Document r677qb0YMOagy8ZvbbrJwyqE

TOXICITY TO AQUATIC PLANTS TEST SUBSTANCE Identity:A mixturecontainingperfluorooctanesulfonatweh,ich may alsobe referredtoas PFOS, FC-95, or as a component ofFC-602. (1Octanesulfoniaccid)(CAS # 2795-39-3). Remarks: The 3M productionlotnumber was notnoted. The testsample isFC-602. Currentinformationindicatesitisa mixtureof1% PFOS, 12% diethyleneglycolbutylether,61.05% water,20% ethyleneglycol,2% Sultone foamer, 1% sodium octylsulfate1,% sodium decylsulfate,1% magnesium sulfate0,.7% xanthan gum, 0.1% starch,0.1% n-(3-chloroallyl)hexaminium chloridea,nd 0.05% tolytriazole. The followingsummary appliesto a mixture with incompletely characterizedconcentrations of impudties. Data may not accurately reflectthe toxicityof the fluorochemical component of the testsample. METHOD: Method: NS-EN ISO 10253, 1998: Water quality- Marine algalgrowth inhibitiotnest Type: Acute Static GLP: No Year completed: 2000 Species: Skeletonemacostatum Source: StrainNIVA BAC1, stockculturemaintainedatRF - Rogaland Research, Stavanger,Norway. Element basis: Estimatebiomass by measuring fluorescence. Exposure period: 72 hours StatisticaMlethods: Growth ratesby Log linearregressionon biomass (fluorescencev)s.time,as describedinNS-EN ISO 10253. Calculatioonf NOEC done by singlefactorANOVA followedby Bonferronisprocedure. Analyticalmonitoring: pH Test Conditions: Algal NutrientMedium: Filterednaturalseawater (34ppt salinityf)rom an unpollutedsiteinBAord, Norway, enrichedwithnutrientasccordingto ISO 10253 and recommendations from the ParisCommission. Thisnutrient medium providedallmineralnutrientesssentialforalgalgrowth and also served as the diluenftorallalgaloperations.The pH ofthissyntheticalgal medium was 8.4. Stock and testsolutionpreparation:A 102.4 mg/L primarystocksolution was prepared by dilutin0g.1024 g oftestsubstance inI L ofgrowth medium. Aliquotswere then added directltyogrowth niedium intestvesselstocreate testsolutions. Exposure vessels: 100 ml flat-boftonifeldaskscontaining50 mi test soluton. Agitation:Shaken continuouslyon an orbitaslhaker. Number of replicates:3 Initiaclellloading: 2.0 X 103 cells/mL Number of concentrations: sixplusa blankcontrol Lighting:Continuous fluorescentlightinagt>50 pE/e sek. Water Chemistry: pH range (0-96hours): 8.3- 8.4(controlexposure) 8.3- 8.4(102.4mg/L exposure) Test temperature range: 20 2 OC RESULTS Nominal concentrations: Bk control,0.32,1,3.2,10,32, and 102.4 mg/L: Reference substance(3,5-dichlorophenoalt)1.5mg/L. AlgalGrowth Response ErCsovalues (based on growth rate) 72-hourErC50= -78 mg/L 72-hour NOEC = 32 rng/L Element valuesare based on nominalconcentrations. Reversibilitoyf Growth InhibitionN:ot conducted. Remarks: Testingwas conducted on a mixtureas describedintheTest Substance Remarks field.The valuesreportedapplytothatmixtureand not the fluorochemicalcomponents alone. CONCLUSIONS FC-602 exhibitsa 72-hour ErC50of~78 nig/L.The 72-hourNo Observed EffectConcentration(NOEC) is32 mg/L forgrowth rate. ValiditcyriterifaulfilleCdo.ntrolcelldensityincreasedby a factorofmore than 16 intestperiodand referencesubstance was withinnormal range. Submitter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA Q ALITY ReliabilityK:limischranking= 2.This studymeets the criterifaorquality testing.However, thestudylacksinformatioonn purityofthetestsubstance and itlacksanalyticaclonfirmationofthe amount offluorochemicalproportion inthe solution. REFERENCES Test was conducted by RF Rogaland Research, ofStavanger,Norway atthe requestof 3M Norge, Lab referencenumber 99312-3,2000. OTHER Last changed: 6/26/00 ia4D.reino.: 99312-3 Page I of31 an AJ iG ik. PM& ROGALAND RESEARCH "FC-602 LightWater Brand ATC plus" Toxicitytests Report RF-2000/003 Lab. ref.no.: 99312-3 No. ofpages: 31 ISBN: Author: FJ[nHorve Crient(s): 3M Norge Distributornestriction: T. VersionNo. date: Vers. 1 /07.012000 Research Program: Open from (date): Summary: The followingtestresultswere obtainedwith"FC-602 LightWater Brand ATC plus": Toxicity:Skeletonema costatum Acartiatonsa Coraphium volutator 72 h ECO 48 h LCSO 10 d LCM (mg/1) -78 (mgA) 200 (mg/kgdryweight) >3070 The resultsrelatetotheproduct as suppliedby Novatech. Key-words: Toxicity,Skeletonema costatum, Acartiatonsa,Corophium volutator. No part of this documerti may be reproduced in any form wftut permission In vvrifingby RF - Rogaland Research 0. A, 7s director lngerUsa Andersen I-L"v forRF - Rogaland Research KAre Netland KVAAGM- pm6sw olm Hanwwvei 15,P.O.B= 2M3 U&m&rjg, 4ogi Skrvanger,Nor@. Tel.+:47 518750 00. FmL +47 51875100. RFR('PN. rr, -Mg Q- KL----- 'rJ - . A7 CC CA '30 Cn C--- . A-? CC C' @O '@ Enmrprisenumber.:9508848M. Lab.refno.: 99312-3 Page 2 of31 CONTENTS: I.PREFACE ...........................................................................3........ 2. TEST FOR TOXICITY 3.nST FOR TOXICITY WITH SKELETOAEMA COSTATUM ......................................4........... wrrh A CARTIA TONSA ...........................................................1.0............... 