 BURN 8 -0.002. , . il ; . -- -- -- ---- -- -- M- FVOL DF BATCH NUMBER 0 1. AVG <ppb> 0.0000 i*RPD 4.6 AVG abs 0.012 . .1 BURN 1 0.013 BURN 8 0.012 . TUBES SAMPLE SIS 3 .. . -- M 09/86/96 15:54 Cl. ASS JVGL/WT 0 FVOL DF BATCH NUMBER 01 - AVG < ppb> 2RPD AVG.^abs 16.1300 0.5 0.039 BURN 1 0.039 BURN 8 0.039: TUBE: SAMPLE sas 4 09/86/96 3lCi U . CLASS JVOL/WT 0 ~ M. - ~ .. . -- M.. M- M. M.. --. -- -- -- ----- --. -- --.. FVOL 'DF BATCH NUMBER .0 1 AVG <Dob> *RPD AVG aba 83.8700 l.-l 0.061 BURN 1 0.061 BURN'S 0.061 TUBE: SAMPLE S40 5 *"*' .....W . .. 09/86/96 16:08 . . Ct ASS rvoL/wr 0 FVOL 0 ... .... b. "***'*" DF BATCH NUMBER 1 --4. AVG(DDb> #RPD AVG aba 37.3800 1.1 0.098 BURN 1 BURN 8 0.098 0.093 TUBE: SAMPLE S50 6 09/86/96 Cl. ASS 16:06 IVOL/WT @ * . ... FVOL 0 --- - --- DF BATCH NUMBER 1 ' AV6<ppb> StRPD AVG 'aba . 49.8100 1.1 0.116. BURN 1 BURN 8 . 0.115 0.117 IUBE s OkPQRe S:i:5 7 09/86/96 .1.6:10 Cl. ASS IVOL/WT 0 AVG < d i.i b> 2RPD 19.5000 '0.3 AVG abs 0.047 ^RECOVERY = 97.9. FVOL DF BATCH NUMBER 01 BURN 1 0.047. BURN 2 0.047 15 b DUP050307919 RUN NONE: 96S708SFB5 PAGE: ANALYSTS 66 LANCASTER LABGRATGRIE INSTRUMENT IDs 84725 OF ftA ELEMENT : Of*. TUBES SAMPLE ICB 8 89/26/96 16s 14 CL* AOB IVOL/WT 0 FVOL DF BftTCH NUMBER . .0 1 ftVGQpb) /RPD AVG atas. ' BURN 1 BURN S "0^9600. 17.a 0.000 "0.001 -0.000 TUBES -9 SAMPLE' ; CRA ~ 09/86/96 16s 16 CyOSB . IVOL/WT -8 , FVOL DF BATCH HUMBER 0.1 AVG <ppb> SiRPP ' AVG abs BURN 1 BURN 2 4.0500 7.5 0,011 . 0.012 0.011 TUB.Es. 10 SftHPLE CCV 1 09/86/96 CL ASS i 16 s 88 TUQL/MT 8 . ' AVGtftpb) IXRPD AVG abs 4.8500 0.7 ,0.059 FVOL DF BATCH HUMBER 0 .1. BURN 1 0.059 BURN 8 0.05^ - /.RECOVERY = 99.4 TUBE: SAMPLE CCB 1 11 09/H6/96; l&xRS CLASS ~ 1 VOL/NT .0 1' * AVG <t>ab> y-RPO AVG abs -1.2380 17.5 -0.001 FVOL DF BOTCH NUMBER 0 1: BURN 1 BURN .' -8.; 881. -0.881 ` . TUBE s IS 89/26/96 16s30 SAMPLE ' Cl OSS IVOL/WT 2583825 ZZZZZZ *** 180 FVOL. 188 ` ... BftTCH MUHBER ' 1 962661856801 ,r AVG < nab) /RPP QVG abs BURN 1. BURN f* RR RD "0.5300 8.2 ' 0.081'. 0.001 0.801 " TUBEs 13 09/26/96 lGs.iS ' . SAMPLE a ' .2583805 L,,fi,, 1 VOL/NT FVOL DF BOTCH NUMBER #** 180 100 1 962661856081 ZZZZZZ ' OVG(pab> /RPO AVG aba BURN 1 ' BURN 12.3100 i.7 0.038 ' STeiia "57030 . /RECOVERY 123.1 15 A. A DU P0503 07920 RUN NflMEs 9627002F05 PAGE: .3 ANALYST : 66 LANCASTER LABORATORIES INSTRUMENT.il>: @4785 Ai'AA ELEMENT: 'SC TUBE: 14 89/86/96 16:39 SAMPLE CL ASS IVQL/WT 2303827 ZZZZZZ " )C }; >! 4! 'ic .180 FVOL -. 108 DF WATCH NUMBER >1 9686010560.81 % AVO<DDb> *RPP ftVQ 1 BURN 1. BURN C RR RD - 0.7300 . 50,8 5. 000 0.001 "8.000 . TUBE: 15 * 09/86/96 .. 16 s 'id SAMPLE IVOL/Wf 250362? zzztzi K n 100 ..........'.......... .. ----; 'FVOL DF BATCH NUMBER 180 1 968601056001 : aysi&aWL StRPP QU&laM.' BURN' 1 BURN n - ' 3.3,1.000 0.S 0.038 0.03,2 0.832 ^RECOVERY **' 131 .0 . ' - TUBE: 16 SAMPLE 2335879 09/86/96 16:47 Cl AS: TVGL/WT 100 FVOL DF BATCH NUMBER .100 5 968691056001 y .AVG'<onb> *RPP AUG ab'a BURN t BURN 8 RR Fib' 19.0700 1.5 0.846' 0.045 0.046. TUBE S 17 89/86/96 16:51 SAMPLE CLASS . IVOL/WT 25S5279 me* as A 180 ........." ---- -- -- -- -- -----.. -- -l ------------------------ FVOL DF BATCH NUMBER .100 5 968691056001, , AVGtPPb) JiRPP. AUG aba 30.0900 0.0 0.873 BURN l 0.073 BURN 8 '0.873. ' ^RECOVERY == 116 .8 . - TUBE: 10 ' SAMPLE 5503879 09/86/96 16:56 CL ACS 1 VQL/W'T 188 . .. . .... ........ . . -- ---- FVOL DF BATCH NUMBER 108 3 968691856081 V AVG <ppb> *RPD. AMC ab-3 BURN t BURN 8 RR Rty -- 80,8100 3. 9 0.84a .0.049 0.847 ___ . TUBE s 19 SAMPLE' 8S33879 ^ 09/26/96 .17:00 CL ASS IVOL/UT B*h k **A* 180- FVOL DF BATCH NUMBER ' -100 ' 3 ?6si"918S6001 AVt?<flpb) XRPP AV6 abs BURN_J. 32.4100 6.7 0.076 0.073 ' BliRM_0 07000 ^RECOVERY 188.0 15 D DUP050307921 RUN NAWEs 9627002F05 PAGES , 4 ANALYST: 68 TUBES. a 89/86/96 3.7:04 SAMPLE Cl. ASS 1 VCtL/UT isasira rv&t^3& 3 ** AV6<pob> *RPD AUG ab-i &. izw 2.0 -04a LANCASTER LABOftATURXLB INSTRUMENT ID: 4755 OF AA CLEMEN I'.: SC FVOL DF BATCH NUMBER 108 5 i&assies&emi BURN 1. BURN 3 RF Rj) 0-849 0.047 TU$Ej s . 51 SAMPLE TZTzi^Z 89/S6/96 178 06 ' , . fit ASS IVOL/MT R *** .8 F_VOL DF . BATCH NUMBER 0 AVG (PE>b) . %RP|> AVG *b& BURN 1 1.7 8.873 0.873 BURN 2 8.074 SHRECOVEKY ' NOT APPLICABLE TUBE:' EE 'SAMPLE. ecu a 09/26/9 17 : 1S Cl. ASS IVOL/MT FVOL DF BATCH NUMBER 0 .1 AVG <(>Db> rtRPD AVG a bs 54.7600 5.4 0.-8S9 BURN 1 0.058 BURN. .2 0.060 ^RECOVERY ~ 99. 0 TUBE: 23 SAMPLE T5 ; a 89/26/96 17:16 CLASS XVOL/WT 0 ** ............. '"* **f "* * FVOL DF BATCH NUMBER 1 AVGdorab) #RP AVO abs -1.4600 54.1 -8.081 BURN 1 BURN.S -0.002' 0,801 TUBE : 54 89/56/96 17 s 2X3 SAMPLE CLASS I VOL/'WT 558527'6 VKflSVv S 8****** 100 - - ".. ..........- * ' ~ ---- FVOL, DF BATCH NUMBER .108 1 965691056801 . A V G < p o b) #RPD AVG alw 1.3788 3.3 .0.005 BURN 1. BURN r> RR RI> 0.885 0.005 TUBE: 5 0S/6/^ & 17 a 54 SAMPLE c:l ASS :r v o l /w t 258527& WL*\S tv1**TM** 180 AV lT...S.J?JRJ.TJL. 34RPJB. AVG abs 18.8980 1.9 0.027 S'. RECOVERY 95. B FVOL DF BATCH NUMBER 100 :l. 965691056081 BURN 1. 8.027 BURN 3 5.826 RUN HAME : 968 70081-05 PACj E s 5 ANALYST s 68 LANCASTER I.ABORATOR IE INSTRUMENT IDs 04785 OFAA ELEMENT ; GC TUBE t se, 09/86/96 J.7s2S sAUp.yi. SOS877 jv\,^.Ar \ T^j CLASS IVQL/I4T .106 FOOL. . ... BATCH HUMBER 100 1 96S69103&001 U AVG.<ppb> *RPD. AUG ab-: BURN L BURN '! RR RD ~:t.0i00 69.a 0.-00i -.sea <9.001 TUB^s &7 09/86/96 17s30 SAMPLE Cl. ASS IVOL/UT FUQL 2585277 jvvfcM & fV *** 100 ' ' 100 DF BATCH HUMBER . I B6B6.91056001 ftVG<ppb> Z-RPP AUG aba- BURN t 9.1508 3.1 S.0S3 0.828 BURN 0 8.023 /RECOVERY = 91.5 TUBE s 28 09/26/96 17a 36 SAMPLE Cl ASS IVOL/MT 2585878 HVViHAS. O * 100 AUG < pptO 2-BR.fi. AUC aba - 8.3900 8. S 8.001 FVOL DF BATCH HUMBER. 100 1 962691036001." BURN I. BURN 8 RR. RD 0. 801 8.001 TUBES 89 6AMRAJL 856527V (39/86/96 '17840 Cl ASS 3 VOL/VIT ^ ::i:*:->:A* 100 AUG<ppb) ZRPfi AUG abs 11.3400 1.6 (3.088 /RECOVERY * 113.4 FVOL DF BATCH NUMBER 108 1 968691056881 BtJRH 1 0.086 BURN 8 '(d . 0**G TUBE i 30 SAMPLE 858528:1 '(YviLA 89/86/96 17*45. Cl ASS IVQI../MT' *****' 180 V . AUG <d pb) /RPP AVG aba 38.9000 2.2 0.09.{ FUQL DF BATCH NUMBER 180 i 968691056001 BURN I. BURN 8 RR R 0.098 0.090 "j0^ TUBES 31 (39/26/96 17:49 SAMPLE Cl.ASS ' IVOL/WT 8585883 ^vv(H\ 4 *S.108 FUQL DF BATCH HUMBER 100 I 968691056001 AVGIppb) , ZRPD AUG aba BURN I. BURN 8 50.7700 1.3" 0.118' 0. 