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CG ' - Cxi ' CODE YE-698-D
O'!?
m^sm ( DATE )
LZftZl 5527# LBS* ^jO
( LOT ) 1 < EST WT )
BLENDED BACK: CG
PROCESSES < ) YE-698-D <T)
APPROVED BY: FWP 10/15/82
CCMTYP JOB NAME: 01YE698DMT
D
-EQUIP MENT
NAME; MOLYBDATE ORANGE
7"usi~~ ~
T"a c c t
LBS
| N-CODE i LBS
PREP 1
359 3
OBTAIN SODIUM SULFATE FOR S-13 1 CALCULATE 6 SET ON BADGER METER F
(NITRIC ACID WEAK> IOBTAIN SODIUM CHLORIDE FOR S-33 I^Kl OBTAIN SODA ASH FOR S~3? |5 I OBTAIN SODIUM SILICATE FOR S-39
LJ5BTAIN SODA ASH FOR S-43 OBTAIN ANTIMONY TRIOXIDE FOR S-46
/ -1.
84 |
'fi !
___1 734 | 146 1 237 | 35 1
70 1
1 08-A
33-D 4-A 3-A
32-D 3-A
711-B
WEIGH SODIUM CHROMATE INTO V-351 * ,, <y , Mil1
OPTR_____, MK^2^/7-C`/^r%
1
OPTR_____, MK
______ _%
J
10-D
I ^TliElGH IN SODIUM MOLYBDATE SOLUTION
3i0L
ii
OPTR
MK &JL, 1-4W_, 4/lZfeX
|I
OPTR_____ , MK____ , T-___, _____ 7,
423-D
I 84
I
1 1 734 1 146 1 237 I 35 I 7
j
1 1885 1
!
1 303
358 4
ft N 1* <500 G) WATER INTO V-358 RUN V-359 INTO V-351.6 PUMP IN V-351
ADJ TO 55- <2600 G)
SIFT IN N-108-A FROM S 1
\#AJr STIR 5 MIN & RECORD: PH__fyL< 9/0-10.) 1 ADJ TO PH 9*8-9-9 6 RECORD: PH______
t (CAUSTIC SODA SOLUTION)
ASSUME 50% ASSUME 667.
ADD N-33-D FROM S 2 USING BADGER METER
TO 66" (3121 G) AT 67-69*F
RECORD; VOL_ijk_" & ^_k.7_F STIR 5 MIN 6 RECORD: PH_____(7.4-7*6) 6
G/ML JJLj A_(1 *O80-1*G83)
) NOTE IF G/ML OUT OF LIMITS FILL. OUT CHECK .
LIST 6 ATTACH* TAKE 1 QT SAMPLE
7-D 33-D
SV <uw 20* (996 G) WATER INTO RECORD N-41-D STORAGE TANK TO PUMP FROM. IROLE ONE: 402 41O 411 420 424 425 CHECK WITH CU SUPV: ^STORAGE TANK MUST CONTAIN AT LEAST 2376 GAL: 402=49", 410=25", 411=48", 420=25",
424=25" 425=31" ^STORAGE'TANK MUST HAVE STIRRED AT LEAST
20 MIN SINCE LAST ADDITION OR ADJUSTMENT I ^STORAGE TANK MUST BE ISOLATED UNTIL ALL >f PUMPING FOR THIS BATCH IS COMPLETE fT i SET METER FOR 30 G 6 PUMP TO SV _____
1982
v,--------- -- COMTYP JOB NAME: 01 YE698DMT PAGE 02
DATE PRINTED : 1 0/tT/82,,
di}U I V 1
1 USE | N-- IACCT
WENT 1 i
SV 1221
51 i CONI 1 1
11
AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY.. RECORD BELOW* IF NOT IN RANGE, STOP PUMPING & SEE SUPV.
* PH: ______ <2.2 *3.7)
LBS 1I I |
| CODE 1 LBS lj
|| | I1 | 1I ||
1 1 * DENSITY:_____ ___ _ G/ML (1.270- 1.328) 1231 IF S-22 OK & WHEN S-21 COMPLETE, RECORD
|| 11|
1 I DENSITY
G/ML ON TRAPPED SAMPLE
1I|
I 1 FROM END OF S-21 PUMPING.
11
1241 USING DENSITY FROM S-23, FIND METER SETTING FOR 1 1 I
1 1 SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
1
1
1 1 ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21 .
!I
f 1 CIRCLE DENSITY 6 SETTING IN TABLE BELOW *
i
11 1 1.
TABLE
1! f1
1 1 G/ML SETTING | G/ML SETTING I G/ML SETTING !
