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Vista Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369*8111 CERTIFICATE OF ANALYSIS (T Date: 21 Aug., 1991 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 20 Aug. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45800 Order No.: 0000684-008 Property Test Method Analysis Moisture, 7. ABR-1AA *................ 16 Bulk Density, GM/CC ABR-2A *.................. ......................... .527 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-1OB Contamination, .024 -...................... --............... .73 .067 . ... .73 .017 .73 .007 .73 Syntron, Blk/Brn ABR-5A Made with decalcified water. 4/7 3 /lO 4/7 5 /iO All particles of contamination are less than .07mm* in size. This product was made with the new reactor rinse spray nozzle. Amy E.JBafgwell/J * Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193258 Vimtm Pa.' Oats: <^'/ i \ MM! fW!% h W ** I m \ AV 1 I 6 ?:r Screen Analysis Mesh 40 Weight , 00 0. o 60 iJ.7 .7 80 HMI ^ 7./ 2J^ 140 Pan -Z/. / 7./ /, Static Flow: X 01 : Color Li ??. S'7 ,?3 b * / AVf. Microns cpa* yf- /40/7 Technician: VAB.0001193259 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Customer: 23 Aug * 1991 American Mirrex P. O. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 22 Aug. 91 VBIAFAX No. 302--836-5972 Product: 5305 Railcar No.: UTCX 46521 Order No.: 0000684-011 Property Moisture, 7. Test Method ABR-1A Bulk Density, GM/CC ABR-2A ............. Particle Size, ABR-3 40 '/. on O oo Ana1vsis 0.10 0.543 60 80 100 120 140 200 PAN 0.8| 16.2 26.1 30.3 17.9 7. l| 1.6| BY COMPARTMENT A CA CB Residual VCM, PPM ABGC--26 Inherent Viscosity ABR--10B Con t amin a tion, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193260 II-.- Vimtm. Mjywmnc I *|jV H*. i.' n* :'-'-;'v'i > *> <* I-';;#* Load I 5308 Product fjo 71&4*1-- Screen Analysis Mesh Height % Static Flows Color Li Technician: X- Glassies: Microns: VAB.0001193261 Vista Polymer? A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369*8111 4 % Date: 22 Aug., 1991 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 21 Aug. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX 46550 Order No.: 0000684-010 Moisture, % Bulk Density, GM/CC Particle Size, % on ABF-1A .............................................. ABR-2A ............................................... 0.16 0.549 ABR-3 40 0.00 60 80 100 120 140 200 PAN 0.7 17.5 28.2 26.0 18.7 7.3 1.6 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193262 Screen Analysis Mesh 40 60 60 100 120 140 200 Pm Static Floe: Color Li It Slassies* Tsehniciint /4H~7 AVf Microns CPAs //,<) VAB.0001193263 Vttlo Wymors A Division of Viski Chomicot Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 rT Date: 20 Aug., 1991 Customer American Mirrex P. 0. Box 720 New Castle, DE 19720 Attention: Lynne Ulebb Date of Shipment: 19 Aug. 91 FAX No. 302-836-5972 VIS1A Product: 5305 Railcar No PLWX 44372 Order No 0000684-002 Property Test Method Analysis Moisture, 7. Bulk Density, GM/CC ABR-1A ABR-2A tee 0.15 e e 0.543 Particle Size, 7. on ABR-3 40 0.00 60 80 100 j 120 140 200 PAN 5.9 19.1 26.8 21.7 17.2 7.5 1.8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water All particles of contamination are less than ,07mmZ in size. This product was made with the new reactor rinse spray nozzle agwe 1 Laboratory Supervisor/Lead Phone (601) 369-0111 VAB.0001193264 Vlatm Larnd Data: Ship Con tuiintt ion X*<W t!' Ip i , *' / '> V.:' r A \. Screen Analysis Mesh Weight % 40 Ou&O 0^0 60 2,94 SV 9 80 ?,r7 100 v/j,*? /?./ 24.,/ StAtic Flow: Color L; X Claesies: b 120 /6L7/ 140 3,r? /7. 2. 200 2. 7X" 2 Pm , ?Z Avf. Microns: CPA: 7/!-* t Technicinn: VAB.0001193265 Vlatfe Pal, l,a^ Ship m&'tmr- /^ifix*TM** ;v:>viu ^r;V/-J *" ^'''/ V I"'' #-* vr-v:-- . ;< Vvfl / 4 Screen Anaijrsia Mesh Weight 40 X Static Flow: Color L: Technician: 100 '.2.7 120 140 -/<2 X Glassies b CPA: Avg. Microns: vs ? Pan c/- VAB.0001193266 1 CERTIFICATE OF ANALYSIS Date: 8/13/91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 8/12/91 FAX No. 302-836-5972 Produc t: 5305 Railcar No.: PLCX--46869 Order No.: 0000684--006 Property Test Method Analysis Moisture, % ABR-1A *********............................ 0.18 Bulk Density, GM/CC Particle Size, 7. on ABR-2A ......................******* 0.532 ABR-3 40 0.00 60 80 100 1 pr 140 | 200 PAN 2.9 23.4 28.5 26.7 12.9 "Trrj 4.0 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR--10B 0.004 II IV 0.73 0.001 1 0.73 0.001 0.73 0.068 0.73 Contamination, Syntron, Blk/Brn ABR-5A 1/ 6 1/ 8 1/ 6 1/ 5 Made with decalcified water. All particles of contamination are less than .07mm* in size. This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193267 \rlltA. MlMHt Load Ship Contamination Syntron Mathod I - ,V y- -f '> '* * : A 1, 'T* Screen Analysis Mesh Weight X !o 40 (9,0 dO Static Flow: Color L; 60 80 too .a M/o X Glassies: b Technician: mt ~rb ~-ft 120 140 ZOO Pan r.s Avt. Microns: CPA t VAB.0001193268 CERTIFICATE OF ANALYSIS Dates 12 Aug. 91 Customers American Mirrex R. 0. Box 728 New Castle, DE 19720 Attentions Lynne Webb Date of Shipments 9 Aug. 91 FAX No. 302-836-5972 Products 5305 Railcar No.s VIPX--45794 Order No.s 0000684--005 Propertv Test Method Analysis Moisture, 7. ABR-1A .........................................