Document rDRZ9neR8rLVKeyw3VMV6KYv
8^920 - R2273 (RUN 03/09/92 ^PKOdCqf: PREQUALIFICATION . BRANCH/SUBMITTER: 015200
JOHN WILSON
PRE1' 'LIFICATION EVALUATION - ENVIROSYSTr GENERATOR SURVEY
* REVISED *
n*.
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
safcrq-HieeQ.
ACCEPT
CONTROL # LAB #
SURVEY #
0000122549-3
0000030083-2 0000260239
CUSTOMER INFORMATION: 0000-60-2789
PPG INDUSTRIES INC COLUMBIA SOUTHERN RD WEST LAKE
ATTN: GERALD L PERRY
LA 70664
FEDERAL EPA ID: LAD008086506 STATE EPA 10:
SALESPERSON: JOHN WILSON
GENERATOR: PPG INDUSTRIES
NATURE OF BUSINESS: CHEMICAL MANUFACTURE
S.I.C. NO:
FEDERAL EPA ID: LAD008086506 IL:
MO: ST: ID:
STATUS: LOG
FACILITY ADDRESS:
BILLING: FOR MANIFEST
COLUMBIA SOUTHERN RD
PO BOX 100O
WESTLAKE
LA 70669
LAKE CHARLES
LA 70602 - 1000
GENERAL DESCRIPTION WASTE OIL
PROCESS DESCRIPTION TRANSFORMER MANTENANCE
GENERATION AMOUNT
5000 GALLONS PER YEAR
AMOUNT ON HAND
100 IN BULK
SHIPPING FREQUENCY OTRLY
IN BULK
A. COLOR ^.AYERS OR PHASES
BROWN ONE
PCT SOLIDS NOT SAMPLED: PHYSICAL STATE LIQUID VISCOSITY: LOW
PH RANGE:
4-10
WPTCRIAL COMPOSITION: VOL%
CODE MAX TYPICAL
OIL. PETROLEUM
0 100.00
ATTACHMENTS NONE
RESTRICTED SUBSTANCES T5CA REGULATED MATERIAL
IDENTIFY PCBS <1OPPM
HAZARD CLASS
NUMBER.
NEED ASSISTANCE
EPA WASTE DESCRIPTION AND TREATMENT STANDARDS: RCRA HAZARDOUS WASTE: NOT SURE
P.O. NO:
TYPE OF SAMPLE: GRAB
* OF DRUMS SAMPLED
1 TAKEN BY: CUSTOMER
NAME: GERALD L PERRY
TITLE: ENV CONTROL SPECIALIST
11/26/1991
(318) 491-4370
COMMENTS: L*30083-2
REVISION: 03/09/1992 13:04 NANCY DROUGAS L0CAT0R2 FR-
TO: 0000602789'
CORPORATE REVIEWS: DISPOSITION REVIEWER DATE
TECHNICAL:
ACCEPT
AAD
12/18/91
P05SIBLE FACILITIES:
PRICING CODE. F7
REGULATORY:
ACCEPT
JHP
12/18/91
658
642
610
____________ OPERATING:
ACCEPT_______ uWH
12/18/91
APPROVED FACILITIES:
(658) SAFETY-KLEEN CORP (642) SAFETY-KLEEN CORP (610) BRESLUBE
STATE HWY 146
581 MILLIKEN OR SE
601 RILEY ROAD
NEW CASTLE KY 40050 FED EPA# KYD053348108 STATE EPA#
HEBRON, OHIO 0HD980S87364
43025
EAST CHICAGO IN 46312 IN0077042034
TELEPHONE 502/845-2453 STATE CODE
614/929-3532
219/397-1131
APPROVD 0001073 DRUM OR BULK
DOT-EPA WASTE OIL
DESC.
(NOT USDOT HAZARDOUS MATERIAL)
0000777 NOT FOR MANIFEST PROPER SHIPPING DESCRIPTION WAS BASED ON THIS SINGLE ANALYSIS. GENERATOR MUST
EPA WASTE CODES NONE
CERTIFY THAT SHIPMENT IS NOT HAZARDOUS.
ENTS: OK FOR SKOS WASTE OIL FUEL.
GENERATOR SENT TCLP FOR METALS. NONVOLATILES
THIS SERVES AS NOTICE PER, 40CFR284.12(B), THAT THE FACILITY(IES) NOTED ABOVE HAS THE APPROPRIATE PERMITS AND IS WILLING TO RECEIVE THE MATERIAL DESCRIBED.
