Document r9O0wjDD10qro45L3Eye6Lee

Ili'spedi^ii m\Mftiiitety}ir4i (*i*itJe 's si 'M l iM a m. M- 1 i.Ms, I JJ 1 , * tM" ` * n'i )A - - VJ*V ''\s\tn 0?99287 ) TOWOLDMON0027872 WATER PCB-00012341 A VsJa1 tnspvchon ........................... *.,., ,13' B, Dielectric Breakdown Voltage . j..... jj : XVII. Inspection Checklist................ ............ ,,:. ,13 i XVIII. Contamination m Transformer* ,,, 4.14 , table VI -Effect ofCommon Insulation Materials on Power Factor and (v Dielectric SnengtV . . ..................... .14 table VII - tiled of Common Insulation > : MalcrialsonVolume Resistivity . (Dwnfemte XIK. of Askarcl ........................... ...................: .14 ASTM Method for Investigating the Comi>atbiltty of Transforms Insulation and Construction Materials In Askareb .. : XX. Refining Askarcl for Ro-Usc ......... A. filtering Through Dry BlollerPaj'cr to Remove Moisture and . . CxUaneous Particles ... j....... . Tabic VIII - Water Removal by filtering AskareM hrough a Paper Press ......; B. Disposal of Solid Wastes ..,.... C. Solid Insulation Requiring Drying . .. SECT ION A j TRANSFORMER AS^ARELS................ ...........................T I. Introduction i........ ... *> v . .>1 II History of Trade Flametypps <* .1 Table 1 The1 Composition of '. -; Transform*; ^skarcb . . - . . ... III. Intci cbangc^llity . ... -- ........... >?. < - ,-2 IV. table II - Official Transformer Amaral \;/ ,^ Shipping Specifications ........ -. V. Orderly Instructions .......... f, . ,t VI. VII. Stability.................................... .. ................ PiecauilonsWben Handling Drums, tank Cari r and When Opening Transformers ......-.V.v.4 A Keep Dry !Dunpg Handling . . . . i / * -4 Table 111 - Handling and , , - ; ; Pumping "temperatures... .> . . .4 B Use Ordinary Personal Precautions ., .4 C. Precautions on Opening an ..... .. . ` XXI. XXII. D. Earth Treatment for Maximum . . Improvement of Power Factor and Volume Resistivity ............ 16 Table IX - Effect of Power : factor and Volume Resistivity ......... ,17 Cleaning Arced Transformers ...........1? Sampling AsVarat ............. II..- srci ion* ASKAREl FILLED SWITCHES AND TERMINAL CHAMBERS ; ....... ...... .19 * .v I. II. rA III. IV. Introduction ............... .19 Sources of Contamination ............. 19 Sealing Switches and Termlnal Chambers ... X) AAarel Used llndor Mild Arcing Conditions .20 V. % VI. Maintenance for Askercl Fitted Switches ... .20 Asharel Under Excessive Temperature ,, or fault Conditions ...................................... .21 I AskarelT rarisformei ......, * i... *>v& a\ UA , VIII. Avoid Environmental Pollution ......... i ^ SCC1I0N60 . 1V. labeling Askariol T1 ransftormers ..-:s xi . . ..... .o6 v v^ AnNrmAIvYiIiItCvAnL SERVICES ON . ' ,1 , >! 2- D isposal of liqui.dw andSohdi.W.iaslses .. .6 ^- a TTRRAANNSSFFOORRhMER ASKAREL >; 3-Condition'lng of New or Recycled Askaiel .B o ./ AVAR ABIE FROM MONSANTO ,..., .2? 4. Teardowij of Transformers . . ^-V.. Typcsof AAnhaa!lysej Available: ... ........... IX. X. XI. XII. ffoorr RReeipaailrt oorr SSccrraapp . ................ .. ,7 , I1I) RRoouuttiinneeMl aintenance Chec^ ....................... .. i?? ; S. transformer Oisposai t |<4<> 7) ComjileU' Analysis ............. .. ..,22.^ ptExpected Service life . ...,.. V>k Ccneral Charjictcrivlic* of Iransformer Ashaiel Fluid....................................#....................... 3| Analysis After Earth Refinement .. AppcndixA - AsVarel Stability and ^' Composition of Arc Formed Gas ................ *............ Sampling transformer Asharcl fluid .. ... .8 Appendix B - Solubility of Gas In ; 3Evaluation o1| Aslarel Rocelvod , , .. . InNcwEqulpmont *..... *.. ,.. ... -6^ Transformer Askarels ......................23 AppcndocC - Cfleet of Temperature on . XIII. DiclcclrlcBr^'downVofiajK - gs Moisture Rel<>1ions1iip .................................. .9 $ Tabic IV - Relation of Dielectric 8realdown DielectricBieakdown Volley*- of Askere! ............. .. *23 Appendix P - Comparison f me Approximate Visooslly in Saybolt Universal Seconds of ; .. : Voltage to Ajnount of Dissolvod Water In \> ^ transformer Askaiels and Mineral Oil . *24 , Askercl ar*d Mineral Oil . .......... .>-. Rt Appendix - The Density of Incrlocn , v. ' Table V - APprodmete Solubility ofWater ; a v-. 51201 KA 7330 9 and Transformer ; XIV. XV. Intransfornibi A^ftr1 and Mineral Oil . .10 tyrant* A13B3B-3 ....................................................... lurbklity ...................................................... Ctieck Points for Maintaining >.10 Apixmdix fThermal Conductivity Values , of Transformer Pyra|}>1 A13B3B-3 ...............................V A&arcl lnstJatk>!,i ................................................10 Appendix C - Heat Capacity -J A General Considerations ^10 Appendix H r Coefficient of Expansion ... .... v*4 XVI. B ModernSeatu>gProcedures . .11 1 D Th^DWcf Scaling ArrangemenU iV...;.1? Periodic Fluff) Inspection and : , . . ; . , What Checkpoints Mean .. .\,.. *^ .. .12 Appendix 1 - fire Resistance ........................................ Ari^ndixl-Scals.Piojreaies . andPiocurement .................................................... * .2* Appendix K - Caution lalxsl -ft. Pyrrho] J0?99?88 TOWOLDMON0027873 WATER PCB-00012342 ' %rrilt hncti t>y |Uf, ASTM af>(l \u< NationalJ V * V W>* V ,m<}r^ 'Co0fi ^lKf*Uy de*i**s 9 t>(M aw of *>n fit ir*o^^ i - * ' *sOSflH synthetic cntortfiMid hydrocarbon tosuletiffl liquids widely used to * ......;-''ji. I #i|p!VjlUI|l |1I%.>H ^kfortjjtorqm%ac*Otf/,*M -pew-.-w^v" au-.-wr ;;v. *"3m ..!/,-v .i.s^^;;.cv;^:,M *`"'.*^.<i'^0Jfn*l4^>Asar^$ot Y*uodj*^rftjHttfti'pha> types are fi\u&'{tor ft# J`;> M9* .wunp .Bf?* ^!^'cpnflitiohfetot- 401^^5 produced,-:dc^ni1i>riSa 4j0fddomjhdt^Oy; i w.. -t'-i%v -'1ilof id*/ ca^ tsoftMto varying *rt WM4 oi * 7110'v, f * .*>4*3.1 r-.i^vWiHSfsUWe #a$ Oqfctiitfity upon the a Mei ty# * ' ___ ____I*-.jmmiti dittoe.s. t.h.e. opere_tirw c.ha. ra. c.te.r<is.t,ics of ,.1anjforrr,,e^' . i, rj * t b<1 qmd irt uftljohVai^t how it tfitfe* hom ftitoe&f oft jyi I ' p i| ; '\ 4 ^ i t " * Appta;*rfst`'heitfliiv dnd di rotft pocoJurtMor teifc ftrap & 3 'jj' * ! * liquid agdStopicgwifd ryatcjisis j'tqivtn toaccor<Vr,fc' vdtojhe " \j ^ Vn\. 1 ** ^ijdeni^$/^4ft)endi,M>yi1^AhicrtcftoNat|od(jt$lo^r'<)ilniUute * , > `` * i *, tofprdiMton Is band on fbH ^aiqpretf py Monsanto ovfcr 40yc$tt *< I * ft ' >4 M a jViodiKX/ 0* ^karcl, iftdsVioy^fdflr gainitf how thp expprjcnce Of 4 J \ > k . {' v t> 1 ti^sfottner maouWuaf^ Add tijfis This gli% outlines toe vefy .' ^ . t , j( i -^~*s Pn'p*'flbfatoiWC*t'c<tfrtffori*1i$rtiflai4tni'tfie0${fiftitwsl(>rmlitt ) } f' /'*' 1 \ h\ f Jl ond g%iS s^MJor.s for sealing artd mainieirtfofla&arel m old unlt> 4. 1 ' C^\s . v 4} > ^> / lulloytfie |ion) Ijliutation service 7 * * tca^doblc mlnimlTm of fliainiei'ian^ II $1 fl* , ' v > " ^ r ^ qupsttof'i^1'^ KlflliOa *o'toe ^ifgtV8 aqd t^uhoing of trarMoihicu, %/ ' >J* r m p * f ( i these ihou\d y^jcWadlor^utaMfoqsforovpr suppliers f ? Jr * * ti*y * ^ * J j 'f 't ^ f f M^ns^qto 0<e^lti{)y a^ViOwltdom ^>e eujdonoe and die ^ 1 " s ponl/JhwtjOnsof^i^to^atflby the lollowtoj} ,,, ' > * j II _. * ', rd*<vdt foMi Gcneiai ^fccirc 1 f, u " i! \ W J 41 \" \ `bfj^K \I *' L >* " li. History 6f 1ro<loN?hie Typ0<. ` "* '' 4 , ' J /i . '. . -a;.. vV :i a , i,' ..', ,, ,' 5 j'/ tmnvo_nco ib) e.ilQdid. 50)Ula(ioii]> ' >v and coo^ijt lusi u cdhyGepciaUcUctneC ;,t9,^Jfor'.Uielr^ j Py. tanof'^krAndnancfircres^Anriui^^nnsfoipp'iiers, ^^linghouie tfccinc .' :'; ,",?. ^t, :.- * ^, .; *-i: \.}',v.>,:cITo'jVr'iixa.