* * * .06 Bulk Density, GM/CC ABR-2A *********** .524 Particle Size, on ABR--3 O oo O o 40 60 80 lOO 120 140 200 PAN 8.2 22. Si 35.2 23.9 8.5 1.7 BY COMPARTMENT CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B 0.001 0.73 0.070 0.73 0.100 0.73 Contamination, Syntron, Blk/Brn ABR--5A T Made with decalcified wate 3/ 6 3/ 7 4/ 8 1 All particles of contamination are less than ,07mm2 in size. This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193269 Vlata. aigibmrz^ f: .y. /: n-".r Load Date , *-&> Product: Car Mo.; \ V /Icf* Tim Lagged In: Logged In Bf Ship Date: Siiolsi Cuatoaer OQC&<*%4f Contamination Syntron Method Screen Analysis Mesh Weight X 40 c e>& AO Static Flow: 4? z Color L: 60 80 100 L &k*7 X Glassies: <2S2f b LW 120 140 200 Pan 487 Avg. Microns: CPA: Technician: VAB.0001193270 CERTIFICATE OF ANALYSIS !- Date: 12 Aug. 91 FAX No. 302-836-5972 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Product: 5305 Attention: Lynne Webb Railcar No.: ACFX-41184 Date of Shipment: 8 Aug. 91 Order No.: 0000684-004 - - -- i sir1,,,:: bib -./r1 ,:r, .."ag.Tr. gr.r'jTi^Tissi,1 as.1 sarm-... ru nwu Property Test Method Analysis Moisture, % ABR--1A ******** 0.10 Bulk Density, GM/CC Particle Size, 7. on ABR--2A ********* 0.534 ABR-3 o oo 40 60 80 100 I 120 140 200 | PAN 0.4 13.2 24.7j 33.0 20.1 6.9 1.7 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.008 0.060 0.008 0.005 Inherent Viscosity ABR-1OB 0.72 0.73 0.74 0.73 Contamination, Syntron, Blk/Brn ABR-5A 5/ 7 8/ 7 9/ 12 4/ 9 Made with decalcified water. All particles of contamination are less than .07mm* in size. This product was made with^ I the new reactor rinse spray nozzle. H.D. Lucas \ \ Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193271 Vlitft. Fnly--f- /' V* + '** r * fcVv *4*^ *\v Load Hate: f-S~- 9/ Product: OL-rcx Gar No.: Ties Louffed In: Logged In Sjr: Ship Date: Siloish 4 ?* Cfc Customer <? Contamination Syntron Method Screen Analysis Mesh 40 Me i gh t CP.> % Z7 V>,o 60 80 100 vJ3-2. Static Flow: Color L: ?T- X Glassies: b 120 5. >7" 140 /?. 200 Avg. Microns CPA: Pan Technician: VAB.0001TO3272 CERTIFICATE OF ANALYSIS Date: 12 Aug. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 8 Aug. 91 FAX No. 302-836-5972 Product: 5305 I Railcar No.: UTCX--46525 Order No.: 0000684--003 Property Test Method Analysis Moisture, 7. Bulk Density, GM/CC ABR-1A ABR-2A 0.09 * * 0.542 Particle Size, 7. on ABR-3 40 60 80 100 120 140 200 PAN 0.00 0.4 15.3 26.4 31.7 17.6 6.8 1I 1.8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.001 0.003 0.011 0.001 Inherent Viscosity ABR-10B 0.73 0.73 0.74 0.73 Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. 6/ 5 | 3/ 4 7/ 5 6/ 5 All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193273 Vista Polymers A Division o( Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 'a {A Date: 9 Aug. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 5 Aug. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: ACFX--41161 Order No.: 0000684-001 Proper ty Test Method Moisture, 7. ABR-1A Bulk Density, 6M/CC ABR-2A Particle Size, ABR-3 V. on Analvsis 0.12 0.526 40 60 80 100 120 140 200 PAN 0.00 0.3 11 .7 23.2 31.5 21.8 8.9 I 2 I BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193274 Vista. Polywit: R?4?mmr~ ,?jr A 7^77'XT?.* %> ' % * Ay Load Data Tina Logged In: Product:I 5308 Car Mo.; Logged In By: / " 'r '// >/ Ship Data SUo(s) Cuatoner Moisture Contamination Syntron Method 1st 2nd 1st )2- 2nd 1 2nd 1 1st 1 .p-T I ,0? 2nd Screen Analysis Mesh Weight 40 ,0/0 X Static Plow: Color L 60 80 100 // 7 X 01 b 120 140 200 Pan Ai.f 4,4s* /2P Avg. Microns CPA: V?< Technician VAB.0001193275 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: 8 Aug. 91 Customer: American Mirrex P. O. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 6 Aug. 91 FAX No 302-836-5972 Product: 5305 Railcar No.: ACFX-41177 Order No.: 0000684-002 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Particle Size, ABR-3 7. on BY COMPARTMENT Ana1vsis ........................................ 0.06 ..................................... 0.544 OD O 40 60 |ioo r 140 200 PAN 0.00 1.0 20.4 28.3 29.3 15.1 -- 4.6 1.3 A CA CB Residual VCM, PPM ABGC-26 0.012 0.087 0.013 0.011 Inherent Viscosity ABR-10B Contamina tion, 0.73 0.72 0.73 0.73 Syntron, Blk/Brn ABR-5A 3/ 5 2/ 6 1/ 7 3/ 8 Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193276 Vista. Polyasra fflfftMqr 2t? Load Ship Contaaination Syntron Method Screen Analysis Mesh 40 Weight % &o Static Flow: Color L: 60 80 100 120 140 200 Pan !6.Ze> v ;v./7 tHSn, gtQ.</l _ X Glassies: Avg. Microns: -XSTJ <Z>-3& b CPA: Technician: VAB.0001193277 CERTIFICATE OF ANALYSIS Date: 26 July 91 Customer: American Mirrex P. . Box 728 New Castle, DE 19720 Attentions Lynne Webb Date of Shipment: 25 July 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45878 Order No.: 0000684-000 Property Test Method Analysis Moisture, V. 0.16 Bulk Density, GM/CC ABR-2A * 0.523 Particle Size, ABR-3 40 60 80 100 120 140 200 7. *on m BY COMPARTMENT 0.Q0` 0.3 11.2 21.9 30.8 22.0 11.0 4 1 1 II 1 II A CB B <L U Residual VCM, PPM ABGC--26 0.058 0.098 0.010 0.030 Inherent Viscosity ABR-10B 0.74 0.72 0.72 0.72 Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. 