1 19 '"i. 17 7 /RECOVERY - MOT APPLICABLE OVER CALIBRATION RANGE r u n Hunt:; PAGE- : ANALYSTs 'j 6 ci / 0 0 c-C id .j 66 TUBE s 3S SAMPLE asasaaa 09/86/96 17:53 C: l- AiSS IVOL/WT 31 4S-4i 108 V AVG<oob> JiRPD AVG abs is.4300 1.3 0.053 LANCASTER LABORATORil.i INSTRUMENT II>s 04725 UVkk e l e me n t sr FVOL DF BATCH NUMBER 108 5 962691856801 BURN t BURN .1 RJg.| RD 0.053 13.854 TUBES 33 .SAMPLE., 2585262 09/26/96 17 s 57. ' IVOL/WT 31 tWSftK 100 AVG(OObV /RPD AVG abs 36.3008 2.0 0.885 ^RECOVERY .139 .5 . FVOL DF BATCH HUMBER 100 5 962691056881 BURN ~1. 0.'084 BURN 2 "0.000 TUBE! 34 SAMPLE' CCV 3 . 09/86/96 16:01 Cf. ASS IVOL/WT 0 AVG < onb) JCRPD AVG abs 24.1800 1.6 . 0.057 *RECOVERY 96. 7 FVOL DF BATCH NUMBER ' BURN 1 . 0.057 BURN 8-. 050 TUBEs 35 SAMPLE CCB 3 , 09/26/96 16:85 Cl. ASS IVOL/WT l 0. AVGCoob) tfRPD ' AVG abs -0. 5680 93. 6' 0.801 FVOL DF BATCH NUMBER . ' 1. . BURN 1 BURN"0 0. 001 ' -0.000 TUBE: 36 89/26/96 16 s08 SAMPLE CM. ASS IVOL/WT 2585263: rc\-V*>v> * >:-); x ii-x 108 <y * A AVGCoob) iRPD AVG " AO'ii -1.3300 22. 1 ' -0.001 FVOL DF BATCH . NUMBER 108 1 962691856801 BURN t . BURN 2. ER RD -0.002 -0.001. " " TUBE: 37 SAMPLE 5585203 89/26/96 18:12 ci Afef; .T.VOL/WT : >; 3: 3131 A33 .1 88 WXAVGCoob) ?RP k ..abs 9.9400 4.3 0.025 SCRECOVERY 99. 4 FVOL DF BATCH NUMBER 188 1 968691856001* BURN I. 0.024 BURN ft i.aas 158 DUP050307924 RUN NAME: 9627002F0S PAGEs -7 ANALYSTS 68 1IIBE: 38 SAMPLE. 2565264 09/26/96 16si? . U&g lVQLZ.WJ. ***** 1 AUGippb> XEPD AUG ab* -i.SS00 ft.a -0.002 l,,ANCArjTEf< LABORATORIES INSTRUMENT IB: 04725. GFAA ELEMENT.! . SC FUQL' 1>F BATCH NUMBER lee i s&sftsisss'eei BURN. 1 BUANJI RR R -0.60S -0.002 TUBE:; 39 SAMPLE. 2585264 09/26/96 16:20, . Cl.ftgO TUOL/UT 4:t:A . 108 V A_V.eJLim.l2i gfi> AVfi_S.fe.ii' 9.9000 0.6 .0.025,' FUQL BF BATCH NUMBER 100 1 962691056.001 BURN 1 0.024 BURN'2 . 0.025 tfRECOUERY. - 99.8 TUBES 40 ' ' SAMPLE . 2585265 09/26/96 XBs.25' Cl ASS IUOL/UT : ******* 188 FVOL 108 BF .BATCH NUMBER 1 962691856801 AUG<PPb> SSRPB . AUG abs BURN 1 BURN 2 ,RR RB -1.0600 30.9 -0.001 -0.001 .-0.000 TUBE: 41 SAMPLE 2565265 09/26/96 IS;29 . Cl. ASS IUPL/NT i00 AUG <DPb) ; /.RPB AUG abs 11.0600 ' 1.3- 0. 027 FVCiL BF BATCH NUMBER 180 1.962691856001 BURN 1 BURN 2~ . 0". 027 . 0l 027 tfRECOUERY- a 110.6 TUBE: 42 SAMPLE PBW -fffijtXi- 09/26/96 .18:33 Cl AST: IUOL/WT ** 100 AUQ (pnb) gRPD AUG aiw -1.3900 13.6 -0.001 FVOL BF BATCH NUMBER 100 1 962691056082 BURN 1 -0.001 BURN 2 ' RR. RD -..002 ______ TUBE: 43 SAMPLE ' PBW 2^f7Xt 09/26/96 16237 CLASS TUOL/UT **A* 100 AVG < cspfa) StRPB AUG abr. 10.9680 4.7 0.027 ' RECOVERY 109.8 FUQL DF BATCH NUMBER; ,*"108 " T 962691056002 BURN 1 0.026 ' BURN 2 026' RUN NAME: 96S.7008F05 PAGE: ft ANALYSTs 6ft LANCASTER LABORATORIES INSTRUMENT Il>s 04725 ' OF A A CLEMENT : SC TUBE t 44 SAMPLE LCSW 09/26/96 lfts41 Cl ACS .JWL/ttT , FVOL ' **** . 1. i 3BMP!JNUMEE 1 962691056088 AVG<pt>b> a.2700 . AVO abs 3.3 0.081 BURN 1 BURN 2 ftft RP 0.021 0.080 TUBES 45 . 09/86/06 lft 45 SAMPLE Cl ASS IVOL/UT. C'csw -rrrrrf ***& i FVOL PF ' BATCH' NUMBER i i sssfeiiciiiei' AVGCoob) irtRPP AUG abs 80.8900 3.8 0.04S BURN 1.' 0.04? BURN 8 0.049 ' JtRECOVERY == 180.2 TUBES 46 cScAMv P4LE; . ' 09/2S/96 10 s 49 " eCLASS IVOL/UT aFVCH. - TPF B""ATC"HJN~U"M"~B"ER AVG(pcfa) XRPP AVG atas BURN 1 24.6708 0.ft- 0.056 ' 0.059 BURN 8 "~0.056 !#! RECOVERY = 9ft.? ' ' TUBE; 4? SAMPLE CCB 4 09/86/96'10853' CL ASS, IVOL/NT 0 AVG '< &pb> XftPP AVG abs -1.1500 14.9 -0.001 FVOL PF BATCH NUMBER ' 0 " A- " ' ........ . BURN 1 BURN 8 -0.001 -i&.mi TUBES 4ft SAMPLE 2565290 09/26/96 1ft:57 CL ACS . IVPL/UT T00 FVOL JgF_ BATCH HUMBER 10 l 962691056008 V AVGtppb) '/-RPP AVG aba BURN 1 BURN 8 ftft. RP ft1.4100 1.9 0.169 0.191 a. iftfe " OVER CALIBRATION RANGE TUBES 49 'SAIlPtC 850589 9/26/96 19:01 Cl. ASS IVOL/WT U*k A* ' 100- FVOL PF - BATCH NUMBER 100 1 9626937056002 AVG tppb) %ftP'P AVG abs 93.0600 "8.& &.815 BURN 1 0.816 0IJEM _fj ~0.818* .^RECOVERY = NOT APPLICABLE OVER CALIBRATION RANGE 160 4 DU PO50307926 LANCASTER - LABORATORIES OR fl I'M ITE FURNACE ATOMIC ABSORPTION l.i AT A RE VIE WI:" & &V DATA VlMFIKD BY 4t7 DATA FILE NAl'ilr t SI' k 7NN5. RAT RUN NAMES 96(5710.1.rOS ANALYST&f. INSTRUMENT NUs 47S5 OKA CORN : b'l ELEMENTS SE LOilCBl'ltTation 1 fe US&d to OVciiuAtii >. i' 1.1? I. !;} r:\ V' With 3, Vi c a I i bratio n r a n ?| e . DUP050307927 RUN N AI'll-. i 96371U .1 T t:i5 PAGE ; :i ANALYST t 06 i . I"l i -H * i rr:ft i..h ;.mj !<kY INSTRUMENT IB; 047,'5 or ivk ELEMENT ; SE IWjgH?. SAMPLE Sft - .1 89/ft6/96 aft s 13 LV.ffiLZI 0 rjm> ...M;_ SfilQH.. e1 ftv.aiftB.fe?-' m& BUBtLl BURhlJS . 8.0000 56. 7 -0.001 . -0.001 -0.00a .LUBE ^r< ft 89/S6./9& as s i ? :f v o l /w t . 0 ................ * V FVOL. 6F BATCH NUMBER ; : i 0.00013 ftv<L.*b_%. StJBiL.1 WUR.M l.H 0.Q15 0.015 0.015 ME:. BAMPyg. 31S 3 09/S6/9& assst CLftS,,s IVOL/UT & fty&s ftftfei- /.r p ;o 0V6 .atia 1ft.6ft00 1.9 0.837 BiOk-JftE BATCH HUMBER 01 gyfib.-L 8.037 0.036 mBE: SAMPLE sas 4 09/S6/O6 cl 2 w 2!?* TVGL/WT 0 AVG(pcb) S3.7700 AVG aba. 1.9 0.059 FVOL . Ij.i .... . BATCH NUMBER 81 BURN 1. SURH.E. 8.65*5 0.860 XUBgj. SAMPLE 340 5 89/S6/9& S.*ift9 PLASH iypL/WT FVOL ft . 0 I)F BATCH.. NUMBER 1 X.R-PD SVG_*ba. 37. t>ae 1.0 0.098 BURN 1 BURN a 0. 090 0.069 IV BE s Zk[\l -f ; 350 & 09/S6/96 assOj ( 1. ACC XVPk/wx 8 ftVG <pjpb>_ CRPfl A.VG.,,.abi=. 50.1300 . 0.S 8. 114 EVPi-. 0 .. BAT CM_N UM B E R 1 BURN 1 0.114 ; ]^_ 0. 114 IV BE:. SAMPLE :i:cv 7 09/S6/9& SSs.17 OI,AOC JVOL/WT & V.Q <p.jbj. TiHKP. AVG...iH.b.a 19.0680 0.3 0. 845 ^RECOVERY * 95. 4 FVQL JOF BATCH NUMBER 01 BURN 1 BURN.ft 0.04S 0.045 :-mn Mftl'lli.. : `.i/.1 U.L I"!-.1 - 1'f H.n-. s P ill ini.YST: .66 TUBE:. ll'IPLE CW * & 09/86/96 28* 41 D! AD!;. TWL/WT 0 ftVG <.ttnh> 2SEPJ. ei.jiiut -1.3600 6.A -0.001 I..H Mu A 5 TER LABORAVUR .1 INSTRUMENT TDs 04725 OPAA El..EM ENTSC FVGL . 1)F .... ANUMBER 01 BURN 1 BURN 8 "0.001 -0.008 3mm& DR ft 9Jh (39/86/96 88*45 WMfc: i EVJ?k _J>P .... BATCH .NUMBER 81 tm..s *s l &L 3.6300 five _*bi ' &UiL,,i IPtLI 4.9 0.011 0.0X1 0.010 ikii*. 10 Wkl CCU 1 .09/86/96 88 * 49 - QJ.- Alii lymvwi ; flVfiiMfel *?& AUG. *b6 ' 84.8680 1.3 8.856 ^RECOVERY = 97. 0 &V0L DF BATCH NUMBER 0 .1 BURN I 0.056 euRfci s 0.857 LUBE:.. 11 fit!RLE ecu 1 09/86/36 88 s 53 GLfiMi l u o d /mi 3 AyGiispb).. *RP -1.6000 7.5 -0.80S FVOL 8 . DF BATCH NUMBER 1 BURN 1 BURN 2 -0.001 0.008 BiSki. 