>, ^rarilt7>o\rx^lu<>/. r <tfIi.cn?ttr^1r\>Atthikd/l nadmnl/c1. linpA^rttde/>w .' ^ ^ ^ , l> Af 4 \ ^ / l)j4TM k j/ 7 V"\ ' '4"1 */, -> vv^ J' `,v ' >f *' ,% * 1 rt `V r L.' ' 1 f, ' ' * \ J* f * koddt#oft jo mwufeciitonp AtodoA |*i1ini)M<d hipheliyl) ;' r> ^ - Mp/seto >Uo ml^g^ ihii di^lfOUip-fluid wldrchtoroh^^epcs to v ^ ' j i r O'tuct di& pK^mly uwd Incitcen and pyundl Meridi doCnhtd In ' / - i^ '' / ^ v1t^dei^kT0anb ir ti vt* it Opu-? v > <?/ * * mark oJ \V<-:,^.^<.>-'. 'J V.TViVi',:,' Cw f:^.:V.. V h'A:-'' _ -4 ' I - ` '\ - -f v N *. . "r.i" / `v.. *t , Vv .................. 0?^9?89 ) %. TOWOLDMON0027874 WATER_PCB-00012343 ' .. * 1' ' ilx Cofia-OA'tJc-n oririiTo!iM6- AS jptft' v p.... . Mc'Jim3AS|`wOM>3 ' ' ' 1 !! t> ..........J...v..i..x....._.............. Jvf fW' wij) " i IncilcCn ' 7030 . Indict^ mu Fyjii'ic/ A13&3B3 tv i.V ` \ * r * t * iJ ' '1`ijit cflirrit (X by Wt | '3 ;; '>An>c3(>r*,,1?l>fl. * 4 -K Arocloi * 1747, i JilcMcXolctotoVi^pp'T' ^'iny ., v, ). KT l6|iloSenii w- ./T^^RiMibxypiOj'Cno oxldt/, v. %"> ' ' b ` . '.pP-WcftOxiQ^isecrvaedvci^^ I IvS MoflifttfASTM O'S 1` 0.18 to 0>} 1 016 lo 0 7? 0.116 to 0.130 ' |^J . ASlM Method D-?233,^l'Qct "Chfvrindtcd Arojunik Hydrocarbons . Mst/w/tf for 'TfMKfofifictb*', 1w lisU the OompOstlon of e'l }t<in<fornifc' C5t nte1t> u-td dt various tlmGs sine* 1932 Monsanto.rn&iiiifacluret $h/iijar tiahsTormcr.^Vaid fluids In tnyterid. jvV rt flc fledc name Pytoclor J$ M*ed. 1 . III. InlcrOitt^e^Viltty , , "' . ,1p 0er>Wa1 lit! Vantf^ruSpr askarcIs are !nter^5(ariflcabfe- Mowcvci, 3t U," v soogestyd that the 'transformer niamifacioiorbc consulted prioi to > tnlKlr\fl In slyulfir^rit jv opinions <X total substitution. ' ! IV. AsWel $i)ij>|>!n5$|V?cTftCtitlon{. > itn ofMa'S'i^^Tt^cificetions ter t7*o throe mod^o tiensTttffViCf./ asUietfiuldvaiesW^inlahteU, ^ Vt Otdirln^ IrutfuitloiH * v Monfanio*! cufit/rf policy If to tell Os^oroJ trpriffonner fluids ortly to .tra'i^fovmci nSyWtartuife^, Othwf 5nteroi\(?(J in fhewr fluids : . codtpci Vio manyfooturcn of askarel tieosfoimer* end l>ol Monty/ilo/^ :;thc .tiai^e^ntir ^anfc pleie Indicates t1*o transforms maker *ncj Uf^aliy olvct sufficient <lafe lo wpntrfy the specific fluid. Msed.;' VI. 6tMhl> v Ct> 111 7! P>11 hD ^ < on > 'AsVaffil liojijd in.\ll0tiof H fligWy puhv fuft^Trwar^t Ij<$u1dyiftide; vnd >: ;dojet^iaifili^ tbnodfHo meet the eXeMrua speelftcattpfo, as show ^ M'It Ki>cyt>t v^iy^n com^osjMori like tlVooInmefcitft iSn&fc ofTM Asheiet iirtulaiton ntUt novel bo mfxbd with mineral oil. Ovcr'two k fK'ioent ot rtunerat of! by volume In a&tatol bcjjlnt lower' iu 'lirQ resIfUnod ' ` , i t n ' ^ " `' 1% ^J)11(cp VO' CJ^ K 1 In modern ttarisforniCi, the Jonh reK'f'efkmf ,ot U 'C^nlaiitnafiQn by Mr', KeC)^ e^kciel w^icf-fioc will, Insure , `fonj "* r '\ Astp'U isbcmio dianwat**!, IfWdtcrtyuuHofiSk^r^Unsuietioii.only I' % 0?6<)?`>0 .? '..5 TOWOLDMON0027875 WATER PCB-00012344 `ft&rG*or?r*!r Atfca^.S^op . Sa*<5TiC*t7OrtPr0C*'trtB ;-- .-: .:>_ -.;. . Co'0^,ApHA " ,, - .Cq*4*'oa. ,-t *.-. :. - / .-...v' WMW,asm. fAS*V4^533-00} x ' Aodrtv, m$-*Ow/a (AS^V. 097455)^ /. 25C,0.',^.fl90r ._fASTVJ0S77^ _ - _ -I,. , 0*ebc^ie Constant* *0CC, 60wz * m <A$TV D92**9> - - Vb'oma ^!<rt'<wfy^/*006Cr - . 500 vo^s OG 0/ >*ch aeo, '05 ohm*cm -v <ASrw 0**69'- '- X$&Vftotf SAWS' ~ v n*^ctJVt^X,2S<C<A5TVt>i^> . . Y.sco".y st 378*0 (AS*V 098-5 Ssvbo'* tfmvera' Seeends - . eoas**iftr`C iASTV 047 57! , SowS<:?r*V>ty26/':S.5"C WS^V.OiS`9), Sumj>o>m'fASrM 092> - - iOiSt'bation ran^* (ASTA/t -DZO-S OT^sctec! -; * stesfsnt!. sarametfic nreasor* > ' OwVm! **Ctr.tCo< , JVWWIA13S38-9 . ASTW 05283 Tyss^i* . 75CmaSc ^ ' -C-'ear 30 max. _ O.OW-max. * 33 <V, m-n, ij} *o * 5 " 00 O.'O mast - '.Sl'OW.C'TO ' AiStoi? -38 o- 'owar '.*95ro '.5'0 9*. Mne*o botUng- ` . . 1st ^00-200*0 m;. ; ?40% tna*} betow 270*C.s- 90% 379 to 39* . tnartaart70*30 **. A$TW &2283-Tyo 0 f : :. . .150 max.. * *- v-ClQ^* 30 max. - O.O'Omtfx. 35 KV.-rmn. - *.2ro*5 - icO _ ' S 'Omax,.^ '8'53t0'.8'73 , 56t6' :' ..: -30 or tower '5-5 *0 '.523 \'on-o bo-'iro 'rttfroB 200"CmM: - 35% below 270*C 90% 379 tO-39* . . WwJnqHoun*-'' :. - .Tfan^omu^ - - , `H^artae* 100*? ** S0m^ 0'**r 35merx:v " 0,0' rftsx. 35 KV.riiri. 47 -c 49' , J00. ,, v'005rtsx, ' '^2*0ro 1.5250 82 '0 97 -'7 or l0*w x l 33' ter'^92 . \'ore to bOAnc ?0%325<r<n. --9075860 max; - C^xed cbl<^nne _ Corfo^On *t , Go's*. A0uA " "r Acd?tV^^^0M/ti . , *rygartiC eOf36s 6i>m " Cc^cibon ` ' Scave*$e* content ,56.*"*-03% 55,6%mifrv *3*0,S% -^wnlnum for *>61 bex&ttde#? oft e<thervsu8Jof1we^hi: <s?ect`0i'arKj tbeaska^vshouW.^'^ttSe 'o,'ow'no sd^cifJcdt^sr.. . 200-max.: ^ O.01*-max^ 0*i6fnax^ Gi&r ,, 200 max. O.^AmaX, 2.0 max. Cieai1 ; - ,;200.maxv;.1 - OsOi'mao^ " 0/5 max. * C`e^ O.*' 5 to 0/36% 0.4S^022% " o^r>dxyoroj>en# oXWe oberto-xyofooert? ox;<t* - Thermak?xsnsorv.. -/ASrV OW, cm?/cm2yc ` A^e'drmad^eses \ v.. *VhodA?rrM 022S3 *orrvo# G, " 0.-0007 00007 . 0.00066 Assets o* v^tOvs eomtos*^^ >Vi?e? f* y5K?- ?V <wt omdyC^, wHk comt*%g - *-:^*r#d<w**rtant*v c* isonniombtfst'b^i^ydmggn-mWiijy.-ean-M^etutfe ysrvm *moftts.of combtttf!b^$aa*oe^?>9. - voon tV sk7e' tyoe -imu!^o system* i*eo*etetH'$-t*es**MreJsa*vi.ceUvte& 0'* otter -ymen a^wtf.-jyodtca-9aow-*n!Xtur:which are. moderay ftemmsW*.' A a orecewt>^, *vch,9j-*NHikS 5e - fmoved from- the askart' by bubb*w<gdryWO0en throv^h Vw.Mkare^antf^hojftmg the-98'SCaoe w>hdy-AJ^oo**t before e^y work oer'ormed on the toovitw. ,-,.. . . ..,,. :. .. . .. 1 *^M9lf^hftuMU8Mtht>OHvete httfrtbey-Hiei^eft 5*20^KA 'or t/Wfteen^O-^OiM-theiV rsveti namb^Mamaa 5*20iCWftw ifwrteen T00^2. ' N> ,< <ts c'*> tfrzrs tb /b lx 'D TOWOLDMON0027876 WATER_PCB-00012345  l<ny entoopi lapproKimauty i?6 ppm) dii-o'w -t ihp ItoMt on '* ir^A'kVi! veiy Involute In v.atr r. only etx>ut 50!) pa^jpe.' of eft ktldiHolyi. Jn wcier, normai Umpeivtorc. ^ = Vil. Pi60 atom When tftmdlioj) Orurnt,'Tfin'k<i*lti#*f*{J When Ogling TrahaloripW i > *^ lh$ Anrrken Institute or f locuifdl end Electronic Engineers Cjldi No 76,, Dccxfjibcr, 195# has been revised to give o>6ie ,VM$llad Instruction* arJ guidance fJ'For Ac&ptanbt an$ w$lnl&i$n<$ :0ft lramfonuN Asf.firvl in Eqi/tpf/iC'\t*'-1hu sulfa h puldtshed by the ' institute of tlcrcl'icet & Electronic* Engineers, 1pcv34& Cast 47th Sluet, New York, N^wYofy 10017. the following mfc significant piecautlons: < ^ <''p' * ' , K Keep Diy During handling' - ' * . In handling, storing; sampling and lnsjcctmfl *<krel ->and in ; operating askarel IranslToiipbrs >- take every precaution to guard , . v- the a&arel Insolation liom exjtosure to. high Jhunpdity and ( ' moisture conuiminotloo, Keep & or &t> gallon duimV pf eskarol - i diy^ lay sided d( unis bn their sides with tlip bunfi at the highest ; , ^ point from floor to koj.'p'wfltcr off ttie dium head twhjch can be / . socked into the askaretby ihc di um ''bi eatliir>g'7.1 hi* precaution v:H pot necessary Wharf drums ere `sto/od .frtfloorf, WWph M the preferred plate for storage >, Ij v . 1' ' ' > *, i'v/fo avoid '.'leakage th<|,drums used lor eskarof re Of heavy ,;'!,' - cOmt/vitViop.$ixtecm f^ugc prciel Is us6d, with spccialrlm seal and ' i v bong construction. th< drums should be drained 6MX>n\p1ctc1y as 1 possible and it it m flushed twice with kerosene typo solvent to -V- ' remove all of the esitarel. Accumulate^ liquids end -washings : ,V should be collectedj ^nd should be Incinerated 'at: tilgffi . temperatures, e.g., about SOCK^F. to destroy the polychlorinated biphenyls (PCBs). See Section A. VII I. / . v. Tank oars used to transport askeieU are \n fXdusfv? service and not used interchangeably lor other products. All cars must be ; unloaded through the top fdome fitting! either by pumping or ( /. With controlled pressur'e using (ky '*lr 01 dry nlliogfux. If nitrogen. \-his been used lor unloading It U necessary to advise the shipper so that when the car returns the nitrogen Can be replaced whli dry alr^ ' v before any one may color tt>Q car. If the car w to bo unloaded by 1 pumping It will be necessary to use Cdr^er on the ah Intake line to remove moisture ( f >'.::. ............... ... ' * ' v - s, ., >... All tank cars kre fitted with steam col1s4*WhlCh pre sV&llaVIe for i ` unloading under extreme low temper ature Conditions.1;; -a.m,' - :, , Convenient handling and pumping temperatures *od the telaiod app'^hhett M.o5<tty r#ngAs arc given In Table III. 51 < k B Use Ord n&i y Personal f i ecautio ts ^' . ..'