2/ 7 3/ 5 2/ 9 3/ 7 _____________i All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 * VAB.0001193278 1 Vista. Polyrti H$Minwr~ zx t t * w r " * 4 % f %vv ` Vi * Load Date Tine Ship Date: l/! W Product 5305 Car No f ; Logged In By: SilofsJ: Cuatoner: QO&D&frfi &oO Contaaination Syntron Method Screen Analysis Mesh Weight 40 O.oO % 60 80 100 Static Flow: X Glassies: Cfi L: 99./0 , (Ves1echnician b 120 140 200 Pan Silt Avg. Microns: CPA VAB.0001193279 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS #* Date: Customer: 10 July 91 American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Ulebb Date of Shipment: 5 July 91 FAX No Product: 5265 Railcar No.: PLCX-44680 Order No.: 0000452--001 Propertv Test Method Analysis Moisture, V. ABR-1A .....................0.03 Bulk Density, GM/CC Particle Size, 7. on ABR-2A ABR-3 0.548 40 0.00 60 80 | 100 120 140 200 PAN 1.0 16.6 24.3 29.8 19.1 7.0 2.2| BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR--10B Contamination, Syntron, Blk/Brn ABR--5A 0.001 0.65 0.006 0.65 0.006 0.65 0.009 0.65 5/ 8 6/ 9 6/ 8 5/ 8 Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193280 Vista Polymers Highway 25 Aberdeen* MS 39730 Load Date RAILCAR ANALYSIS Mu'/. . qq logo Ship nl o Moisture Contamination Bulk Density BD w/antistat Viscosity RVCM / -SV7 .00/ 2nd 1st 1 _ /, 1 Mirrex Shipments ONLY Tappi Test Con tarnination Composite . 06 or 2nd 2nd 2nd 9/8 s-yp on 4iV ^ __ i otinu Screen Analysis Mesh 40 Weight % sp ao 60 iff 80 jAih. 100 fr% 98.3 120 sf.e 140 Ml /? / Static Flow: & / 7- / Avg. Microns 200 7-0 Pan A af 9- Color L: a 0-7? b /-& Technician: VAB.0001193281 Vista Potymon A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 397 Phone (601) 369-8111 4 CERTIFICATE OF ANALYSIS Date: 5 July 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb VKI\FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX-46440 Date of Shipment: 3 July 91 Order No.: 0000452-000 Property m Moisture, 7. Test Method ABR-1A Analysis 0.12 Bulk Density, GM/CC Particle Size, 7. on ABR-2A * 0.544 ABR-3 40 60 80 1 100 120 I 0.00 16.3l 23.4| 27. b| .....:: 200 PAN BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-lOB Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than .07mmz in si2e. This product was made with the new reactor rinse spray nozzle. Bi 1 ry P * Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193282 Viata Polymers Load Date Time Logged Highway 25 Abardaanv MS 39730 A RAILCAR ANALYSIS Product: 5265 Car No. MTCX 4-(pW0 Moisture Contamination Bulk Density BD w/antistat Viscosity RVCM 1' I .US [ 1st I 2nd I 1st ,/0 __________ ,// Is 73 l U .544- ,so 2nd 2nd Mirrex Shipments ONLY Tappi Test Contamination Composite Screen Analysis Mesh 40 60 80 Weight 0*Q0 .1 % LI /(,. 3 Static Flow: f> / f.z Color L: 100 23. 120 13.9* 140 9.7? 200 Avg. Microns: tvu a AS? b Pan /,3z. Technician: VAB.0001193283 Vote Potym*re A Division of Vista Chemical Company 21 Offico Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 4 CERTIFICATE OF ANALYSIS Dates 5 July 91 Customer: American Mirrex P. 0. Box 720 New Castle, DE 19720 Attention: Lynne Webb FAX No. 302-036-5972 Product: 5305 Railcar No.: VIPX-45740 Date of Shipment: 2 July 91 Order No.: 0000134--012 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Particle Size, ABR-3 7. on O oo Analysis 0.09 0.530 40 60 00 0.2 9.7 120 30.9 BY COMPARTMENT CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369--0111 VAB.0001193284 Vista Polyaerm Highways 25* """V* I * T'.L '* WV - -'fiiM ^ ffr \ wt V V*. / * PVC RAILCAR ANALYSIS Load Date Tine Ship Date Product: Car No.: In: /^ : t:rg; Logged In By Silo(s): Customer: Contanination Syntron Method Met Method Bulk Density | 1 BD w/antistat 1 1 Viscosity RVCM I , //7 1 Blown Film ).&X> 7/^| /on\ . SSlS'l I, y/H m | .rjo 7/S 1 </2/ Screen Analysis Mesh 40 Weight X Static Flow: Co lor L 60 . 8 ao 100 120 140 200 Pan }S<Q7 -f> --* 2o-8 97). 1 //<? >5-*? X Glassies: a a.zs h /-si* Avg. Microns: CPAs Technician: VAB.0001193285 Vista Polymer* A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-009 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: 3 July 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynne Webb 19720 Date of Shipment: 1 July 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX-46583 Order No.: 0000134-010 Moisture, % Bulk Density, GM/CC Particle Size, % on AABBRR--11AA .............................................. ABR-2A ............................................... 0.12 0.526 ABR-3 40 60 80 100 120 140 200 | PAN 0.00 0.0 9.3 19.4| 29.2 24.5 13.8 3.8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than .07mm* in size. This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193286 Vista. Polysors HiiiMirzr * Load Ship Date: AJ<? 'PlefaL____ Product: /v> ' * -'.'r \A T :W- * -v mx Screen Analysis Mesh Weight % Static Flow; Color Technician: X OlAmmiea: o.aG? Microns: VAB.0001193287 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-00 Phone (601) 369-8111 i A CERTIFICATE OF ANALYSIS Date: 3 July 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynne Webb 19720 Date of Shipment: 1 July 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45898 Order No.: 0000134-011 Moisture, % Bulk Density, GM/CC Particle Size, % on ABR-1A ............................................. ABR-2A ............................................. 0.06 0.531 ABR-3 40 60 0.00 | 0.0 80 100 120 140 200 PAN 7.0 17.3 29.6 26.7 15.6 3.8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B 0.218 0.231 0.72 1 0.72 0.012 0.73 0.010 0.72 Contamination, Syntron, Blk/Brn ABR-5A 3/ 4 4/ 2 H 3/ 3 2/ 4 Made with decalcified water All particles of contamination are less than ,07mm2 in size. This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead * Phone (601) 369-8111 VAB.0001193288 Vista Pol Load Date: Ship fdo Tflstft Contaaination Syntron Method Hi|janr28r ^wrc'een . *I .i*1*} ft**] I**1*'1 it :h .iM" \ % *7 #gi` % Screen Analysis Mesh 40 Weight * 6,0 Static Plow: Color L: 60 o,o! 6, a 80 100 3-S( v f.S vJd /7-3 120 140 200 /4- 7(o /J.