4. TEST FOR TO)ACITY WITH COROPHIUM VOL UTA TOR ...........................................1.5............. S. DATA SHEET(S) ........................................................................2.0........... Lab.ref7o.: 99312-3 Page3of31 PP&EFACE.- EcOtOxic0logictaelstwsereperformedon "FC-602LighWtaterBrandATC plus"inagreementwith NOvatech-Thesampleisa concentrattehatnormallywillbe usedina 3% AFFF16% AR solutionT-estswereconductedinaccordancewiththe'HarmonisedOffshoreChemical NotificatiFoonrmal"(OSPARCOM 19951SFT 1998). Theprojectwas carriedoutat RF -RogalandResearchfor3M Norge. Alithetestswere perfor?nebdYRF -Miljolab.Studydirectowras SeniorEngineerIngerLisaAndersen. The testresultasrepresentedinseparatesectionsT.heresultrselatetotheproductassupplied by Novatech. Thistestreportisissuedbya laboratorayccreditebdyNorwegianAccreditatio(nNA). The accreditatisotnatetshatthelaboratormyeetstheNA requirementcsoncerningcompetence, equipmentand workingproceduresfoarllthetestmethodscontainedintheaccreditation. Italsostatesthatthelaboratorhyasa satisfactoqruyalitayssurancesystem,whichincludes internaqlualitcyontroslchemes,participatiionninterlaboratocroymparisons,and theuseof certifierdeferencmeaterialasnd secondaryreferencmeaterials. The testpserfor?neadrecoveredby theaccreditation. Yhistestreportmay notbe reproducedinanyform otherthaninfullw,ithouttheper?nissioinn writingby PF -Miljolab. Lab.i-ef.no.: 99312-3 Page 4 of31 TEST FOR TOXICITY Marinealga:Skeletonecmoastatum Lab.refn.o.: 99312-3 Page 5 of3l TEST RFPORT GROWTH INHMITION TEST WITH THE MARINE ALGASkeletonemacostatum an IG Nr.POIS ROGALAND RESEARCH TEST SUBSTANCE: "FC-602 LightWater Brand ATC plus" TEST RESULT: The 72 hours EC50 Was calculatedto-78 mg/l. The testsubstancewas suppliedby Novatech,and thetestresultrselatetothisproduct. TEST DETAILS: METHOD: TEST ORGANISM: NS-EN ISO 10253, 1998:Water quality-Marine algalgrowth inhibitiotnest withSkeletonemacostatumand Phaeodactylumtricornutum. Skeletonemacostatum,straiNnIVA BAC 1. A stockcultureof thetest organismiskept atRF - RogalandResearch. PREPARATIONS: INCUBATION: Naturalseawater(salinit3y4: @oo)from an unpollutedsiteinBAord was used asbasisforthegrowth medium. The waterwas filteretdhrougha GF/C filter, and brieflhyeatedtoabout75*C priortouse. The seawaterwas enrichedwith nutrientasccordingtoISO 10253,and recommendationsfrom theParis Commission. Testsolutionwsere preparedfrom a stocksolutionA. stocksolutioonf 102.4 mg/lwas preparedby stirrin0g.1024grams of theproductin I litroefgrowth medium. Other concentrationwsere preparedfrom thisstocksolution. Testculturesof 50 ml were incubatedin 100 ml flat-bottomefdlaskson an orbitaslhaker,3 replicatefsoreach concentrationT.estcultureswere inocu- latedtoabout2000 cellshnflrom an exponentiallI_y?owing . mo culum culture. The testwas rtm under continuouslight(.> 50 pE/m -sek)from fluorescent tubesof universalnaturalwhitetype,ata temperatureof20:t 2*C. The testwas run forabout 72 hours,and subsamplesof 5 ml were takenfrom thetestflaskseach day forgrowthmeasurements.Algalgrowth was measured by fluorescencep.H measurements were performedas indicatedon datasheet. R:ProfemrOav Hanswsvei15.P.O.Box2503Ullandhou4g0,91 Stayanw,N@orwayT.el.+:47 5187 @Orw) P,@- A7 1;1 A7 r rV) 0r)AAAA(Y) Lab.refno.: 99312-3 Page6of31 DATA ANALYSIS: CALCULATIONS: Growthratewserecalculabtyeldoglineraergressioonnbiomas(sfluorescence) versutsimea,sdescribienNdS-ENISO 10253. ErCso: The inhibitory effect on the growth of Skeletonema costatum is expressed as the concentrationof a product giving 50% reduction of growth rate(EC50). This effecctoncentratiownas calculatebdy interpolatiboentween 32mg/i and 102.4mg/l.. NOEC: CalculatioonfNOEC (No ObservedEffectConcentrationi)sdone by singlefactoArNOVA followedby Bonferronipsrocedureforcomparingeach concentratiomnean with thecontrolmean. TEST RESULTS: CONU%4ENTS: VALIDANON: Table1. EC andNOEC valueosbtainewdithSkeletonemcaostatum. Testsubstance FClo FCso ECgo "FC-602LighWtater BrandATC plus" -78 >102.4 NOEC: 32 Valuejind@te concentrationgsiving10?lo5,001oand 9VIo inhibitioonfgrowth rate.Unitsinmgl7. Valuesarecalculatedby interpolationN.OEC arecalculatedby using thecomputerprogramme GraphPad InStat3.0. The resultasrebased on growth ratesforthetimespan 0 - 72 h,theperiod duringwhich thegrowth isconsideretdobe exponentialinthecontrolcultures (seegrowth curves). The validitcyriterigaiveninthetestprotocolarefulfilleidn,thatthecontrol celldensityincreasedby a factorofmore than 16 inthetestperiod (correspondintgoa growthrateofmore than0,9d-1)t,hecontrolpH didnot varyby more than 1,0unitsduringthetestand the72 hours testresultwsith 3,5-dichlorophenwoals intherangenormallyfound. Lab. ref.no.: Sample received.: Testperiod: Report date: 99312-3 20.09.99 22-25.11.99 07.01.2000 ElinHorve kge Molversmyr Engineer SeniorResearch Scientist Analyticatlechnician QualityAssurance Enclosed: Data sheets ThistestreportisissuebdyalaborataocrcyredibtyeNdorwegiaAnccredita(tNiAo)n.Therepormtaynotbereproduciendany