-Tiantfomiftr askare! ha? becivmade, handled, and used for over 40 years It can be .handled safely vvltti recommended ixocaytlom. If ' ' ec<?ldcnlarfy spilled On pends,, nd'scrlousikln irrltallon Will occur'. ` However, JfqUid cskarft has( a solvr faction fsilitlar to painjl Pioduct , tah)e)fl , 'v Handling end Pumping Tenuscratutas t -.Unloading, . vHandlirrg ai^J ,v.-- Pumping / Temperature *C 1 Pyranol A13H3P3 Incitcen 70 30 , IrieiUut 100-42 > wW t ?o e& V 3&-?$ TOWOLDMON0027877 WATER_PCB-00012346 ' i ,, <. t * ;; (hinM <wj, ll lei). 90$ ^.<rf;!N?v*MMFHS JW*N#J l(rt>yte90iodiy)f|pMtf(a4'l^'*,>'*Wn ^ ,' ; ' l>j?:* '''-i'S f j' 'A'. j- ''' f ' - J'.I<n<ased? contactfy**kir< Wvi W*addv^fer,remove phd.: . i dry plean -$atur|ted Cle^i* spill* With r&ty., trnydust ind. , ^.absorbent 4ay. fye Poftt*4jft*ynksi4i %painfut .u rttafipn but nf*' ' jsun.orionf flfniag* to i<5< k. If t/ic ryes, Nosh with , ` lege Wount* of wain. At With *'? rye hr** aid/Te to 4 v phy0clan;*To trlieye pSiys?^erii bevelled apopthtfmlc.' anestheK sofupod welf ys obthatp-tfc cortisone estate solution,-. ' or castor oil * Influent expostne to a<karcl vapor* wiU not cause ill effects. '-iv.Howc^'PfoiOAj^d expWre.to high vapor concentrations should , . , avoided, If hot Eskarci most be bundled in a closed 01 oonhnod, provt(Je the areaTvith mechanical ^kh$u$t Ventilation .<- of'' nyoa* n organic raitldgi respirator approved by tlic US Bureau ol Miop5f ' w / x- ' * v' Prtcftuuoni On Opening ap AskarcfJian^om^r' t .<. , ;^r---r:.. AskafeH.ipf. various comp^sitlppal types are used. Under .arcing conditions ibe gates produpod, while consisting'of predominantly' qcm-cbnpbust'iblchydrogen Witoridc, can yield Varying amdunts of ' con^l)Ustiblcgc'Si.j<Ji'ptiidin'i|Ui^onlii^a<.Vae1 type. ' ' Insulation ^yste^s Incorpdribng these, ask^el$ and ce'ltMlppc p., other .organic:; materials may/vfUqn arced/ produne gosepus mixture which are mc-dfratoly flrxunaVc As > precaution, such _ gases should by '-removed .Ir^m the Jskaipl by bubbling dry, oitrogep through ,fl*e..reskaral #i>d flyshipg the .gas space With dry n trpg ti ptforc apy work upeilprmed on the apparatus VIII. Avoid f nvlronmrntdl Pollution ,, ` . IransforAiei Askar^U contain potycMorlnatod biphenyls (PCB) vWiich have been used in Ihfr'United States and elsewhere over the past 40 years fpi'.to^y indusitla) and consumer applications. Dining the past sevpi at years ev1dencebes'a6c0hMa\e<t to indicate that PCBs are widely dispersed throughout the Environment and that they can have adverse ccpiogicaj ax!l tpxicologiuij effect* r * The Untcd Staits'Govuonicnrs'lntercApa^M* r*tpl Task force on PCHs Com?? 10419, in thch 'March20, Im report mitd. t ^'PolyctyQrfrmed 'tifiheiyU ancf fhc fnvfronjriciit''. KfCorpmended fcStncCingPCbsto uselncapacapr* and bansfomiCrs this report js-distributed by tlil- National Technical Information \ .; $crvlccj,US.Ocparimpnt of Commerce, Springfield, Virginia 2?151. A document titled. 'Gwdd/not for fondhrv at<f Dtsfio&l of Cfy^rtUH ' and Transformer Crude Afrarch, Cont&himg Polychlorinated Qiphonytf'i has bccn preparOd and is .ayajiabte from tfe American. . National Standards Jnstituie, Comn)ifiep,.ClQVt&S fasl 4.4th SuceV, . New York, NcVvYoii- 1001?, 5 ^ The scope;objcctrves End the oo^po^iion of ty\i (wnmljte? arE- v ;x - .* ' ', ,' AN*>ICon.nilIitcC)07 Sco|H-.' ' ./ iF^oceduft* a d gildcf for *?fe use, mat Heftange and dis/Josa' of 't^-'iWiiiikaref.^nd oskar'el-fpaked ftiaterlais used to etccTricjal equlpnient. ^ 4 i i ` .4 M ^v i t' r 1 j^bjectlhtJ , *" . T;)1,' ^d'ce of technicai <hfor6atidn pd. advice for federal, ,Statef lopai authorities fihd all dthm concerned ' ^ 'tPcOdf&gp8devciPpment{pf surtabfe drWsaT facilities and ;< fiH concerned mfo ` ; > Serve as tli^ pdvlsbry groupior UmtedStates participation in ^ c interoatiohel Orga'ii7fit?on' Cf ^ tfC^CtGRt ) S0Z^9?93 TOWOLDMON0027878 WATER_PCB-00012347 'OncUpOwlt^}' tt -' 0;yifv*a<lo is ac^vt in of, iej n<>{5 by thU AN$>i -t^xoiiHUu j y fftimvfc-follftntf Eletbtaaf MfehbWuftyi Aj$ocrHk>iv^liori}t v, Wp^re); Astoc]a(io^ irip,<ulk qf "fye<,(i*Wi <and Iconic J fginCt t, American Society foi Tt ling and Maierralj., UMnc i t ltyh\ >0 POftt Awwat Oft, OjI1k1 6*11?$ V? ijhlClomtS ,->; A A*totf3tio/i;. 'ffjylronrncntat JWi'cbc# Agency; Office of v ': f.hybpn}Hentai Affairs; tJeofcf ai $civr<?e* AdnrlqisVAfioh; Naf?on^1..$ bureau of Stand^d , Pcpaitnient of lK Asmy; { Verification Administration; Division foI tnvlronmrntet ytHealdh,- 1VA; 1 America^ : Kibhc Pov/^t Association/Water .v- ,Rotlulron Control federation; Food and Drug Achmrflsirirtlon; ^ ir_,v \\ fVtlcpal tife Pro\octton Association; 0nderwrite[,i tabofatofici,''- j.> and v.'vci^l sections of die U^S. Duparpncnt qT Jnlunot.v t- v The following aie pcmijent exempts taken horn the ANSI Guidelines : ^ fof iskprettransfer mitij '< \ < * I. tAeri INGASKARCtTftA^SfOfiMOtS v ''All hewad^rrt U&'itfo nicisiliouldt>t labeled 1 Caution , f 3* 1 ', Ihd fnsujatlng Uquid In 1hs ?/jn$former Contains Polychlorinated Diphenyls <PCB$1 Cire Should Be ^aken To Pitvont tntty Into The ErWfroiimeny In CaSe Of Malfunction Or te^ks, Cphsdlt The Instruction Manual i)r The Wand facturei. " i ,. i, , ' k y r t r v; * ; The transTprn^v manufacturer shodtd make simitar, warping /, v;, r.:*,.laUo'Tt available for use on previously Installed transformers.*' ' ? OISfOSAI Of UQUID AND SOLID WASUS 1 .-i, ?'> *'C)i$po$a1of ^ske^el fluid pnd askard-soak^d materials must / vt\ . ,vi -1>0 accomplished fey mfram )n wltlcti there Is no significant ` ~< > . ;n1 release of askan^ to the envlronrnen'.. At present, disposal is ^ :' :. accomplished rhy'vcatefutly.- controlled .ftigli ^tcmpcratyle >~ "'* i ' rncinC'anon ol ftquidk and soaked >fwuai;. and by . , . ? controlled dry land fill bunal of ajiparatus end oihei , - *}:.\ ,/ .hardware ^rum which astcarelhas been previously drained and vi adicd * ' JVrC`Xlnl knov>Kdg indicat s\ha\ p oper mc*n,'ialiOn should ( involve -a 1 suitable ^balance befvvcpn xdwptj bore /and '.s^ v , :.N - , fe(vi|>craWre If) the incmeretor plus oxygen availability And 4 fina'ly tulbiblc sCiuMrcrs to uinnvt, HCt formed, ^g,, ttj twoxxxmd due1! ^ime at appioxiniairly 2000"F and 3^OvCess oxyg<nfin stack gas, f2) 1 \V* second dvdl irmt el ??(Xrf ind^exe oxyft'iun stack - i' . v v Ttie ^4^1 Gu1&: trsls die locations of facilities that conform > : / yvith the &b0Ve . fequlremeMS* Monsanto has such an -v ....\.;- Incinerator at i flic W, G. Krummrich Plant, Ocpartmt-nt. * A-?4C, Saugrt, Illinois 62201, where arang^n\c'Hs con he :/v;;-,-v,'/::. ^ado 'foi scrap askflrel hquid disjosaf for:41 modest fee, * . ,1.. . Cou^rAty 3 cpW pci pound, ^or disf>osa!-dl solid ferap p y. co0t(ol]od dry la d Ml be us d where permitted by FcfluatfJtau ftrtd total rogulaitfofis v ,, J 3 CONDltiONlNGOl- NEWORtiECVCifO ASKARtt, . - '-Jvi OohdnjPMng of ncW askardl oi fecyCted askaret requires f ullof's canh tieaimc ut \ic spentf vfler's carlh In <;d`tridyis > or 1m<> when replaced should be ahoWcd to tl oroughly drain tovo dh pirns to Kntovt as muc?i liquid teiel a^> possible ; A' v. 1 f*c c^rtmlgr units <>ksteel nic>h c^'iShtklion should be m thcf'3teel Oopjiaotinated -wfth A^karet" container/' 1 (for disposition,tlop' bags filled wrlh f ullcv's earth st*outd t>e > pla <d In 0t 'Scrap burnable AskareJ WdSle" cpnlalnu for dltyOptiori 1- ` TOWOLDMON0027879 WATER_PCB-00012348 1 i " vM,t''`V ^ ' ' s ', * * ix`` Mji-jiffsitlor) flier? W#* wttitldM linn,fy< pll ' k ,i I|'...l` it - 1 n it it * <T l I ! Vf* well# <*-! *k ' t) 0-VfH'iu, b fsi-irtwy tf .f, (i,: . .., J J\?. i.,.. ... ,. ,V)) .,, '. .. JitiiUv >1 ,,<>f tf'f, S A.Jl -.,,. a**^-'.v*......