021749 SL
V 5-
80920 - R2273 (RUN 03709/92)
BRANCH/SUBMITTER: 015200 JOHN WILSON
PREr LIFICATION EVALUATION - ENVIROSYSTF'"" MATERIAL ANALYSIS
ACCEPT
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
** REVISED * *
PAGE 2 COMPLETED: 12/19/91
REVISED: 03/09/92
s
ACCEPT
CONTROL 0: 0122549-3 SURVEY 0: 260239
GENERAL ANALYSIS OF TOTAL SAMPLE
COLOR
BROWN
WATER CONTENT
< 0.1 WT%
NON-VOLATILE RESIDUE:
98.0 WT'/o DESCRIPTION: OIL
flammability
NO FLASH AT 142 F BY SETAFLASH
FLAMMABILITY
NO FLASH AT 102 F BY SETAFLASH
PH EXTRACT BY METER 6.6
RADIOACTIVITY
NONE DETECTED
COMMENTS: NO FLASH AT 202F
FUEL
EVALUATION OF TOTAL SAMPLE
HEAT CONTENT:
TOTAL BROMINE
BR:
TOTAL FLUORINE
F:
comments, chloride by
19400 BTU/LB < 0.1 WT1/, < 0.1 WT%
tox isppm
ASH UPON COMBUSTION: <
TOTAL CHLORINE CL : <
TOTAL SULFUR
S<
1.0 WT1/ 0.1 WT1/, 0,1 WT1/
METALS CONTENT OF TOTAL SAMPLE
BARIUM (D005) BA :
SILVER (0011) AG. <
CADMIUM (D006) CD : <
NICKEL
NI : <
SELENIUM (DO10) SE : <
ZINC
ZN: <
(PPM): 7
5 1 1 5 1
DIGEST
BY: ICP
IRON
FE:
ARSENIC (D004) AS :
CHROMIUM (D007) CR:
PHOSPHORUS
P:
TITANIUM
TI :
< < < <
7 MAGNESIUM
MG:
5 BERYLLIUM
BE : <
1 MERCURY (D009) HG: <
1 LEAD
(D008) PB : <
1 THALLIUM
TL : <
8 1
5 1 1
GENERAL COMPOSITION:
AQUEOUS PHASE (FREE WATER) .. ORGANIC PHASE (FEEDSTOCK).......... BOTTOM SLUDGE (SEMISOLIDS) BOTTOM SOLID (SETTLED SOLIDS)
SPECIFIC GRAVITY
VISCOSITY (CENTIPOISE)
GENERAL COMPOSITION BY:
CENTRIFUGE APPEARANCE TOTAL
(VOL%)
(VOL%) (WT %)
0.0 0.0 0.0
100.0
100.0
100.0
0.0 0.0
0.0 0.0
0.1i
TOTAL
.890
50 CPS
100.0
100.0
100.0
SPECIFIC COMPOSITION OF TOTAL SAMPLE
COMPOSITION OF:
TOTAL
SAMPLE
(WT%)
WATER CONTENT.........................................................................
0.1
NON-VOLATILE RESIDUE
DESCRIPTION: OIL.................................................................... 98.0
VOLATILE ORGANICS BY DIFFERENCE.....................................................................................................................
1.9
TOTAL
SAMPLE (WT%) 0.1
98.0 1,9
TOTAL
100.0 100.0
VOLATILE ORGANIC COMPOSITION SAMPLE PREPARATION DETECTION METHO0S
COMPOUND NAME TRACES OF VOLATILE ORGANICS
OF TOTAL METHODS:
DETECTED
SAMPLE BY GAS CHROMATOGRAPHY CS2-EXTRACT
FID. FID, MASS-SPEC COMPOSITION OF:
(<1.0% EACH)
CODE CAS NUMBER TR 0-27-1
VOLATILE ORGANICS
(WT%)
100.0
VOLATILE ORGANICS
(WT%)
100.0
TOTAL SAMPLE
(WT%)
19
TOTAL
100.0
100.0
1 .9
SUMMARY OF VOLATILE ORGANIC COMPOSITION BY COMPOUND CHEMICAL CLASS WTV
alcohols
aliphatic hydrocarbons
AROMATICHYDROCARBONS
CHLORINATED SOLVENTS
ESTERS
ETHERS
GLYCOL ETHERS
INHIBITORS
KETONES
NITROGEN COMPOUNDS
SPECIFIC ORGANIC COMPOSITION POLYCHLORINATED BIPHENYLS (PCBS): DETECTED SAFETY-KLEEN REGULATED COMPOUNDS: NONE DETECTED
ADDITIONAL ANALYTICAL INFORMATION: AR1242=4 .35PPM
4 PPM AROCHLOR. 1242
f
CONTINUED ON NEXT PAGE
S0920 - R2273 (RUN 03/09/92)
" . BRANCH/SUBMITTER: 015200
JOHN WILSON
PRE' UIFICATION EVALUATION - ENVIROSYST MATERIAL ANALYSIS
CCE PT
Qvirqsystems fuels PPG INDUSTRIES WASTE OIL
* REVISED * *
PAGE 3
COMPLETED: 12/19/91 REVISED: 03/09/92
ACCEPT
CONTROL rf: 0122549-3 SURVEY #: 260239
LABORATORY REVIEW- A
LEVEL-
SEG CODE:
RELEASED:
LAB REVIEWERS-
AJ AJ
ANALYZED:
PCB'S DETECTED/NVR ESTIMATED BY DIFFERENCE.
12/19/91 12/17/91
TRACKING INFORMATION: SURVEY RECEIVED SAMPLE RECEIVED RESAMPLE SHIPPED RESAMPLE RECEIVED
DATE
FACILITY
12/05/91 SK TECHNICAL CEN
12/05/91
THE ANALYSES CONTAINED HEREIN ARE PERFORMED SOLELY FOR THE PURPOSE OF QUALIFYING THE ANALYZED MATERIALS FOR ACCEPTANCE BY SAFETY-KLEEN IN ACCORDANCE WITH ITS PERMITS AND PROCESSING CAPABILITY.