18 09/86/36 88 * 57 SAMPLE ' PL0- .LV0.d 2.w t 2563863 n\9J\U-i .*** OtSfik ...ML. BATCH NUMBER 188 2 968691056001 A ay&.<kfikL *r p & AVG. abx ' RURH.J-. BURN 8 RR. RD 80.0500 1.. 1 0.047 0.8,47 0.847 13 89/86/96 83 s 01 SftW.PJ.E_ 111 AM- lyoL/ui 2365261 rriUtvX^ (X * * * * Ax 100 ,' FVOk JPJL. `; k 5 a ...NUMBER 100 8 968691056081 eycK&EM: *; bcj > e.w...sbfe 89.5600 8.1 0.1366 ; defu . 0,. 06? ; ur n r 0.069 A . ^RECOVERY * 95. 1 16? ii- :l: 1 ; :! DUP050307929 RUN WAHL: 9fc>27 X A IF AS 1:'AGE : 3 ANAL YST s T,S TU&E.5. 14 SAMPLE 2685890 09/86/96 83 3 06 If VQL/VIT tl 4! .1.00 8.yj2.1ia.ii?-fe>_ ytRt-'D Auc &bv. "Tv. 4tiS ~i.1; 7" B. 46 LANCAG l > .! . LA DORA"! uRj.LS INSTRUMENT IDs 64785 0Ph A LU'iHEwr.!, sr FyOL _ftF_ ejftT.CHJMWMBER 100 S 968691056068 SIJNN l SUNN 3 .NR HD 0.046 0.045 ~~ I.g; h.L i s 09/S6/V6 83 s.10 .A WALE. < I.ASS IM.Q.W./WJ- asasaVtf Z2ZZZZ t.l>:i;:: A .1.00 ftVp<BBb) XRPO AVG aba "iiTsies. ~s 7a " ~ 0.070 t^ecevEKY 111.6 FVOL _ _. BATCH HUMBER 100 5 96a6910E->i.0a BURN t ' .0W078. SURNjl0.069 ;njBt:s_ SAMPLE. 2585890 0.9/86/96 essi* ckJM* LV.Qk/iI 2Z2ZZZ *li*,:** 100 AVGtppb) 16.5400 yRl-'O AVG Ab'A 4.6 0.044 F.y0.k .j>F.._ BATCH NUMBER 10 5 968691056008' nop; u r n i ; r> Ri< Rl) 0.045 0.048 TUBE* 17 09/86/96 83s 18 ikjklm : 5 l ftGf; :rypi./wT 585290 ZZZZZZ *ft* 100 OiOk . J?!:L. BATCH. HUMBER '106 5 968691056008 A AVG<ftpb> *RPD AUB abs BURN 1 BURN >9 A 30.1700 1.3 0.070* 0.070 ~i'. 069 . tfRtXGVEESY * life. 3 11.3BEs IS 09/26/96 83822 : AMPLE C:1 AS& XMOL/UT -- 65290 ZZZZZZ "* 1 00 fiL"!ii.5..13.E.fe.L %RPP AVG a 80.5300 0.6 0.046 .. FypL ,J>F_. BATCH NUMBER 100 5 968691056008 BURN. t. BURN 2 !<R I/O 0. 04 S 0. 04S i ABEs. 1.9 .`AMPLE!;. J.. ji, . 69/26/96 83s 6 ca. ASS ry.OL/WT R*)5KflK 0 FVOL F BATCH HUMBER 05 AVGtpplA jtliPO AVG. abb 38.4008 0.2 0.075 BURN 1. 0. W74 BURN 8 0. 1975 %REUUUEf: Y = HUT APPl.. I CABLE DUP050307930 Se -,4:'- ..lift NftHF; 9627.1. WlFttS 1-TiAh: . in-ii iLYST : 63 ' :tuft-s aa 09/06/96. a3i- MUM,;., zSSZZM * 100 9. mismki mm mskj&as. 5.0400 i.a , 0,,&a LAHCftSTFrt LABURATORI EC INSTRUMENT ID: 0471X5 or ft ft 5 qrsrn t.! or: FVOt.. DF PATCH NUMBER 100 5 96S691856803 &UBUL1 0.053 sa aa 0.85^ ___ fUBEj. 81 fWWlg. 09/06/96 23 s 35 : Ifflywi. .!53t>a9C r-'??yyj> 160 BPk _M..,, BftICH.l!UMWER 108. 5 68691856888 avG.iB.Rk>., mv>. avfi,,ak.s SURH.1 36.5500 0.5 8.034 8.034 OUftW j* 8/08.3 ^RECOVERY 115.1 ma&i as GBilM ccv a 89/E6/96 a?# 39 ;;t. age TVOL/WT & av.G <a?J>b).. gRPD. S.VG' abs, 3.3000 0.3 0.055 JlRECOVERY = 95. a 1 D8E.s.' S3 SAMPLE ecu a 09/36/96 343 eussiL IVOL/WT 0 AVGiBBM. *H &ytL*ki -1.3980 a.8 -0.801 FVOL 1>F BATCH HUMBER 81 BURN 1 0.055 BURN S' 0.056 ` - FVOL. DF BATCH NUMBER 01 \ BURhLl yMJl -8.001 -8..00.1. OAT A REVIEWED BY gP*f*BATft VERIFIED BYs ekW ` 165 i 1 l 4 i i i i t t < < i 0 DU P050307931 'i .. ' ' " 1 '> ' ' C. . ft. LANCASTER LABORATORIES DATA FILL" NAME:! 5::EP71I,, RAT RUN WANE* 96371OSRaS ANALYST 6SS INSTRUMENT NO* 0474*5 DKG CORR.: BZ ELEMENTS BE .66 Concentration ife ui&ed' to evaluate i. f -.iAiyi.il.ii v-a-iwU;-. ar.i within calibration range.- i DUP050307932 RUN MANE s' 9627102F85 iP'ABE s i ANALYSTS 659 TjUBEs 1 SAMPLE SO 09/27/96 01 slS Cl ASS 1VQL/WT 5 AV6<ppb). B`i> AVG abb 0.0000- 8. 5 -8.803 LANCi-lSI LSi LABUKAI UK AIIHSTRUMEHT IDs 84735 tukk e i.5 vwxyz ,r>r FVOL. _DF_ BATCH NUMBER 1 BURN 3. BURN a --e taii 0.000 TUBE s SAMPLE S5 a 09/37/96 01 a 14 CLAST: JVOL/WT 0. AVG < ppb) JCRP.D AVG aba 0.5555 8.0 ' 0.013 FVOL -DF BATCH NUMBER 0. I BURN 1 BURN B 0.(313 0.000 TUgEj. SSjAMFLE 545 3, 09/37/96 81s16CLASS 0 . AVQ(DDb> &RPj> AVG aba 15.0900 5.5 0. 836 FVOL . PF_ BATCH NUMBER 01 BURN . |, ' BURN...B 0.(336 5.000 TUBE: SAMPLE sas 4' 09/37/96 01s 16 CLASS :i VOL/WT.0 AVG(cob) StRPD AUG ct bis- S3;fiS0 8.0 8.860' FVOL. PF BATCH NUMBER 01 BURN 1 BURN a 5.060 0.0130 TUuEs SAMPLE S48 5 89/37/96 81s20 Cl.. ASS JVGL/WT 8 AyG_?..PJJ_bj_ 5CRP.P . AVG.abs 37.3700 . 5.5 0.891 FVOL PF BATCH NUMBER 01 ; ur n i 0.091 Bu r n a 0.000 TUBEs SAMPLE ' S50 6 09/27/96 ,01s 22 L:K ASS :i:v o l ./w i. 49 AVG(DDb> 25BM "AVG aba 49.3908 8. 0 0.114 FVOL jjF_ BATCH. NUMBER 01 BURN 3 BURN a 0.11-3 0.000 TUBE s SAMPLE 1CV 7 09/27/96 01 a as Cl. ASS 1VOL/WT .. FVOL ' PF -BATCH NUMBEk '0 01 AVG(ppb) rtRp'p1 AVG; .aba 19.0100 0.0 0.045 BURN 1 0.045 BURN 2 '0755(3 /(RECOVERY * 95.0' RUN HOMES 9627108F05 PAGE a f ANALYST s . 659 . TUBES SAHfcl-E ICB 8. 09/27/96 Bis27 Cl ASS IUOL/WT .S ' %RPX> AMS abfe -0.7500 "i7i 8.000 LANCASTER LAOORATORIES INSTRUMENT IDs 84725 Si - AA ELl.HHM t > SI... FMOt. DF. BATCH..tjUl'IBEH S . 1. BURN 1 BURN ' 0.080 0.000 TUBES 9 SAMPLE CRA 89/27/96 Bis 29 Cl ASS IVOL/WT 8 FMPL 0 DF BATCH NUMBER 1 AMS <prjb> %RPD AMG abs " 41 5400 8.8 0-012 BURN 1 BURN .0.812 0.000 TUBE; 10 SAMPLE' CCV 1 09/27/96 01.31 . Cl. ABC IVOL/WT 0 FVOL DF HATCH NUMBER 01 AVGlmjb) J6RPD . AVG abs 24.6200 , 0.0 .0.057 BURN 1 BURN 8.057 0.800 /.RECOVERY 98. 5 . TUBES 11 SAMPLE CCB i 89/27/96 01s 3 3 ' . CLASS IVOL/WT 0 AVGImM &r p d AVG'abfe >0.6900 0.0 0.000 FVOL DF BATCH NUMBER 01 .BURN 1 BURN 2 8.088 0.880 TUBE! 12 09/27/96. 01-s'35 SAMPLE . Cl ASS IVOL/WT 2563633 ZZZZZZ <D . 3 00 CQNC< ppb) 14.3600 BURN 1 0.034' FVOL DF BATCH NUMBER ` 100 10 962681856002 TUBEs 13 09/27/96 01s37 SAMPLE Cl ASS 1UOL/MT 2563633 ZZZZZZ \ **J* 100 ' FVOL 100 DF BATCH NUMBER 10 962661056802 COHC(ppb) 19.5800 BURN 1 0.046 . ' TUBE s 14 SAMPLE 09/27/96 Bis39 CLASS I VOL/NT 2583633 2ZZ2P'r: 7KM*tKp,: 180' .. FVOL DF BATCH NUMBER 100 10 962661056002 MNCjti?itk>.. BURN...1 23. 9688 . . 8.056 [ i # . - O 1 RUN WAMEs 962710SF85 PAGE s >:*. ANALYST: 639 LANCASTi...Au3RATURjCEt INST Ft UMENT ' IDs 0-4 V 25 0FAA ELCMCM P: SC TUPEs IS 09/87/96 01s41 SAMPLE - Cl. ASA -IVOL/MT 2503033 77ZZZZ 3>h :-;-k -k 3k 100 EVOL. ...Df.. BATCH. NUMBER 100 10 9ca60 i w56uw CONS<ppb) ' 28.480 BURN.1. " 0.066 ' X INT CORK CGEF SLOPE Y INT = 16.33073 HH = 8.99693 . - 8.08818 0.03460 RO. TUBEs. 16 iSfflMLe . '-8305879 09/87/96 01 s43 Ft ASS IVOL/UT . 10 ' CONG Coob) 19.900 t BURN 1 8.047 FOOL DF BATCH NUMBER 188 .S 968691856001 TUBE: 17 09/87-/96. 01s45 . - SAMPLE ' CLASS SVQL/MT FVOL 2505279100" 180 DF -BATCH NUMBER S 962691056001 CONCC ppb) 24.4800 8UBIU." 0.857 TUBE: 18 09/27/96- 01*47 SAMPLE CL ASS 1UOL/UT ' FVOL _DF__ BATCH NUMBER 2565879 'fY\L<\3^ ,,j|Mc * 100 100 5 962691056001 'CONG <aob) 20.6308 BURN' 1. 