>-r*j' '-*; * --A~- {KxoVH.'^nIM 0>(W *ite<-4 *i> ftc Boo* to i rJ>|- * > v'. \ < 6!^1-!U'tM m** 'r * ^'v ' ^ , v-*' S*,i * < 1, 'fv; I...> v * ;.*yj ,s ^ * i::.--r^<-::>'- ^v'j ** repdrdKf* ^Mfflhy,\$h^u^ ',!?$ m lf>|0 l|>& j ,Y ^ cO^^oj^for^swln^ * "* ' . 5 ' IftANSfOHMtRofaWl /' ' ' _-***-** xJie^s:^ af-jh * , , *<fc>r,,4.!.1.1iej 10 eilltff d< *V9 ViCI/l : c> U W^or^Wf|l>ay ,l)fe; - ' "' '' s;.-,. ' `,-i | ,, T / *, b^miSarisof juh^oj:,'-'; .. .,:S5}6[> ^Cultf^ dlfllltt llO VcHC5C<J UUjeSS .S.IrilllSfpl.lJM .}$ ., 1; ` i fir$l droned, fossil by sosklnijOf tf>pipteii^r wlitui ' ' ontfiliW sotaL *dc*t ^ Siet'osen^AcaiiiiOIsloa liquid'' Tt end v idling; 'fni ,|y <1 >j*:r<J of Jt/.|b(!< eartii . * iii txj.&cnd S5ivice ijfe ' .raw <Jeigfiep pW }n*tn1i<<i wwl lAtr-'?!^*KiifArtiiwrt 'rf>rf 1 ^ -i ' "V: r ' A ' s'k* " X;'. ,\'iv 1 , ,* I'': v :* ,x , \ u `^V - fi ,> i ,(3 >' >*iv** *? i?v., ...... . n 1' a ri ', ;w./ ,| * f|. ?,; ;j/ ..........................-if.*. '' '........ .................................................... lasfi.^' TOWOLDMON0027880 WATER PCB-00012349 Culdc . , , ^ ......nw,in'r}n*Wfi>V<>< .onV5... ... .1.... U. r `* %' > l (r^tivt. <$n mW) bf a^aiel r * *HwU\% |ti*n 1), WO* i *Ad tfmt Olkl *lk Pf<& Ifcffy to tin':'!>! , ',? ?<nf*fouftd?\oi lh? tufla^Thi i^^fn,pto,.,(Vlte.refof/o:,Vcfprj5t^ ted toJa% 2 . XII. t valuator! o( Askarai Rccoivtd In CrU* ; r <1 a I a> 1 m ll . * I -t * ' }M\ i *\ aod tramod pp&gtyftg wp iMw y*Tl*#*;>!** ' ^1 infMinjt' ntMil '<r>i*i t?d In et'f.Wiis1 iWfijf'taa must (p A ^ I vW *. * < / i 'Uf 4 S' 2 ;:" Uiiwi' `:" " '.' -v 'M ; *&*. r.r**** jtsu , % f;.'.?fi'.,^ js;'ow- ; j(V<V ''/ Sfufy*'^*fl' fo***!"# HIMkI '<fA fo# nv>'`^Jif(oruW, ,, 1 >,iK- K" I.'V n>ij.<tm <;a K(lc;> O.c fi'-ucc of Y^ ' 2'' iiMdh-i A&V *S\ te.-t- n unwind oIjMtlC %da\rJvlv^n yjstt i}t O' !<( -.tr*f > X V ' y ,S5ta &X. S'?.*'... VI V\ .to, % 1 2 r 1 i \" , ` * .v ' v . w3 , '. '*. ' v<v t ^ \ * -~ 1 * *? ^ ;*>v >> 4, ' ' **'v w , < 0<i^,9^<)b TOWOLDMON0027881 WATER PCB-00012350 st* ..'V. ],v *,V f '\ i.' .',;^;V:S./.')," * sy , < *9 V *a'i' ^,`f^'|^'*v'^f,y,,;!r ' ; '- :,y-;:A'., i . (o<Utw Hr/ii>fCA(lt'ijyd(.rcrHn<Ht>fiwl* rioim , , ? ,' . v,*. ' '1 - ' Y* ; '> , ' .' <4 -''' I 1 \t , ,J 7 ;i , '* * .,< {,' , ' Oita VifiA Jvmw. r.,u-At. <J.<!cclii< it (ftK'Wu*.'-feW#.XNM nii>0uV (. ctoitVti V.-HJ. till) fk*$ .*;*** ' v<*ijf, cty.) x*W ': ft'tf *hwW W,,, ' < - If \ ....... Xt>ltil i titivd.ci^paiiic*, Boie.aiM.1 oAtv- .<ni nVotuy . MMoru.iitolirltePRfetpl.ltttiloifOtfUslliVipin ' t,1 riho dn-K|>KVt?M<A\S yrf?4* dTafe'e'iS KJfcktt i <. ' * norW^ltjv? to pfJin^Y.di^OiVcd the., *<. \ f ''d4tltfeotctnfctc tbatrp-AVddVV'Vo/n *vo>it'it$#jAih ft tHo)vfyndywWd ttyy'Wynt L ,fe *7 ' / I L\ ^Dt^svsrt-im^c^ ^ ^ ^ ' * v s; ' ft1 1 v 1.1 `A*^ .t i.,r>*iAr*><x -kts rci?ii'M?(5(if<rJi rfkta-titooddiiccaallllvy aarrttild, * rtfcristdfe' ]ptdk-uf. arcing; pi 1 lOpjV;d to ?0 KV pi' >ypd fn pi .46, '<, corrections.. * ^ l- < p,of>tur$ tind JaH)e V lnb,k-nU^nnual^re M*' 4 - Mfj' i*, J ^ j t^ he ,, i, f *'> > , , ^ 50'u " /' '/ , * ^ I ^ R S| * 'w V* , ' * , ^r /!'cVjtlon okf JPi,c!,*t\l.'i<i' *lrca1 dTo^wlinlcVIoVtU^tf.*** toA AAnynft.oiAO<nuhh!lnpff 1t)i'-4ltfC*i t V > ` / ttali, ' ^i.i r Wl Com6 (fffi) Brrcc^jlV'ddov>viftnfi VoltdgplASlM . &5,'is'4' , ! * v\ r-, *- * ItS i: > . >,. ;* < JlffSAjS:.; >. '' * 'o '' , ` `' ' 50 KV 3S , 30 20 ,9t , 6B IA .* >* '/ f*i i w^ ' f i% ^ J ** \ i r 5 ' , > v- !t ^ ' ** iA ^ v * ?>* ,, , v 1 i` - * *v , * * r ' >sis'4 I / ,, J V* 5 "v * i /' *`V | , , 1 /. ' '' }t . iA vf A' 02'i9?97 -- -^ T TOWOLDMON0027882 WATER_PCB-00012351 #v - ^ 10 ^ u , ( ' 3> 1 ilO ' M> ..> t - Hi 1^ , 30, ' > ' 40 i 08 80 1 1 ii04 A ( >' h xiv:/. Turbidity 170 > <* * ,, T 'V 1 h" ,< , 130 "v > fiisy ty thft Visual siinh,ft1,M(f)rfjs^vf <J,water dirt,, ^ fn^y $$o Cr^fn ffctyd. j>t^Jjpi^(ioi't ff On fcUttwhy) . t f i t) , yifei ti^d 1ft i'j ''. iff fiOVYiftwiii m iMnfirtK AriUnil ?<!tOV'1fO'^' "; vdtjWvO^n^0l^}iat1rtflo^3^-f^nd<iil^ti<>fi.> if ts r ^\ > A i,/r 1j ' %1c<JV5 UfiaWnwii vi>}tfr&e ^Wilj iHfipMVi ifufipirt? %j( >ftV M J..')>jrbid(iy piOi'ftl <>.not lle i-1 A^ll! * ^jKY* ntylrtM should t><? detofttfnUj. ifyr# tlx * f{ Fjchkrft't^hod . JASIMDIM30W f >, I) i , *'t J ? ^ , *.,> vV'fc 1 j i lhf'JtitifcUfc pn^tfopp vohey inf frf qskfiw Xeimfiatpatityrtty ^ i J\ mtJtmrt (or, fntfkhvts it h Wtet twmohi^onmfnaftitfMf* vat v* ** fo< h'i}i>\f<itti'i$i tli&et it * ^ ` < (* i ' "> ,, a j ii ' f VXVV/(j QrloljAoc/'kt' PnellinthkffoorrtosintglningAAstftraareAtl Instuullaaftiifotnn " *. > . . ! > 1f ] V* A , tavityral CoMidtnWph \* * * \ *' * { . j j * * K^oticin iftprdl^ntfprM^rstytyyi wcffJcd pftWin>n orjilitoftB * 1 ^ > I`K \ , ** Of Vitort* flydceU <b$i$ hQ^-C0yf(> switch -etid U"n}fWj ^ J *& * t'' v ' Opnjnal'poont i<ov6id ^nd.,WHb. pfOpcMy v^>CM^%rof?tctS ' icQulre 1^i(c -pi r^(? fft^n^nanw * * iUaftS^'inefJ, Bj|n(aM6r fien^iaiTinud^ yi&M^ Ift^cllnh ,,.v- v. o- dit1u.jijQv)?rtd.,d^'\/i)j foj *-\ 0i?,-eJ<|Kvi* -dvcr jfntfny year* pf t * f 1 I 5il''l,U/ ' j-1 y i ^ ,1" , * llowi 1(51, >11 *i*y ',K,irc1 WiiH Vrtre'losul'cd In 11if eiMiy 1031K - s' tyfp/fl ti>? ^ftydoprncnt of ?of la\iir Woden* , o)o bofo|f- Wif>rov^ df^ans w ftiff df yduf^d (or V o\>\ tftoUufC* i?e, ??>d fort bts, ;.J ... ,;,. ^fjaky.or Octeiipri^d 8askoi$ <hQ^d ^c./epia<>o<S^lf sbP i r )i^b('<i*hi'fi^htarttn<ud<(t^o^)db favorrdHlprtrd Au|*tWM' ^ \ \|nic, 9 gCU'i d plcaVi^p t>f tl6.jC*n't Ppd ^oi.^it>)p rennJsW^oft^y b$ $ t dctuawL , 11 \ 1 4 `J ^ < 1 , *, '.r, ,1 , '? ^,, f> * . {] ' ij > , i\ i` .. llCit jsbot c*:-'iyeft1c?l Jo an 61d Jik|fotjtoei'ouV&f service f.oi'- :^-:.-;or. ffcji>lfs,`<cAyfirtikotiWiWjfrfcdte^j^rdyby^ ovtri tP^rky fro wijbopoxy^-^^t 3t ^ *!> ^ v tt li v *. i x v< A . ' V. , . . .r V i O - . . 1? Yl It ^ h; t....... t" Ibi >*' i ^ i > , bifi\cJT(y*\tn#pK<$m%!iufc '* F^iiTw^ / v, ^ Jl* /< ,* f" L \ ^7 ^ ,* ^v : f 1^1 fO t * ]* ** 111 i! ii <\ ** 11 ".i k j. /' ^,,1 3 * i V !.., *;,* .W! ? /.. (y i / ` J* **, r f >* ^)\, i* '*, -<* ^ *' i o*'# * '* TOWOLDMON0027883 WATER PCB-00012352 W w #>;r J ;.; vy y '/ , ..................... ;j | *I * :l^x; * 7m &x%%$s ^ t%> Election throng *tf "1 w?11' *****''*t,,e4 ? M . - i* It t I , , Ci.( K.l W'-'1l v ''> * n''^ V '1(1 *'* " ; " iKi hirig iru:* yt sWhHe Metf Of fcot'f'f, if' i( Htf&l vlth 11 '? Uf A il.r- ^sndftaMCrtWt'bybt.nsMtejWo ,f i. \_ ,'. mo-* fflym>vct*f#rdeinp ' " ' v ,u tt*p oniltti <<*(r W e'lliel'pf MWtSi'V Wti'A^o', ' \ ,3 Wl Vw Wh*?o< VSbfh, not PAIN'S t<> i `3 m'toiwcTon m *Vw> ^y1'1 *Wr` * V w f;jrt S riX'thV *urtji iW n" rl 7 'jjjistlel till* beiWi tlf IsMnM'onf rf ***, i ll iu C v^i'Ln M iWff * groove * - . othtT&W mele.sl.ly Kt|chM <> ll.e.fleW' <>< ^ /" ' <<. t ^ 1 V H " y J ( '. ` ,, "' / 'the eilkow tCu.fel'M^ be WCorning No ^ ' 1 ' -' Siis.no* *. of'.'iflvftatei't, Iho b e low eoi'f'" ^n "SiiXei, to"V<A*W$ W* b V ' V.# nil>V 1 <^rvn`*n <>' 4f?t,w< <* `t(,p',<,l ^ ' , etlo^jo, this ?o y 1, , 1 i r,.*'','iJ`'... > ii;.'^4Si4sSalSS ' 11 (T Vi a* Oti if' ` l*'** C^Te, ' Tr*^ F ` *kl** * \ 4 < **1* ftJ \ * *f 'i Him, n r ^ ~ t a, 'Tf: TOWOLDMON0027884 uiATrn nnn r\r\r\* ooco *\i > X'' , n*i , (j ^ fr a ufrmbmfiiit Vti . niolrtoitbwfc ` / , N01{. 