Document qkKLR5w25rqVBpOaqKGJ7gq8R
MICROBICS MICROTOX@) TOXICITY TEST
TEST SUBSTANCE
Identity:Perfluorodecanesulfonatea,mmonium salt;may also be referred toas PFDS, FC-1 20, or 3M Sample J2905-1.(1-Decanesulfonic acid,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,1100-,10, heneicosafluoro-a,mmonium salt,CAS # 67906-42-7)
Remarks: Test sample isa mixtureofthe testsubstance inwater and butylcellosolve(approximately25% testsubstance,37.5% butyl cellosolveand 37.5% water).Allvaluesreportedrelatetothismixture. No calculationwsere made toadjustforthe actualconcentrationofthe testsubstance inthe testsample. Test sample was from 3M Lot 164.
METHOD
Method: MicrobicsMicrotox@"BASIC" Procedure Test type: Staticacute GLP: No Year Completed: 1992 Species: Photobacteriumphosphoreum Analyticalmonitoring:None Statisticamlethods: Microbicscomputersoftwarepackage Test organism source: MicrobicsMicrotox@Reagent Test conditions:Per Microbicsmethod Replicates:Two
RESULTS
Nominal concentrations: 125,250, 500, 1000 mg/L Test Sample Element values: 30-minute EC,o = 79 (65 - 96) mg/L
30-minuteEC5o = 327 (299 - 358) mg/L
CONCLUSIONS
FC-120 exhibiteda 30-minuteEC5o forPhotobacterium phosphoreum of 327 mg/L.
Testingwas conducted on the "as-sold"mixtureofthe subjectmaterialin water (-25% subjectmate@al).The valuesreportedapplyto thatmixture and not directltyothe subjectmaterial.
Submifter:3M Company,EnvironmentLalboratorPy.,O.Box33331, St.Paul,Minnesota,55133
DATA QUALITY
Reliability::Klimischranking2. Thisstudy,whilewellconducted,lacks 'analyticdaaltafor:determinationofthetestsubstance concentrationinthe testsolutionsa;nd determinatioonfthesample purity.Because a mixture was tested,care must be takenwhen interpretitnhge results.The solvent inthemixturecouldhave enhanced or restrictebdiologicaulptakeand/or toxicitoyf thefluorochemicaclomponent.
REFERENCES
This studywas conducted by the3M Company, Environmental Laboratory,St Paul,MN, Lab Request number J2904, 4/20/92.
OTHER
Lastchanged: 5/18/00
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Sample Description )DO
Ln-T
Environmental Lab - Work
16A
Sheet
Lab Request No.
P,,e
of
Date: A"o@
YSrj
l@nr)fn @ C)0 rnv@ 0
k,.1-"
P-1
I
Li
sk
-OA@_
CP
t$CL-T-
10
FINAL RESULTS
'NUME'ER ------
3 4
5 6 7 a
COi'4C. ---------
250.0000 251).4)000 500.0000 500.0000 1004).04)00 1000.04>00:.
GAM?I#A
C-AvoMA EST.
--------- -----------
0.1277 C#. 1:7-i :-@ 0 - -@712 -1 0. "->9-@ci
o>. 1 --:'71 (-$.1.@-7 1 'C.sZ 685 Co.
0.58Z-.B
5
Co. 57'-"@@-
t'
% EFFECT ---------
94
C 0 =1660.7427 ma/L (q54 CONFIDEt4CE
TO
&',"LCTot.tctSvPIACE-PAR to continoie....
Koo mmm
0.
I
L 1.
PILE NAME: J2904-I.K5 SamDle Descriotion:
MICROTOX
DATA REPORR
TEST DATE-. TEST TIME:
FC-124'.)LOT 164 YELLOW COLORLESS
LIQUID:
TEST CONCENTRATIONS
ARE CLEAR.
Procedure: BASIC I!iit,,-.Caolncentration Test 7ime: 5 minutes
: 1000 mall
Osmotic AdiLtstment: NaCl Dilution Fa.=tor : '-n Conc:entreti-on in-.ts: ,r-ri-L
NUMBER -----
1 2
4 5 6 7 8
IC)/IT
-------
E34/ 48 49
SO/ 43 84/ 45 75/ ::,7 $311 -@8. Si/ 711 8-@l/ 3
R-ONC. ---
125.000t') 125.0000 25(1. 4-jOOO 25C).0000 5C)O.0()00 51.)4-0)0.00 1;)04.-0@0.00 1000.0000
GAMMA ---------
O.C,6075 0:0267@@-x 0.1-e-77;-# 0.13146# 0.22867# 0. Z-9i-@4)4# 0.58..@-79# C,. --p7.-1tC-31#
CONTROI- IT/I() = 55/ 9--
BLANK RATIO = 0.6C'o'-
I f',')L)DDL)DDL)Lr)DDDDDDDDDDZ)LlVDDDDDDDDDDDDDDDDD.-'7DDDDI)1)1)1,)Lr)DD[)#Z't)DrD.D:)?