8.066 TUBE s 19 09/27/96 01*49 SAMPLE Cl. ASS SVPL/WT 2565279Uw***3* . 1.08 .. CONCCppb) 32.9600 BURN 1 0. 076 FVOL DF BATCH NUMBER 100 . 5 i626910S681 X INI'=`.''4.33185 RR. CORR COEF = 0.99970 __ SLOPE Y INT = 0.80198 = 0.04710 RD 1_ TUBE:. SO 89/27/96 01 a51 SANPCE Ct ASS IVOL/UT 8505279 ' ' D***0* D Ct 100 CONC (ppb? BURN 1- 20.5308 0.040 FVOL DF- BATCH NUMBER 100 5 962691056001 iG DUP050307935 RUN NAMES 9687108F05 PAGE s 4 ANALYST: 859 LANCAO it :ft {k; |}k~}e s INSTRUMENT 11): 04725. or Aft ELEMENT.: or TUBE: 81 9/87/96 01*53 SAMPLE CL ACC 1UCIL/WT FUQL 8565879^^0^ .^IMUMUCl* 100 , 10 PI- BATCH NUMBER 8 962691056001 QQMSijifiJaL . 84.6100 6URN-1- 0.<il5B ' TUBE: 88 89/87/96 QlsSS SAMPLE '' . ' Ct ASP IVPL/MT P565879 P'*KKP nr&ftas .p-a, 108 COMC(DDb) BURN .1 88.4100 0.. 066 FVDL )PF, BATCH NUMBER 100 5 962691056081 TUBE: 83 SAMPLE ` ases879 09/87/96 01.857 ' CLASS; 1V0L/UT ***">**' 100 CUNCTopb) 38.4700 BURN 1 0.075 FVOL PF ' BATCH NUMBER 100 5 968691056001 X TNT ; COftft COEF = SLOPE = Y INT = 87.19101ftft RP a.99918 0.00176 0.04840 TUBE: 24 . 09/87/96 01s59 SAMPLE . . Cf. ASS TVOL/MT 8585888 KK*3i0- 10.0 . rnRASLS <T ' COMC< ppb). 84.5500- BURN 1 0.057 FVOL DF BATCH HUMBER 180 S 968691856801 TUBEs 25 . 09/27/96 02s08 SAMPLE CL ASS JVOL/UT 8565862. ,, ' ! . 180 mjfv.2r5 v. - CONC < pa-b) . BURN 1 : 89.2500 $*066 FV.OL PF BATCH NUMBER 108 5 968691056001 . TJJBEi. 86 SAMPLE 2565262 ; 09/87/96 02 s 08 ; CL. ACC TV PL./NT 5^ JKKK*C 100 CDNC(ppb) 32,4400 BURN -1 0.075 FVOL PF BATCH NUMBER TSS '5 968691056001 170 DUP050307936 RUN NANEs 962710HF05 PAGE# 5 ANALYST! B59 TUBE; '27 SAMPLE - .09/27/96 02 s04 . CL ASS IVOL/WT asasaaa^flA^r-3 100 36.5400 .BURN 1 @.064 LANCASTER LABORATDR .t Li INSTRUMENT IPs -04726 OFAA ELEMENT:. SC FVOL PF BATCH... NUMBER 100 S 962691056001 X TNT = 32.. 64891 KH. :CORK COEF * 8.99640 1... SLOPE = 0.80176 Y INT - 8.85760 TUBE f 26 ' 89/27/96 02s8& SAMPLE Cl. ASS IVQL/WT 2565290 222222 <P 1>*,0k 188 CONG <1313 b> . . BURN 1 9.-6208 0.024 FVOL OF BATCH NUMBER 100- 10 962691056002 TUBgs 29 SAMPLE 09/27/96 02s86 : - CL ASS TVOL/UT 2565298 2ZZZZZ f *** !f;l iF . 1.00 CONG <ippb) 14.6988 BURN 1 ' 8.835 FVOL. OF BATCH NUMBER 100 10 962691056002 TUBEs. 30 09/27/96 82s.11 SAMPLE ' CLASS '1VPL/MT 256529 WTH# ***- 180 'CONG < ttttfa) ' 16.5900' BURN 1 ' 0.044 FVOL PF BATCH NUMBER 188 10 962691056882 TUBILL 31 SAMPLE 2565298 09/27/96 02 s13 1 Cl ACC 1 VOL/LIT Pk k *3k - 100- CQNC <pwfa> 23.1280 BURN 1 0.. 054 FVOL PF BATCH NUMBER .188 18 962691856002 X. INT ' ,, ' > CORK COEF SLOPE ' - Y INT ' 12.32323 0.99929 '0.00196 0.02440 RR. TUBEs 32 SAMPLE ' CCv"s 09/27/96.02s IS CL ASS IUOL/WT. ' S' FVOL PF BATCH NUMBER S1 r ' ' .......... AVG<qpb> gRPlD AVG abs> 24.5580 0.8 8.057 .^RECOVERY 98. 2 BURN 1 0.057 BURN 2 0.000 Up*. _ #: # j RUN NAME: 9627i02F05 PAGE s ANALYST: 659 ' TUBE: 33 SAMPLE CCB"2 " 09/27/96 02:17 CLASS :i VOL/WT 8 AVGtppb) WPP .AVG aba -0.5100 . 0.0- 8.801 r TUBE: 34 SAMPLE- - ..2585292. 09/27/96 02:19 Cl ASS IVOL/WT 0j( 108 CONC <ppb> 13;1608 BURN 1 0,032 ' LANCASTER LABORATORIES INSTRUMENT IP: 04725 OFAA ELEMENT: >E FVOL ' PF BATCH NUMBER 0 -1 ' BURN 1 BURN 2 0.881 0.000 FVOL PF BATCH NUMBER 188 .18 962691856802 TUBEs 35SAMPLE 2565292 '09/27/96 02:21. '' CLASS IVOL/WT 1B0 CONC<DPb> 17.4380 BURN 1 0.041 FVOL DF BATCH NUMBER 100 i0 962691856802 TUBEi 36 .SAMPLE aslssie' 09/27/96 02:23 Cl ASS . ;!VQL/UT , 180 21.9400 BURN -1 3. 021 FVOL DF BATCH' NUMBER 180 18 962691056082 TUBE a 37. SAMPLE 2565292 89/27/96 02 s25 . ` . Cl AST: IVOL/WT . FVOL PF BATCH HUMBER 188' 180 , 18 962691856002 X CONC(DDb)' 26.2600 ` BURN 1 0.061 X INF = 16. .14821 CORK COEF =- 8.99966 SLOPE = 0.88194 Y INT . - 0.83178 m I. ! A TUBE: 36 SAMPLE ecu 3 '. 09/27/96 02:27 Cl ASS IVOL/WT 0 FVOL DF BATCH NUMBER ( 01 ! . AVQCppb) StRPP AVG abs 24..^180 -0.0 .0.056 BURN 1 0.056 BURN 2 0.000 1 * ^RECOVERY 96.0 1X * O DUP05 0307938 LANCASTER LABORATORIES GRAPHITE FURNACE ATOMIC ABSORPTION BATA REVIEWED BY* DATA VERIFIED BY DATA F It I. E NAME'11 f*.93 S' RUN NAMES '36S7O01Fai ANALYST; W- INSTRUMENT NO; 0!6(33 DKG CORKi BD ELEMENT: Tt. Covicentraticm ia used to evaluate if c a 1 i.h r a tin Vi r a nqe. 17-5 v*>su I. Us ar-e witlvir. DUP050307939 RUM HftflLi 962706J.F81 ( `H(iL S .( ANALYSTS 66 ; . SJMEL 30 09/25/96 21 a 01 LHi IVBLZMI B RVG<p'P.b.).. *RPO AVS ab.fi 0.0000 0.0 -0.004 k 5 ks f ; uibunw i u k .u .. 1N8T KUMh MV HA) s Id a 6 03 ftpAft e l e me n t t i. .PJifik 0 PJJB.li.JL 8MBJUL -0.089 0.80(3 TUBES'. SAMPLE 9>;t fci 2 (39/25/96 2Is05 ULBSli 0 Em. JBE-. IMfcL,,NUJ!LKH 01 ftVG (pcb) *KP.fl AUG,. aba, 18.0000 6.3 0.042 gUM--L BJJfifcLJ(3.045 (3.(340 TUBE* 3 SR MALE 620 ' 89/25/96 Sis06 C:t,AU.U ' M_/MI ' F-VPk ..JPJ:... BATCH .FllWBER 81 AVS umb> XRPO AUG ab.ft-. PU,!!.& >0.0(300 5.3 0.1(39 ..^13 (3. 1(35 TUBES. SAMPLE. 348 4 (39/25/96 21s 12 PLASI: 0 AWLimllL 2EBEJSL AV.G *> 4(3.0(300 S. 1 8.S07 E.U0L I) BATCH NUMBER e .1 P1L'2 0.2(34 0.21(3 IWJ&&L kp l e . S6B 5 (33/5/9 fa 21sl6 CLAMl im/w.i "0 AVG<QPb> fiM'P. Wfs A**. 60.01300 8.5 0.2S1 FUGL. 8 ' BAXC.tL_hlU.WBER :L MJBfcl S 0.262 026(3 TUBE a SAMPLE 308 6 09/25/96 21sl9 CLSSfcL IVOL/MT AyPiRRfeL *KPP (Wi-afei 60.0(300 .1.0 0.364 . Biffi*. -Jit BATCH NUMBER 81 BURW....1 BURK a 0. 366 0. 361 L; &j l 9.0MULE :i;cv 7 09/2S/96 Els 3 CLfiSitL IVOLVMI 0 . AVGjC..fij?b_)_ :*.RPo 0V.1LA&S. 50.1900 1.9 0. 246. /.RECOVERY 108. 4 FVOL _JDF ... BATCH. NUMBER 0 1 0.251 BURH..a 0. 244 174 RUM NAMEs 9&a7B0lE0,'l PAGE s ANALYST s r 66 TUBE: SAMPLE I OB & 09/8S/9& 81 s 86 Cl...AUC JVpL/UJL 0 AUG (DDb) JiRPO AUG abs -0. sm& 99.9 603- I..ANCAO TER'LABORATORIES INSTRUMENT IDs 08603 GCAA ELEMENT: TL FUGL PF BATCH NUMBER 01 BURN 1 BURN a -0.005 0. 001 1 IJftfc. s SAMPLE OKA 9 09/85/96 SlaHO k 1 VtlL/WT 0 AUG (nob) JCRPD AUG alas 14.0900 8.7 0. 066 FVOL 0 ................. .. 1>F ; k 5 _; I BURN 1 BURN 8 0. 067 0. 064 TUBE s 10 SAMPLE 222222 09/85/96 81 s 33 gjftSfi 3VPL/UT ***. 0 AUG (prb) /RPD A.VG.._.a;b.ft 38.4000 8.4 0.171 ' ............" '' FVOL DF BAT CH,,N UMBER. 0i BURN 1 BURN a 0. 166 0.174 TUBE s 11 SAMPLE ecu :l. 09/85/96 81 *36 CLASH IVOL/WT 0 AVG<j>pbJ J4RP.P AUG abs> 41.5500 1.1 0. 