&4- Z%6 2&>*7 IS, b Pan /,<?z 3,? X Glassies: Sty- 5 Avg. Microns: CPA: Technician: VAB.0001193289 Vista Polyaers Hi(bw ' JJ+ 2fr b4 4 c?Aberdeen, MS 39730 RAILCAR ANALYSIS U ro y Load Date: ~13 w<? / Product: Car No U>H4A Time Logged In: \ \ QQ ,7S Logged In By: T Ship Date: as# rn& Moisture Contamination Bulk Density BD w/antistat Viscosity RVCM I 1st I 2nd / o? 11 7 1 rI 1st I 2nd 1 , fo ___ 1 .6sr\ 1 tiftt 1 I I 1st 1 \ ,H I 2nd m I s' _]_ I 1st I 2nd \.s<c> 1 .SV7 ra Mirrex Shipments ONLY Screen Analysis Mesh 40 Weight % 60 80 3, SO 0't Static Flow: Color L: 100 ?/? ULSL 120 /7-s< 140 13-ls- Si. 200 7. A/ /-3 Avg Microns 131.C Pan /ZD S. <3 O.SH b I-si Technician: re- ^y>_s VAB.0001193290 f. ANA1. >1*4- Date: 3-18-91 Customers American Mirrex - (J. Box /28 New Castle, DF A11en t i on : L vn n Webb Da t.e of 8hi pmen t s 3 15--9.1 -- i 9 / 7O F A X No - 3O 2 - 8 3 6 -5972 P r odu c t Railcar No It M UTCX-46442 Order No It It 900738-003 WMi w**--***< ***** **** mintn**j#** i HWtNi^N M4 *l * *44+*-**-* mmum im Propertv riO X E> LU Y &* **tvi H 4- I 1 l*-* /**#, *v / Test Me thod HIM '* - i. A An a 1 vei s ff IlMlB FB*|i 14 14 - + o .1 i - B u 1 k D e r i s i t v f* GM / CC*% M* Par t ic 1 S.12e , X. on f^ r.i4 tvl*r *, f*a*i % M *r_ itH "r n ^ *"t *M* tt tJ | l' |IMI*IUiM^4 Iftf **** Mai-* n-| 40 **** * ift**a*a * * fl4 H**HI**IH Bp- M4M1H *n tm*tMM*M*lnaM I 60 SO hi -*pM***imihmw* iiHim MaiMawtH **MiiMl - PPM h#i >iit PpT *)*4p4*4**t*p* a* H* W* Mi 1*1 *** *!* *** |B H***al *****<* **mhi 1 OO *A* *./ %*+ *1x* 4-. o*>* .14 0 7 o f)\*f %PJ PAN |<M*a^H|4HHi p***^ **# iMmaaMtiaarlMMM1 ** >*W*I * MH***** O,,00 + l ^ *4 0t *1 fl fla H M *Mt**MIMaMi| * ItMtiltMltUVUMMIHI' **-**!-* l**MWil*HHH k H H*4***H | 1*4 *4 l-**B-M* **p I ^HHI *MM iH aHt>lM*il 'TP* H| H imHiHlMHHl **niMita M*a*M*>tw< "7 AJ" tt *** 14 4 ! 3 5 5 106 3*A* IP Xr*I I %* tt t** j *!* Vfti tV *iaJ^ 14 3 4 X* f l| *!* *-*p t* |4*f*f | H*|Will*HiH*wH*ii O4 | ,V*Af || || ' !***<# fit rMHilftllt '* ' ' *H<**hi**MM4H< Ml**a>HtWtHHIHtF IMlHIntMIHH * P** * *! K**4 ItMmfiiM* *1 *M' 4|?4l**l I44* M*U H*aall***H*tWmal lt*p*M*iMi4M*i*MH'f f !!! In mmj f ........................ l*4 | r*ft ****H + * l*MM***4*t M i * M4i*HHi*H%H*4 -tfntf--TT --~ T1 i~-~T4*1 f *tf T ' Ml^ Hillnitlil* * j J^I r^Htl r. ff BY COMPARTMENT *** ITHHI**IH<Mm'4***4 !* ^-i*+ -ap 4*4 >*IM* w 1 MfcHMUHit Residual VCM. PPM ABGC-26 I n h eren t V i s <::: o s i t y A B R--.10 B Con t am i n a t i. on Mi l*| >**!! !fr* MH *** ra i 1 i * **4M* |M*IH liiT**mB*f h-*** 1 *H **-- f Mf| Ml Mull HMMil r**#k-a4p**i*HM H1MMM k*M*|< *4 **iMwiiii*iili>i|iWiMaa***M * *WaH*W**i *** 0 ,, 08.1 f ) f )P\*' *.J tt s.r 4*14 U . Uli * ** OI*. - 079 m k *** > ** +* - ft** kl M* | o AA *Hr tt W.1 t t**MH****tM- > t> t:>i' '14* ft * |*F H **4**t4> ****** 0 66 4 H4**4***kil*i>--!**<* f) AT ** * *4 L./ r HIMHlM**Ti4i*iti<*'flMi**t*i-******i4**i ****** i*H*BHM*f**t**4r -*-< 14*441 * !--*+* -p I --* +>4m**M*M ***.*4*H>44*4**4**Hl n **Pl 8 v n t r on B1 k / B r n ;'TM5A lk1*-* ,i l*!1 / 9 y/ V*i< * 1 *j i A* */*** 7/ r: 4/ 4tn M IHiiliHI H***t****tk*hi*i *1 M>M*l*i !#** ******* |T**4**4k >*a* * *** -<*4HiT*4T**l H**M4***4H*4*4*****k4H* il-i IU*Mifl|*f*f|Hi 4**-k * r T* 1~T~ I T* ^T! fc "--------T i ********* *an* m4* **i P4* 4* a** a * ** M4*wi ****** iM*aan*M* n ifHHiM *f***H if44*MHItil**t* *>***P41 im****4 muni tw4 Mi M#**r|* 1 *9l**iii lA Ml* Ml H|NI*I>*m M 14* |H ttt MiMi **' ** H MHil 1*-- ** I * !*<*** lT*44iiH**l lip*--*i|MH*M I lilMHflHMIMl M D . Lucas l***#4-p* -44M4f*'*pfMM4 I** M*.M*MIHlM***Mn4*i***aM*'N*>** *** IMI44I--4**TkH*MMMIM***l4**HiMMk * WIm'Mh L a bo r a t o r y 8u p e r v i s o r / L. e a d P hone <601) 369-8111 VAB.0001193291 Visto Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 * CERTIFICATE OF ANALYSIS Date: 7 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 4 June 91 VEC\FAX No. 302-836-5972 Produc t: 5305 Railcar No.: ACFX-4115B Order No.: 0000097--002 Propertv Test Method Moisture, V, ABR-1A Bulk Density, GM/CC ABR-2A Particle Size, ABR-3 7. on Analysis 0.11 0.524 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR--10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193292 Vista Polymers Highway 25 Aberdeen, MS 39730 f0* H ( RAILCAR ANALYSIS \ <f Vi.. * Load Date : ' 3-?/ Product: Car No.: Time Logged In: /0S0 Logged In By: Ai^C Ship Date: Silo(s): 6/6 &>71 Customer as* W & Contamination Syntron Method Screen Analysis Mesh Weight % 40 Oo 60 Jt J. 80 100 LAZ v /o.Lt fh 4 zt. 120 14.7? 2%3 140 200 ft A 2/,t Pan LAl 2-C Static Flow: l / /// % Glassies: <J.?* jj Avg. Microns: /4Z.S Color L: 7. 13 a .*? b ?.&C CPA : F9(* Technician: 4^T^B VAB.0001193293 Yitta Polymers A Division of Vista Chomicol Compony Adsrdam, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: 7 June 91 Customers American Mirrex P. O. Box 728 New Castle, DE i9720 Attentions Lynne Webb FAX No. 302--B36--5972 Products 5305 Railcar No.s UTCX--46553 Date of Shipment: 4 June 91 Order No.s 0000097-00I Property Test Method Analysis Moisture, 7. ABR--1A ...............* * .03 Bulk Density, GM/CC ABR-2A ****** .546 Particle Size, 7. on ABR-3 60 80 100 4.0 21. l| 24.6 200 6.1 BY COMPARTMENT A CA CB Residual VCM, PPM AB6C-26 .059 Inherent Viscosity ABR--lOB Contamination, Syntron, Blk/Brn ABR--5A 4/4 Made with decalcified water. All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. A4 Laboratory Supervisor/Lead Phone (601) 369--8111 mmmm m m i VAB.0001193294 Vista Polymers Highway 25 Aberdeen |! MS ^ ^l '* f %p 1 -kd # y r^A RAILCAR ANALYSX S Load Date: Time Logged In: Product 5305 Car No. i_j4LLLi pop Logged In By: A Ship Date Silo(s): Customer: Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film 1st 2nd CB B 11st 2nd 1st 2nd 1 \.o^~ I 1st 1 ,a^ 2nd | 1|[J5L ^! 