1
1 1 1 .270 1678 1 1 .291 1534 1 1.312 1410 1 1 1
i 1 1 .271 1670 | 1 .292 1 527 1 1.313 1404 1
1
1 i 1.272 1663
j 1 .293 1521
1 1.314 1399 1
1
1 1 1.273 1656 J 1.294 1515 1 1.315 1394 1 1 [
I 1 1.274 1649 | 1 .295 1509 1 1.316 1388 1 1 [
1 1 1.275 1641 | 1 .296 1503 f 1.317 1383 1 I 1
t 1 1 .276 1634 I 1 .297 1 497 1 1.318 1378 I I I
I 1 1.277 1627 | 1 .298 1490 1 1.319 1372 1 1 1
1 1 1 .278 1620 | 1.299 . 1484 1 1.32 1367 1
1
1 1 1 .279 1614 I 1 .300 1478 1 1.321 1362
I
1 1 1.280 1607 | 1 .301 1473 1 1.322 1357 1
1
"'' tJ-/' -
1
1 1 1 .281 160 | 1 .302 1 467 1 1 .323 1 351 !
i
1'
1 1 1 .282 1593 | 1 .303 1 461
1 1.324 1346 \
1 <J
.i.-ns;
1 1 1 .283 1586 | 1 .304 1455 1 1.325 1341
1
1 1 1 .284 1580 1 1 .305 1449 i 1.326 1336 I 1 1 '
I I 1.285 1573 1 1.306 1444 1 1.327 1331 1 1 1
I 1 1.286 1566 1 1 .307 1438 1 1.328 1326 1
1
1 1 1 .286 1566 | 1.307 1 438 1 1.328 1326 1 1 1
1 1 1 .287 1559 ! 1 .308 1432 1 1.329 1543 1
1
I 1 1.288 1553 | 1 .309 1427 1 1.330 1537 1 1 L
) 1 1 .289 i 546 | 1 .310 1421
1 1 ,331
1532
1 i v.'.,.*
1 1 1 .290 1540 | 1 .311 1415 1 1.332 1526 1
1
11 I25| SET METER & PUMP
i11
(RECORD FROM TABLE)
!
1
I
1 1 FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 1 i I
1 1 30 SECONDS 1261 ADJ LEAD NITRATE TO 76 * <3625 G) AT 67-69*F.
1 1 41 -D | 51 iV
1 f RECORD1
F
1 I 57-A 1.
1271 STIR 5 MIN 6 RECORD PH: ____ <2 .2-3.7)
!11
1281 IF NECESSARY ADJ TO PH 3 .0-3.1
ASSUME 66%| ________ ! 33-D 1. ^_______
1 1 6 RECORD PH: _
ASSUME 50%1 I_________________
7-D |
! 1 NOTE: DILUTE N-7 --D~ 1*0 : 1 WITH WATER BEFORE ADDING| 1 1 '
1291 RECORD : _______ G/ML C 1 .1 43-1 .1 44 > IF OUT OF SPEC! 1 1
1 I FILL OUT CHECK LIST it ATTACH.
-
I1
'.
1301 STIR AT 67-69*F FOR S-31 . TAKE 1 QT SAMPLE.
1 'Mz.
DUP050059698
^?*cnr:_______ ^vEQUIP I
COMTYP JOB NAME: 01YE698DMT PAGE 01
Dffc|RIfEBi10^g6f2
r*MENT
<3-221. AT APPROX 100. G WHILE CONTINUING TO PUMP rrr^S i | CHECK PH 6 DENSITY. RECORD BELOW, IF NOT ptrONTI | IN RANGE, STOP PUMPING & SEE SUPV.
I LBS 1 CODE | LBS
-I--___ _i___ ___ I____
I 1 .!
I !
i
! I ' PH`. J&Jfe? <2,2-3.?)
' '< I f >* DENSITY:
G/ML < 1 *270-1 *328)
\2zyiF s-22 o k & w h e n s-21 c o mp l e t e , r e c o r d
l DENSITY 'Ji.jLL G/ML ON TRAPPED SAMPLE
' * , FROM END OF S-21 PUMPING,
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW, NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21,
CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
TABLE
\
^ .... k:__... ,, rrr .... ...i IT 1(IT ..- w
__________ _ ]
G/ML SETTING | G/ML SETTING 1 G/ML SETTING|
| 1
1 .27 1644 1 1 .291 1504 1 1.312 1382 |
|
1 .271 1 4- 77! 7Am
163? 1630
| 1 .292 1487 | 1,293 1491
! 1.313 1 1.314
1376 1 1371 1
1 j
1 .273 1623 1 1 .294 1485 1 1 ,315 1367 1
|
1 ,274 1616 ! 1 .295 1 479 i 1 .316 1361 1
1
1 ,275 1609 1 1 .296 1473 1 1 .317 1356 |
i
1 .276 1602 | 1 .297 1467 1 1.318 1351 j
]
1 , 277 1595 1 1,298 1461 1 1 .319 1345 |
|
1 .278 1588 1 1,299 1455 1 1 .320 134 |
j
1 .279 1 .280 1 .281
1582 1575 1568
1 1 ,30 1 errm"" 1 VrwKf*^1438
1 1,321 1,322 1 ,323
1335 1330 1324
1 1 1
1 I 1
1 .282 1562 1 1,303 1432 i 1 .324 1319 |
1
1 ,283 1555 1 1,304 1 426 i 1..325 1315 1
1
1 .284 1549 ! 1 ,305 1420 i 1.326 1310 | %
|
! 1 1 ,285 1542 ! 1 ,306 1416 i 1--327 1305 1 v
1
1 .286 1535 1 1,30? 1410 i 1.328 130 j
j
1 .287 1528 ! 1 .308 1404 i 1 ,329 1295 1
i|
1 .288 1522 I 1,309 1399 i 1.330 1290 |
|
1 .289 1 1515 1 1,310 1393 i 1 ,331 1285 1
1
1 ,290 1510 ! 1 .311 1387 l 1 .332 1280 !