6;' Sfeiilr.jj Wl(Haf<l,'Mi^'it|i')wIHsurt-1ytilitlot / v* \ Elastic $>v s^'1 p'1 IdbilcalcH* to all |i<hsToimeJ ti^ouVM41* <>r T^ey jvIH fyrtjlsti , <ia SC( Apptf)d`X K $CiH. fNopqiUC). , I'jociirt'ncru v, C |H t)ldu Sealing AnlsriginiCiiti 1 ^^ T lie olfyi type gatyeb tonsil pf either oork or cork nitrile fublx-t ' 6on|WrejtonsorUdt5hH>itintVuW*cr , is 1, Co/kNttnip Combinatrontf ^ Covert for UK maim tank, hind hole*. Witch o id teiminal chambers., relief diaphrahis, ix"r''/: v o|c;,fenj hold ip plate by stuck welder} to tb flange or by - x: bolt*. The gasket* $re cut with openings and placed over the k - bolts. Often ShillM? (Vycstinghousc Style No 11U041&, or Genff*1 ^Jecuk Company'* Giypial* t?76) s used to cement the gorts ip the Hinges v - - * ' . . |W following k recommended for,seeing Vitlj the cotk * ; ; nitilfouibbei cbtWln&tions r >J ........... . -ii{ , > ' * -1 - * Use Atmsirong NC-7&7 ork-n]uilc m&tonal or odOlyatpnt:'-.;,. 1 tie gasket i ait fye cut front 8 single slice* or by scarfing strips ' B0l4G01,(aVr>!lt$1B) ." *"$& ''h'. ; ';' V.'jv'?''-iA"V' V' 4'V" The joints and a'so the gasket - should be cemented to the : 'flange, u*tf*o ope of tiicahov^ tjciVients. fxc&s^ oeMei'rt should ' . ; no* bc^ellowc'd Ip rebels tlie Intel lor of the Uanstotfi'ioiv -1 v> ' After Installation and bolting, the outside edge oftbc flasket . should he ooatea thoroughly with epoxy cement to Increase 1 leather mjstandc^ ,* * J ' , : v. . i 1 his epoxy cempn* is a paste to which a curing catalyst is ' - added immediately before use, Typical are;, .,-v : a fphxy Patch Kt i IjC w'..... . *: . ' ( ; ';,.<'. Hysol Corporation,, Olcan, Now York , iV" ' b, ScotchcastY R<tt'n f 4 :r..\ , < , Vi", r , tomheiota Minii^l & Manufacturing Conpapy : $* Paul, Minnesota , c Adheslvt A*1 Bird Actlvato TyptQ " * , Ai msiiorw piodnqH Company " ' Aigoiine Poal.WdisawJndiana U Adhcfivc 9BG01. Synthetics Organic Con'ipanv, , vv CtcvclaivJ. Ohio, used witli actWator dielhylcne uianiine * ' (Carbide ahp fcat^On Chemical Coptpany) t ' ?. Straight-NitijViRubhcr; When straight bitrllc /ubl*tn wa^ .. : v> :' t 'OMflipally used, ihvenably the yoskel Was recessed in agiOyvc., , . V; : This weii to jpicyoui gaskot flow and to protect fle`material -, i against exct'ssiyc compession. Although tins' type tea! was , , not c^niciilod.Uic nitrile rUbUr gasket n not reuseable, Since gfOQvc.s\<h ttops have already T>ecn provided for the ' . nlliUe rubVi K^bSdastlc bf) canbe eashy iiibstnutid and Is v /ecornmc.*di Thls'tonforni$ with modemp actioe r J^VI. Purlcklic fluid InsjtccTton arid \Hm Cticc?t|>oinu Wusn pn (vgula' jchidult * at *!*. nine, of i^elvt month intem* - nifk? $ simple vlsuifl inspection of your od^arel jr\sut|at.*prt a^d tun $ d`e!$?Uic b>ealdoW<> voltage Olitclc. * K x \ fk * of Goi>eral.|ifiMi:}c Cditippny VII raden^dt Or 'Wirjijns |> TitenmUita^tw'iijg Coftipariy O7AQ300 TOWOLDMON0027885 WATER PCB-00012354 ? ,,k...... .fc,....,r' ___ J *....A.t ..................4 .Vmigf IfHpetftion v >' * r 1 ...... * Ashotpl Ai a <1** r famt y.1low bcpd, -Abel1 1ong*,erm tier this coto 4t%*/ g mtc<i{?f^ to light bro^ii Ihe fluid shdpld rmffrt dteA ,M liec f0,ntwlUJ'iy cm <1oid.hc>6 *' ! i Any, t<Apt_j to $ gVoA ^ *- Indicate*' J extrarhon of impurities {color higv rials) horn the solid insulation ; * If,.?: 4t$ti(Ki^of^n'iKAof-.'fidkhp I* <io{ed,!fJhedk the complete "i . > .tappe ^pfl^cVtcal dharaCt<?flst'fos:,*0i1 notify the transformer ; / m^ker. Blackening of the a^arel May Indicate an arcing condition. yiV : 0^cr `IooIcm'. Change* Vone. ^* hdl danger signals .finoe the . , dictccUfp hieaVdowo'volieje H oot likely to be impaired, . : vj ..'. ji-: Pic|ofctric Breakdown Voltag^ ' ' ' , Jf the diefoplnf bffcskdown^w^e. haj ^. > T` from the Iasi imjocijon, or it a has^tacltiallyjtJecieased below70 KN/ range {at 7b*$ - pUN A CMCCK fOH MOlS'lUftt. Use v , ASfMD1b3^!Kr1MsdhrMckli^d|. ,, ,Tbe dielectric breakdown Vottete of ask^re! Is the major indicator 'V to the Operating efficiency of your liquid insulation, Besides the : :: Visyal jny'pcnort tests, dielwuric bit-aVdown voltage U the .only !>,?. ' test Dtcev^^y 'to rup on * routine basis. .VVell-veylud askarc! .V; .'transformer have service records pf Pfy io 30 year* on the original \ \ " e^kar# w . ^ * t*. XVII. Inspection Checklist ' k 1. I If askaiel H dear v cVeil though darkened to fight biowp, hat no V^ or turbidity, has dielectric breakdown voltage over 2$ , ,* * KV ~ igtve it toi* instfMJciioQ *k* v, , If eskar^l is dear,, but hasto/ergri color of hlue.s'ccn, red... It it 1 Y "cxtiacbng color*' front Internal materials. 1 his U not, of itself, an > operating batord when the dielectric breakdown voltage stays Over .'.. 20 KV and moisture remains low. however, this rare occurrence, f; cells for checking iptothe condition of the interior const!uciion r - and compiling the transferipQt .i^Sker. However, 4wleo sampling V' ? die fluid ectre should bo taken'to avoid goumg color into the <s l askaret Iroro paint that may be Inside or oufside ol the iarhjflc . valve, i ** r jf ^ ^ . * V'if the moisture content is found to be above 70 ppm at operating v '>. i. temp$ratufe, %thensampling should be done more frequent (:' * intervals to establish * .possible Vend, pamculaily on outdopi* ., instillation^ 'v K' *" 1 j;- If osk^rel I* clear, but dielcctilc^riakd^wn Voltage dro'ps to 2? or >! .' tower KV, ^nd moisture .-rist^f" over 80 ppm. wfien sarripled at .. ' operating tempe^tlir^ 'i -> 'ie ia&are] Is feady 'for;simple ^retinlng'VH lli? moisture near the saturation level (atout 120 */. * vppiT\(room temperature) thoiougii Inspection should bcVnadc . .. v for ' w&tei droplet* in, the tramtorniei .tank, and even for ` 'Vobules**'of water fjopttng bn fle askaic! surface. If found, the v-: trar^loimcr manufactu ci shot/1^ tx1 consulted for rc'-on^ilioning .'. ^ bot^ the tjanslojmcl and the Uixd. i * t * * r.H ftsksr^l h dark brown to Vlacki if black particles of carb(n are V W'cm ind^iclectiic sh engtli p ,ioy^,*. the askaret has been broken v dowp by arcing/ft c^nhbj, bejnstined apd tsflotild be r^moVed and ,\f:- tncinerile^ Under poper pondmons. fSec AMSf Committee CIO? /CJXnl on V#' #'>0 Pftf>PCif .x>T.A$kflr(`1 antf AskarctSpdkeJ . e ' /4jl&C iisV44tU Strei;Nc^ Y^tkJ^le^.VorX lODl?). % >;>;: if ny of these fiye :sirpj>lf msppcdorl fists appear ot^t of the , V^* ordinary r the reletiorishlp between ap^aranco and (nt values Is V al^ofrpll,: /Contact yopi1 V^^P1T,,W supplier ior a odfyfflete/ '..; oija'ysts , , ' Wtwr^ycr '&sample 1* to be slilpixrd to Monsanto, please follow the - directions shown undef. "'SAMPI INC ASKARC l*' ' (Y mi: TOWOLDMON0027886 WATER_PCB-00012355 .\ . lH >t A*<'J SC tfoli/i Ir, Asm'll (.11CK>C ,r , , 1 ' ; ' ' W> ^ j* ! K A'-.s.cl^tovtK,.;.,!^*- : %V' ,;;;, fc$r *#?' , I ,, J V' ' a y ffifWIUHW S*l'V`l* * tftofairUtu'ini'llm1mintoVciHHdd *** * Wc1- , i,(oX0)`,C(` Hv ' ^ ; 'Vll Nor.c'lco <)'<') ' ` , -' ?? \. , 'KV '' "1 ) , Cn,r * v' BlarV vat Ashed <?oV> <, ' i5 ?/ . ,v WV,IV ............. .. *............i--t-K...... V'A " ,K' w S *9 1 ; i|1lapa(*r , ' ' ', jhM fomiatfltjWw Mfi\ , t 9 ` J * i* ; it <t !1 /?#? ": 1 i1' 4 *! . _ . . - * * J,, ' 1 s-r KVrtWtftW tM '* t.?oo TOWOLDMONOQ27887 WATER_PCB-00012356 f 'i'C' .ii ',........ . ,, 1 i'. ;.. I,'-* a'u, I w */>* f,,.,.,^4 . ),, r`* V' s, S^p^rtXTrsulhipiiihdl^iia^^nnwMtW.^orjfei IfftOuili' y.-v . .. vs'U . ' --.rao-. ..;: > 4,^. .,. - -, - , , ,, , ^ fU* hi"1 * !v^ til# 4if3&tM4j|bfW<( wit^* Vf^toi1^ & 1 ' k v *> > .v'v ? ' , - * A\t * f i*,`* i, * v (Vop&ty^ proportion^* n-f^ctnie^i of tf>0 ir^qTaiton c>r sf'uuo'^ , tfta&Kfyd comjiatw *a<M a conti ol$ampte of toe Salt i mtnr^yA 9**t w of Uw t Specimens r \ i ' ' * ,; '. , > , '. H f., ,Vt.ooftiorl*$l*.iDBi4|ttrfj laQOiOltlucrtmlaustd Ho <Uel fluid rofliJbyM"wa!tu(irt.iiiMA<tisspa1>nfaclot , (,,cloM)pi)fl^,.VHC^'60H*o<,pt o.ax OtJWofidgO . i > < '/ ' , mere ri*t A *f # *i ttirtwo t 00/5 ' ........ .....>.... ................ .......T' ,r'YW . h Mita in ]p>M.ntx <jt tlic P-si *pccaf<ir ri an 0 ?(> al IWC end 60 Ha J0VSa'?6`CandK(fl/ ' ,, r ',> ..'>, '! ^ ` l ' ,l\ ...'U%>.'!,> , 1': iv ...i. n < ' '-.""''vxvx - rftmafiknltnan#fAW^l<inwrna' *fed *tlcutf' ~' . ( . s, , , f( [,(}<! jpjf UnvmiU Diy1 lily'll Paper to Rom Oe Moisture and Exllan'OM fVUcK ' r' ' I Most Ofitl'sU'rs ptfl( I ptntiO-lt relihins apparaWs. * ich as a plate ,f V ' pfess'fi.fltfd Willi a'doliy. Mplftfle (pmi, Sparklet, fduwMcln, i ''.i , ` ;- ' '.....v,,...., ' ...../;. . .l.'-H lIillliinliooiiss OOff GGeenoa PUcitir Company, PufsticUl, Map-nJnutU, ot $*$$...'..........J.. * '1 ` iistiiai ritler ' Corps,o.awtiowi., t^dvV...n,,on.,.,........,.,jeri/otitie.Plata.' pplloosws' 'tsttee iavvaaflltaeWf#f sluoan Cal) Srs'tlcl.'w bnd Sol.uf'K Corjlpany,1 ........... , fJcv pan.pViirt! Bf.dJiVafioloOUiru ol fill, i ja'csst- li ttd k* If .vk 1 I* todoni in>ytiritKIYiWi^io fluid <Ma(u>is 1t/Kd villi Siliwai^'Viton O' le". * f IkdMc iliaa' melt if\ O'B 'u 1 ; 'd'. i \ I'Wt.; ,/ *to in'p^Ktajwn ov 'ASf^i, os o( ftii^iw i.t . ii/. -s / . l * ,.V,'j.... .. i, . a 1r ' , {> ' i t* ` O*W03______): TOWOLDMON0027888 WATER PCB-00012357 I^ J , ItMeVlU ,' Guide to Rale of f>issolved Wain Removal 8y Filtering AsMe!Through IRspCrRmsh ^j^osThi'feugt) ' . _faf*r)Pie . ` Wafer In Askaret `V '* W>M 0 `' ' '' , 115 . . -1 \ '3 3 4, 6 S \. . .w | | 1 '' V 1 . . 35 n 18 12 10 10 . i <, *s Disposal of Solid Wastes j . 'v 1 he ANSI Guide states' that, "All Solid wastes which have been saturated with askercl should be disposed of by the following piocedum: ''' ' 1. The saturated wastes should be placed Into leak*pr6of> " containers and transported to a supervised dry landfill site - meeting State riquirepvjnts. Alternatively, they can be disposed or by incineration in State app* oved facilities. ; ?;e :>:; 2, Solid absorbents .used tor spills can, be disposed of *..* : unc^nlalncd In the'supervised pry landfill ote;transport to?. v . the site should be m closed containers. Alternatively, 1/ , Incineration can be used In accordance with par. 8 (See' Section 4 for litlcrj *' ' , Solid Insulation Requiring Drying* > If tlic solid insulation of the transfermcrVeqjircs drylng/consutt the transformer manufacturer or an apparatus service shop, as In' ; Such case oven drying Is preened v 1 Saril. I'reetoicnt for Maxlfnyrtt Improvement of Rower,factorihd Volume Resistivity'* We question whether pufnpfng end filtering d>e fluid solely to etileve a change in powjcr factor br,volume resistivity alone is justified in today's ecological chpiate ^regarding PC$s, We recommend that In thctc situations the original transformer, manufacturer be contacted V l, ` * p'*'\ ' 1. Riocedurt ,, ,r The askercl liquid fhould be relatively dry prior, to tho . t following eatth filt*at*on, >H * / As g coating on thsJ filter paper surface use finofy divided Attapolgu* clay or'fuller's carpi dried and activated by **. heating for 12 hours at 300 3&(f> immediately prior to use. . . - : The amount of earth used should be 0.1 to 0.2 percent by .>.' weight on the weight of the askjre) to be treated, Askaret 1 weighs about 12 pounds per gallon, -i ` *( / . f 7o deposit the earth evenly, stir one third of the earth with a smell portion of askeiel in a clean container) Rump then . mixture through the filter and follow with two. more"' < one third portions, then'circulate askarel taken frgnmear > j-'j / tle top of the transformer, pasj it warn) (not over 5&*C1 - . ' fhrough the earth-coated filter and feed back through the f v bottom transformed Outlet Continue xlrcufatiph until tta > * fluid is clear and teft shows that tine, electrical proper tios'arc , fully restored 1 , 2 Efftct of Carlh on Removal of ScavCtig^rs 1 ' Only Might and insignificant loss by selocbyc absorption of . ; tin tetraphen^l end,epoxides occyts when asl^ret H refined by tioatrnent with 0.1 to 0-2 percent by weight^ earth. 1o ''i. remove significant , amount^ of die scavengers .jreciu^es .* repetitious tieatrnentwhh much larger amounts of garth.'. n ^ r^v 'M 0249304 .... TOWOLDMON0027889 WATER_PCB-00012358 - fable IX c Approximate Relationship Showing the Insignificant ;s Effect of Rower Factor oncf Volume Resistivity on Dielectric Breakdown Voltage of 1 ransTormcr AsfcaiQl v Volurhc Resistivity Power F acior : :*.%& ohpvcrn {at -. Breakdown (60 cvc ) [ 100C.BOO Volts - Voltage . ]O0C ?b*C,, ,, DC, Or gap] 2b*C,0 r gap J% 66% 16% 20 25% 40 50% ' 00G% 01% ' 0 7% 4 20% ; -i 1800 600 100* , 60 70 u ^ 2b , ^ * ft 36 KV 36 3. 35 35 ' XXI. Cleaning Arced IrsnsfoiniBr* If a uru| has arced so that the as*ate! is no longer fit for use. a thorough .' cleaning of the unit is necessary before refitting with new aSkarel - insulation and returning It to service*. Follow this procedure:p v- v v* /A, Drain out all oark/c&rbon contaminated askalef. Arrange to have ;v I the scrap fluid incinerated under proper .conditions, (See ANSI * : Committee CIO/ report.) / . t . *i \v - ; : - , -.*. : '.B. Carefully brush carbondejk*1tsfrcmhMerna!i>arts and insulation, *v w-v'vn -using a soft bristle brush mdHtng suf^tliat insufatipn is roJ * damaged, 'h ' . ' . ^ * *, i , J ^ < . ' ,* : . C. .RWi thoroughly using new askarej.-A not an 611, not a cleaning solvent > (1 * *l D, Flush a second time with fresh askarel; dram; then fill to the ; 1 proper level with itywaskarct * * , E. Energize transformer to warm the fluid for 24 to 48 hours; then : - circulate the, askorct through a filler, returning it to tin unlt^ - filtcied and ready for U't , v, v /This assumes that the cause of arcing hasbedn established and corrections made^ .1 . * Wt^n evere arcing occurs, major repeH usue'W nccesswy and the unty, : rabuJIt. This procedure cen be appll^ for flushing Out the repaired units. ` -..Vs. t- XXfl. Sampling Askaref . -lake a sample as dose to the top of the liquid surface as possible. Many .large askarel transformers have a built-in sampling tube near the surface .,.for convenient sampling. Then, to make sure that your sample truly represents yogr askarel Insulation, take another sample from the / ; ,'rboupni, If additional sampling tube connections are contrived on the ft v vefves for easier sampling, make the tubes of clean glass, stainless steel,;,: ; .- aluminum Of.tin for rigid types; and *lhconcorViiob 6rteflon tubmgft. - for flexible types ' / / " -' ............ ' '' x;V,yft/'ft' /Use NEW containers for the eskaret sample. A new and thoroughly' - . pf e-dried,small-n\outh quart glass bottle fitted with aBakehte* screw / t /.'cap wjth aluminum or tin car> liner is recomptended for quick, on-site / y* testing. (If complete analysts k to be made, 4 6-pinl Size sample k/' required I ,> Be sure that the new bottle doc-s not stand open to collect dust or 1 /ft moisture. Rinse the iamplp'bottle and cap Ttniridtwo or three times , V with askaf^l frorTi the bansfprmer, then tfiH it. if the sample wltl.be f tested piomptly, a* char glass bottle can be used If sample k to b " stored indefinitely, ute ap amber glass bottle or wrap clear glass with ft aluminum fgil ^ ^ V A. Select a dry day* t>o not sa/npie insulation bn a yv3r,m moist day t whet) humidity exceeds >b%, and,.,, " ` . ^tradi'rttarliUnion Carbide Comiheporr t 11'//024930^ TOWOLDMON0027890 WATER PCB-00012359 * -4 *A i j * / ''> >1' ; r, t r* i ; i ' >* i ' * '' '* i ,! tf l'* * >? ,v *>t s* l\ ( iV'V l'' f!f , ! ! a' ' ,, ( i A <, ` i <.< < ,$ ` - < - . < i' ,' / -t... v t' \ </: * ;^.t8sr,!a * r *"'!*"Jj*"E* ,'t '' /lbcprJlwUTefti^er^t19l)orJbt^pliatt^tvloe, > y i* jM^ji ^/AV^iflJtii'i,fo|M^;j>)i!li^rMtWil(:t(0>'havcb<aAjfigseft?boyt ' C1.;tnbm Iji? fjojltiw A5St U* tya&flitoW ,* ( 1 v* A> f ` , ; -a *, ' >, *, ) f, * * in } i < f I MW *Cfct <i! COrk, (Write rylMt,'Smjl nllttlei*iMiW Spcl-pork . n y ' v , '*> ^ f iriiiiK'ifs v>ort wtf WhitMi.WKw <p< ? pwW * | , *. pi i Alula's l^hfioi fcp'.