SL 021751
T0920 - R2273 (RUN 02/05/92 PROJECT: PREQUALIFICATION .BRANCH/SUBMITTER: 015200 JOHN WILSON
PREP*`ALIFICATION EVALUATION - ENVIROSYSTF" GENERATOR SURVEY
CCE P T
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
REVISED *
safeii-meen,
ACCEPT
CONTROL 0: 0000122549-3 LAB 0: 0000030083-2
SURVEY 0: 0000260239
CUSTOMER INFORMATION: 0000-60-2789 -- tc'O
PPG INDUSTRIES INC COLUMBIA SOUTHERN RD WEST LAKE
ATTN: GERALD L PERRY
LA 70664
FEDERAL EPA ID: LAD008086S06 STATE EPA ID:
SALESPERSON: JOHN WILSON
GENERATOR: PPG INDUSTRIES
NATURE OF BUSINESS: CHEMICAL MANUFACTURE
S.I.C. NO:
FEDERAL EPA ID: LAD008086506 IL :
MO: ST: ID:
STATUS: LOG
FACILITY ADDRESS:
BILLING: FOR MANIFEST
COLUMBIA SOUTHERN RD
PO BOX 1000
WESTLAKE GENERAL DESCRIPTION
LA 70669 WASTE OIL
LAKE CHARLES
LA 70602 --1 QOS__________
PROCESS DESCRIPTION TRANSFORMER MANTENANCE
GENERATION AMOUNT
5000 GALLONS PER YEAR
AMOUNT ON HAND
100 IN BULK
SHIPPING FREQUENCY QTRLY
IN BULK
COLOR lAYERS OR PHASES
BROWN
PCT SOLIDS NOT SAMPLED:
ONE_______ PHYSICAL STATE- LIQUID VISCOSITY: LOW
PH RANGE:
4- 10
ERIAL COMPOSITION: VOL%
CODE MAX TYPICAL
ATTACHMENTS NONE
RESTRICTED SUBSTANCES TSCA REGULATED MATERIAL
IDENTIFY PCBS <10PPM
HAZARD CLASS
NUMBER
NEED ASSISTANCE
EPA WASTE DESCRIPTION AND TREATMENT STANDARDS: RCRA HAZARDOUS WASTE: NOT SURE
P.O. NO:
TYPE OF SAMPLE: GRAB
* OF DRUMS SAMPLED:
NAME: GERALD L PERRY
TITLE ENV CONTROL SPECIALIST
11/26/1991
COMMENTS: L*30083-2
1 TAKEN BY: CUSTOMER (318) 491-4370
CORPORATE REVIEWS: TECHNICAL:
REGULATORY: OPERATING-
DISPOSITION REVIEWER
ACCEPT
AAD
ACCEPT
JHP
ACCEPT
JWH
DATE 12/18/91 12/18/91 12/18/91
--
POSSIBLE FACILITIES: 658 642
PRICING CODE: F7
itjoSi 5AFETY-KLEEN CORP STATE HWY 146
NEW CASTLE KY 40050 FED EPA# KYD053348108 STATE EPA# TELEPHONE 502/845-2453 STATE CODE
(642)
SAFETY-KLEEN 581 MILLIKEN HEBRON, OHIO 0HD9S0587364
614/929-3532
CORP DR SE
43025
APPROVD 0001073 DRUM OR BULK
OOT-EPA WASTE OIL
DESC.
(NOT USDOT HAZARDOUS MATERIAL)
COMMENTS: OK FOR WASTE OIL FUEL GENERATOR SENT TCLP FOR METALS,
0000777 NOT FOR MANIFEST PROPER SHIPPING DESCRIPTION WAS BASED ON THIS SINGLE ANALYSIS. GENERATOR MUST CERTIFY THAT SHIPMENT IS NOT HAZARDOUS.
NONVOLATILES
EPA WASTE COOES NONE
THIS SERVES AS NOTICE PER. 40CFR264.12(B), THAT THE FACILITY!IES) NOTED ABOVE HAS THE APPROPRIATE PERMITS AND IS WILLING TO RECEIVE THE MATERIAL DESCRIBED.