14 ^RECOVERY 103.9 FVOL 0 ' PE BATCH NUMBER 1 BURN 1 0.816 BURN a 0.818 TUBEt 18 SAMPLE CCB 1 09/85/96 1 140 GLASS!. IVOL/WT 0 AUG < ppfo) JCRPJP AUG abs 0.8400 99.9 0.001 FVOL ..DF BATCH NUMBER 01 BURN 1 BURN 8 0.000 0- 008 TUBE s SAMPLE PBM P^>uu 13 09/8S/96 8.1. s 43 ULfiiii 3TWL/UT ** 100 fl_V GJLQ.B.!.?JL X"' 'iTssii' XRPI> IiTT AUG_ "'.004 FVPy DF BATCH HUMBER 100 i 968691036001 auSiLi.. our<H r> r<R r j d -0.004 --0. 0(33 17 5 DUP050307941 KUN Nil'll: !. V-.,jWi I `AUb s 3 AMALYSfs 66 T ; ?. n SAHPUE. 'PI,W 89/25/96 21 : 46 OlAStfl - IWQL/UT. :1.08 r.MNKvl ) I - iv .. INSTRUMENT IDs W260.i or Aft f l e me n rt l E.VOL, PF..... ; k 5 ... ; er . 1 mi 1 962691056001 ftVG(pQta) -%mP ft.VB..JibJL 20.2200 a.4 .Ha BURN_J,. ' By.SEL.ii 8.100 0.112 J6RECOVERY " '103-1. TS^BEs 15 s mir u e . LLSW 09/25/96 21 i:58 feu^s*imzEMVfXik JD_ BMCH...MUMBER. >:<>*1 1 1 9626910516001 ;l aLii.iaE.tei... mts. G2SLJ&&. 50.9300 3.7 8-258 v.............................................................. ............ ............ TUBE". 1& smvZe L(;3W 89/25/96 21353 GJLfif4i im/W.I . **** :L QURW 1 8JML3. 8fi` BE' 8.257 0.244 ___ ___ 'Em, JHL. 1 1 902091050001 ftvs < ppb) 70.4900 mm. ffifflLafea. 1.4 0.325 BUfflUL 0.322 . 8.326 ^RECOVERY - 97.6 17 09725/96 21s 56 PljBELi*. 3VQL/WT 3-'3 180 WGtppb) *r p p . A VP..4b:i "0.3200 93.4 -0.081 FVGL F... Mlfib ..NUMBER 100 1 962691056001 BURfcLl S.y.iMJl-' SR RE -0.002 0.000 ___ ___ 16 9/25/96 22s08 5 ,k .66 I.WL7WI f v g l ,,p__ mrjPJLMUSmBi U>; ".>: >:A* .100 100 1 962691056001 AMG l R.pb.>... %RPD ftVG,,AM. 19.6900 12.5 .107 BURN..1. 0.097' BURtLlt 0.116 i* RECOVERY * 96. 4 TUBES 19 '09/25/96 22::03 SAMPLE ClARR JVOL/WT 2565279 J>->: -j : -j : -i: -} -i: / T\vof\3.`b > 180 v aVGjEabl. XRRD -0.5600 99.9 -0.802 FVpL., JOF. BATCH.. NUMBER. 180 1. 962691056081 UmjL M1J1- SR Sfi. 0.001 "0.086 RUN HAME s 9687081F81 PAGE* A ANALYST tf 66 LANCASTER LABORATORIES INSTRUMENT IDs 62803 ' GEAA ElEMENT 4 TL TUBE;: .20 ' 09/25/96 2S: 07 SAMPLE Cl ASS IVQl/WT 2585273 Jv k k k k A* n\(LA3k*b OPv 108 AVG(ppb> /RPO AVG abs 19.1180 5.1 .0.'10a FOOL DF BATCH NUMBER i0 1 '362691056083. BURN 1 0.105 BURN 2 0.098 %RECOVERY 95.6 TUBE s *21 89/25/96 22 s 10 SAMPLE f:i ASli IVPL/UT 2535279 KUK-K /ntLi\svs> 5 188 flUB(ppb) itBPB AVG aib<* ' a s .a300 1.6 " "0.aa9 f vol 188 i>f Bk 5 ; e r 1 968691056803. BURN I. BURN 8 RR RJD . ..aai i.ail TUBEt 28 SAMPLE zzzzzi 09/25/96- 22.114 Cl ASS 1VOL/WT R*-*Rk 0 FVOL _D_ BATCH NUMBER 81 AVG<ppb> /RPB AVG abs 65.3588 0.2 8'. 385 BURN 1 0.386 BURN 2 5.305 /.RECOVERY => MOT APPLICABLE TUBES 23 SAMPLE CCV 2 89/25/516 28s 17 Cl. ASS IVOL/U f "0 AVG < ppb) ZRPO AVG abs 68.9308 0.8 . 0.820 /RECOVERY- = 187.3 FVOL 1>'F BATCH NUMBER 81 BURN 1 8.228 BURN 8 5.219 TUBE s 24 SAMPLE CcB 8 09/85/96 Cl. ASS 228 1VOL/UT 0 AVG < ppb? R.P AVG abs -0.4380 99.9 -0.088 FVOL J)F BATCH NUMBER 0 BURN 1 BURN a -0.007 8.803 TUBE!; 89/85/96 88s83 Cl ASS IVOL/UT Cr\VjT\v 188 AVGJ_Bjg_b>_ /RPO ftvG AlJv. 8.7200 5s.0 0.083 FVOL 1>F BATCH NUMBER 188 .1. 968691056881 BURN 1. BURN 0 RR RB 0.001 0.005 ` ~.......... . DUP050307943 RUN HAUL PAGE 5 ANALYST s 3627001Fl 3 &a TUBE; 86 B9/a.S/96. 22*87 SAMPLE Ft ASS LV!k&X 2385276 ,, . nr.*A* trvOJFKvS k. 100 ftVGiRfefel '*KPP AUG aba S1.0900 2.7 0.115 j RECOVERY 105.4 . (..A NR ASTER - LABORATORIES INSTRUMENT IDs 82603 OF AA ELEMSNfs TL FVOL _J>F_ BATCH NUMBER 100 1'962691056001 BURN 1 0. il-l BURN .7 0. i 17 CUBE 27 SAMP 250X277 09/25/96 22a30 t::|. ASS 1V0L/WT lit AVG(ppb) XRPP A VO at>-* 7 - j.T 3 300 A 7. S' -0. 006 FVOL DF BATCH NUMBER 100 i 962691056001 BURN I. BURN 2 -0.004 -8.000- -RD. (UBC r. 20 09/25/96 22 s 34 SAMPLE SI ASS IVOL/WT. 2505277, >; Alt 'm.eAvti ^ lie AVG <ppb) %t~:P'0- AVG aba- 21.2506 2.6 8. 116 KRECOVERY 106 . 2 TUBE 29 SAMPLE^ 2565276 09/25/96 22 s.>7 Cl. ASS -fVQL/Wi S'4:**:*K* 10 -/ AVG. i p.pb>.. *RPD -(3.4900 99.9 k ail's -0.02 FVOl- 1>F BATCH NUMBER 108 :i , 962691056001 BURN 1 i.iia BURN 2 i.ili FVOL DF BATCH NUMBER 100 1 962691036081 BURN 1. BURN 2 RR RD 0.081 -0.005 ..._........ . TiOBEs 30 SAMPLE 2565276 09/25/96 22 ;46 SI. ASS 1VGL/WT ^4i * * A* 100 AVQ<ppb> gREJ?. AVG -ci fe 16.3780 16.1 8.896 ^RECOVERY 91.6 FVOL DF BATCH NUMBER 1.00 1 962691056001 BURN 1. 0.065 BURN 2 0.107 (P DUP0503 07944 RUN NAMEs 9627801F81 PAGE s .6 ANALYST s 66 LANCA: JlfER LABORATORIES INSTRUMENT IBs 02683 OFAA ELEMENT: TL TUBEs 32 89/25/96 22:47 SAMPLE GLASS. 2565261 Tt\3L3Y-\^ & S WL/WX :t 00 Awpioafei. -imp APS...aM- 19.4380 2.4 0. 184 F,y.OL. _.I)F_ BMCH.....WUJ1BE.R. 100 1 962691056081 BURN 1 0. 103 BMIM !. 0. 106 jSRECBV'ERY 97. a me&x 33 09/25/96 aa s' GGftgS MLJTf . -:: > j : 108 *BE QVL-*M. 32.4 0.001 FVOL 108 s j ml j l 8.001 B0ICJi..!UMBEB. 1 962691056f 001 mmui m ts. 0.000 ke 2555262 09/25/96 22a S'! PlfiSS HfPUKL A 108 ft aytiiaaiii. jssEJt 21.6600 4.2 8.119 RECOVERY = 109.4 f. 188 SftIH,,WUl1BER 1 .962691056001 SUBN....1. 0.123. am..3, .0.115 lUBEi. 3 SAMPLE CSV 3 09/25/96 22s57 GLASS M 0 F.m......p k ...aicH...wm!!iER. 81 flV8.<p.p.b2. &; & aa.g.-&fa&. am_j, ; ; a 42.6980 4.4 0.219 0.212 0.225 *RECOVERY 186.7 TUBES .36 09/25/96 23s08 A sIwgLi. UUB 3 .GJ.ft#. lyOL/WT 0 FOOL BATCH _NU.MiR 81 avGi&EM.. *k e.v.6....kka. ; ; msn-g 0.0500 99.9 0.000 "0.882 0.003 TUBEs 37 09/25/96 23 a03 SAMPLE CLASS iy.PL/WT. 256/5^:63 ;:>n: )::: !:): TM\'LSX'5.V5 180s %RD ay<i.,,..sLLi=. 0.3600 14.4 8. 002 FOOL ..J>F.. BeTCH.,,.WUMBER. 100 1.962691056081 BUlJjLfi R.R RJD 0.002 0.801 __........ ..... . i 79 DUP050307945  i-aii-i k i 'fouiajyll-n I. Pf lblT. i 7 ANALYST t &a TUlifej. 3 09/85/96 83s07- 8HMELE as<*saa3 t y \04s ^5 ^:**:*4;A* 106 QVRABfiM. *BPi> amAks. IS.310 6.9 8.163 ^RECOVERY * 96.6 LANCASTER LABORATOR i Lb INSTRUMENT -ID* B2tiki3 g f Aft e l e me n t : n. FVBk Jit- SfimiJUJIlS 10 1 962691856881 BURN 1 8.100 BURN 2 0.896 IMSLl ssrni asas i'3 09/83/96 83 s 10 u m&l im/wi fwci^oa ******* lee fitffilftfikL *B1> amm -0.4880 99.9 -0.008 EffiL JB_ MmuBWWMS 16)0 1 968691856081 mm...i 8.081 oymji S& -8.004 ..... ; > ..... ke 09/85/96 831:14 CLASH IffiM ,2505804 r.iir.xi:ft* CrxCL^O W\ 10 Ayi3i.RR.bjL j s s e d flm,,.Aka. 1,6.6408 8.0 0.108 ^RECOVERY - 94.8 Bfflk _B_ sanaLjauRusEa 188 1 968691056081 siassuL 0.890 gyiaLa 8.181 TUSEi 41 09/85/96 83s17 k mp l e . CLLSiiii lEHL/wi pm ..BE... WLT.CH_.NUMBER A 856580/ ^ 7 <Y\<X^V> *:**: :*k 188 100 1 968691056081 srsL. 'fty^iaakL *&$& eyfiLAk*. / 0.0608 64.1 0.088 mm-A. mm~Ji m es. 0.800 0.001 lUBEj. 42 89/85/96 83s21 SAMPLE CLflHU 1MI 250580' (v\*uv;-e, W' i;: . i; A : :l 88 AyGiERb).. WRP.D AVG_a.bg, a3.6380 a.a 0.189 3tRECOVERY = 119.2 Em _J>.._ MTje.H_liMWB.gS. . 