|
I 1 i 1 1 1 1 1 } 1 1 1 1
1 1
1 1
1
1
1 i 1
1
SET METER & PUMP IMll ._& (RECORD. FROM TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
SECONDS
|
ADJ LEAD NITRATE TO 3625 G (76"-242/245 6 74,5" |
I
247) AT 67-69F
'
Ii
RECORD: ___ fe,,X_,,.*F 6 ICE CONSUMED <330*/BL0CK)
! :2?T STIR 5 MIN 6 RECORD PH:
(2,2-3.?)
1330X2 ! |
USE TITRIMETER TO ADJUST N-41-D PH ###*
|
IF NECESSARY ADJ TO PH 3.0-3. 1
ASSUME 667.1
I ! h RECORD PH: 3_'jL_
ASSUME 50%|,,jE__
NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING!
RECORD: /
G/ML (1.143-1.144) IF OUT OF SPEC!
u FILL GUT CHECK LIST 6 ATTACH,
j
STIR AT 67~69F FOR S-31. TAKE 1 QT SAMPLE.
|
4157-
33- -D 7- D
il TO
v
DUP050059699
LOT: . fgirap
ENT f
COMTYP JOB NAME: 1YE698DMT PAGE 03
DATE PRI I USE i LBS
SV I ^TtiBTAIN 1 QT SAMPLES OF S-18 6 S-3 SOLUTIONS
15 -1 I N TITRATE TWICE
CONTI
I NOTIFY SUPV IF ML N -i-D IS NOT IN RANGE
I 7,1-7,4 OR IF THE TWO TITRATIONS DIFFER BY
I_____ I
i |
I MORE THAN 0.1 ML N-10-D (IF YES, FLUSH I EQUIPMENT & REPEAT TITRATIONS)* DO NO
I PROCEED IF N-10-D TITRATION IS OUT 0
I ADJUST V-358 FOR A TITRATION PH OF-frrt I FROfLFIN^k IN-LINE TITRATJONj^RECORD LOWEST I PH JLxiJL ML N-1
I_____
WHEN S-31 TITRATION OK , STRIKE V-358 THRU
SV I BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
6 | 16-18 MIN
/&
I RECORD: START 4.^.lC.__XTOTAL MIN__lH
| NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
U & bu bbl es appear in s ig h t g l as s es 33^T IMMEDIATELY DUMP IN N-4-A FROM S 3 h SET TIMER
JT' FOR 15 MINUTES
34 | DURING S 33, WASH IN V-358 ,
35XT STIR 2 MIN & RECORD PH.3f_i-/._< 1 *8-2*5)
' PBXS,_4^---(MUST BE + )
STIR TOTAL OF 15 MJ ROM S-33 &
' X""
RECORD: TEMP_J*<L_.#F (67-73#F)
3/F I DUMP N-3-A FROM S-4
3^ STIR 3 MIN 3Vjr POUR IN N-32-D FROM S-5
4#'> STIR 2 MIN
AyJ( RUN IN LIQUID ALUM USING BADGER METER
WJ STIR 3 MIN & FLUSH ALUM LINE WITH WATER v DUMP IN N-3 FROM S-6
\ STIR 4 MIN FOR S-48
,`
734
TED : 1 415/82 N~ ACCT
CODE LBS
367
RUN IN HYDROCHLORIC ACID USING WEIGHT 6 FLOW,.
39 CONTROL PANEL
MK______ ,
7 MK ______ ,
\J(g| DURING S-44 SIFT N-711-B FROM S~7 INTO V-39
WITH AGITATOR ON IN 1-2 MIN
STIR 1-2 MIN TO MILKY SOLUTION
| I J~%P.
I______ | I I
28 ~D 28-D
1 5
SV WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B I 8 I SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
| WATCH FOAM!\ ! IF FOAMING IS EXCESSIVE, STOP
J UNTIL FOAM SUBSIDES.
AJt? TV! (HP TW R|
FTXF M
33 vX"i28-A 33
SI WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
I TOP OF PAGE 1
J, RECORD : CODE ____ ^Trr LOT
5<>' STIR 2 MIN
-
5i>KREC0RD : PH_<5, 8-6. >
52T 1 IF NECESSARY, ADJ TO PH 5.EH6.0
ASSUME 5%
7-D
LX & RECORD; PH-______ ASSUME 66%
3 3-D
34/1 FLOOD TO 153" (7298 G) 6 STOP AGITATOR
I
I
DUP050059700