Si*
80920 - R2273 (RUN 02/08792)
BRANCH/SUBMITTER: 015200 JOHN WILSON
PREQUALIFICATION EVALUATION - ENVIROSYSTEMS MATERIAL ANALYSIS
ACCEPT
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
* REVISED * *
PAGE 2 ' COMPLETED: 12/16/91
REVISED: 02/05/92
ACCEPT
CONTROL *: 0122549-3 -- SURVEY 0: 260239
GENERAL ANALYSIS OF TOTAL SAMPLE
COLOR
BROWN
WATER CONTENT
< 0.1 WT%
NON-VOLATILE RESIDUE:
98.0 WT% DESCRIPTION: OIL
FLAMMABILITY
NO FLASH AT 142 F BY SETAFLASH
FLAMMABILITY
NO FLASH AT 102 F BY SETAFLASH
PH EXTRACT BY METER 6-6
RADIOACTIVITY
NONE DETECTED
COMMENTS: NO FLASH AT 202F
FUEL EVALUATION OF TOTAL SAMPLE
HEAT CONTENT:
19400 BTU/LB
TOTAL BROMINE
BR: < 0.1 WT%
TOTAL FLUORINE
F : < 0.1 WT%
COMMENTS. CHLORIDE BY TOX 18PPM
ASH UPON COMBUSTION. <
TOTAL CHLORINE CL: <
TOTAL SULFUR
S.<
1 0 WT% 0 1 WT% 0 1 WT/o
METALS CONTENT OF TOTAL SAMPLE
BARIUM (0005) BA:
SILVER (D011) AG. <
CADMIUM (0006) CD: <
NICKEL
NI: <
SELENIUM (0010) SE: <
ZINC
ZN: <
(PPM):
7 5 1 1 5 1
DIGEST
BY: ICP
IRON
FE
ARSENIC (0004) AS :
CHROMIUM (D007) CR :
PHOSPHORUS
P
TITANIUM
TI :
< < <
<
7 MAGNESIUM
MG :
5 BERYLLIUM
BE: <
1 MERCURY (D0O9) HG: <
i LEAD
(0008) PB: <
1 THALLIUM
TL: <
8 1
5 1
1
GENERAL COMPOSITION: SPECIFIC GRAVITY
AQUEOUS PHASE (FREE WATER) . ORGANIC PHASE (FEEDSTOCK)..
BOTTOM SLUDGE (SEMISOLIDS). BOTTOM SOLID (SETTLED SOLIDS)........................................
VISCOSITY (CENTIPOISE)
GENERAL COMPOSITION BY:
CENTRIFUGE APPEARANCE TOTAL
(VOL%)
(VOL%) <WT %)
.....................
0.0
0.0
00
..................... 100.0
100.0 0.0
iooO. .mfl
.....................
0.0
0.0
0^
TOTAL
.890
< 50 CPS
100.0
100.0
100.0
SPECIFIC COMPOSITION OF TOTAL SAMPLE
COMPOSITION OF:
WATER CONTENT................
NON-VOLATILE RESIDUE
DESCRIPTION: OIL................
VOLATILE ORGANICS BY DIFFERENCE..................................
TOTAL SAMPLE
(WT%)
0. 1 98.0
1.9
TOTAL SAMPLE
(WT%)
0. 1
98.0 1.9
TOTAL
100.0 100.0
VOLATILE ORGANIC COMPOSITION OF TOTAL SAMPLE BY GAS CHROMATOGRAPHY
SAMPLE PREPARATION METHODS: CS2-EXTRACT
DETECTION METHODS
FID. FID. MASS-SPEC
COMPOSITION OF. VOLATILE
ORGANICS
COMPOUND NAME
CODE CAS NUMBER
(WTV)
TRACES OF VOLATILE ORGANICS DETECTED (<1.0% EACH)
TR
0-27-1
100.0
VOLATILE ORGANICS
(WTV)
100.0
TOTAL
sample
<WT%) 1.9
TOTAL
SUMMARY OF VOLATILE ORGANIC COMPOSITION BY COMPOUND CHEMICAL CLASS WT%:
ALCOHOLS
ALIPHATIC HYDROCARBONS
AROMATIC HYDROCARBONS
CHLORINATEO SOLVENTS
ESTERS
ETHERS
GLYCOL ETHERS
INHIBITORS
KETONES
NITROGEN COMPOUNDS
100.0
100.0
1 ,9
SPECIFIC ORGANIC COMPOSITION POLYCHLORINATED BIPHENYLS (PCBS): DETECTED SAFETY-KLEEN REGULATED COMPOUNDS: NONE DETECTEO
4 PPM AROCHLOR: 1242
ADDITIONAL ANALYTICAL INFORMATION: AR1242-4 .35PPM
CONTINUED ON NEXT PAGE
021753 St
2920 - R2273 (RUN 02/0S/92)
t BRANCH/SUBMITTER: 01S200 JOHN WILSON
PRETMIALIFICATION EVALUATION - ENVIROSYSTpuS MATERIAL ANALYSIS
#C C E P T IVIROSYSTEMS FUELS ^PPiG INDUSTRIES
WASTE OIL
* REVISED * *
PAGE 3 COMPLETED: 12/19/91
REVISED: 02/05/92
ACCEPT
CONTROL 0: 0122549-3 SURVEY 0: 260239
LABORATORY REVIEW. A
LEVEL:
SEG CODE:
RELEASED:
LAB REVIEWERS:
AJ Ad
ANALYZED:
PCB'S DETECTED/NVR ESTIMATED BY DIFFERENCE.
12/19/91 12/17/91
TRACKING INFORMATIONSURVEY RECEIVED SAMPLE RECEIVED RESAMPLE SHIPPED : RESAMPLE RECEIVED.
DATE
FACILITY
12/05/91 SK TECHNICAL CEN
12/05/91
THE ANALYSES CONTAINED HEREIN ARE PERFORMED SOLELY FOR THE PURPOSE OF QUALIFYING THE ANALYZED MATERIALS FOR ACCEPTANCE BY SAFETY-KLEEN IN ACCORDANCE WITH ITS PERMITS AND PROCESSING CAPABILITY.