180 1 968691856801 gyiauL 0.127 %miui 0.131 (UBEs 43 . SAMPLE PBW TZira 89/25/96 83s84 5 k imvwi r. >: >: -i: r.-x 100 y; ayjitM&L *; aye...to 0.6400 99.9 0. 083 "T00 ~.....1 isasiiisi'^ia SMUHJ, WmL& SB BM 0.003 8.000 180 DUP050307946 RUN NAMEt 9&S7kt01F01 PAGEs ft ANALYSTS 6ft TUBES 44 '.'AMPLE PBW ZZZZZZ 09/85/96 23 s 87 CLAGG 1VOL/WT ): * *A* 100 flVG(ppb) X.RPI) AVG aba 23.5400 1.4 . 0.-187 :K RECOVERY 117.7 l,ANCA:>TGA LABORATORIES INSTRUMENT IBs 6HS03 GI-AA ELEMEN t Tl. FVOL OF... BATCH NUMBER 100 1 962691056008 BURN 1 0.129 BURN n 0. 126 $> TUBE; 4E SAM PL I::;. LCSW Z2ZZ22 09/85796 23s3t CL ftS JVOL/WT AVG(cab) *RPD AVG Abs 55.8100 2.6 0.265 FVOL mDF_ BATCH NUMBER . 1 i 962691056008 BURN I. BURN 8 RR RD 0~870 0.260 TUBE s 46 SAMPLE LCSW 09/85/96 83 i 3's Ok AGO . :rvriL/WT -5 ; A->: i AUG(opb5 gtRPO AVG abB 70.9400 4.2 0.327 ^RECOVERY = '78. 6 FVOL 1)F BATCH NUMBER 1 X 968691056808 BURN L 0. 317 BURN 8 0.336 TUBE 5 47 SAMPLE CCV 4 09/85/96 3 s 3ft C::l. AGO T VOL/WT. 8 AVG < cob) ?;r p o AVG a b ft 48.3100 3.8 0. 217 %RECOVERY 105 8 TUBE-. 48 SAMPLE COB 4 89/85/96 83 s 41. t:T. AGO JVOL/WT & AVG <r>bb) AVG aba 8.5300 99.9 0. 002 TUBE: 49 SAMPLE 2585290 09/15/96 2 3 s 4 < :l. AGO IVOL/WT l!: :l 88 V AVG < d n b) %RP AVG aba 0. 86,80 59. 6 0. 804 FVOL OF BATCH NUMBER 81 BURN .1. 0.883 BURN 2 8.8,11 " "" **" -- -- FVOL OF BATCH NUMBER 01 BURN 1 0.084 BURN 2 0.001 * * ............... -- .. .... ~ -- -- -- FVOL OF BATCH NUMBER 180 1 962691056008 BURN 1. BURN 8 RR RO 0.008 . 0. 005 3 181 DU P050307947 Mercury Data DUP050307948 LHNUAU I I::. K L.A.LUk H I UK .i. t... > MERCURY ANALYZER DATA REVIEWED BY: /l/-5A?223 4 j2A ( *} & BATA- FILE NAME* 96P6903.|:*RM RUM NAI'lEs 9686903803 ANALYST ss 683 'INSTRUMENT WO: 05880 ELEMENT: HG 183 DUP050307949 RUM HAHL ':.'o2690.:>iTU,:; PAGE s ;i ANALYS t u 023 TUBE 5 .1 mmp l e S0 09/25/96 17 s 14 ) CL ASS IWt /UJ **** 8 WGiPEb) 0T0000 Intensity 773-. 0 LANLAG (1 h ;.ik h i 1.1 k If-iSl KUMEM't .LUs CV CLEMEN I' UG 1.. . FUPL .0 DF .1 BATCH NUMBER TUBE; 2 SAMPLE S0.2 v 09/25/96 17,; 16 . -Cl. ASS 3 VUL/UiT *** 0 Ay (3 < g_pb_> "078000 I ntei~is.1 ty 20160". 0 FVQL ,B DF 1 BATCH HUMBER TUBEs 3 SAMPLE S0 5 TUBE; A SAMPLE S1.0 09/25/96 17 s 10 Cl ASS :fWL/WT 0 AMG <ppb) 0.5008 Intensity . 54192.0 09/25/96 :i.7f;n CL ASS J'gOL/WT 0 1.8088' *"l033&T. 0 FVGL 0 FVOL '0 E>F BATCH HUMBEK 1 DF . ; k 5 HUMBER 1 TUBE s 5 SAMPLE S 2.5 09/25/96 17s 23 CL ASS 3V0L/WT -KKttW3C4* 0 AUG<ppb) a.5000 Intensity 249425.0 FVOL 8 DF 1 BATCH NUMBER TUBE;; 6 . SAMPLE S5.0 09/25/96 17s 26 CLASS If VOL /UTI **** 0 AUG < ppb) 5.0000 I nteytsi ty . A 96 2 96.0 FVOL '0 DF 1 BATCH HUMBER Sorrel ation Coefficient -- 0.99996; TUBE: s kmp l e : :tcv 7 . 09/25/96 17s26 C-L ASS :i VC'L/UT K--KKHXK-K- ^ FVOL DF BATCH HUM BELL' s j~*; I i AVG <ppb> 2.0408 Intensity 20424,7.0 JiRECOVERY 102.0 18 DUP050307950 RUN NAME:; 968 69031'l03 PAGE s ANALYSTS 083 TUBE s 0 SAMPLE ICB 09/85/96 17 s 31 Cl. ASS 3 VOI. /WT *#*** 0 AVO(o p b> "-0.0170- Intensity 539.0 FVOL 0 i.AACAS i i .Au k A i'QK INSTRUMENT IDs US5 CV ELEMENT : PIG DP BATCH NUMBER 1 TUBEs 9 SAMPLE CHA 09/85/96 I?a33 *, Cl. ASS :i VOI. /WT 0 AVGdaDb) 0.1900 Intensity 81058.0 FVQL 0 DP 1 BATCH NUMBER TUBE! 10 SAMPLE cdv I TUBE s 11 SAMPLE CCB 1 09/85/96 17 a.B5 Cl. AGO :i VOL/WT * * 0- PVOL 8 DP 3. BATCH NUMBER AVG (pi)b>, 1. 040 Intensity 105717.0 . ^RECOVERY = 104.0 09/85/96 17 s 30 CLASS . 3VOL/WT tt **** 0 - FVQL 0 DP 1 BATCH NUMBER AVG<ob> -0.0880 Intensity 889. 0 TUBES SAMPLE PBW y7 18 . ZZZ2ZZ 89/85/96 Cl ASS x AVG<nb> . 0.0100 . 17.: 40 :i VOL/WT 0 Intwn-i. L by 3816.0 FVQL 6 DP 1 BATCH NUMBER 968600081001 !]sl 0 TUBE; SAMPLE LCSW" 13 Z22222 09/85/96 17.: 48 Cl. ACC k -k >:)( 1VOL/WT 3 AVG <ppb> 0.OB80 Jtvvton-vi.j^^ 01088.0 FVOL I DP i BATCH NUMBER 9 6& 6 0 8O 810 01 R TUBE s 14 SAMPLE 8503805 09/85/96 17a 45 Cl. ft SO avai/wT flVG ( ppb > -0.008" I nten-ai By 8000.' 0 FVQL o DP T BATCH NUMBER 9686O0081001 18& BJB. DUP050307951 UUW t'll-irtl:.. k s ANALYST s 623 TUBE; 15 SAMPLE 2563206 89/25/96 1? s 47 5 :l k iv o l /u t ::-x -Ki: C. F VOL & I .Mi'll I I , I .1'. ' I l.A, .1 l l I.. , . I im; i r u mu i-i i :i. d s w . i i OV ELEMEHi : ilC DF A BATCH HUMBER 9 6 2 6 6 86 2 1 00 5. &.0068 Inberm i by 2767.0 ijci< R0 TUBE; 16 SAMPLE &S&3BB7 'ZZZZ2 x 09/25/96 17-.! 4 9 Cl. ASS JVCU./WT . ****)! 6, AVG < pb) 8 ..011 Int.isi by 3S43.0 FVDL 8 DF 1 BATCH NUMBER 962668621801 HR RD TUBES 17 SAMPLE asasaec 09/215/96 17k St CLASS TVOL/WT :i h k j : '{?. FVDL a DF 1 BATCH NUMBER 962660621001 AUG <p 13la) ' -.Wees In bensi. fay 2670.0 AD TUBE s 16 SAMPLE 2563289 89/25/96- 17 s 5 -"i --' Cl. ASS IVOL/WT (.!** 6 V AVG < ppb) In L>-;rri L fay "0.0030 2494.0 F VOL DF 81 BATCH HUMBER 962660621001 HR RD TUBE; .1.9 89/25/96 17 8 56 SAMPLE 2563209 ZZZZZZ Cl. ASS *** TVPL /WT AUG(BPb) 8.0040 In~bem> 1 fay ~2631.0 FVQL a DF. i BATCH. NUMBEft 96&&M&Iwr r<K RD TUBE s 20 SAMPLE 09/25/96 1756 Cl. ASS 1 VCil. /WT ZZZZZZ K*'**k * 6 AVG(ppb? 1.8900 I n faevri-i. fay 118152.0 FVOL . 8 DF 1 BATCH -HUMBER 962680621081 XX KjO 1 8--................ - - * DUP050307952 RUN NAME s '*>269031103 PAGEm 4 ANALYST: 623 TUBES 21 SAMPLE 256321 0 09/2 5/96 16 00 772ZZ2 CL ASS :k >'.::>: 1V0L/WT r-. flUB < ii'Db) "'(3.0170 Ini;T?n-.v i. fry 3666. (3 I.HMEH'i I Li'-' L.; BHh I UL-.I6.. INsTRlMnbM i I i)0p2i:.:u CV ELEMENT : HC FVOL 6 I?I1 BATCH NUMBER 9t2ett06c*l00l ;<:< r d TUBE s 22 SAMPLE CCV 2 TUBE: 3 SAMPLE COB 2 09/25/96 16:103 CLASS i VOL./WT #*####* 0 FVOL 8 I)F 1 1 BATCH NUMBER AVG <jepb> 1.05(30 Intensity 186169.0 JfiRECGVERY " 105.0 : 09/25/96 16:05 Ci. ASS 3 VOL /WT 0 FVOL 8 DF 1 BATCH NUMBER AVG (opb) ' 0.0260 Intensity -616.0 TUBES 24 SAMPLE ZZZZZZ 89/25/96 16;: 87 CL ASS **** :i VOL/UIT a ftVG(DDb) 0.0(390 Intensity 3866.0 FVOL 6 BF 1 BATCH HUMBER 96 2668621001 !<>< RD TUBE s 25 SAMPLE 2563624 09/25/96 16 ;09 Cl. ASS . I VOL /U)T *** 6 FVOL 6 BF 1 BATCH NUMBER 962668621001 AVG<PPb) 0.0810 In ten stty ~2252."0 RD TUBE; 6 SAMPLE 2563625 '.ch 09/25/96 16:: 12 CL ft SC :i VOL /NT M * & ftVG<PPb> 8. (301 I Ti ben-.ri. fry 2263.8 FVOL 6 BF 1 BATCH NUMBER 962660621001 RB TUBES 27 ' SAMPLE asaiaifc ZZZZZZ 89/25/96 16:: 1. '; ' CL_ASC- i VOI. /NT ** e flVG < ppb> -0.018 .t?itfc'n->L by ' 2879.8 FVOL 6 BF 1 BATCH NUMBER 962668621081. R.D nr O DUP050307953 h u h Hunts ut.c'&yu.Ji'U-'ju PAGE 3 u ANALYSTS 823 TUBE;; 28 SAMPLE 2583827 T 89/25/96 18; 16 C:|, ASS 1 V01./WT K']i*KB 6 AVGfppb). 