Document rBYVELR5k4akq4BrBNzBxL6ne
Rufcoma&ad-
KY-9Q.7-D
rhVJ 0H' J.vqdW
1080^
LBS.
PKG-
c.v.
'STD. HRS. .
_______ TIME __, , .
,14 YC-2-B 3 4
14 YC-2-S 93 4 LotZA'jTaX -LOadt
14 YC-2-B 93 4 Lot "
4
MAKING INSTRUCTIONS: BATCH UNIT
//
D.V.
PROCESSES
APPROVED BY
{ ) KY-907-D (D :WK 12/12/77
( ) ( ) 5COZ7I3777
( ) ( ) MW 12/15/77
() {)
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Total Weight - 3480#
EQUIPMENT
isr
k RQLORS) y el l o w me d iu m
tun 3y--f5ee~frl water into V~2Q3<
four In
>ump in
Record: Start
&
USE l bs.
NOH-BLEEDING
TN
ACCt.
COPE
LBS.
-32JL
,M=,P m
48 x 50
Poo
lC.-2.rB.
2m.
7"p-?S.
.IjfcQ t NP (3200 ft)
\ _A
-V-203 thru Homog #3 at -1860-2200- psi into V-265- *Z- W
then V-203 HTY, wash color thru Homog at 1800-2200 psi using
minimum water. '_______________________
fcecord V-2QMWT'*"
~& adi to 60" (2100 G)
Inspect Homog strainer & clean if necessary
Jr
10" (514 6) water into SV & start agitator ^mp V-205 thru Homog at 48QO~5?OO r)^i intnV- , .SL
Record; Time Start <4-?Totai Min /
*
NOTE: If Homog pressure 'fills below 4800' psi, 3-way valve
will re...c..i.r..c..u. la... t-e .s...l.u...r..rJyL to V-205 len V-205 MTY, run In 5" (240 G) water and Pump thru
at 4800-5200 psi
SP JfeSK:Step.,,ai3g,
fljmila-%1 actor to position #2 (V-243) or
3&
..---- ^fr(V-244)
__________
CP I Press.. SV^rgr^l^H^HiLJ.nt,AutP... Remote.
iTersperature.1.,s set..at -19.0-194,, F.)..
^^r|Record 1 evej s nd set Raw Materials Counter #1 as follows
% - preset #1
80 Gal
Set strike flow controllers as follows:
X^3nEJMMSQnEmEnKMml.
020 (N-27--CD Water) in Manual Local
(N-27-CP/Wfter flatM
__(Nr32-.D. Contrail en),..,.in.Manual-
, 0..63 6PM 5.28 GPH
. Q..M. JLM.GPM.
:^C^C2Q._ (N-32-D Water) in Manual 1 oral
_4.-47-.GRM.
^-.aBC2.a,4M^ fft. 8nFrRn1in0 (N--32--*D* /Wa_ter Ratio)
____
0.83
JLdL JLfiO. .27,fO. -215.
32=0- 4840-
ator Step PB
_________ ;________ .
________
ecord Level 2 LG O ji If below 35^ follow .soTution,
makerup -pro-ce.d.u.ra._fQ.r.. N-2,7-:It
,ftdj-to .48" .(2470 G)
pH . / ?-*Jssl to 11.1-11 3 using N-7-0 diltitod to 5%
-Assume. 501
_1_1_11_j_J_A_c_t_s_-_M_a_t_er -tfiIl.p.a.rtH-7-4)V
Siphon into SV Record: pH //#/
- J&z. gpecator-StfiP-EB
< 13620 REV*
ZrD "
iq u ip meh t
pag e 2 c g 03 c o d e KY-9Q7-D (D) e$t . w g t . 3480
l bs.
USE N ACCT. LBS. CODE LBS.
5V SP -<
zSf Step 06/39 - After heat u d Records d HTi &.5-10.0) Switch 3FC20, 8FCio! 8FC2Q to Auto
& J&r "Operator Step PB
;
CP S
'
j&r "SP SteD 10/43 ^ Switch 3FC10
When 3FC28. 8FC10. to Auto. Operator
8FC20 water Step PB
flows
In
limits
SP Steo 11/44 - When 3FC10. 3FC20 flows in limits, switch
-- 3FC20 to Remote Operator Steo PB
*28 ,0iMiia^iato<-.8ecQrd- pH .&..tiiBe. as follows.:._______ __________ SP Step
1.