R E V I S ION NOTES ** (02/05/92) ** (0002) REVISED FOR NONHAZ APPROVA.C (0003) CHANGED ERROR.
oil-15''
80920 - R2273 (RUN 01/24/92 PROJECT: PPEQUALIFICATION BRANCH/SUBMITTER: 015200 JOHN WILSON
PRF M.IFICATION EVALUATION - ENVIROSYST GENERATOR SURVEY
CCE PT
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
REVISED *
sabtyliieu.
CUSTOMER INFORMATION: 0000-60-2789
PPG INDUSTRIES INC COLUMBIA SOUTHERN RD WEST LAKE
ATTN: GERALD L PERRY
LA 70664
ACCEPT
CONTROL # LAB 0
SURVEY 0
0000122549-3 0000030083-2
0000260239
FEDERAL EPA ID: LA0008086506 STATE EPA ID:
SALESPERSON: JOHN WILSON
GENERATOR: PPG INDUSTRIES
NATURE OF BUSINESS: CHEMICAL MANUFACTURE FEDERAL EPA ID: LADOOSOS6506 IL: FACILITY AOORESS:
COLUMBIA SOUTHERN RD
WESTLAKE
--LA 7Q669
S . I . C . NO: MO: ST: ID:
BILLING: FOR MANIFEST PO BOX 1000 LAKE CHARLES
STATUS: LOG -4 7Q602 -1000
PROCESS DESCRIPTION TRANSFORMER MANTENANCE
GENERATION AMOUNT
5000 GALLONS PER YEAR
AMOUNT ON HAND
100 IN BULK
SHIPPING FREQUENCY OTRLY
IN BULK
COLOR lAYERS OR PHASES
BROWN ONE
PCT SOLIDS NOT SAMPLED: PHYSICAL STATE LIQUID VISCOSITY: LOW
PH RANGE
4- 10
MATERIAL COMPOSITION: VOLX
CODE MAX TYPICAL
OIL. PETROLEUM ATTACHMENTS
NONE
0 100.00
RESTRICTED SUBSTANCES TSCA REGULATED MATERIAL
IDENTIFY PCBS <10PPM
HAZARD CLASS
NUMBER:
NEED ASSISTANCE
EPA WASTE DESCRIPTION ANO TREATMENT STANDARDS: RCRA HAZARDOUS WASTE: NOT SURE
P.O. NO:
TYPE OF SAMPLE: GRAB
0 OF DRUMS SAMPLED:
1 TAKEN BY: CUSTOMER
NAME: GERALD L PERRY COMMENTS: L#30083-2
TITLE: ENV CONTROL SPECIALIST
1 1/26/1991
(318) 491-4370
CORPORATE REVIEWS: TECHNICAL:
REGULATORY: OPERATING:
DISPOSITION REVIEWER DATE
ACCEPT
AAO 12/18/91
ACCEPT
JHP 12/18/91
accept___ ___ JWH
-13/18/91
r~-------------------------------------------
POSSIBLE FACILITIES: 658 642
PRICING CODE: F7
(658) SAFETY-KLEEN CORP
STATE HWY 146
NEW CASTLE KY 40050 FED EPA#: KYD053348108 STATE EPA#: TELEPHONE: 502/845-2453 STATE CODE:
(642)
SAFETY-KLEEN 581 MILLIKEN HEBRON. OHIO 0HD98O587364
614/929-3532
CORP OR SE
43025
APPROVD 0001061 DRUM OR BULK OOT-EPA PETROLEUM OIL DESC. COMBUSTIBLE LIQUID NA1270(ERG 027)
COMMENTS: OK FOR WASTE OIL FUEL
0000777 NOT FOR MANIFEST PROPER SHIPPING DESCRIPTION WAS BASED ON THIS SINGLE ANALYSIS. GENERATOR MUST CERTIFY THAT SHIPMENT IS NOT HA2ARD0US.
EPA WASTE CODES NONE
THIS SERVES AS NOTICE PER, 40CFR264.12(6). THAT THE FACILITYtIES) NOTED ABOVE HAS THE APPROPRIATE PERMITS ANO IS WILLING TO RECEIVE THE MATERIAL DESCRIBED.