&pcqftf^ jWKjrt Itt.-ttit i&ptoiKltipV life of.s r v`, { , */ ir?'!-, :.k : *!....Si1 sd&tjhit jvpWiVotfe'te isWt'M'Uy'.,; W? .;.<of. pciRvf -*() jiiM. >.;. v 'vr.av '<,iyrj , vy ;>^r.-. 'V'' iOMmciit MS fe()SrltaJH| yi WAI *f>roua>< tytweh tihheff'bjxow)f|illnrss*i.i.i liwlPcl iVfioK, fcustitrfyAii! Aputy ix(9 toxT lioriutly 1, >, ' i 1' iriste'U'J.ilicie is ho U` ii^ t'riO&tfn'OOniwo O!xjonn.;ii,M.Hiuififli,cna t1o6(|Altfroolhbcur Vudtli t * } '*, < 1 t a \ j pbw botWitfl tfult anail|plcmnui|lnhW|diaeuiiniiyyi'/r.'8st^Ki/iey,ctihtisi!:iWwiKSl&j,p.poo!(tiiniiotf - ' ` <6n[,>oafi1i of ca'ilp oil n Kt^Cc|,> lI91jlo0 tlliec'aassOOaa'tf,VVi(jhcfnn (hhec.iicfwimnntial ; 1 ^ &. \ '-v`,, a; O--l-ia--n--r-i-lx--t- --i-t---f-i-o-j-o--w-----t-i-l-t;---s--v--.-i-I-c-K-----S--'-)-a---l-t-!-- o---n- {Iroln (nto -<--l-ii---(-u--n---i-na' 1; % sj , . * olwnlW.V { >'' xV ff,, *i >'......... ..................................................... i x 1 j, ' > y V - v vms t * '\ j> , ^ ,`J 4 / 1j. 1 ^ * ys \* * *s * fH \ ', \ volMfr^ it>t as^ro' ip M^>e< px tc /VUoat c^*4/it>es vyt^h tautiy 0c atofp o(cpn>rn|a3i^o <jen ^ r^at'ycly U\& ^ xf^tep(e'-i}SSl^rt tlist 0/i of fcutd'fert a^^refSvH^ioriJu^thcpt^fft^offaiiMfWlsfext^ntclythkHJl.Wnen UltiUc'<ihfoMnd|}^)ostfa*fur^o'rJ6lrtaic(mtiitswit^> hi **> ^ ' * t t *J ^ ^ w . 1 ?% f' ; ; h * 1 4VhCVJl)'e''ieMfr^l Uiam^cr tyWloW the isvitc1`ci^r/tKfi, the pc.ttir^ ;. .>; i * V* * ^ a ** n t ^w ^ ^ WWty .V V 'lv^''lV'''""" ^Y'f',''''''t^'T''`','vv''' -ty)i fa Pty" ' t ' . Vx ? Jactyr 8!^ WacJuM*vn 9\fa p^U.ng 5<)npou^i W c4Me oil Bod 1 ^ i 4 ^ <K^lpphc^tf<>fwd^ivtrljiQ U^iSftiJ^un^^favmln^tlKj^bie ^ lf-*'>. 'V'" 2' *.;tfv '#' -'. "' ''' . 'k'AfSx'' 3 Jig)0?A<5307 sJL TOWOLDMON0027892 WATER PCB-00012361 vj;', u f ;V iv V.';*'*:1'V*.;';V':''. /' n(- m^} <m * v , < f'u *' ,>>* I * "' , `( `I>V , *// f ' ft '" ^ "" lA ' r HI inn I TOWOLDMON0027893 WATER_PCB-000123 :y ' ^ o>t>y sA'Cjlinfl 'arid cracKjr* Of the- >(poed edgrvfn cau> !? . ' ;: % \ " > V^fe^e^rjlo^tj^ijQWt^a^lfUw^VprctfcnT, 6 Check for Ifipf a# *i pa?*- ii>d gland of switching shall l| leaking icpdck vyitk $ Silastic itnj, type gaP-el *i j VI A*k$r$! ilndci Excc^lvc Ternpeieture or Fault < Conditions r . 'i. ' Ihcltff Guid<> alsopointsouUhat. - vt ^ ^ChWro1>cnz^rtcjt`Vs&d ^ VansTormcr askareH bog'n ic bolt at v . - ' temj>cr&tures of etout20&C,under atmospheric fondmons. If the . ;;:. -`materiel \s heated to such h1# temperature 3n a seated system, ` . f->!' pressure develops; Pressure will also devcjop In the system If the ;. .< ~?.carced sufficiently to$erter*ie copious hydrogen chloride , ; : -A gas > tt. . -v,'. netefore, St Is refcomrnended that'wherever possible, seated *:^iskare1-frileiS equipment he provided with pressure relief devices. >; . v r 7has* devices must f^e large enough to provide immediate relief at ' V` . i definite pressure, and to prevent further build up of pressure II '. x . * peoontpOS{Hon conlinuct.vH mUi be femembeied that the * . y presence of devices of this sort do?s not necessarily preclude the ? 1 .v. < torturing oT containing vessels; since pressure build up can be - ^,;extfern61V pldunder tflolc^arcingconditions."^- ,*-' :. :v '/ * TOWOLDMON0027894 WATER_PCB-00012363 u. ' gfetstaii Analytical Services :r. ..;'6iO'i#isfoncr Askafcl: '. . , Available I'Yotn Monsanto \? , ' ^ iiwii not wishing to.vMfye.$i6b'.f>w/). fluid analyses fctawtylsi.lhe^ylce.ffOm Monsanto..Simply .cont*vt Monsanto6 . ; : arid specify wb&V$rta1y$c& ere V^nt^ YouVvltf benefit the f^or er-stze^ cleaniehtple confiner, Mtd with a ptopet label. When $ ;*vyoy ro'^Wjj ih1s,-.-.^areMly. teke .yogr.^r^ple. (following flic jtfbcodufe for^qtftong id thls guide).end.tbe boluatner w *? , 'Monspnio'*lal*orelory,Ctipi8BS1ifit^.lrtc1udp^nip1epootaiQp(,sh)ppinfl,t)antf)ipS8n(J Ub.orat0fy <^u.. ...... Types of An V* Available * - , * ' Analysts t) 1 ' ' flplN tl^C MAINl l NANCt CHtCfc - TptatCharge $?GOQ 1 , ,,4 4 .^T^detoirt^M^fl^ncr^ condilJon ot tye fluid *nd ffc0 Whetherfurther dnal/sl$.|$ nooe$s$ry.Joiie-<|Uari mpic required) ; * PtoptdiovTeslKl [ ' * V/ DivtodlncBreakdownVoltagf' * ` ....................... ' ' Color ind Condition' - * Mwoistiure 1 ' -> >^ : . Ypu will be ootifKtf oT fic results gf this tesl.if funh<?r tilling is indicated, and you want * complete analysis, you will be , fivoplnt am|>tc container This sample will be used for the following series of 4es.& ,, - ...,.-.?*>..'../;- < f: : . ,- , Analysis 2) * QOVPUH ANALYSIS! ., * Total Charge $5b00 .* - .t (1) to determine i\)t extent of, fluid cohtaibinaflprbTi?) earth refinement to deterrrjtpt Wt*a\ degree 6f miotation of etgeuleal and .$? insulating proputies Is possible, 13)check test to sec how the fluid msponded to fca fl treatment Km\ a) Complete Apatysis: to determine Uic extern of contamination , v. :>. ' v .v- ' - - - - < / Pio^rtiislested free Chlorides Cblpi end Condition , 1 ' Acidity . v>' ' RSpocrrplhlbecGGrraaUvitvy . ' v. ' Dieclleecctlrticicff'caeafckddcowwnnVVoollttaaggee 1v> ; BcfiactWc Index ,^:,v! . Power Factor, Dielectric Constant,^ Resistivity, ,, . m ` ,, ; ..j,., ................,. , ....................... ..... ......... . , . \,. , ?;.. 4v.a b) CMill iRehnimcnl ftesoonsc ^ ' .v ;CohsKk bf Uoatntcni Tor ?.5 hour's 01 bO BtyC. with 0.1 to 0.? percent toy weight of properly conditioned AtiapUtgus c?ay -,& iv 1 and tVep filtration JthVough dry filter paper, v ....... - - - "...... .......... . ............. ' . -*S c) Analysis Aftei l aleatory tarlh Refinement;,' < Properties tested . Acidity j flefiawtlve fndex^ * ; 'Dlieleocctriic Breakdown,.VVoollttaagge v :j f Watof'v 'l V 's \ Power fFaaccttoor. Dielectric Constant, end fRtee^siissttiivvlittVy c^ 2 ^ ;.?;.: - You yyitt be notified Of th? results of tfiis test ^riei on your saorplo. Thcb after refunlnfl yqur entity transformer fluid 1M you . ^ can check 00 the result) by requesting the fo'lowlng analysis | Anafysu 3) ANALYSIS Arif R f AffTH HFFlf'lFVICNI tptalChaigc $3b00 4 , * '' - fT his charge Wilt not apply when ' / , ( r 'I > Analyses 1 and, 2 have already heed made.) '1 ....................... : " To determine Whether' tfo eiit*^ lot of fl>e adorel Ml responded tOtthe $am^ Extent as die. laboratory siqiple. (five-pmt sample (>- . /cqUired)/. *, ... . . .- v. Piopcitie,Tested < ' , Color and Condition Rcha uvcUk! k VVatef l r f ___ _ ... J....... .............................. free CtdorldiS , ,, Acidity r PKlQctricBreakdo^nVoHugt Powcf FactorDielcitnc Constant, and Resistivity .... ; To anaigetor the hsU d( ^rlbcd above Wnie to ibt following address > Padl 9 Btnlgnuj \ \ , s ' ^ `` v . ^f \ ' t MotsantoCompe-ny 1 ' , BOO Not lh Undtx, rgti Blvd. Bt touts,Wr>uUij63fBG* * <(> tv ' "... v (' t* *1 Samplct 1o bt tf.oiflij tf clcstly hiaikcd lor idcnbl icfitiort inti sent duccify to, Mohsirito Chinniest Coittj>ai|y .. ' ,< tV G KrumdilkM m.oratoty ' ' ' , Ss.aot,1Hmol(6?l '' / , An.:it'>o:, R K to' ' ... ' ;.' *' r ' , J07*9310 TOWOLDMON0027895 WATER PCB-00012364 APPENDIX A ' ,' , ' ' ' ' , ,4-*.. *;! ;.*'"-.H-':. 'AiVwcl Stability And.ComjKstftlon of Arc Foimcd <a$: Askercl insulation is one of the most Inert, ^icmWly stable heal mMenh non-corrosive liquids known. UwW not bre&k doyvTb oxidize or sludge when exposed to air and high teirijECiatutes, 160C- or ovon^onjCwfiaf higher Arcing, however* will bresiH^OWn lOie cornpoyniHo jiberfita $op)h hydrogen chloride end amount* of oaibort. / `n * >i t ,, <, , ", ^ *t \'1 ' ' < ' * APPROXIMATE COMPOSITION 1 ' * *% s i 1 * ' .! , ' ARC-FORMED GA$ FROM TRANSFORMS ASKARtLplENDS , ASfM TYRES p AND C ` lINfRllCN 70 30 AND PYRANOl A130303. RESPtCl IVEIY) t , 1J s , 1 (' Ga^ ' > * f Cdiboo monoxide ' coilKSn dioxide ,' ` oxygen v v tncftgaift ',, hydrogen dMoitye * fnot^ Uit absence of phosgene) v_ , 4 % v * * 4. ' Amount 0% 0 3% 0.0% t tt 14>% At 97,3%' ' . t - this artfountdgasjffoni ASlMTypcD end Type f tiAnsfornVcr adcdrels is non flammable end non-oonilMKiiWe.'