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Southeastern Operations
400 Chastain Ctr. Blvd., NW Suite 490 Kennesaw, GA 30144 (404) 499-7S00 Fax (404) 499-7511
Clayton
ENVIRONMENTAL CONSULTANTS
October 19,1992
Ms. Darlene S. Creel DOW CHEMICAL Industrial Pfygiene, Building 3502-W
P. O. Box 150 Plaquemine, Louisiana 70765-0500
Clayton Project No. 44372.00 Purchase Order No. 1588298 MSI No. 163110 Lab Report No. 92J037
Dear Ms. Creel: Attached is our analytical report for the samples received on October 15,1992.
Please note that any unused portion of the samples will be disposed of in 30 days, unless you have requested otherwise.
We appreciate the opportunity to be of assistance to you. If you have any questions, please call me.
Sincerely,
Owen S. Crankshaw Supervisor, Microscopy Services Southeastern Operations
OSC/bjm
Attachment
Clayton Environmental Consultant!, Inc. A Marsh A McLennan Company Detroit New York/Newark Atlanta San Francisco Los Angeles Honolulu Boston Windsor, ON Toronto Birmingham, U.K. London, ll.K. Southhampton, U.K.
Lab Sample No. 47049 47050
47051 47052 47053 47054 47055
Client Sample Identification
Dumpster Core Sample
Composite Sample
#4 - Center of Boiler Floor
#1 - Below Debris
#2 - Below Debris
#3 - Below Debris
#4 - Below Debris
Results of Analysis of Bulk Samples for Asbestos Content
for Dow Chemical Company
Clayton Project No. 44372.00 Kennesaw Lab Report No. 92J037
October 19,1992
Sample Description
% and Type Asbestos
Brown fiber & mineral mixture, inhomogeneous
Brown fiber & mineral mixture, inhomogeneous
5 Chrysotile
Trace, < 1 Chrysotile
Brown fiber & mineral mixture, inhomogeneous
Brown fiber & mineral mixture, inhomogeneous
Brown fiber & mineral mixture, inhomogeneous
Brown fiber & mineral mixture, inhomogeneous
Brown fiber & mineral mixture, inhomogeneous
Trace, < 1 Chrysotile
Trace, < 1 Chrysotile
Trace, < 1 Chrysotile
Trace, < 1 Chrysotile
Trace, < 1 Chrysotile
Clayton
ENVIRONMENTAL CONSULTANTS
Page 1 of 3
% and Type Non-asbestos
Fibers
Type Non-fibrous
Materials
10 Cellulose 30 Fibrous glass
10 Cellulose 40 Fibrous glass
20 Cellulose 40 Fibrous glass
10 Cellulose 25 Fibrous glass
10 Cellulose 25 Fibrous glass
10 Cellulose 25 Fibrous glass
10 Cellulose 25 Fibrous glass
Binder/Filler, Paint, Quartz
Binder/Filler, Perlite, Quartz, Calcite
Binder/Filler, Calcite, Quartz
Binder/Filler, Perlite, Quartz
Binder/Filler, Perlite, Quartz
Binder/Filler, Perlite, Quartz
Binder/Filler, Perlite, Quartz, Calcite
DO 0 114097
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Clayton
ENVIRONMENTAL CONSULTANTS
Clayton Project No. 44372.00 Kennesaw Lab Report No. 92J037
Page 2 of 3
United States Environmental Protection Agency. Environmental Monitoring Systems Laboratory. 1982. Interim Methodfor the Determination ofAsbestos in Bulk Insulation Samples. EPA-600/M4-82-020. Washington: GPO, December.
Percentages are visual estimates based on volume.
Limit of Detection: <1% Limit of Quantitation: Wo
NOTE: The reliable limit of quantitation of the method is Wo, although asbestos may be qualitatively detected at concentrations less than Wo. Samples for which asbestos is detected at < Wo are reported as "trace, < Wo". No asbestos detected (NAD) indicates that no fibers were observed.
Clayton's Kennesaw, Georgia laboratoiy is accredited by the National Institute of Standards and Technology's National Voluntary Laboratoiy Accreditation Program (NVLAP Lab No. 1125-00). This test report relates only to the items tested and may not be used to claim product endorsement by NVLAP or any agency of the u.S. Government.
_D A 114698
ONr TDFNTIAL
Clayton
"environmental CONSULTANTS
Page 3 of 3
ANALYTICAL METHOD FOR ASBESTOS IN BULK SAMPLES USING POLARIZED LIGHT MICROSCOPY (PLM)
A representative portion of the bulk sample is transferred to a small dish. The sample is examined under a stereo-microscope at 10 to 40 X magnification to determine if the material is fibrous and to note the physical characteristics of the sample. If fibers are present, fiber morphology is noted. Forceps are used to extract fibers from the sample. At least one fiber representative of each type observed in the sample under the stereomicroscope is extracted and mounted on a microscope slide using a refractive index liquid (Cargille Series E: HD [high dispersion]). After mounting, the fibers are analyzed and identified using polarized light microscopy (PLM) supplemented by dispersion staining. After fiber identification using PLM, a visual estimate is made of tne percent composition by type of asbestos present and by type of other fibrous materials identified. The visual estimate is based on volume and is accomplished using stereomicroscopic examination of the bulk sample.
References
McCrone, Waller C 1980. The Asbestos Particle Atlas. Ann Arbor, MI: Ann Arbor Science Publishers, Inc.
United States Environmental Protection Agency. Environmental Monitoring Systems Laboratory. 1982. Interim Methodfor the Determination ofAsbestos in Bulk Insulation Samples. EPA-600/M4-82-020. Washington: GPO, December.
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