formothetrhaninfullw,ithotuhteperfnissiinwornitibnygRF-Miliolab. Lab.refno.: 99312-3 Page 7of31 PRIMARYDATA..GrowthinhibititoenstwithSkeletonemacostatum Testsubstance:"FC-602Ught Water Brand ATC plus" Lab.ref.9:9312-3 Stardtate:22.11.99 Conc.unit:MgA Measurement:The biomasswas measuredbyfluorescencvea;luesinfluorescencuenits rwne: 22.11.99 23-11.99 24.11.99 25.11.99 Con *ntration 13:40 11:50 13:20 14:45 Growth rate day -1 pH pH Corre- atstart atend lation of test oftest 0 0.06 0.32 1.5 8.2 0 0.06 0.23 1.7 9.3 0 0.06 0.46 3 11 0 0.07 0.46 2.15 11 0 0.07 0.35 1.9 9 0 ---0.12 0.4 2.35 11.5 0.32 0.32 0.32 0.07 0.42 2.4 11.5 0.09 0.55 2.5 12.5 0.07 .5 2.65 12 1 0.08 0.66 3.4 14.5 1 0.07 .0.64 3 13 1 0.09 0.5 2.7 12.5 1.61 0.999 1.66 0.999 1.71 0.992 8.4 8.3 1.66 0.997 1.59 0.999 1.50 0.999 1.68 0.998 1.62 0.998 8.4 8.2 1.69 0.996 1.71 0.993 1.72 0.991 8.4 8.2 1.62 0.999 3.2 0.08 0.58 3.4 15 3.2 0.09 0.45 3 13 3.2 0.09 0.38 2.95 13 1.72 0.996 1.63 0.998 8.4 8.2 1.63 0.998 10 0.1 0.35 3.1 15 1.65 0.997 10 0.1 0.43 3.1 14.5 1.63 0.999 8.4 8.2 10 0.07 0.43 2.6 14 1.74 0.999 32 0.5 2.7 14.5 1.67 0.999 32 00..0098- 0.46 2.1 11 1.62 0.998 8.4 8.3 32 0.09 0.43 2.9 13 1.63 0.999 102.4 102.4 102.4 0.1 0.07 0.09 0.13 0.08 0.1 0.2 0.18 0.2 0.43 0.43 0.73 0.48 0.979 0.60 0.971 8.4 8.3 0.69 1 0.944 Reference subst ce (3,5-dichbmhenol): 1.5 mg/i o.i o.16 0.48 1.1 1.5 mg/i 0.07 0.18 0.44 1.4 1.5 mg/i 0.1 0.15 0.38 1.15 Mean values: 0 0.07 0.4 2 10 0.32 0.08 0.5 3 12 1 0.08 0.6 3 13 3.2 0.09 0.5 3 14 10 0.09 0.4 3 15 32 0.09 0.5 3 13 102.4 0.09 0.1 0 1 Reference --- E4 0.79 0.993 0.98 0.999 1 8.3t 8.2 0.80 0.987 1.62 1.66 1.68 1.66 1,67 1.64 0.59 0.999 0.997 0.995 0.998 0,999 0.999 0.964 The resulotfthe reference substanc(e53% inhibitiiosn) ,ilhihne range normallfyound (20-80%) Lab.i-e;fio.: 99312-3 Page8 of31 GROWTH CURVES: GrowthinhibititoenstwithSkeletonemacostatum Testsubstance:"FC-602LightWaterBrandATC plus" Lab.ref.:99312-3 7- Control U) E :5 1 0 -3 i 48 72 tessttdurraation(hours) 7 5 c 23 0 E0 :5 1 -3 0 0.32 mg/l 48 72 48 testduration(hours) duration(hours) 7-, 51 (D 3 1 mg/i 0 :5 -1 ,D@X4 -3 48 72 t,,tduration(hoursl duration(hours) 7 5. e 30 10 mg/l E :5 a1 0 -3@@test 48 72 duratio(nhours) 7 -e 5 e0 3- 3.2 mg/i 0 :5 -1 @test -3 48 72 48 dratio(nhours) uratio(nhours) 71 (D '0ei,351 'A 'A I -3 32 mg/i 48 72 duration(hours) 7-, 102.4 mg/i 5 E0 .3-.. @4 48 estduration(hours) Lab.ref.no.: 99312-3 page9of31 Inhibition of the growth of Skeletonema costatum with: mg/l (FC-602 Light Water Brand ATC plus) --------------------------------------------------------------------------- Experimental data: ---------------------------------------------------------------------- Concentration in Growth rate FC-602 Light Water Brand ATC plus Inhibition in percent ---------------------------------------------------------------------- Control 1 Control 2 Control 3 Control 4 Control 5 Control 6 1.61 1.66 1.71 - 1.66 - 1.59 - 1.50 - Control mean 1.62 0 0.32 0.32 0,32 1.68 0.0 1.62 0.1 1.69 0.0 1.00 1.00 1.00 1.71 1.72 1.62 0.0 -0.0 0.1 3.20 3.20 3.20 1.72 0.0 1.63 0.0 1.63 0.0 10.00 10.00 10.00 1.65 0.0 1.63 0.0 1.74 0.0 32.00 32.00 32.00 1.67 0.0 1.62 0.1 1.63 0.0 102.40 0.48 70.4 102.40 0.60 63.0 102.40 0.69 57.5 ---------------------------------------------------------------------- Lab.refno.: 99312-3 Page 10of3/ TEST FOR TOXICITY MarineherbivorAec:artitaonsa Lab.,-efno.: 99312-3 Page II of31 TEST REPORT ACUTE TOXICITY TEST WITH THE MARINE COPEPODAcartia tonsa na 4G f#rm.s ROGALAND RESEARCH TEST SUBSTANCE: "FC-602 Light Water Brand ATC plus" TEST RESULT: The 48 hours LC50 was calculatedto200 mg/l. The testsubstancewas suppliedby Novatech, and the testresultsrelatetothisproduct. TEST DETAILS: METHOD: ISO/DIS 14669 - 1997:Water quality- Determinationof acutelethatloxicity tomarine copepods (Copepoda, Crustacea). TEST ORGANISM: Acartiatonsa (Dana),suppliedby theMarine BiologicalLaboratory, Universityof Copenhagen. CULTIVATION: The testorganisms were suppliedaseggs,and were cultivateidnaccordance with the"ParisCommission - Ring TestProtocol"(VKI). Largecopepodites and adultswere used in thetest. PREPARATIONS: Naturalseawater(salinity3:4 %0) from an unpollutedsiteinBAord was used as basisforthe dilutionwater. The water was filteretdhrougha GF/C filter priorto use. INCU13ATION: Testsolutionswere preparedfrom a stocksolution.A stocksolutionof 1000 mg/l was preparedby stirrin0g.9998 grams oftheproductin I litroefdilution water. Other concentrationwsere preparedfrom thisstocksolution. The testwas run in glasscontainers(28 ml rolledrim vialse)ach containing 25 ml oftestsolutionand 5 animals,4 replicatefsoreach concentrationT.he vialswere kept under a 16h/8h light/darpkhotoperiodata temperatureof 20 I 'C. pH and oxygen measurements were performed as indicatedon the data sheet. Lab.t-enfo.: 99312-3 Page12of31 DATA ANALYSIS: CALCULATIONS: The effecotnthesurvivoaflAcartitaonsiasexpressaesdtheconcentratoifon a