- . fpi eh practical pmpdsfeh ^`c efnount ol gas liberated from eskarql under a given set of emng conditions H about 100 cubic centimUcfi pci Wtow^l-ttfppruJ t,, v -^ *> *t > ) 1 ,* APPENDIX B solubiuivof ga$ in transformer askarus * A$1M T^PCS O ANt> 0 * ' . ^ ` CerVoo do>dd An Nitrogen ' * HydiogcndMorld'1 * * Mn ebsertC^ of 5cevCrtge| rc<r , Percent of Gas By Volume Conic led to 20 C 760 mm ?0*C ' WC 71% 6.7 w37.8 ; E7% ^.9 > 609 r OC- 700 fis'h - > '-o. 10OC 4' ' . 68 '65 ` 6,0 4.4 l E APPCNDIXC Ef FECI QF 1 FMPERAlORl ON plFt-fCERIC BREAKDOWN VOLTAGE OF ASKAREt VeAtf>Ci eturt *C t > ; f ,r" *' < '*9 ;t w 8(1 , Dir.'lrrtiic R riMV<trnv:'i. Votiaje ASIMDS77 e?Kv - A? , , a ' , <*!$*' - *,: *o 60 ',W * . <te' , . 1 TOWOLDMON0027896 WATER PCB-00012365 APPENDIX t> OO^r'ARI&ON Of 7HE APPftOXIMAU \rfi&X*t1 f IN $AYft>t f UNlVlftSALEOOND$ ., OP TRANSFORM* 6 ASKARFIA ANPMlNtAAt OIL ' letup 3J : ' ` -?P o> 1 20 *0 - ; 60 ' 60 \ 100 ' ' , PywtwA t < _ A13R36 3 ' ' `"owo" ,,v< , ' OH * l/)00 100 , > 100 20 80 48 - ' 49 39 40 34 , 34 30 . 30 r i. ` * . liurteen 20 30 28M 100 - 80 60 40 30 33 APPIND1XC ! " ! 1 ,, ' f ., 'i 1 ' THE DENSITY OF INERUtN2030 ANDlftANSFORMER PYRANOl A13P363 \, Approx Densely #m/ot * ' V^ * 1 Cil.p < , '0 20 - <0 60 ( 80 * ) 4 tneuecn 7030 ' H ` ~ J.574 1.602 1*629 1.607 ' Pyierrof ; > \ A13036 3 " 1.672 1600' 163? 1610 ' 1.486 APPENDIX f . 'Tho tlicrmdl conductivity values oT tr^nsTofmot Tyiavtol AJ3B3B-3 el 27C end 68"C a)e 28,2 and 2b,8 x 10 s calori centimcterst,, desert centigiadc ^ second-*, respectively. Or, approximately O.OC 81U pet <hrj iv. ft.) <*f.) pet too Ttits some approximation applies to Incrteel 70 30 APPENDIXO ;*'............. ................ .... '"`V"... .............. ................... - Heat Capacity v `v 4 1 , Over the temporgiurc ratye of r2&* to 128*0 the specific heat ot trahsfonnct wkarot 1$ dose to 0,30 calories per gram per decree, * * ( s 1' < v *i ' ' *K , * APPENDIX H * *> 1 Coefficient ot |E section ' the average coefficient ot expansion of transtoimci askarel over <he temperature range 20to 100"C is 0-0007 oc/cc/'C.One Ration Would Ino-easf to 1.006 gallons onfieaiing Rom 20 to tOOC.' , ^ : /,,. . ' APPENDIX 1 1 1 '' ' flreRcsIsienoe <\ ** * Askereh of various compositional typos are usod.Undcr arclr^g conditions the pest's produced. White consisting of predominantly i>o>V<!tmbuttibk hydrogen chloride cart yield varying amount* ot combustible gases depending upon the askaiel type, s'1 ,` ' ' . Insulation systems lf\coi porting these askarek and cellulpsic or other organic materials, may. when arood, produce gaseous mixtures wliic^t arc moderately fld'unu'hlc. As a precaution, sutft0u ^ptfldbr removed from Hit aiWrcl by bubbling d'y nllrog . through tta aSka cl arxj Rushing the g&f space with dry nltiog^n before: any work is performed on \H jy&r*ujs 0? TOWOLDMON0027897 WATER_PCB-00012366 APPENDIX J .'-j. 1 ' ; . Seals, Properties arxiPtocuremcfu 1. ^ '' '' ., . .. Dow Doming Corporation, Midland, Michigan with Districts at Atlanta, Boston, Chicago, Cleveland, Dellas, Los Angeles, New York City, Washington, D.C, and Toronto has available Bulletin 09-018, August 196? entitled "Silastic Design Data". This lists the gasket fabricators throughout the country from vs/horti the "Silastic 60" gasketing can be purchased In sheet, extrusions or molded shapes. ' Generally, Silastic 60 sheet goexj!s are stocked by local die cutters, hence, could be generally purchased locally. Usually small quantities of gaskets are die iut. (f larger quantities are needed, tools are made of the same type used to cut other elastomers. Where the gasket Is extruded lor fitting into a machined groove or between gasket stops, Dow Corning advises use of a scarvcd joint. This joint is thet cemented using Dow Coming's Silastic 140 (dear) or their R1V 731 (white) materials, which air cure, Dow Corning points out that tic local "rubber" fabricators purchase the Silastic 60 in billet form. This is worked on a roll mill in preparation for sheeting1 or extrusion. Then to obtain the desired physical properties the fabricator must oven cure the Silastic 60 for 24 hours at 4&0F. SPECIFICATIONS11 AST M D676 ASTMD412 ASTM D412 ASTM D396 Color Specific Gravity at 77`f Hardness, Shore A. Scale Tensile Strength, psf, min Elongation, percent, min Compression Set after 22 hrs at 300"F, percent, max White 1.20 4 0.02 46 to 60 600 260 30 *AH physical properties mcasured on 0.075 indr thick samples molded 6 minutes at 24DF, end oven cured 24 hours at 480F. APPENDIX K Caution label The following or equivalent reution statements should be fixed on ell containers of transformer askarel* and the transformers themselves: This product contains Polychlorinated 8iphenyl$ (PCBs). Care should be taken to prevent entry into the environment through spills, leakage, use, vaporization, or disposal of liquid or containers, Avoid prolonged breathing of vapors or mists. Avoid contact with eyes or prolonged contact with skin. If skin contact occurs, remove by washing with soap and water. Following eye contact, flush frith water. In case of spillage onto clothing, the clothing should be removed as soon as practical, skin washed, and clothing laundered. MONSANTO INDUSTRIAL CHEMICALS COMPANY SPECIALTY PRODUCTS GROUP BOON.LINDBERGH BLVD. SI.LOUIS,MISSOURI 63166 The Information herein regarding obtal ning optimum results from askarel fluids In your transformer has been accumulated by Monsanto for over 40 years from the exporionoe of makers anjii|d users of askarel transformers and It is believed wilt be helpful. Nothing herein shall t>e construed as - plying to other than askarel insulation. Data and maintenance suggestions herein do nol apply to the other conijorients cl the transformer, All oj orating and maintenance suggestions recommended by the manufacturer of the transformer should also bo carefully tollovued. Because these maintenance directions .apply only to tlic askarel insulation, Monsanto disclaims any liability for damage to property or injury to persons arising Iron* transformer opcie'ilion. - . 0?49313 ) TOWOLDMON0027898 WATER_PCB-00012367 cusiQMnt mm cttmfis , * 'i f AKRON, onto mis ` 200 Spungsufe Drhi > j - let (716)560 4111 AUAWA CCORGtA 30339 > .- 320JfflerSwe fifwtft Peftwy ,: Sufic 600 Jet {404)431-7111 '-v. BOS)ON, MASSACHUSEIJS 02149, Cvetett Station ' Jel (617) 387-5010 CHICAGO, \lLUNOlS ' ' . 3153 t>cs Plainer Avt, . : . t>es PJcJript, IffxioU 6001$ 1 fe/ (312) 7*0 &BB CtNCiNNAK OHIO 4533$ 9041 Holbrook Road HI (513)904 1100 ,1 ' bUROff. MICHIGAN. i' 500 Northland 7owort West Southfield Mt$hkidn 43076 ` fef (313) 307-0910 x ", H0VS1ON. UXAS 7/037 1301 Post Oek lower , , . ,^ $051 Wertheimer fioetf . . < : 7et f71$!f21-$556 t 10S ANGLES. CALIFORNIA 9002? 6570 , fjofflh St let (313) 773-2493 * . MW YORK MW YORK 1003$ ' 1114 Avenue of (he Amerku s, nt (>12) 764 SOM ' ST. LOUli MISSOURI 63166 600 H IMkcreh Bhd III. 1314} 694 J000 ' < ` SAN FRANCISCO BAY AREA 3710 htpyotli . Sinle Clin, tiltfomh 9?062 - ' III (406) 343 0414 'A ; \1 SIATUF. WASHINGTON $3121 - . 2112 )Md Ann is Til (20t) 623 4203 ,e _ WILMINOtON. DUAWARE 19310 ' Suits 204. 6mcioft Btde 3411 Slhettlde Rood 1 - hi (30i) 476 4600 'a 1 Monsanto Industrial Chemicals Co A Unit of Monsanto Comj'Snj 800 N. llndkr(,t, Bivd. St.UolS. Mo,$l$0 ; J Monsanto 0?*931<i ) s-Jos VI) 0 tuv it \ f TOWOLDMON0027899 WATER PCB-00012368