021755 SL
80920 - R2273 (RUN 01/24/92)
BRANCH/SUBMITTER: 015200 U0H4 WILSON
PREQT TFICATION EVALUATION - ENVIRQSYSTEN*' MATERIAL ANALYSIS
ACCEPT
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
revised *
PAGE 2 COMPLETED: 12/19/91
REVISED: Ol>2*i/92
ACCEPT
CONTROL 0: 0122549-3 SURVEY 0: 280239
GENERAL ANALYSIS OF TOTAL SAMPLE
color
BROWN
WATER CONTENT
< 0.1 WT%
NON-VOLATILE RESIDUE
98.0 WT% DESCRIPTION: OIL
FLAMMABILITY
NO FLASH AT 142 F BY SETAFLASH
FLAMMABILITY
NO FLASH AT 102 F BY SETAFLASH
PH EXTRACT BY METER G .6
RADIOACTIVITY
NONE DETECTED
FUEL EVALUATION OF TOTAL SAMPLE
HEAT CONTENT:
19400 BTU/LB
TOTAL BROMINE
BR: < 0.1 WT%
TOTAL FLUORINE
F : < 0.1 WT%
ASH UPON COMBUSTION: <
TOTAL CHLORINE CL: <
TOTAL SULFUR
S:<
1.0 WT% 0. 1 WT% 0. 1 WT%
METALS CONTENT OF TOTAL BARIUM (0005) SILVER (0011) CADMIUM (D006) NICKEL SELENIUM (0010) 2 INC
SAMPLE
BA AG < CD < NI < SE < ZN <
(PPM) : 7
5 1 1 5 1
DIGEST
BY: ICP
IRON
FE
ARSENIC (0004) AS :
CHROMIUM (D007) CR :
PHOSPHORUS
P:
TITANIUM
TI :
< < < <
7 MAGNESIUM
MG
5 BERYLLIUM
BE : <
1 MERCURY (0009) HG : <
1 LEAD
(0008) PB ; <
1 THALLIUM
TL ; <
8 1 5 1 1
GENERAL COMPOSITION:
SPECIFIC GRAVITY AQUEOUS phase (FREE WATER) ORGANIC PHASE (FEEDSTOCK). BOTTOM SLUDGE (SEMISOLIOS) BOTTOM SOLID (SETTLED SOLIDS)........................................
TOTAL
.890
VISCOSITY (CENTIPOISE)
GENERAL COMPOSITION BY:
CENTRIFUGE APPEARANCE TOTAL
(VQL%)
(VOL%) (WT %)
.....................
0.0
0.0
0.0
100.0
100.0
.....................
0.0
0.0
0.0
0.0
< 50 CPS
100.0
100.0
100TM
SPECIFIC COMPOSITION OF TOTAL SAMPLE
COMPOSITION OF:
TOTAL
SAMPLE
<wr%)
WATER CONTENT.............................................................................................................................................................................
0.1
NON-VOLATILE RESIOUE
DESCRIPTION: OIL............................................................... 98.0
VOLATILE ORGANICS BY DIFFERENCE............................................................................................................................
1.9
TOTAL SAMPLE
(wt%) 0.1
98.0 1.9
TOTAL
100.0 100.0
VOLATILE ORGANIC COMPOSITION OF TOTAL SAMPLE BY GAS CHROMATOGRAPHY
SAMPLE PREPARATION METH005: CS2-EXTRACT
DETECTION METHOOS
: FIO. FID, MASS-SPEC
COMPOSITION OF: VOLATILE
ORGANICS
COMPOUNO NAME
COOE CAS NUMBER
(WT%)
TRACES OF VOLATILE ORGANICS DETECTED (<1.0% EACH)
TR
0-27-1
100.0
VOLATILE ORGANICS
(WT%)
100.0
TOTAL SAMPLE
(WT%)
1 .9
TOTAL
100.0
100.0
1.9
SUMMARY OF VOLATILE ORGANIC COMPOSITION BY COMPOUND CHEMICAL CLASS WTV
ALCOHOLS
ALIPHATIC HYDROCARBONS
AROMATIC HYDROCARBONS
CHLORINATED SOLVENTS
ESTERS
ETHERS
GLYCOL ETHERS
INHIBITORS
KETONES
NITROGEN COMPOUNDS
SPECIFIC ORGANIC COMPOSITION POLYCHLORINATED BIPHENYLS (PCBS): DETECTED SAFETY-KLEEN REGULATED COMPOUNDS: NONE OETECTED
4 PPM AROCHLOR: 1242
ADDITIONAL ANALYTICAL INFORMATION: AR1242-4.35PPM
LABORATORY REVIEW: A
LEVEL:
SEG CODE:
RELEASED;
LAB REVIEWERS:
AJ AJ
ANALYZED:
PCB'S DETECTED/NVR ESTIMATED BY DIFFERENCE.
12/19/91 12/17/91
TRACKING INFORMATION: SURVEY RECEIVED SAMPLE RECEIVED RESAMPLE SHIPPED : RESAMPLE RECEIVED:
lATE
FACILITY
2/05/91 SK TECHNICAL CEN
2/05/91
CONTINUED ON NEXT PAGE
SL 021756
30920 - R2273 (RUN 01/24/92)
BRANCH/SUBMITTER: 015200 (JOHN WILSON
PR*- 'ALIFICATION EVALUATION - ENVIROSYS" MATERIAL ANALYSIS
CCE P T
IROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
* * REVISED * *
S
PACE 3 COMPLETED: 12/19/91
REVISED- 01/24/92
ACCEPT
CONTROL #: 0122549-3 SURVEY #: 260239
THE ANALYSES CONTAINED HEREIN ARE PERFORMED SOLELY FOR THE PURPOSE OF QUALIFYING THE ANALY2ED MATERIALS FOR ACCEPTANCE BY SAFETY-KLEEN IN ACCORDANCE WITH ITS PERMITS AND PROCESSING CAPABILITY.