productlethatlo 50% ofthetestanimals(LCso).The combined mortality pertestconcentratiownere used forcalculation'.Me 24 hoursand 48 hours LC50 valuesand the95% confidencelimitwere calculatebdy usingthe standardprocedurePROBIT AnalysisN,ationalSwedish Environmental ProtectioBnoard (Version2.3,1990).Thisprogramme alsocalculatteest concentrationlsethalto 10% and 90% of thetestanimals. NOEC: CalculatioonfNOEC (No ObservedEffectConcentrationi)sdone by singlefactorANOVA followedby Bonferronisprocedureforcomparingeach concentratiomnean with thecontrolmean. TEST RESULTS: Table 1. LC and NOEC valuesobtainedwith"FC-602 LightWater Brand ATC plus" Acartiatonsa 24 hours 48 hours LC]o 120 (56-190) 87 (42-130) LC50 350 (250-490) 200 (140-270) LC90 970 (650-2200) 450 (320- 900) NOEC--- 100 100 Valuesindicate100/o5.001oand 90% lethalitayfter24 and 48 hours.Unitsinmgll.Valuesare calculatebdy PROBIT anainis,and 95% confidenceintervalasreindicatedN.OEC arecalculatebdy thecomputerprogramme GraphPadInStat3.0. VALIDATION: The validitycriterigaiven in the testprotocolare fulfilledi,nthatthedissolved oxygen concentratioanttheend of thetestwas greaterthanor equalto4 mg/l, thepercentagemortalityinthecontrolswas lessthan 10%, and the48 hours LC50 of 3,5-dichloropheno(lreferencew)as intherangenormallyfound. Lab.refno.: Sample received.: Testperiod: Reportdate: 99312-3 20.09.99 22-25.11.99 07.01.2000 Enclosed: Data sheets \\p Y-X-@ ElinHorve Age Molversmyr Engineer SeniorResearch Scientist Analyticaltechnician QualityAssurance Thistesrteporitsissuedbya laboratoarcycreditebdy NorwegianAccreditati(oNnA). The repormtay notbereproduceidnany formotherthaninfullw,ithouthepermissioinnwritinbgy RF -Miijolab. Lab.ref.iio.: 99312-3 Page 13 of31 PRIMARY DATA: AcutetoxicittyestwithAcartitaonsa Testsubstance: "FC-602 Light Water Brand ATC plus" Lab. ref.: Startdate: Measurement: 99312-3 10.11.99 Number of dead Concentration (mgA) Control 10 32 100 320 1000 Total number Number of specimen pr.vessel Specimen A C E pr.conc. B D F 556 30 4 55 5 55 20 5 5 55 20 5 5 55 20 5 6 54 20 5 5 64 20 5 NUMBER OF DEAD 24 hours A CE B DF Total 000 000 0 48 hours ACE B DF Total 0 01 0 00 1 1 00 1 00 0 1 0 1 0 00 002 0 0 0 '2 0 10 020 1 2 1 @3 410 443 2 7 4 15 5 54 564 5 19 5 20 Reference substanc (3,5-dichl phenol): 1.0 mgA 30_] 5 5 5 6 4 5 0=01 1 01 3 331 0 11 9 The resuftwith the reference substance is withinthe range normally found. Lab.refno.: 99312-3 Page 14 of31 Testsubstance:"FC-602 LightWater Brand ATC plus" Lab. ref.: Startdate: 99312-3 10.11.99 Afeasurementsofoxygen and pH. Concentration (mgA) Control 10 Start Oxygen pH (mgA) - 7.3 8.2 7.6 8.2 24 hours 48 hours Oxygen pH Oxygen pH (mgA) (mgA) - 7.4 8.2 7.3 8.2 32 7.6 8.2 100 7.6 8.2 320 7.6 8.2 1000 7.4 8..2 7.2 8.2 7.1 8.2 6.7 8.1 5.7 8.0 .-. I --- T Referencesubstanc (3,5-dichlorophenol): 1.m0gA L 7.3 8.2 8.2 i Lab.refno.: 9 312-3 i I Page / 5 of 31 TEST FOR TOXICITY Marine Amphipode: Corophium volutator II i Lab.i-ef.iio.: 99312-3 Page 16of31 TEST REPORT ACUTE TOXICITY SEDIMENT TEST WITH THE MARINE AMPHIPOD Corophium volutator noNMSK AKKAEDrrr:RING ROGALAND RESEARCH TEST SUBSTANCE: "FC-602 LightWater Brand ATC plus" TEST RESULT: The IOd LCSOwas calculatetdo>3070 mg kg-1dryweightsediment. The testsubstancewas suppliedby Novatech,and thetestresultsrelatteo thisproduct. TEST DETAILS: METHOD: ASTM E 1367-90,StandardGuide For Conducting10 day StaticSediment ToxicityTestswith Marine and EstuarineSediments. TEST ORGANISM: Corophiumvolutatofrr,oman unpollutesditenearTrondheim. CULTIVATION: The testorganismswere suppliedas adults(4-8mm insize)and were heldin aeratedseawaterat 15'C. A smallamount ofnaturalseaweed was used for feeding. PREPARATION: Naturalseawater(salinit3y4:%o)froman unpollutesditeinBAorden outside Stavangerwas used fordilutiownater.Sedimentcollectedatan unpollutedsite was used forpreparingtestsediments.The sedimentisa muddy sand and was analysedfororganiccontentand proportionsilftoreach test. Each testconcentratiownas preparedby addingtheproductin600 grams of damp sedimentina plastibcucket.200 mi of seawaterwas added and the bucketwas shakenfor3 hours.The sedimentwas dividedintothreebeakers, 400 ml of seawaterwas added toeach,and thebeakerswere aeratedover night.10 animalswere thenrandomlyselectefdoreachbeaker.A sample of thedamp sedimentwas analysedforwater contenta,nd allconcentrationasre calculateads'mg kg-1sedimentdryweight. INCUBATION: The testwas run inglasscontainer(s600ml) eachcontaining200 g of test sediment,app.400 ml of seawaterand 10 animals,3 replicatefsoreach concentrationT.he beakerswere keptunder continuousaerationata temperatureof 15 :tIOC. pH and oxygen measurements were performed as indicatedon thedatasheet. 