0.B030 Int^n-ilLy , 2486.0 u-mi,H .. t; !; i i iUr;i-i u r o. . INSTRUMENT .1 i.) ; E;.r.>22w CV 1 !IG FVOL 6 PF 1 BATCH NUMBER 962680821001 5 r RD TUBE s 29 s kmp l e : PBW " 09/25/96 18a 10 ci. k sc ivcn. /w t .***** 6 f vol 8 pf 1 ItftTCH HUMBER 9626&W8212 AVG < ppb) 0. 0000 In b >->i by 2237.0 RR KD TUBE: 30 SAMPLE LCSW 9/25/96 13 a 21 CL ACC :t VOL/WT '7-da . -ic-x-Ji 1 flVG <ppb) 1.070 In i. by 108785.0 FV0L 1 1)F 1 BATCH NUMBER 962680821002 i'<D TUBE: 31 SAMPLE 2583222 ZIZZZZ 09/25/96 18a23 CL ft5:':S3 T VOI../WT AVGfppb) 0.0030 Inberr-i i'ty 2489.0 FVOL 8 I)F BATCH NUMBER 1 962680821002 i<i< RD A TUBE: 32 09/25/96 182 5 SAMPLE Cl. ACC - :r VOL/WT FVOL DF BATCH NUMBER 2583223 , " ' ^ ^ ; 6 8 1 96268082 i 0 0 2 AVG i ppb) 0T0010 Inb:?tvi by 2244.0 RR RD TUBE s 33 SAMPLE 2583224 / ..... . 09/25/96 10,! 27 CL ACC 3 VOL/WT >; 8 AVG<pb> 0.0070 Iriby 2908.0 FVOL 8 DF 1 BATCH NUMBER 962680821002 r r< R i) DUP050307954 RUN NAME!, PACE : (. ANALYSTS iit- i> LHHI..H.J 1 '..is ! UKJ 1 l'l S 1' K U M E N i 1 P : b ... L CV f : UC TUBE; 34 SAMPLE CCV 3? " 09/25/96 16s 30 CL ASS TVOL/WT **(( ** 0 FVOL 8 DF 1 BATCH NUMBER AVG<&pb> 0.9660 Intensity 98844.8 ^RECOVERY = 96. 6 TUBES 35 SAMPLE CCB~ 3 89/25/96 18 s'32 Cl. ASS I VOL. /WT #**** .......... ..... .8 FVOL 0 l>F 1 BATCH HUMBER AVG(pb> Intensity t -8.8310 -870.0 TUBITs 36 SAMPLE. 2563225- 2ZZZZ2E 89/25/96 18 a 34 CL. ASS J VQL/WT ******** 6 FVOL 8 DF 1 BATCH HUMBER 962660821(302 flVGXppb) 0.0470' I-nbiansvby 6853.0 hr ko TUBES 37 SAMPLE 2583226 Z2ZZZI 09/25/96 la.i.T? CL ASS T VOL / WT UM-K -KM 8 i/ AVGippb) `-0.0010 Int^n-i i. by 2096.0 FVOL 8 DF i BATCH HUMBER 96268082 A W02 t i R i) TUBES 36 SAMPLE 2563226 09/25/96 1839 . CLASS IVOL/WT !> )( ft>1-KICK ft AVG(iipb) 8,,0838 Infceivi i fcy 2487.0 FVOL 8 * DF '1 BATCH NUMBER 9 >2660621002 RR RD TUBES 39 SAMPLE 2563226 <LL 09/25/96. 16 a 41 ci. ASS TVOL/WT RX-KKXXK ft */ <y AVG(nob) 1.0680 Irtten-Ai. by 107281.0 TUBES 40 SAMPLE 2583227 % 09/25/96 18.14 4 .CLASP TV01. /NT ::k s :x --x ft AVG (pub) ' -0.0(310 Xnbiaival by 2128.0 FVOL 8 FVOL ft DF .1 BATCH NUMBER HR RD DF 1 BATCH NUMBER j o '. 962680821602 X O - RR R t) DUP050307955 KUM NAME; 962698008.:! PAGE s ANALYST s 823 TUBES 41 09/25/96 18s 46 SAMPLE Cl. ACC J MOL. /WT 2583830 V7ZZZZ **** 6 AMO < ppb? &7&&70 Inb^n-vi. by -8698. 0 . FMOL 8 i..h N k :> i ;_R .h o Rm i u>; INSTRUMENT IBs 05; CM ELEMENT: HG 1>F 1 BATCH NUMBER 962680821862 ( ::< RD TUBE s 4 <2 SAMPLE 2583831 ~Z.Z 09/25/96 18u48 CM. ASS 3 MOL /UT a AMO < ppb) ' a.0070 InteiwL by 2&51.B ryo l a i:>r i BATCH NUMBER 36268882 I 882 Ry TUBEs 43 ; 09/25/96 18 .: 5 SAMPLE ... T--y)- CL ASS I MOL /UT ff MOL i>F BATCH HUMBER ^ asa3~a3e ** a . a i 962680821002 M AMO(ppb) In tens i. by 0. 0030' "2466.0 {<i< F<J> TUBE 44 SAMPLE 2583833 ZZZZZZ 09/25/96 t::i k 13;: 53 .1 MOL /UT 8 . FMOL '8 DF 1 BATCH NUMBER 9626888 21002 :/ AMG<BBb) 0.0068 A In benwL by 2826.8. RR RB TUBE45 SAMPLE 2583634 ZZZZZZ 89/25/96 :L 8 55 CL AOS :i MOL /WT Kw:KMi 8 FMOL a I>F 1 BATCH NUMBER 962680881882 AM(3<srj'b> 0.0030 I Vi ben-it'i. by ~2469 7(3 31 *' Ks 0 TUBE? 46 SAMPLE COM 4 09/25/96 10557 CL ASS *** IMOI. /UT 0 F'MOL 0 Pi1 BATCH NUMBER ... ..... t u; e a SAMPLE CCB 4 47 AVO < peJ:j )_ 1.0300 In bensi t^1049107(3- ' 09/25/96 IS;59 Ct ASS: I MOL /UT Si-** * > 0 JiRECOVERY * 103.0 FMOL 0 _J>F_ 1 BATCH NUMBER ....... .. ............ 19^ X AVOjCjgjgJb^ -0.0290 In-tensity -682.0 DUP050307956 RUN W Ail El: 368 6O03M03 PAUL; 6 ANALYSTs 623 TUBES 46 SAMPLE PBW P7-,^ 09/85/96 . 19a08 CLASS :r vcu /w t ft } 'S(-,'K )( {I "! : .6 AVO <, ppb) 0. BBS" 1 i. by 2969.. 8 FVOL a LANCASTER l ABRA'I UR.I.L' 1MSIRUWL Wi IDs 0388 fe> CV ELLHENi . HC DF 1 BATCH NUMBER 968660681003 RD TUBE s 49 SAMPLE LCSW 09/85/96 :1.9 r. 0 4 CLASS ;r veil, /w t . k k k ih u m: ;i FVOL 1 s/ AVG Cob> 1.0500 Inliwiity 106676.8 DF 1 BATCH HUMBER 96866068100 3 iif< RD TUBEs 58 SAMPLE. 2565276 rrse^O 09/85/36. 19 a 06 ~ Cl ASS JVPl, /WT #** a FVOL .a DF -BATCH NUMBER i 968668621003 V jauo (ppb) 1-Q.feki'LiXtX. 8.. 8008 2145.0 RA HD TUB lii s 31 SAMPLE 8305277 ^ O, 89/83/36 19 r 80 Cl. ASS TVOI./WT y. X AVG < ppb) @.0080 lyybieiViti by 8396.0 FVQL a DF i BATCH NUMBER 968&&8aai003 RD JUBE: SAMPLE 505870 83/85/36 10,1.11 CL ASS IVCU. /WT *** ** 6 FVOL DF 01 BATCH HUMBER 968660081883 AUG < ppb) 0.0878 Ivi Lir>rr>l by 2 8 4 0.0 RR RD TUBE; 53 09/25/96 19.il 3 SAMPLE . CLASS JVPL /LIT 8565879 \fr\^X\'7_S U ->:* ,6 AVG <ppb) 0.0070 2669.0 FVOL 6 DF 1 BATCH NUMBER 968660621003 RD i9l DUP050307957 kuh t u^a69B3MU3 k s 9 ANALYST: 623 . TUBE: 54 SAMPLE 2505279 09/25/96 19 s IS CLASS Ji UPL /WT IHcxx-` 6 C* AUG(ppb) 0.0140 In b=.nwi. by 3604.0 FUOL a i.h h i h *> i 1... R '-.-isH I i. ;i. H O 11: U M E N I .i: D '. w;. 2 11 CV CLEMEN f ; MG DF i BATCH...NUMBER '96266002:1003 HR RD TUBE s 55 SAMPLE 2565279 fiTNG.Pia-tE 09/25/96 19-s 1ft ci. k :i u o l /u t Rh >( 6 FUDL a DF 1 BATCH NUMBER 962660621003 U/ ^ is AUG <ppb> ~ 1..J.100 Inbiv*i by .112402.0 RD TUBE: 56 SAMPLE 256526.1 09/213/96 19a 2 Cl. ASS TUPI. /WT : : 6 AUG<pob) 0.0020 Inbwa.i. by 2364.0 FUOL .6 DF 1 BATCH NUMBER 962660621003 RR RI> TUBE: 57 SAMPLE A 2565262 09/25/96 19;; 22 CLASS iiUOL/WT * a aFUDL DF 1 BATCH NUMBER 962660621003 Au AUG <ppb) . 0."aTi InL-->iii-:ri. 'ey 23ia.0 r<r< r d TUBE: 56 SAMPLE CCU 5 TUBE a 59 SAMPLE CCB ~S 09/25/96 19 a 25 CL ASS :i'UOL/WT :;* xx-)( B. FUOL 0 DF 1 BATCH NUMBER AUG <ppb> 1.0300 In-bens! 103994.0 ^RECOVERY = 1B3.B 09/25/96 19 s37 Cl. ASS IVCU /UT ** ' 0 AUG < ppb) -0.0290' lyrbenisl'by -662. 0 FUOL DF_ .' 0 1 BATCH NUMBER TUBE: 60 SAMPL.E ssaseaa 09/25/96 19 ;; 29 Cl. ASS :i WL/WT "**** * u AUG topb) Ill.fei-J.LiLii'X 0.0060 2736.0 FUOL 6 Dl1 BA_TCH NUMBER 96266062100^ $ RD DUP050307958 RUM -Mi'll'lt.: 9626903M03 PAUEs. .i Ei ANALYSTS 583 Uygil* 61 gAMPLE 25852S4 09/25/96 19s 32 C:[,,ASS ` IVOL/WT *** " "7{ FVQL S I.BMCMC J EH I .AURA Ji.iR l INSTRUMENT lu: WL-Ji-S./.W OV EL.EMEM r: MG PF. 1 BATCH HUMBER 9&2650 62i0W 3 AVG(ppb) (3,, 01.10 gTvbetvvLfey 3856-0 RH KB TUBEs 62 SAMPLE 2565265 09/25/96 1.9 4 3-i CLASS 1 VOL /WT '** 6 FVQL. 6 PK 1 BATCH...HUHBER 968660681003 AVG <ppb) iTaass In bow*i by "27010 HR Ri) TUBE a 63 SAMPLE CCV 6 89/25/96 19s36 Cl. ASS 1 'v'CU. /UT FVQL 0 PF 1 BATCH NUMBER. AVjGjCpjjfe). 