5T7 Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight X .06 . 15 * aonv ^ 60 A9i* 80 100 120 fAgth1 /g 3Q /3.&7 avjh 140 ?W 200 Static Flow: 6 S3 L X Glassies <!% Avg. Microns: OU Pan Color L: ab CPA : Technician: VAB.0001193295 Vista Polyarn Hifinwr 26" A"Mrceen YS 4., PVC RAILCAR ANAL Load Date: Product:I 5305 Car No Time Logged In; ff- Logged In By: Ship Date: Silo(s): Cuetoe oc o /34- ( i ^ / ' Contain nation Syntron Method Screen Mesh Weight % Static Flow: Color L: AOeil X Glassies: ab Technician Avg. Microns /?? .C CPA: TTT8-692 (T09) aubqd VAB.0001193296 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS S \ j * ' 'Hi . Date: 26 June 91 Customers American Mirrex P. 0. Box 728 New Castle, OE 19720 Attentions Lynne Webb FAX No. 302-836-5972 Product: 5305 Railcar No.s UTCX-46563 Date of Shipment: 25 June 91 Order No.s 0000134-009 Property Test Method Analysis Moisture, V. ABR-1A...............*.................................. 0.18 Bulk Density, GM/CC ABR-2A ............................ 0.530 Particle Size, ABR-3 60 7. on 0.0 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A 0.013 0.025 0.72 0.72 : 0.014 0.72 0.017 0.72 1 4/ 9 3/ 10 6/ 12 3/ 10 Made with decalcified water. All particles of contamination are less than .07mmz in size. i_ This product was made with the new reactor rinse spray nozzle. H-D. Lucas L' I '' 1 Laboratory Supervisor/Lead VAB.0001193297 Vista Polymers Highway* 25~ A'serc.een >>Vjfr**r\^ i+IT.\ tf-f*1** if:' h 4* >: f *. * l Load Date: Product: Car No .: Tine Logged In: Logged In By: <r o Ship Date:. < 2 ^~7/ Silo(s): Customer 0060/^4 Q3> P C .Y Contamination Syntron Method Screen Analysis Mesh 40 Weight o. go X 0.0 Static Flow: 60 80 100 120 140 200 0.062 X Glassies <\% Avj. Microns: : flr.7 Color L 0 Qd b CPA: Pan Technician: ***** VAB.0001193298 mm mmmmmmm T"........... T CERTIFICATE OF ANALYSIS Dates 26 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Ulebb \\ Date of Shipment: 23 June 91 \ FAX No. 302-836-5972 Product: 5305 Railcar No.: GACX-73412 s Order No.: 0000134-008 * Propertv Test Method Moisture, 7. M^lBR-lA * Bulk Density, GM/CC Particle Si2e, ABR-2A ABR-3 1 40 BBBSSaSB' 60 O o 7. on 0.1 Analysis 0.08 0.53B BY COMPARTMENT A CA CB Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-10B 0.167 _ . _ . . i-v*. \ 0.72 0.402 0.71 0.067 0.72 0.005 0.72 Contamination, Syhtron, Blk/Brn . ABR--5A K f Made with decalcified water. 12/ 12 11/ 5 15/ 3 1 7/ All particles of This product was v contamination 3I made wilh the are new less than .07mm2 in reactor rink* sprky size, nozzle. 2 H.D. Lucas Laboratory Supervisor/Lead VAB.0001193299 Vista Poiyasra Higlwsr 2r AmMrc*een* \ XS**/****** *>:' *.r S *',p" :""" ',r'"s Load Date: Product: Car No.: * > / y^4:> ^ ,7 Time Logged In: / . ^ '2-4~*?/ Ship Date Silo(s) Logged In By: 6>t7/&** Customer MJA/Ml a /* 0 00 OO 92 - c4- Contamination Syntron Method Wet Method Bulk Density w/antistat Viscosity RVCM Blown Film % \3/*\ i^i 1 9c l _______ , _______1 ,-SBs _______ , v-o 076 , Tappi Test Contamination Composite Screen Analysi Mesh Weight % 40 QX>V & S> Static Flow: OL Color L: 60 80 100 120 140 200 Pan .ot 'ML 1 so 2Al IQ*Q ill JZS.Q 2S.V IM- iL m X Glassies: /./% Avg. Microns: a 02.| b (? CPA: ' / 7. Technician: 6d X- Tb VAB.0001193300 CERTIFICATE OF ANALYSIS Date: 26 June 91 Customer: American Mirrex P. O. Box 728 New Castle, DE 19720 Attention: Lynne Webb FAX No. 302-836-5972 Product: 5305 Railcar No.: PLWX-44567 Date of Shipment: 24 June 91 I Property Test Method Moisture, 7. ABR-1A.............* * * Bulk Density, GM/CC ABR-2A ...................... Particle Size, ABR-3 7. on Order No.: 0000097-004 Analysis 0.16 0.539 BY COMPARTMENT CA aar,:iajm.lr=a^uia nsnasass CB B Residual VCM, PPM AB6C-26 Inherent Viscosity ABR-10B Contamination, 0.075 0.74 0.081 0.73 0.067 0.74 0.078 I 0.73 Syntron, Blk/Brn ABR-5A 2/ 9 3/ 3 7/ 13 2/ 6 Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193301 Vista Polywers Highway 25 Aiarcften Load Date: Product: 5305 i,t r< x Car No : S'.JTt Time Logged In: Ship Date: 14 -CU Silo(s): Logged In By 6> rv- 6/ 7 :Customer fkmui. (6S(L no m&fai Mesh 40 60 80 100 120 140 200 Pan Weight *rr./o V tl& /3.71 /3-ST2 f,J/ /.n % 0- 0 , z~ 9./ 2~P. 0 J. 7 Static Flow: X Glassies: L Avg. Microns: !3L J Color L: 9% /2~ a , 2 7 CPA: 7/L f Technician: VAB.0001193302 CERTIFICATE OF ANALYSIS Dates 25 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 24 June 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX-46556 Order No.: 0000097--003 Property Test Method Analvsis Moisture, 7. ABR-1A ........................................................ 0.13 Bulk Density, GM/CC Particle Size, 7. on ABR--2A ABR-3 0.538 40 60 80 100 120 |l40 200 PAN 0.00 0.2 9.1 16.7 26.7 27.0 16.6 3.7 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, 0.002 0.72 0.008 . 