0": Pro6sm Olav Hanssensvei 15, P.O. Sm 2503 U16n&", 4091 Sta@anw, Nor@ay. Tel.:+47 51 87 50 00. Fax: +47 51 8752 00. Enterprisenumber.:950884800. -47 r@ 5A @10@r' rn. @A7 'Z@@A IR AO Lab.ref.no.: 99312-3 Page 17 of31 DATA ANALYSIS: CALcuLATiONS: The effecotnthesurvivaolfCorophiumvolutatiosrexpresseadstheconcentratioonfa productlethatlo 50% of thetestanimals(LC50).The combined mortalityper testconcentrationwere used forcalculationT.he 10 day LC5o valueand the 95% confidencelimitarecalculatebdy usingthestandard PROBIT Analysis,NationalSwedish EnvirorunentaPlrotectioBnoard (Version 2.3,1990).This programme alsocalculatteestconcentrationlsethalto 10% and 90% of thetestanimals. NOEC: Calculatioonf NOEC (No Observed EffectConcentration)isdone by singlefactorANOVA followedby Bonferronisprocedureforcomparing each concentrationmean with thecontrolmean. TEST RESULTS: VALIDATION: Table 1. LC and NOEC valuesobtained with "FC-602 LightWater Brand ATC plus". Corophiumvolutator 10days LC,o 1750 LCso >3070 Lcgo >3070 NOEC: 3070 Values indicate10*lo.50*/oand 90*lolethalitayfter10 days. Unitsin mg kjf'sediment dry weight. Values are calculatedby PROBIT analysis.NOEC are calculatedby the computerprogramme GraphPad InStat3.0. The validitcyriterigaiveninthetestprotocolarefulfilleidn,thatthedissolved oxygen concentrationatthe end ofthetestwas greaterthanorequalto60 %, thepercentagemortalityinthecontrolswere lessthan 15% and a testwith Fluorantene(referencew)as intherangenormallyfound. The sedimentused isfound tobe withinacceptedlimitsfororganiccontentbut thesiltfractionis recommended higher. Table2. Characteristiocfsthesedimentused fortesting Organiccontent(0/o) 0.7 Siltfi-action 0.8 Lab. ref.no.: Sample received.: Test period: Report date: 99312-3 20.09.99 03-12.1@.99 07.01.2000 ElinHorve Engineer Analyticaltechnician SeniorResearch Scientist QualityAssurance Enclosed: Data sheets ThistesrteporitsissuebdyalaboratoarcycredibtyeNdorwegiaAnccreditat(NiAo)n. The reportmay notbereproduciendany formotherthaninfullw,ithouthepermissioinnwritinbgy RF - Miliolab. Lab.rqfno.: 99312-3 Page18of31 PRIMARY DATA: AcutetoxicityestwithCorophiumvolutator Testsubstance: "FC-602 LightWater Brand ATC plus" Lab. ref.: Startdate: Measurement: 99312-3 03-12.99 Number ofdead Total number Number of specimen pr.vessel Concentration Specimen (mg/kgdryweight) pr.conc. ACE BDF Control 10 10 10 60 10 10 10 10 10 10 257 30 10 10 10 478 30 10 10 10 1050 30 10 10 10 3070 30 NUMBER OF DEAD 5 days ACE BDF Total 10 days ACE B DF Total 000 000 0 1 00 1 010 1 310 4 201 3 Reference substanc (fluorantnhe): 10 10 10 20.3 30 3 22 7 The resultwith the reference substance iswithinthe range normally found. Lab.ref.no.: 99312-3 Page 19of31 Test substance: "FC-602 Light Water Brand ATC plus" Lab. ref.: Startdate: 99312-3 03.12.99 Measurements of oxygen and pH. Start Concentration Oxygen pH (mg/kg dry weight) (%) Control 94 8.1 5 days Oxygen pH 91 8.1 257 93 8.1 92 8.1 478 93 8.1 91 8.1 1050 95 8.1 92 8.0 3070 96 8.1 88 7.9 10 days Oxygen pH 91 8.0 82 8.1 81 8.1 90 8.1 89 8.1 I Reference substance (fluranthene): 20.3 95 8.1 90 8 .1 T 90 8.1 L.UU.fv.liv.. 99312-3 A tit;(;:v (@/11 DATA SHEETS I 11 99312-3 HMS-DAT.KBLAO (=else-, M4-1-4,oo-g S4-kkerhetsdatablad) Dokumentnr.: Er3ta-.ter : 07-2573-9 Utg;-tt 08/1-0/97 Skrevet ut : 10/11/98 Versjon : 11/11/98 S4-de 05.00 1 av 11 H,MS-databladem er utarbe;-dez av Miljoavdelingen Tele.'on: 63 84 75 00 / Telefax: 63 84 17 88 ved 3,4Norge A/S. -----------------------------------------------------------------------1 !DENTT7T'KASJON Nli KJ--M:<.Ul7T OG A-NSV.A-RLIG FIR,%iA. ------------------------------------------------------------------------ importor: 3,4Norge k/S Handelsnavn: .-C-201.1'-z WA:7-.R (TM) 11 AF,7F (FREEZE PROTECTED) Deklarasjonsnu-nme=, Produktreg4-steret: Tele!on, Gi.'z;-n--2or-ias4onssentralen: 22 59 1-300 ------------------------------------------------------------------------ 2 OPPLYSNINGER OM Kj7-i47-SK SAm4'4ENSETNING. -------------------------;------------------------------------------------ Informasjon om enkeitkamoonenter, faresymbol(er) og r;-s4-kosetninger STOFFNAVN CAS-n:, V---XT-?ROSEN'-r ------------------------------------------------------------------- VANN 2-(2-BUTOKSYT-T-OKSY)-ET.!k.NOL 7732-18-5 112-34-5 35.0 - 39.0 17.0 - 21.0 (DIETYL7-NGLYKOL,%IONOBUTYT-ET---R) Faresymboler/risikosetninger: Xi; R:36 1,2-ET,'@4NDIOL Faresymbol-er/r4-si-kosetninger: Xn; R:22 107-21-1 14.0 PUMFOTER FLUOROALKYLAL*4!D-DERIVAT ALKYL-SULFAT-SALTER TRIETANOLAMIN Trade Secret Trade Secret 102-71-6 5.0 - 10.0 14.0 - 16.0 = 3.0 PERFLUOROALKICL-SULFONAT-SALTER RESTER AV ORGANZSK7- FLUORKJEMIKALIER Trade Secret Trade Secret 1.0 - S.0 Ikke kjent 99312-3 FC-201AZ- LIGHT WATER (TM) 1% Arrr (FR--EZE PROTECTED) -----------------------------------------------------------------------3 VT-KTIGSTE .7A.R=-MOMENT=-.R. V4-k-:;-gsteskadev4-rkni-nge:, ------------------------------------------------------------------------ Helse-@-are: L@LR:TERENDE (Xi-) -,rr4-terer eynene. S;-kkerhet: M;-Ijofare: 4 FORSTE=:T-LPSTILTkK ------------------------------------------------------------------------ '-r-61-taokyne: Skyll szraks oynene grund4-g med ri-kelige mengder vann ;-m;-ns-@1-5* minu@@ler. Kantak@- lege umiddelbart. Skylling under transport. Ti-l-takhud:. Sky!