REVISION NOTES ** (01/24/92) * (0001) REVISED TO NONHAZ. PCB CERTIFICATION RECEIVED.CC
SL 021757
30920 - R2273 (RUN 12/19/91) PROJECT: PRPQUALIFICATION BRANCH/SUBMITTER: 01S200 'JOHN WILSON
CCEP T
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
PREQI'ALIFICATION EVALUATION - ENVIROSYSTE*"
cGENERATOR SURVEY
satetyuieefl.
.5-0 -i)
;e i 19/91 19/91
VV
CONTROL #: LAB #:
SURVEY #:
0000122549-3 0000030083-2
0000260239
CUSTOMER INFORMATION:
PPG INDUSTRIES COLUMBIA SOUTHERN RD WESTLAKE
LA 70669
FEDERAL EPA 10: STATE EPA 10:
ATTN: GERALD L PERRY
SALESPERSON: JOHN WILSON
GENERATOR: PPG INDUSTRIES
NATURE OF BUSINESS: CHEMICAL MANUFACTURE FEDERAL EPA ID: LAD008086506 IL:
FACILITY ADDRESS:
S.I.C . NO : MO: ST: ID:
BILLING: FOR MANIFEST
STATUS : LOG
COLUMBIA SOUTHERN RO
PO BOX lOQO
WESTLAKE
LA 70669_______
LAKE CHARLES
LA 70602
GENERAL DESCRIPTION WASTE OIL
PROCESS DESCRIPTION TRANSFORMER MANTENANCE
GENERATION AMOUNT
5000 GALLONS PER YEAR
AMOUNT ON HAND
lOO IN BULK
CUPPING FREQUENCY OTRLY
IN BULK
COLOR BROWN
PCT SOLIDS NOT SAMPLED:
PH RANGE:
4-10
^^AYERS OR PHASES ONE
PHYSICAL STATE: LIQUID VISCOSITY: LOW
MATERIAL COMPOSITION: VOLX
CODE MAX TYPICAL
OIL. PETROLEUM_______________________________________________________________ g............................... ...... 100.00 ATTACHMENTS NONE
RESTRICTED SUBSTANCES TSCA REGULATED MATERIAL
IDENTIFY PCBS <10PPM
HAZARD CLASS
,,. .
NUMBER:
NEED ASSISTANCE
EPA WASTE DESCRIPTION AND TREATMENT STANDARDS: RCRA HAZARDOUS WASTE: NOT SURE
P 0 NO:TYPE OF SAMPLE:
GRAB* OF DRUMS SAMPLED:1 TAKEN BY . CUSTOMER
NAME: GERALD L PERRY
TITLE: ENV CONTROL SPECIALIST
11/26/1991 (318) 491-4370
COMMENTS: L*30083-2
CORPORATE REVIEWS: DISPOSITION REVIEWER
TECHNICAL: REGULATORY:
ACCEPT ACCEPT
AAO JHP
OPERATING:
ACCEPT
JWH
APPROVED FACILITIES:
(658) SAFETY-KLEEN CORP
STATE HWY 146
NEW CASTLE KY 40030
FED EPA#: KYD053348108
STATE EPA#:
TELEPHONE: 502/845-2453
STATE CODE:
APPROVD 0001038 DRUM OR BULK DOT-EPA RO WASTE OIL OESC. COMBUSTIBLE LIQUID NA1270
(D001)(ERG *27) COMMENTS: OK FOR FUEL.
Bate 12/18/91
12/18/91
r--
POSSIBLE FACILITIES: 658
PRICING CODE: FI
0000999 NOT FOR MANIFEST PROPER SHIPPING DESCRIPTION WAS BASED ON KNOWLEDGE OF SIMILIAR WASTES. AND WAS NOT BASEO ON THIS SINGLE ANALYSIS.
EPA WASTE 0001
CODES
THIS SERVES AS NOTICE PER, 40CFR284.12(8). THAT THE FACILITY*IES) NOTED ABOVE HAS THE APPROPRIATE PERMITS AND IS WILLING TO RECEIVE THE MATERIAL DESCRIBED.