.3SLOPE
1.0786
3
.3
G .3
A .3 m3 m
A. 3
.3
>zzzzzzzzzzzzzzzzzzzzzz-.
.3 13
.3
.3
3
.3
6
.3
5
.3 4
EC 50
.10 @DDDDDDDDDDDDDDDDDDD*-DDD.DDDDDDDDDDDDDDD@DDDDDDDDVDDDDDDDPDVY
ICp(.0
CONCENTRATION
IOE4
.3 .3 -1 3
.3 .3
3 13 3 13
ICIE5
EC 5c) =1660.7427
(95% CONFIDENCE
RANGE:1319.82'-'@O TO z-;OB9.7'->58)
Used for calculations Invali-d oammas
STATISTICAL
REPORT FOR DATC- FILE J29t.-p4-l.t'--?
ESTIMATING
EOUATT-ON:
LOG C = Cx.9129 < L'IG b -*3.2207,
NUMBER OF DATA PAIRS USED:
6
RESIDUAL VARIANCE:
t:).(-)(:)17@c?
95% CONFIDENCE
FACTOR:
FOR EC5".
CORRELATION
COEFFICIENT:
R = 0.99229
EFFECTIVE
CONCENTRATIONS
(9-j% CONFIDENCE
RANGE):
EC 5C) =1660.741-7 ma/L EC 2(-)= 468.4890 m9/L EC 10 = -:@23.461-@- ma/L EC 1 = '-?5.0@@49 mc?/L
@1-19.e@22C) i 4"@@4.7483 ( 188.4842 ( !4.7624
TO --@'c)89.7258)***
TO 516.7341)
TO 264.9290)***
TO
42.4556)***
EXTRAPOLATED
F,*ESULTS
F7INAL F;.ESLILT,-,
j-9C)4-I.KI5
-----I2
4
6
a
---------
'-'5. 1--
--------4).16136
25(). 5(- (),JO 5o(-.(.-)o(-)()
14)4.)0".)Ooc)
I
0(@)OO.)
44 9--64 9886 2.756:-7, -:. 84-:@o-P
GAMMA EST. -----------
cl. 1 --139 1). 0. -;-646
6 ().99'-Tl C). 99@-'1 2.74C)46 2. 71:p46
% EFFECT ----------
14. 4'-;@9 1i-I5.11
5 - 1 '-6?
4t-@. e26 49.714
. 78 7.. 4)19
EC
_',C),-.).949m6a/L
(95% CONFIDENCE
RANGE: 46@@-.6E347 TO
541.2094)
L'CCCTot-tch SPACE BAR
to contlr--Lte
.... CCCI L
PC) io
MICROTOX DATA REPORT
;71LE NAME: 3'@.904-1.t'%15 Sample Description:
TEST DATE: TEST TIME:
-@O LOT 164 YELLOW I:)RLESS
LIQUID:
TEST CONCENTRATIONS
ARE CLEAR.
F'rocedLtre: BASIC Initial Concentration Test Time: 15 minutes
: 1000 mall
Osmotic Adjustment: NaCl Dilution Factoi-- : -@ Concentration Units: mo-/L
NUMBER -----
1 2 Z. 4 5 6 7 J3
10/IT -------
84/ 3(1 83/ 31 BO/ 25 84/ 26 75/ 16 BI/ 17 al/ 9 83/ 9
CONC. ----- ----
125.0000 125.0000 250.0000 250.0000 500.0000 500.0000 1000.0000 1000.0000
GAMMA ---------
0.16862# 0.11746# 0.33557# 0.34841# 0.95640# 0.9886-",# 2.756299 2.849@^-@l#
CONTROL IT/I()
38/ 92
BLANK RATIO
0.4174
10 ZDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDI-,DDDDDDDDDDn
.3SLOPE
1.4454
.3
3 .3
.3
-3
.3.