0.71 0.064 0.72 0.101 0.72 Syntron, Blk/Brn ABR-5A 4/ 8 2/ 6 5/ 7 8/ 8 Made with decalcified water. All particles of contamination are less than .07mmz in size. This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193303 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS 24 June 91 Customer: American Mirrex P. 0. Box 720 New Castle, DE 19720 Attentions Lynne Webb Date of Shipment: 21 June 91 VB1AFAX No. 3O2-036-*5972 Product: 5305 Railcar No.: UTCX-46407 Order No.: 0000134--004 Property Test Method Moisture, X ABR-1A Bulk Density, BM/CC ABR-2A Particle Size, ABR-3 '/. on Analysis 0.13 0.539 40 II 60 00 ||iOO 120 140 ||200 jpAN 0.00 0.1 0.0 10.7 20.2 25.2 15.5 3.5 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than .07mm* in size. This product was made with the new reactor rinse spray nozzle P. Siz Laboratory Supervisor/Lead Phone (601) 369-0111 * VAB.0001193304 Vista Polymers . io sip Load Date: Highway 25 A anrcner., " *V i ** % w RAILCAR I It ,{r. AANAL. VS E S It, in' * I ^ Product: 5305 . (:L7Q'7 Car Ho + * Time Logged In:. Logged In By Ship Date Silo(s):___Cp Customer Contamination Syntron Method Wet Method Bulk Density w/antistat Viscosity RVCM Blown Film 1 .L 57 Tappi Test Contamination Composite Screen Analysis Mesh Weight Xp 40 & <0 0 .06 60 o3 80 Y`P && 100 'ZUL /g*7 120 140 200 Pan / ~.S L2A- 3. s Static Flow: O rf-D X Glassies Avg. Microns: Color L: 94,2 v a 0*/8 b /-3S CPA: //? O Technician: /A?, VAB.0001193305 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS 24 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 21 June 91 VEC\FAX No. 302--B36--5972 Product: 5305 Railcar No.: UTCX-45799 Order No.: 0000134--005 Propertv Test Method Analysis Moisture, X ABR-1A ttt 0.07 Bulk Density, BM/CC ABR-2A * 0.538 Particle Size, ABR-3 40 60 80 lOO 120 140 200 PAN 7. on 0.00 0.1 8.3 18.0 28.1 25.0 16.8 3.7 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR--lOB 0.003 0.73 0.004 0.72 0.058 0.72 0.037 0.72 Contamination, Syntron, Blk/Brn ABR-5A 6/ 3 4/ 8 5/ 7 6/ 5 Made with decalcified water All particles of contamination are less than .07mm* in size. This product was made with the new reactor rinse spray nozzle Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 i VAB.0001193306 Vista Polymers Highway 25 Aberdeeni /MS ft9730 t0 Load Date: PVC ai- q! RAILCAR ANALYSX S / i Product 5305 Car No.: VS 7 M filHTime Logged In: Logged In By: J 5 Ship Date: Silo(s): Customer: Contamination Syntron Method Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % -p o 60 _J. 80 100 120 140 200 Pan 32"9.00 /3VS ;j.8 Li > <2Sz> 3-1 _ Static Flow: % Glassies: Avg. Microns: /jv- Color L: 99-o7 a b /-2T0 CPA: Technician: \ | 1 1 .p I" .............. .... fciT! VAB.0001193307 rI Vista Polymers A Division of Vista Chemical Company Highway 25 Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: 22 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 19 June 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45804 Order No.: 0000134-003 Moisture, % Bulk Density, GM/CC Particle Size, % on ABR-1A .............................................. ABR-2A .............................................. 0.11 0.539 ABR-3 40 0.00 i 60 80 100 120 140 200 PAN 3.7 14.7 19.1 29.0 21.3 9.2 3.0 BY COMPARTMENT Residual VCM, PPM ABGC-26 0.120 0.118 0.138 0.011 Inherent Viscosity ABR-10B 0.73 0.73 0.73 0.73 Contamination, Syntron, Blk/Brn ABR-5A 4/ 15 3/ 18 4/ 12 3/ 11 Made with decalcified water. All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193308 Vista Polymers Highway 25 A asrc^r**4 *4 * ^ i4 ;f y **w ..,.,'W ,, V^v \K V RAILCAR ANALYSIS 7j7'X Load Date: 6'/?- 9/ Product:! 5305 Car No.: Time Logged In: //Qo Ship Date: f*J Silo(s ) : Logged In By: 6??. 4/o Customer Syntron Method Wet Method 7/C J/ /// Bulk Density BD w/antistat 1 sz*) \.s*/ Viscosity 1 RVCM Film 1 _1 l I I 1 CJ7 I Tappi Test o n l Am i n l x o n Composite 1 i 1 Screen Analysis Mesh 40 Weight X D. 00 0. o .06 or less ^7/Z~ 60 ML 3.7 80 7 Jr .07---------- .15 100 ?.fL n. i 120 zl.o .20---------- .60 140 /S.LS^ Z/.3 200 .60 %Z Pan A -Jt *7 Static Flow 0 /7,2 X Glassies <^/ 7. Avg. Microns: Color L; 9$*f3 a .Z? b /.^r CPA: Af.7 Technician: VAB.0001193309 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: 22 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 17 June 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45897 Order No.: 0000134-002 Moisture, % Bulk Density, GM/CC Particle Size, % on ABR-1A .............................................. ABR-2A .............................................. .07 .557 ABR-3 40 60 80 100 120 140 200 PAN 0.0 0.1 7.5 14.7 23.6 26.3 22.9 4.9 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. t Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 i VAB.0001193310 Vista Polymers Load Date: Time Logged Ship Date: Highway- 2!> Afaerceen, >YS o f ^ rr'" ^'T"\ i %> < u RAILCAR ANALYSIS Vifo Product 5305 Car No.: us;:?*' Contamination Syntron Method Wet Method Bulk Density w/antistat Viscosity RVCM Blown Film .0/7 Tappi Test Contamination Composite .06 or less Screen Analysis Mesh Weight X 40 O.o o o .* V 60 80 zn \r 100 an 120 ii.&i n,L 140 200 i3n ml Pan C\ Mt U 313 3^.9 H- ? Static Flow: 0 L Color L: % Glassies Avg. Microns: / zs-.i a* b LZ CPA: Technician: <c VAB.0001193311 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: 22 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Idebb Date of Shipment: 14 June 91 FAX No Product: 5305 Railcar No.: UTCX-46492 Order No.: 0000134-001 Property Test Method Ana1vsis Moisture, 7. ABR-1A * 0.01 Bulk Density, GM/CC ABR-2A 0.556 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN 7. on 0.00 0.2 8.7 18.2 27.1 25.5 16.8 3.5 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B 0.217 0.72 0.154 0.73 0.024 0.73 0.298 0.72 J Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. 3/ 4 2/ 5 1/ 4 3/ 4 1 All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone ( 6j01 ) 369-8111 ' 1- i VAB.0001193312 .. .. f. Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR h h ANALYSX S $/rc7 Load Date:. Time Logged In; Product: 5305 Car No.: Logged In By <&rr Ship Date -It Silof s ): Customer Contamination Syntron Method Wet Method Bulk Density w/antistat Viscosity RVCM Blown Fil 1/ 1 ,A&\ 1.29* Tappi Test Contamination Composite .06 or less Screen Analysis Mesh 40 60 80 Weight O'fiO V. J 1 X >< ,*70 3 i. ? .07 .15 .20 .60 100 LK2 120 *34/ I 140 12. 