SL 021758
30920 - R2273 (RUN 12/19/91) BRANCH/SUBMITTER:
PRE'' LIFICATION EVALUATION - ENVIROSYSTF MATERIAL ANALYSIS
ACCEPT
ENVIROSYSTEMS FUELS PPG INDUSTRIES WASTE OIL
PAGE 2 COMPLETED: 12/19/91
REVISED: 12/19/9i
ACCEPT
CONTROL #: 0122S49-3 SURVEY 0: 260239
GENERAL ANALYSIS OF TOTAL SAMPLE
COLOR
SROWN
WATER CONTENT
: < 0.1 WT%
NON-VOLATILE RESIDUE:
98.0 WT% DESCRIPTION: OIL
FLAMMABILITY
FLAMMABILITY
, NO FLASH AT 102 F BY SETAFLASH
PH EXTRACT BY METER 6.S
RADIOACTIVITY
: NONE DETECTED
FUEL
EVALUATION OF TOTAL SAMPLE
HEAT CONTENT:
TOTAL BROMINE
BR:
TOTAL FLUORINE
F
< <
19400 BTU/LB 0.1 WT% 0.1 WT%
ASH UPON COMBUSTION: <
TOTAL CHLORINE CL: <
TOTAL SULFUR
S:<
1 0 WT% 0.1 WT% 0,1 WT%
METALS CONTENT OF TOTAL SAMPLE
BARIUM (DOOS) BA
SILVER (D011) AG <
CADMIUM (D006) CD <
NICKEL
NI <
SELENIUM (0010) SE <
ZINC
ZN <
(PPM): 7 5 1 1
5 1
OIGEST
BY: ICP
IRON
FE :
ARSENIC (0004) AS :
CHROMIUM (D007) CR:
PHOSPHORUS
P:
TITANIUM
TI :
< < < <
7 MAGNESIUM
MG:
5 BERYLLIUM
BE: <
1 MERCURY (D009) HG: <
1 LEAD
(0008) PB: <
1 THALLIUM
TL: <
8 1
5 1 1
GENERAL COMPOSITION:
AOUEOUS PHASE (FREE WATER)... ORGANIC PHASE (FEEDSTOCK).... BOTTOM SLUDGE (SEMISOLIDS)... BOTTOM SOLID (SETTLED SOLIDS)
GENERAL COMPOSITION BY:
SPECIFIC
VISCOSITY
CENTRIFUGE APPEARANCE TOTAL
GRAVITY (CENTIPOISE)
(VOL%)
(VOL%) (WT %)
............................................................................... 0.0
0.0
0.0
..................................................................................... 100.0
100.0 100-0
..................................................................................... 0.0
0.0
0
..................................................................................... 0.0
0.0
0
TOTAL SPECIFIC COMPOSITION OF TOTAL SAMPLE
WATER CONTENT............................................. NON-VOLATILE RESIDUE VOLATILE ORGANICS BY DIFFERENCE
.890
< SO CPS
1C0.0
100.0
COMPOSITION OF:
TOTAL
SAMPLE
(WTO)
................................................................................... 0.1
DESCRIPTION: OIL..................................................................... 98.0
...............................................................................................................
1.9
100.0
TOTAL SAMPLE
(WTO)
01 98.0
1.9
TOTAL
100.0 100.0
VOLATILE ORGANIC COMPOSITION OF TOTAL
SAMPLE PREPARATION METHODS:
DETECTION METHODS
:
COMPOUND NAME TRACES OF VOLATILE ORGANICS DETECTED
SAMPLE BY GAS CHROMATOGRAPHY CS2-EXTRACT
FID. FID. MASS-SPEC COMPOSITION OF:
(<1.0% EACH)
CODE CAS NUMBER TR 0-27-1
VOLATILE ORGANICS
(WTO)
100.0
VOLATILE ORGANICS
(WTO)
100.0
TOTAL SAMPLE
(WTO)
i .9
TOTAL
100.0
100.0
i9
SUMMARY OF VOLATILE ORGANIC COMPOSITION BY COMPOUND CHEMICAL CLASS WTO:
ALCOHOLS
ALIPHATIC HYDROCARBONS
AROMATIC HYDROCARBONS
CHLORINATED SOLVENTS
ESTERS
ETHERS
GLYCOL ETHERS
INHIBITORS
KETONES
NITROGEN COMPOUNDS
SPECIFIC ORGANIC COMPOSITION POLYCHLORINATED BIPHENYLS (PCBS ) : DETECTED SAFETY-KLEEN REGULATED COMPOUNOS: NONE DETECTED
4 PPM AROCHLOR : 1242
ADDITIONAL ANALYTICAL INFORMATION: AR12424 35PPM
LABORATORY REVIEW. A
LEVEL.
SEG CODE
RELEASED-
LAS REVIEWERS:
AJ AJ
ANALYZED.
PCB'S DETECTED/NVR ESTIMATED BY DIFFERENCE
12/19/91 12/17/91
TRACKING INFORMATION: SURVEY RECEIVED SAMPLE RECEIVED RESAMPLE SHIPPED : RESAMPLE RECEIVED:
date
12/05/91 12/05/91
a
fac:.:-SK "ECHNiICA^ ;e
SL 021759
CONTINUEO ON NEXT PAGE
80920 - R2273 (RUN 12/19/91)
* BRANCH/SUBMITTER:
CCE P T
IROSYSTEMS FUELS INDUSTRIES
WASTE OIL
PRQl'*'.IFICATION EVALUATION - ENVIR05YSTEK MATERIAL ANALYSIS
PAGE 3 COMPLETED: 12/19/91
REVISED: 12/19/91
ACCEPT
CONTROL #: 0122S49-3 SURVEY 0: 2B0239
THE ANALYSES CONTAINED HEREIN ARE PERFORMED SOLELY FOR THE PURPOSE OF QUALIFYING THE ANALYZED MATERIALS FOR ACCEPTANCE BY SAFETY-KLEEN IN ACCORDANCE WITH ITS PERMITS AND PROCESSING CAPABILITY.
NOTICE OF LAND DISPOSAL RESTRICTION OF WASTE IS REQUIRED UNDER 40 CFR PART 268. EPA WASTE CODES FOR LOR: D001 ANALYSIS DOES NOT INDICATE THAT MATERIAL IS CALIFORNIA LIST HALOGENATED ORGANIC COMPOUND WASTE.
SL 021760