1 .3
3
-3 nk 3
.3
.3
1 >zzzzzzzzzzzz
6
3
3
3
4-
.3 1
EC 50
32
.10 ODDDDDDDDDDDDD.DDDDV^DDDDDDDDDDDDDDDDDDD-DDDDDDDDDDDDDDDDDDVY
1 f)O
1000 CONCENTRATION
lOE4
3 IOE5
7-C 50
500.9496
(95% CONFIDENCE RANSE::.463.6847
TO 541.2094)
Used -For calculations
,PC)-
STATISTICAL REPORT FOR DATA FILE J2904-l.Kl5
ESTIt'IATING EOUATION:
LciG C = (--).6661 LOG b +2.6998
NUMBER OF DATA PAIRS USED: 8
RESIDUAL VARIANCE: 0.00125
95% CONFIDENCE FACTOR: 1.080-@-7 FOR EC50
CORRELATION COEFFICIENT: R = 0.99585
EFFECTIVE CONCENTRATIONS
(95% C-UNPIDENCE RANGE):
EC 50 = 500.9496 EC 20 = 193.5175 EC 10 = 110.9398 EC I = 21.4065
ma/L mall ma/L mall
( 46'@-r.6847TO ( 176.9699 TO ( 97.,c--970TO ( 16.4163 TO
541.@4094) 211.6124) 1'-75.9777)***
27.9189)*St
EXTRAPOLATED
RESULTS
7-
crIC-)
FINAL RESULTS
Hill-IMMIP-IINKI-ipti!ll
NUMBER
CONC.
------
---------
GAMMA ---------
1
125. Ot:)()O
0.1916
17
125.
0.2264
3
250.0000
0.7732
4
250.0t)()O
0.6550
5
500.0000
2.3247
6
50,).Oof-)O
-e_.1917
7
loo(--).oc)(:)o 4.7451
a
I oo(,)C.)oi)c)
4.SB70
GAMMA EST. -----------
0.2306 0. 2@@-06 0.6639 0.6639 1.9118 1.911B 5.5052 5.5052
EC @-JO 327.3192 ma/L (9--,% CONFIDENCE
RANGE:
J2'704-I.KZO
% EFFECT ----------
16.07B IB.464 43.604 -7,9.576 69.922 68.669 B2.594 83.013
299.190-*t TO Z%58.C@9'-7'6)
rccrtouch
SPACE BAR to continue....
crrccrrccrrrrrrrrccccrrrcrccrlrcrfcrrrccccrrrr
C)c*ir@)
MICROTOX DATA REPORT
FILE NAME: j2904-1.11:'@'O SamDle DescriDtion:
TEST DATE: TEST TIME:
FC-120 LOT 164 YELLOW COLORLESS
LIQUID:
TEST CONCENTRATIONS
ARE CLEAR.
ProcedLtr-e: BASIC Initial Concentration Test Tiffie:30 minutes
: It')t'm-a)/O.L
Osmotic Adjust".ent: NaCl Dilution Factor : "-@' Concentration Units: mg/L
NUMBER
1
4 5 6 7
1(71/IT -------
84/ 25 E3--/ 24 Gt)/ 16 84/ IS 75/ 8
el/ 9
Bl/ 5 8--/ 5
CONC. ----- ---
125.0000 125.0000 250.0000 250.0000 500.0000 500.0000 1000.0000 1000.0000
G"^MMA ---------
0.19158# 0.2264'4 0.7731,-0# 1:;.65497# 2. -@'-@'741 '-;'.1917--@# 4.74T.1i'lu 4.eS696#
CONTROL IT/IO
32/ 92
BLANK RATIO
10 4'DDDVDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDDVDDPDDDDDDDDDD?
.3$LOPE =.1.525?
..3
.3
.3
3
.3
a
.3
.3
m3 t'i .3
.3 .6
A .3
@3
.3
-3
I >zzzzzzzzzzzzzzzzzzzzzii@-zzzzl
3
.3
.3
.3
.3
.3
2
.3
EC
.3
.10 P-DDDDDDDDDDDDDDDDDDD-DDDDDDDbD.DDDDDDDDD*"DDDDDDODDDDDDDDDDD@Yl''
100 CONCENTRATION 1000
.3 .3
IOE4:
EC 0 -3Z7.3.1-92 (95% CONFIDENCE
RAk6@'.1"299.1904 TO 358.092'6)..
Used +or calculations'.....,
STATISI TICAL REPORT FOR DATA FILE
ESTIMATING EOUATION:
LOG C = 0.6466 x LOG b
NUMBER OF'DATA PAIRS USED: 8
RESIDUAL VARIANCE:
0.00201
95% CONFIDENCE FACTOR: 1.09 402 FOR EC50
CORRELATION
COEFFICIENT:
R
0.99331
EFFECTIVE CONCENTRATIONS
(95% CONFIDENCE RANGE):
EC 50 = 327.3192 mall
EC
= 133.5555 mall
EC 11) = 79.0551 mg/L
EC I = 16.7701 mall
( 299.1904 TO 358.0926) ( 115.6267 TO 154.26431
65.0098 TD 96.1@@49)9** 11.6396 TO d@-4.162i:#',*$*
EXTRAPOLATED
RESULTS