7C 200 ICJ Pan t. 75 3.5 Static Flow: 7-9 X Glassies: zj v? Avg Microns; Color L: 47*/ 7 a Technician: b 7^7 CPA: zJ. 3 V VAB.0001193313 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS j Date: 19 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Nebb Date of Shipment: 7 June 91 FAX No Product: 5265 Railcar No.: PLCX-43862 Order No.: 0000166-002 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, 6M/CC ABR-2A * Particle Size, ABR-3 7. on Analysis 0.12 0.544 40 60 80 100 120 140 200 PAN 0.00 2.3 22.2 25.7 28.2 14.8 4.6 2.2 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR--lOB Contamination, Syntron, Blk/Brn ABR-5A 0.001 0.67 0.061 0 66 0.067 0.65 0.063 0.66 3/ 7 5/ 11 4/ 13 2/ 8 Laboratory Supervisor/Lead Phone (601) 369-8111 i VAB.0001193314 Vista Polymers Highway 25 Abe MS 39730 Load Date: RAILCAR ANALYSTS /J.CX Product 5265 Car No. 4-3?2, Time Logged In: Logged In By: A?A Ship Date: /<? if8 Customer /Wo 1 st 2nd I 1st 2nd 1st 2nd 1st 2nd Moisture Contamination Bulk Density w/antistat i . OL 3 ? S3f > oy s K l.Svo Viscosity RVCM 0 to 1 i 1 1 1 to'* Mirrex Shipments ONLY Tappi Test Contamination Composite .06 or less -- .15 .20----- Screen Analysis Mesh 40 Weigh L X 0,00 0.0 60 ldk 33 80 JJJZ 100 120 12.is- w.QZ QL1 Jg.z, 140 7.7$ n/,2 200 ?. 3p \Lk Pan 141 Static Flow: 0 Avg. Microns: /S77 Colo r L: 7^30 At b L39 Techniclan: r VAB.0001193315 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 /J- dr t1 CERTIFICATE OF ANALYSIS Date: Customer: 19 June 91 American Nirrex P. 0. Box New Castle, DE 19720 Attentions Lynne Webb Date of Shipments 6 June 91 VBIAFAX No. 302-836-5972 Products 5305 Railcar No.s VIPX--45820 Order No.s 0000097-000 Property Test Method Analysis Moisture, 7, ABR-1A 0.12 Bulk Density, GM/CC Particle Size, ABR-2A t 0.549 ABR-3 40 I 60 80 100 120 140 200 PAN 7. on 0.00 0.5 12.1 19.5 27.5 22.2 14.9 3.3 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR--10B 0.043 0.73 0.044 0.73 0.001 0.72 0.001 0.73 Contamination, Syntron, Blk/Brn ABR-5A 4/ 7 5/ 8 4/ 9 3/ 7 Made with decalcified water. Ail particles of contamination are less than .07mm2 in size. This product was made with the new reactor rinse spray nozzle izemore Laboratory Supervisor/Lead Phone (601) 369-8111 t VAB.0001193316 f t Vista Polymers G 3Load Date : Highway 25 A aerceen, **% RAILCAR ANALYSIS Product 5305 Car No.; a MM#* \\9 < >/ ' > si it. 4-&0Time Logged In: Logged In By: Ship Date: Silols): bi3lb$4- Customer: no yne Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM * J1 .at3\ Blown Film Tappi Test Contamination Composite Screen Analysis Mesh Weight X 40 0 .OO 0,0 60 80 100 120 140 200 Pan Zl v 3.77 i3.*r h.dl 7. H- i.Ltr /Z. / /9.ST 3.3 Static Flow: Color L: X Glassies: a Si b 2 3^ Avg. Microns: /?/ 3 CPA: Z. 2- Technician: VAB.0001193317 CERTIFICATE OF ANALYSIS Date: 27 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb FAX No. 302--836--5972 Product: 5305 Railcar No.: UTCX--46456 Date of Shipment: 25 June 91 Order No.: 0000134-007 Property Test Method Analysis Moisture, 7. ABR--1A 0.13 Bulk Density, GM/CC ABR--2A * 0.533 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN 7. on 0.00 0.1 8.8 18.5 30.2 24.8 14.2 3.4 BY COMPARTMENT A CA CB Residual VCM, PPM ABGC-26 0.081 0.065 0.018 Inherent Viscosity ABR-lOB Contamination, 0.72 0.72 1 0.72 Syntron, Blk/Brn ABR-5A Made with decalcified water. 4/ 6 2/ 7 3/ 5 1 ---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- All particles of contamination are less than .07mm2 in size. This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193318 r CERTIFICATE OF ANALYSIS Date: 27 June 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 25 June 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX--46456 Order No.: 0000134--007 Property Test Method Ana1vsis Moisture, V. ABR-1A 0.13 Bulk Density, GM/CC ABR-2A * * 0.533 4 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN v * r oo "i o 7. on * 0.1 8.8 18.5 30.2 24.8 14.2 3.4 BY COMPARTMENT A CA CB Residual VCM, PPM ABGC--26 0.081 0.065 0.018 v i* scositi y ABR--10B 0.72 I 0.72 I Inherent 0.72 | Contamination, ' Syntron, Blk/Brn ABR--5A ------------------- j------------------- j------------------- j- Made with decalcified water. All particles of contamination are less than .07mmz in size. This product was made with the new reactor rinse spray nozzle. H.D. Lucas Laboratory Supervisor/Lead VAB.0001193319 1P it Vista Polymers Highway- 2C Aierceen* Af j 1 * u- % y PVC RAILCAR ANAL.YSXI5 Load Date: * Product: I 5305 Car No; : TAX Time Logged In: /3&& Ship Date: Silo(s): Logged In By: -d>3o Customer ^ '//,. V> /V/fif-iA Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % c.o 60 ct. .1 80 -y. /./ 100 1 1L 120 JO, 2^ 140 yy. 2Y./ 200 Z /o /2, 2 Pan /** Static Flow: a / f. t> Color L: 7 9. // X Glassies: ^/ Avg. Microns: a b /'f(* CPA : /// Technician: /H*L + T ii VAB.0001193320 f CERTIFICATE OF ANALYSIS Date: pHFtRIRFF? 