-' s@@raks huden med sipe tilsolt toy. Hvi-s sympt6mer toy !or det brukes igjen og og rikelige mengder vann. Fjern oppstil--ikonta.c@,lege. Vask tilsolt kas-@ tilsolt sko@@oy. T;-'-takinn&nd;-ng: Hv;-s sy-np-lomerooosti-@--,bring eksooneringsk;-'-den. Sorg for kontak-: lege. vedkonmende frisk luft. bor@- fra Hv4-s symptomene vedvarer, T;-'-taksve'-g@-ng: Kon--akt lege umiddelbart. Fremkall brekn4-nger kun i sam--id med med;-s;-nskpe*=-sore'-'-G.;- aldri noe gjennom munnen til en beviss"@los person. -----------------------------------------------------------------------5 TILTAY% V---DBRANNSLUKi.4!NG. ------------------------------------------------------------------------ Egnet brannslukningsm.,Lddel: Produktet er et brannslukkingsmiddel. Ikke egnet brannslukningsmiddel: Eksponeringsrisiko ved brann: 99312-3 FC-201AF LIGHT WATER (TM) 1% AFFF (NMEZE PROTECT--D) Forbrenn4--gs@rociukter ved brann: ?zosedyrer ved slukk;@ng av brann: -----------------------------------------------------------------------6 T---LTk:<VED UTILS'-rKTr-TUTSLIP?. ------------------------------------------------------------------------ Personl4-ge vernetiltak: Se vernez;-I-takunder andre punkter i dette H,%IS-databladet. T"-Itakved i,@ils4ktet utslipp: Venti_'_-_ormr&det. Soi-I-Iavgrenses umiddelbart. De.<k ti-Imed at absorberende materi-ale. Spill samles oup um;ddelbazz. Rengjor omradet med vann. ?Iasseres i en egne't beholder med lokk. Fjezning av k-i@em;-kaj'.ieaalvlf: Se -ounk-:1-3,Fjerni-ng av kjer,;-kalieav-lall. ------------ ----------------------------------------------------------7 :i.L-NDTER7-Nr.OC- OP?SEV.-,.R:@IJC-. ------------------------------------------------------------------------ Bez4-ngelser for s4kker oapbevaring: Mi ikke lag?--esi omr&der hvor produktet kan komme 4 kontakt med mat e'-Iez legemi-dier. Lagres ved tempe--atur under 49 grader celsius. Lagres ved temperaturer over 0 grader cels;us. Hold beholderen tett lukke@-.n&r produktet ikke er i bruk. U@'orenel;-ge materialer: Ventilasjon: 0-opbevar emballasjen p& et godt ventilert sted. S4-kkerhetst;-I-r-afkor A forhindz-e brann: S;-kkerhetstiltak for A forh;-ndre eksplosjon: Ikkebrennbar. Sikkerhetst;-I-takfor & forh;-ndre statisk elektrisitet: Forholdsregier ved bruk: Hold emballasjen tett lukket. Royking forbudt: Under bruk av produktet kan reyking forirsake forurensning av tobakken og/eller royken og farlige dekomponeringsprodukter kan dannes. Se punkt 10, stabilitet og reaktivitet, skadelige dekomponenter. L Lab.ref.no.: 99312-3 Page 24qf31 FC-201AF LIGHT WATER (TM) 1% AFFY (FREEZE PROTEcTzD) ------------------------------------------------------------------------ 8 EKS?ON7-RZNGSKON-@Ror-r- OG P7-RSONLIG V-mRN7-UTSTYR. ------------------------------------------------------------------------ Oyevern: unng& A f& da-.ip,spray eller vernebr;-Iler med vent;-Ier. t&ke i eynene. Bruk tette H&ndvezn: Bruk egnede verne;-ansker h&ndter;-ng av produkzet. anbefales: Butylgumm-*-. av hens i-k!--s-,nessm4a-tgeri-ale ved Vernehansker av fol-gende mater;-ale(r) Anne,. hudvern enn hindvern: Unng& hudkontakt. indedrettsvern: unng& inn&ndin; av lu--@zb&re@-materi-a-l-e.Basert a& konsentrasjonen av lu-4t@4orurensn;--,ger4- arbei-dsa@-mos---arenvelges en av folgende type(r) godkjenz iiidedrettsvezn: halvmaske med -F;-I-temrot organ;-ske damcer og vaskeformi-ge parti-klez: k/P2SL. Sve',-g--r,g: De@"-m& i-kke sp;-ses, drikkes eller reykes under arbeid med produktet. Vask utsat--e omr&de-@ grundig med sipe og vann. hende@e etter hindte=-;-ng og for sp;-s4-ng. Vask Anbefalt ventilasjon: Ev;-s utsugningsvent;-l---s4on4-kke er tilstrekkeli-g, ml egnet godki,ent &ndedrettsvern benyt--es. Sorg for t;-I-strekkelig venti-'---sjosn!4-k at damokonsent.-asjonene holdes under anbe!alte ad,n4-n4-strativenormoir ag/eller kon-@roller saray eller t&ke. Adm. normer for @-Forurensn4-ng 4-arbe4@dsatmosfere, .7eb-ruar1996: VANN (7732-18-5) A-i.-nerkn4-ngeie-.-::tgenacin. norm. 2-(2-BUTOKSY7-TOKSY)-T-'-*AL40L / (0@-r-TYLENGLYKOL,40NOBU,@-'YLT-TE.R)(112-34-5) 8-t;-.Inervserd;- oom: 35 Anmerkninger: Amerikansk grenseverd;- anbe-@2a!tav produsenten. (ingen norsk adm. norm). 1,2-ET.kNO10L (107-21-1) 8-timers verd;-ppm: - (stov) 8-timers verd'@ mg/m3: 10 (stov) Takverdi ppm: 25 (damp) Takverdi mg/m3: - (damp) AMFOTER FLUOROALKYL,@.M!D-DERIVAT (Trade Secret) A.nmerkninger: ingen adm. norm. ALK@'L- SULFAT -SALTER (Trade Secret) Anmerkninger: ingen adm. norm. Lao.rei.no.: @6' 99312-3 FC-201A-%"LIGHT WATER (T,4) It AYrr (FRI-PEZEPROTECTED) 8-t;-.mersverd4- ppm: 8-timers verd4- mg/m3: 5 ?7-R.7LUOROALKYL-SULFONAT-SALTr-.R (Trade Secret) 8-timers verd;- mg/m3: 0,1 Anmerkni-nger: Ameri-kansk grenseverd;- anbefalt (Ingen norsk adm. no=). av produsenten. R=-ST-v-ARV ORGANISKT- FLUORKJ7-Ml'<ALIER (Trade Secret) 8-timers verd;- mg/m3: 0,1 Grenseverdi- anbefalt av 3M. --------------------------------------------------------------------9 -TYST-c-XzO-G Kj=-MISKT- EGENSKA-MER. ------------------------------------------------------------------------ T4-1-s-:ands@lormf,arge, lukt: Kokeounkt/-i-nterva'--I: S,-ielzenunkt/-intervall: Klar rav-4arget vas'<e. 7.5 - 8.5 100 C (Begynnende kakeounkt) Zkke relevant > 100 C (,%i;-nlia-sfh) Se',-va.n-lennelighet: Eksolosjonsgrenser, nedre: Ekszl-osjonsgrenser, avre: Dan--azz,ikk: Loselighet i vann: S.oes@-.g.i-kvkekt: Damutetllhet: Ikke relevant ikke relevant ikke relevant 16 =Fg (Kaikulert v/20 C) B'6a-dbar - 1.10 (vann=l) - 1.0 (laft-1) (Kalkulert v/20 C) Flykti-georganiske forbi-ndelser (VOC) 359 g/l SCAQMD produktat) (g/l. av Fordamon;-ngshastighet: V;-skositet: 1 (butylacetat-1) 18 centipoise Lab.ref.no.: 99312-3 Page 26 OJJI FC-201A-Z LIGEIT WATER (Txt) 1% AFFF (FREEZE PROTECTED) ----------------------------------------------------------------------10 STAB:LZTT-T OG R-TAKTIVITET. ------------------------------------------------------------------------ Forhol-d som ska! unng&s: mater;-aler som skal unngis: ikke kjent. Farlige sdaitni-ngsprodukter: Kar'oonmonoks4-d og karbondioksid. Hydrogen.Iluorid. Giftige damper, gasser eller part;-kler. Te--m;-skdekomoonering av bruksferdig bland;-ng forventes ikke i reoresentere noen risiko. Stab;-I;-'----otg reak@:@-v4-t--et: S:abi-l-t.Farli-g polymer;-sasjon vi-1 ikke forekomne. ------------------------------------------------------------------------ 11 OPPLYSNINGER OM Er-LS=-.7AR-=. ------------------------------------------------------------------------ Z-.@fe'<tereyne: ,Moderat oye;-rri-i---asjons:ymptome@- kan vere s,nerter,tirer og uklart syn. rodhet, hevelse, Effekter hud: Modera@@ hud4-rri@@asjon (et-@er langvar;-g eller gjentatt symptomer kan vare rodhet, hevelse, kloe og torrhet. kontakt): Langvarig eller gi4entatt eks.ooneri-ngkin fore t4-l-: Allergi-sk hudreaksjon: og kloe. symptomer kan vere rodhet, hevelse, bi-er=er Effek--er innSLndi-ng: En enkelt overeksconering no--mer, kan fore til: som overstiger anbe@Ialte administrative P&virkning av sentralnervesvstemet: symptomer kan vare hodepine, orhet, sovnighet, manglende koordinasjonsevne, nedsatt reaksjonsevne, sioret tale,-svi=elhet og i ekstreme ti'Lfeller beviss'tloshet. irritasjon (ovre luftveier): symptomer kan vare sirhet i nese og svelg, hosting og nysing. Ef"lekter svelging: oyreforsok utfort med organiske fluorkjemikalier, som finnes i dette produktet, viser effekter som leverforstyrrelser, vekttap manglende appetitt, slovhet samt effekter som plvirker neurologi, bukspytt, binyre og hematologi. Det foreligger ingen kjente helseeffekter for mennesker fra eksponering overfor organiske fluorkjemikalier n&r de brukes som forutsatt og i henhold til Lab.ref.no.: 99312-3 FC-201A-7 LIGHT WATER Page 27 of31 1 (TM) 1% AFFF (FR--EZE PROTECTED) ve4-ledn;-.-g. Sveig4-ng kan 4-ore t;-'-: ?iv4-rkn;--gav nvrene: symptomer kan vare redusert urinmengde, blod uriren og --yg'gs-.nerzer. Asz4-asionsoneumoni (Lungebetennelse som skyldes at fre=edlegemer kommer ned i lungene. En aim;-nnel4-gArsak t;-l ti-lstanden er opokas"6.): symptomer kan vare hosting, pustevansker, giso;-ng, hoste ooo blod og lungebetennelse som kan vare 14-vstruende. Informasjon am allerg;-, overfelsomhet: Kre@'tfre.mkalleide egenska=ez: A--vestoffskadel;-ge egenskazer: Rearoduksjonsskadel;-ge egenskamer: Andre skadevirkn;-nger, he!-se: Det-leproduktet ;-nneholder en eller flere organ;-ske fluorkjem;-kaliez, som -,uuligenskan absorbe=es ag lagres i kro-o-cen over lengre ti-d,enze- som utgangsmolekylet elle= Sam nedbrytni-ngsstof--Ier(;-,ietabol4-tter)o,g kan akkumuleres ved gjentatte eksponeri--ger. Det foreli-gger i-ngen kiente helseeffekter -6'or mennesker fra eksmoner4-ng over-'or organi-ske fluorkjem;-kaii-er nir de brukes som -foru@---sato-g@ 4-hen*-.old t;-'-ve;-Iedn-@ng. -7orekomst--enav organ4@ske 16!uorkiemi-kalier i blodet til den generelle befolkningen og undernooulasjoner som arbeidere, har vart publisert,siden 1970 Arene. 3-Msepidemiologiske studier av egne arbeidere viser :.ngen skadelige e.Ifekl,er. ------------------------------------------------------------------------ 12 OPPLYSNINGER OM MILJOFkR-=. ------------------------------------------------------------------------ Persisl@ens/Biologisk nedbrytbarhet: Dette produktet inneholder en eller flere organiske fluorkjemikalier som muligens ikke ar nedbrytbare og forblir i miljoet (persistente). Andre skadevirkninger, Nedbrytning: m;-I-jo: COD (Chemical Oxygen Demand) - 1 710 000 mg/kg; BOD 20 dagers (Biochern;-caloxygen Demand) - 494 000 mg/kg; B0020/COD - 29%. Akvatisk giftighet: ,Lao.rej.no.: j 99312-3 FC-201AZ- LIGHT WATER (TM) 1% AFFF (FMEZE PROTECTED) 96 t4-.nersLCSO !or -4;-sk(Fathead minnow (Pimephales promelas)) 310 msil; 43 timers EC50 for dam*-nia (water flea (Daphnia magna)) > looo mg/l; 96 timers ICSO for alge - > 1000 mg/l; 30 min,,tters ECSO, m;-crotox (Photobacteri-um phosphoreum) 63 mg/l; 3 timers EC50, Act;-vated Sludge Resp;-ration inh;-b4-tion- > 1000 mg/l. Sorg for avfallshindtering iht. gjeldende forskz4--'ter. -----------------------------------------------------------------------13 FJ=-@LIT-NG AV ------------------------------------------------------------------------ Metoder for @--jern;-nagv kjem;-ka!4-eavfall: Soesialav!all. Lever altg-allt;-'-en offentlig godkjen-@ i-nnsamier, mottaks- eller behand!4@ngsanlegg for spesi-alavfall. .knbe!alte av'.alisgruope=: HOV-=DK.k--':-'GOR0I7: AV.7.ALL F?