&
... / j
y
V-243/V-244
pH Range
Time
13/46 (30 min) ?/7 _ S-O^IO.O
9*.
14/47 (60 min).
9.0-10.0
fyi TH?
15/48 2 hrs .. y*O-iG.0 7ft ; rr
16/49 ' 2 ftrs 25 nffnMV. 9.0.10.0 j/{
17/50 ( 3 hrs Final) %L*t LL* 7.5- 8.5 //T lT
NOTE:fl) If pH not as specified notify Supervisor & note
in To# (2) If final pH is above 8.5. adf pH to 73-8.5 &
. __Recordt pH lift In
~
Assume 78% ^ -50
27-D 128-A 50
302 >0 Add 17" (208 Gl water to V-302 e; Add & stir 2 min for 558
" Assume 501 100
7-D 50
PT * rSS" 'During strike pump into PT
............
.......
7 ,, -S3 Pump in ....................... ......... . 0 :-3H Pump in .*- -fifi Stir JO min with lightning mixer for $39
T............... ........
. .................... .. /*/" ..... ....................
356 , 36- Dur.ina strike run '20* f244 Gl water into V*356 8< Turn on steam
-Adi to
317 6V at 178-lQW CW-S-Z * .
.........
--M*W Pump PT mixture from S35 thru undersurface............ ............. . 0 nist.rihutor AFAP
e Rinse PT with hot water from hot water mixer & pump in
r --4r- Shut, off pump
C
*- -#T Stir 30 min at
for S49
r-r no not chut, off agitator
-** .
sv y^rr^9Q complete, heat SV to 198-200F in 5-10 min & w ''Glaserwater line & discharge valves at stearate pump
SP 'ffSflrr'V-356 Discharae valves to stearate Dump inlet
9 4v 'uperi water valve at stearate pump & run water thru
Ijanwfg at 2900-3100 psi to sewer
48** "RlnJe' Homo? water at 2900-3100 psi. open Homog V -rfTV^korrpa Valye* tn SV A rinse* valvp to pw*r
4?. jaffl^diafe-lv open stearate pump discharge valve.
"Tum-ap^ymp & Homog V-356 to SV at 2900-3100 psi
M%mn SV at 198-200F .......... _........ ' ......................... . 50 IRJl !4^ Homoq V-356 to SV. shut off water valve at
pump ASAP
5l* '"Wneivdiomoq complete, rinse In V-356 with hot water * fJPfwn hot water mixer
318
36 36
169-A 318 155-A 36 160-A 36
DUP050092921
V ^*2+ ^ ^
EQUIPMENT
p a g e 3. c g 03 c o d e KY-9G7-D (D) e s t . w g t .
--^
-
3480
l bs. ........
USE LBS.
N CODE
ACCT. LBS.
SV S3- S51 complete turn off Momoa & stearate pump
& 53, ^r 5 min at 198-2QGF. .
SP
9
54 SJiu*rioff steam h&a~S54 complete. Operator PB
/
Oon'T
SUSttb 23/53 Record' d H H t T 13.3-3.7) `ff' necessary dj pH to (.1.3-3.7).(DOWN ONLY) Record nH
15-A
NOTE; Dissolve extra N-15-A In water at 110-120F in drum
Use + 30 aal of water to 50# N-15-A. Stir SV 5 min
<?:.. after each addition
;
1?un in N-7-D from 331 in 10^1.2 min A stir f> min
59 Record: pH*/y V (4.2-4.4) & if necessary ad.i d H 4.2-4.4
& RecoirdT W
Assumed
7-D
(Dilute ID parts water to 1 part N-7-Dl
Assume 7M
71 -n
Siphon N-7-D into SV
flpjrator Step PB
frT tjperfAor Step PB Q2* iSP^tep fiD - Batch complete
.......... . _..........
START
b*. /-iff "
Time
SP Step
/~7 - rri* r .S S OOP
.
..
. i / p^i
FINISH:
0PTR
Time
SP Step
Moot* i/ioP . .
a. ,v!?V',i4r 2--
...........
y
SL ff**\
............ Z&2. --
?
.J
=
:
DUP050092922
DUP050092923
DUP050092924
DUP050092925
DUP050092926
DUP050092927