1-0208 Intensity ""103422. 0 ^RECOVERY 102.0 TUBEs 64 k : CCB 6 ' 89/25/96. 19s38, Cl ASS x*kxx-xx I VOL/WT 8 AUG <ppb> "- 0. 03.1.8 Intensity -a40.0 F VOL .0 1) F 1 BATCH NUMBER - DATA REVIEWED BYs A/MFJ13_____9/ ie': DUPO 50307959 Extraction/Distillation/Digestion Logs i94 DUP050307960 Water Digestion Logbook ICP-20 1151 Rev. 08/22ft5 DUP050307961 196 DUP050307962 Analysis #0821 Water Digestion Logbook 4VH U -Hill- 3> 19' DUP050307963 Chain-of-Custody Record 19 DUP050307964 DUP050307965 DUP050307966 5 2J25 NnrrtDJant) P&t lr>Ct FA I7601-59S4 Sample Administration Receipt Documentation Log %(e> 0-5%-ttt!--l5 ' CI!ent/Pro]ect: _ Date of Receipt: Time of Receipt: Source Code: MO CO Lb-bO Co-i COC SealC Presents/ Not Present on cooler Brofcer^/J^iSt^ Package: Not Chilted Unpacker Emp. No.: 2(b ______________ Temperature of Samples Thermometer ID: #1 i(!)i(Xb Thermometer ID: #2 Corrected Temo.: pottle Wet lcV Dry `Ice / Ice Packs Ice Present?d'Y\/ N "i #3 Thermometer ID: Corrected Temo.: Bottle / Air Wet ice / Dry ice / Ice Packs Ice Present? Y / N Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N #4 Thermometer ID: Corrected Temp.: Bottle / Air Wet ice / Dry Ice / Ice Packs Ice Present? Y / N Paperwork Discrepancy/Unpacking Problems: ............... Name ---------------- Sample*Administration Chain of Custody Date Time KOf mo Reason for Transfer Unpacking ____ Place in Storage or Q Entry/ ( Remove from Storage Place in Storage or Entry Entry 201 Rev. 2174 09/09/96 DUP050307967 Lancaster Laboratories 'ft New HoHind le UneiiBifiMJ<0M9M Sample Administration Receipt Documentation Log it Client/Project: _ Date of Receipt: Time of Receipt: Source Code: A/OCO |4fa icr&o CoA COC Seal^ Presents/ Not Present on cooler Broker Package: ChiHeo* Not Chilled Unpacker Emp. No.: 2(os Thermometer ID: Corrected Temp.: #1 i&tiXS 1 a ^Bottle Wet icgV Dry;lce / Ice Packs Ice PresentX^Vy/ N #3 Thermometer ID: Corrected Temp.: Bottle / Air Wet ice / Dry Ice / Ice Packs Ice Present? Y / N Temperature of Samples #2 Thermometer ID: Corrected Temp.: Bottle / Air Wet Ice / Dry Ice / Ice Packs Ice Present? Y / N #4 Thermometer ID: Corrected Temp.: . Bottle / Air Wet Ice / Dry Ice / ice Packs ice Present? Y / N Paperwork Discrepancy/Unpacking Problems: ________________ t .V Name "cr Sample Administration Chain of Custody Date Time Reason for Transfer __ IMhi..... 1(0*1 /aoo Unpacking Place in Storage or Entry* ( Remove from Storage Place in Storage or Entry . Entry Rev. 2174 09/09/96 20 ;o DUP050307968 ^Lancaster Laboratories 3425 Nfw Holland PikeLancaster. I7$0t-59?W Locked Storage Chain of Custody Original Sample Client/Project: Preservative: 4'(AJ/r)% Sample # Range of Entry Group: Utf (Z A jfVladfeirvT. Matrix: IV UJ SDG: fl4lb <93 Bottle Type: gOSnd? Sample Numbers! Released Received Date of Time of in Custody By ..B.y---a. Transfer Transfer ^kraM sST pn Stacos^ n6) n^d w \*P . 330 pjm $&3 f^A )9-50 9l23j% 0500 S/asA 0515- /53b Oyi&SMt, *h*f $2-3 %!u U &i7 m ~Y* <-v- sizfa e/jiL^r 0(jrlO Reason for Change of Custody 3bra^f-' Ciuefc J Dist., Extr., or Digest Chain Created (X) *orr --<N-5S~ ^ T&'-/?zZt' 9-3S^ w\^ - . 2QB 2016 Rev. 09/05/95 _Lf _i Page DUP0503 07969 ant^ster Laboratories >USIwMoiinrfPa*UnBistJ 17601-5994 Locked Storage Chain of Custody Metals Client/Proj/eecctt: ~~V R^-v ~V Sample#: o --.\~ Digest Type (circle one}: Hg etatsj'' GF Hydrides SDG: F^-vvv^ ~^rrS Trial No: (If not 1, fill in) Batch No: o. ~L-. Lo J5. 7_ c> ril Sample Number(s) in Custody ^ ~ V5 Released By '~~7* 21-SS <3SSS-1R- 51-SS .......... ` 1 CPsttnaoe . 'T'lUnwlU C Wr Received By Date of Transfer tiJ/irrar^....... . --r~. " <{ * LtrwlllC- J Time of Reason for Change Transfer of Custody fb:/> 'iffLv&h/ |1QS 17*15 \Cfa/ioJU^4 J \cP3morf~^ % 2231 Rev. 09/21/95 204 Page _J__ of _2 DUP050307970 F ^25NewHcA^^*Uneaftcr.Ml760l'S994 Locked Storage Chain of Custody Metals Client/Project: Sample#: Digest Type (circle one): Hg 5 *t w . "jr __________ Metals (j GF^ Hydrides ____________________ SDG: _J^rri^) 3^ Trial No: ____ (If not 1, fill in) Batch No: 6- 2_ <r> 9l . \ H w1 in. fMp'- Sample Numberfs) in Custody =2S&S-2~?C ~ ?? Released By -y *?&.*&^LtxfZSrf Date of Time of Reason for Change Received By Transfer Transfer of Custody /5-`^ A^ert /^tza.^Jl i5?J? zsfr<. *3Lzdefr3 Sr/-'SrS-' | ^oSQ^'T^, ^-"aS ZStOTOr cu */) V Ak^i . * ..... //o { ^sw*. 4-ZScWe 19:19 9ZS-% IS`.20 >4k .iLv \ .o t 4s u Shv/jg Jfcj < 9 dJLj He'.bb . AtLcuLjfaA00___ ZVzfoS&k'&i'*1'** 25a-5ru,,-'R .su-is Z^znu-Tt 2^S2%\ 4k qon.v-&5 5U<O3ff..V OJvp ( ^iLL/aS* A4sw*,~, ^S^rva*.^ C\A ^-1^% iyio l`S4& 19-M9 ^VtsVc^ 2Sxi AYz&tet, 23>C3S ^ist-sx. 25to Ja -' >4y\eJL^~l~T\ <2'Wv*Cl _0 P ykjc 6 A^a.JL>-*tjcv /^`b 6 Afl- AshuJUffi** 1b 26.<fe7A\. H.VT& ^ItSlSL 2-to SCfl-laoSL. ,q A Jsvsn\o--vk<i\ -as &vsni0--a,<U-'K> ' Q\luVvv. O4co ^Vl u VX rwi<r 'w**' < **> At)^j Z.(/X 2231 Rev. OS/21/95 Page 1 of ~7- DUP050307971 /In . i angaster Laboratories Mjf Ssv-hot j t - u*t-twovsss- Locked Storage Chain of Custody Metals .lient/Project: ^~V YOrA- VtQ^vCbf'!^ Sample #: 7m S2~k.-~iq Xt-is Digest Type (circle one): Hg Metals Hydrides s d g : VrftbQz* Trial No: lf (If not 1, fill in) Batch No: miziUq ! O 3 (o o o _lL_ Sample Number(s) in Custody 73LST7L Released By Received By AA ............................... --e. W"ter* cX 23\^)ZlL fi A^SW^ Date of Transfer tfZ&frL Time of Reason for Change Transfer of Custody o4h Jn*64du,i*> ~S o h q <t ' +2y&t#jrf itf'iQ- s2-x-yr /I i 2*s- SZ-X'T? A &/ ~^<r" *%/*^<r RHSTC T^sa-si C Jmc L** 144. J ^ JULJsA CStZV'tt-fy*- 10.1** %Tb'fib 1^.30 (-TU-He ZZ-Z3 %U>3b a?', id S5 . 1 5Wkk , A-4 yW ra3iuriLi $<-- | (ji SWo^ .*44 l&&Cf\xXL J ftA 5 n ^VertfiLs^_j 2fS52.7T.T7 ' Info CftS5 O' ' , tot Olio I <r f IL... .. 2231 Rev. 09/21/95 JtfUt- Page of ~2- DUP050307972 Alancaster Laboratories 5 s Hodjriti f*ke uncajten PA 17601.5994 Locked Storage Chain of Custody Metals Client/Project: p 2$ -- 2?^ paLi 4 F&r'4 Sample #: 9 ST Digest Type (circle oneU^HeJ Metals GF Hydrides SDG: Thai No: (if not 1, fid in) Batch No: c 6$ 3 Sample Number(s) in Custody SLSfFXI i - 7 f %<T2 S'fLZt 2.-Z8 S2r7fc-Tl Z-SSS2-81 -8% iU-B$-x7> - 7* 0.C9 rJL&t - FS s Released By ftf Received By Date of Time of Reason for Change Transfer Transfer of Custody &P2l <9& %*}% SU>> 07 2>o 8 SL^ / >2? 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