-A,ORGANISXF. PROSESSER. UNDERK.k-TT-GOR! 07 06: kv@-Fall fra PBDB av fetts--oA'4-@er,s&-oe, rengjor;-ngsmidler, des4-nfeksjonsmidler og kosmetikk. EA:<-kode 07 06 03: 1.alogenerte organiske losem;-dlez, vaskevasker og moderlut. Av!alls--of-4numn,er:7151 organ;-sk av!all med halogen. SDesiell-e komponenter: fluorforb;-ndelser. ----------------------------------------------------------------------- 14 OPPLYSNINGT-R OM TRA-NS?OR'-r. ------------------------------------------------------------------------ ADR-kiasse: - siffer: - bokstav: - margnummer: - CEFIC-kort: - UN-nummer: - ICAO-klasse: IMDG-kiasse: - Lab.ref.no.: 99312-3 Page29of31 FC-201A-- LIGHT WATER (TM) it AFFF (?It--EZE PROTECTED) IMDG-s;-de: EMS-nr.: M-7AG: evrige oool-vsn;-nger: ikke transport!ar!4-ggods. -----------------------------------------------------------------------15 OPPLYSNINGER OM LOV---ROG FORSKRI.7T7-R. ------------------------------------------------------------------------ Merkeel.ikett: Symbol(er): H=-LS7-S<'ADEL IG (Xi) inneholder: 2-(2-bu-@oksyetoksy)-emanal 19 Etylenglykol 14 % R-setn;-nger: Farlig ved svelging. 7-----;-tereeyrnene. S-setni-nger: Unng& inninding av d---in/soreytek-AkeU.nng& kontakt med oynene og langvar;-gkontakt med huden. Fi:-man stoA'&'eit eynene; skyll straks grundig med szore mengder vann og kontak- lege. Etter hudkor.takt, vask me.--s4&oe og vann. Ved svelging, kontakt lege omg&ende og vis cenne beholderen eller eti-ke-Iten. YL-gru,ace: 00 Korr. yrkeshvg. lgftbehot: 0-30 M3/1 ovrige opplysninger om me=keetiketten: ovennev,itemerk;ng er basert p& tidligere merke'.orskrifterog vil vare & finne p& produk-.eten tid fremover. merk;-ngenvil imidler-liderstattes av folgende merking, som er basert PA reviderte merkefors'<z;-fterav januar 1998. symbol: IRRITER-=NDE (Xi) Inneholder: 2-(2-butoksyetoksy)-etanol, 1,2-etandiol Irriterer oynene. Unng& inn&nding av damp/sproytethke. Unng& kontakt med oynene. unngi lanqvarig eller gjentatt kontakt med huden. F&r man stof4et i oynene; skyll straks grundig med store mengder vann og konzakt lege. Etter hudkontakt, vask med sipe og vann. Ved svelging, drikk to glass vann og kontakt lege um;-ddelbart. Lab.refn.o.: 99312-3 Page30 of31 rC-201AZ* LIGHT WATER (TM) 1% AFRF (FMEZE PROTECTED) YL-gruppe: 00 Spes4-elle lover og beste=elser: 1. Forskz4--4tom uta:be;-delse og di-stri-busjonav Heise-, m,'-Ijo-og Sikkerhetsdatablad -for farlige kjemikalier. 2. For3kri-zt om klass4--4iseringog merk4-ng av farlige kjemikal;-er. 3. Forskrift om klass;-@li-sering,merk;-ng m.v. av sto,.2fsom kan med,zere miljofa=e. 4. rorskr;-,It om sto@@@fkartotek. S. Forskr;--4tom spes;-alavfall. 6. Etc. -----------------------------------------------------------------------16 ANDR-7 OP?LYSNT-NGER kV B7-'-nYDNT-NG.--OR BRUK7-RN7-S SIK-.<ER.H--rTOG HELST-. ------------------------------------------------------------------------ Anveidel-sesomzide:-: Fil.mdannende skumkonsen@@ra@@ for slukki-ng av brann i hyd-@okarboner.. V;-'-,t;-gstk-;;--'--de(r) ved u-:a:-!--e4-deLseanv ;LMS-da@--abladet: Datablad fra 3,14General 04-@-@@i-ceSst,. Paul, M4-nneso-@a, USA. irsak til obodatering: Lzel.eda-abladet er rev4-dert. Ti-l-passe-n.ye merke- og HMS-dat&bladforskz4.-----erf,astsatt i januar 1998. Etc. Egne o.oolysn;-nger: In@--o--masjonen piL del@te FMS-databladet er i henhold til v&re niverende ooolysninger og beste opp-4atning angiende riktig bruk og h&ndteringen av dette Droduktet under normale forhold. Enhver bruk av produktez tam ikke er i samsvar med detze F.,MS-databladet, eller som medforer bruk av produktet i kombirlasjon med andre produkter eller enhver annen prosess er brukerens ansvar. Lab.ref.no.: 99312-3 Page 31 of3i FC-ZOIAF LIC;EETWA= (TM) 1% -KFFF (FREEZE PROTECTED) : FOLCENDE PRODUKTE:T D7-XK=-'SAV DT-TTE HMS-DATABLADET: 3,4 ID-nr. : ZF-0002-0842-9 3M L;-ght Water 1% A-7FF Fire Fighz;-ng .7oam, FC-20!A-7, 200 L 3M ID-nr. : Z---0002-0841-1 3M Light Water 1% A.7.7FFire F;ghting Foam, FC-201AF,1000 L 3M ID-nr. : X.7-0008-0205-8 3,%1Li-git Water 1% AFF.7 F;---e F;-ght;-ng .7oa.,n,FC-201.;-7, Bulk 3,4 10-nr. : XF-0008-0203-3 3M Light Water 1% AFF.7 Fire Fighting Foam, FC-201AF,1000 L 3M.10-nr. : X7-0008-0202-5 3,'4Light Water 1% A-7FF Fire F'-ght;-ng .7oam, FC-201A'.@',200 L 3'4 10-nr. X"2*-0008-0200-9 3M Light Water F4-ghtiig Foam, 1% AFF=' Fire FC-201A:-, 20 L RF - Rogaland Research RO.Box 2503 Ullandhaug 4004 Stavanger Norway Telephone:+47 51 87 50 00 Telefax: +47 5187 52 00 Visitingaddress: Professor Olav Hanssensvei 15 Bergen: Thormohlensgt. 55 5008 Bergen Norway Telephone:+47 55 54 38 50 Telefax: +47 55 54 38 60 Interneth:ttp://www.rfno