27 June 91 AfllFFipan Miftp* P. . Box 728 New Castle, DE 19720 Attention: Lynne Webb FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45757 Date of Shipment: 24 June 91 Order No.: 0000134--006 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Particle Size, 7. on ABR-3 0.00 60 -k o * o o Analysis 0.14 0.536 80 100 120 140 200 PAN 7.7 18.2 29.2 26.0 15.1 3.8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 0.027 0.078 0.315 0.006 Inherent Viscosity ABR-10B 0.74 0.73 0.71 0.72 Contamination, 4* Syntron, Blk/Brn ABR--5A Made with decalcified water 6/ 12 6/ 8 6/ 7 7/ 7 -- All particles of contamination are less than .07mmz in size. This product was made with the new reactor rinse spray nozzle H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193321 4l sf;a o..ymers Highway 25 Aberdeenv MS 39730 Load Date: (p-2 2-^1 Product: 5305 Car No.: v/fx Time Logged In: o Ship Date: tzlL+ -* i -*0=- Silofs): Logged In By: /// (.89 nxCustomer: 'YUM CO 6*0 ac6 Mesh Weight *_p 40 0.V 60 0.02 0/0 80 100 7-2 te. Static Flow: t? / ~7*b> % Glassies: 120 / <p 140 /J 2to 200 /SZ Pan /.9o 3. ? P,l Avg. Microns: //// & Co lor L: a O'Z/? b CPA: Technician: /H VAB.0001193322 Vista Polymers A Division of Vista Chemical Company Highway 2 5 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Dates 30 May 91 Customer: American Mirrex P. 0. Box 720 New Castle, DE 19720 Attention: Lynne Webb FAX No. 302~836~5972 Product; 5305 Railcar No. : UTCX--46506 Date of Shipment: 28 May 91 Order No.: 897918--062 Proper tv Test Method Analvsis Moisture, V. ABR-1A ...................................... 0.11 Bulk Density, GM/CC ABR--2A ** 0.534 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN 7. on 0.00 2.1 23.B 29.1 25.9 12.1 5.0 2.0 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than ,07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193323 Vista Polymers Highway 25 Aberdeen 39730 FI AI LCAR ANALYSIS Load Date: M-?/ Product 5305 Time Logged In: /5()0 Logged In Ship Date: Silo(s): ('aPd Car No. :_ Customer Moisture Contamination Syntron Method A 1st 2nd , oip CA 1st 2nd CB 1 st 2nd // 1st 1 Jd B 2nd Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % 0*0 0^0 . 06 or less J/* 60 ), o 4 2J 80 //.-?/ 23J .07 -------- .15 100 l+.Cf 29. f 120 u.e? 2Ci .20 --------- . 60 140 (,.ol HJ 200 2,-f? S', o Pan hoo 2.0 Static Flow: 0 / ^3 % Glassies: C olor L: *9 7. htf' tL b 2.2-/ Avg. Microns: iLc. 0 CPA: UJ_ Technician: VAB.0001193324 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Date: 29 May 91 Customer American Mirrex P. 0. Box New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 24 May 91 VISIAFAX No. 302-836-5972 Product: 5305 Railcar No.: ACFX-41164 Order No.: 897918-061 Propertv Test Method Analvsis Moisture, 7. ABR-1A 0.09 Bulk Density, GM/CC ABR-2A 0.550 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN 7. on 0.00 2.3 21.3 25.5 26.1 14.9 7.2 2.7 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.065 0.150 0.101 0.001 Inherent Viscosity ABR-10B 0.73 0.72 0.73 0.72 Contamination, Syntron, Blk/Brn ABR-5A 2/ 5 3/ 7 4/ 6 2/ 5 Made with decalcified water All particles of contamination are less than .07mm2 in size. This product was made with the new reactor rinse spray nozzle Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193325 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSX S Load Date: Time Ship Product: /jcc Logged Car No i b- ?:- - y- A 1st 2nd Moisture Contamination Syntron ot . CA 1st 2nd . 65" CB 1st 2nd .09 B 1st 2nd , oU k 1 1 o 1 1 1 o * Tappi Test Contain inat ion Composite .06 or less 56- --- .15 Screen Analysis Mesh Weight % 40 QiO 60 h/<f <3.3 80 /Q.btf 100 L22 120 ./ 140 7d.1 /Y,9 200 ^.62. 7.-2. Static Flow: u D/ % Glassies A / /Af 4 - Avg. Microns Color L : .LQ a b y? CPA: ( w I 4 . 60 Pan /.?* /S4 Technician: r- ' 4 C VAB.0001193326 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 / Date: 23 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 21 May 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: PLWX-44680 Order No.: 897918-060 Moisture, % Bulk Density, GM/CC Particle Size, % on ABR-1A ................................................ ABR-2A ................................................. 0.02 0.553 ABR-3 40 60 80 100 120 140 200 PAN 0.00 3.0 24.8 26.3 25.0 12.8 6.2 1.9 BY COMPARTMENT Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. Bil Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193327 Vista Polymers Highway 25 Aberdeen. MS 39730 "V RAILCAR ANALYSIS Load Date: Z#'9/ Product: 5305 Car No.: Time Logged In: Logged In By: Ship Date: M Silo ( s ) : 6>87. i f<3 Customer tl 7/16, 1 Moisture Contamination Syntron Method A CA 1st 2nd 1st 2nd 1 ^3--___________________ . CB B 1st 2nd 1st 2nd * _____ 1 .0 3- Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % A a.o Static Flow: ^ . 06 or less % . 07 ----------.15 .20 . 60 60 3. > 80 Z4:S 100 r2-\7 2QS 120 Z5.6 % Glassies: IM 140 200 Pan *?./a 2 A? Avg. Microns: Color L: ab CPA = /7.o Technician: lirr-hHPL. VAB.0001193328 r r t- t L - *H * - P" tt Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 0 Date; 21 May 91 Customer; American Mirrex P. O. Box 728 New Castle, DE 19720 Attention; Lynne Webb Date of Shipment: 20 May 91 FAX No Product; 5305 Railcar No.: ACFX-41145 Order No.; 897918-059 Property Test Method Analvsis Moisture, 7. ABR --1A ** 0.13 Bulk Density, GM/CC ABR-2A .................................................... 0.545 Particle Size, 7. on ABR-3 40 60 80 100 120 140 200 PAN 0.00 1.0 26.5 32.2 25.0 O O 3.2 2.1 BY COMPARTMENT Residual VCM, PPM ABGC-26 A 0.065 CA h 0.028 CB 0.667 B 0.597 Inherent Viscosity ABR-10B 0.72 0.72 0.73 0.73 Contamination, Syntron, Blk/Brn ABR-5A 2/ 7 3/ 5 2/ 4 4/ 9 Made with decalcified water. All particles of contamination are less than .07mm2 in size. This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193329 Vista Polymers Highway 25 Aberdeen MS 39730 Load Date: Time RA X LCAR ANALYSIS Product: 5305 Car No.: (IMS' Contamination Syntron Method Wet Method Bulk Density BD w/antistat I Viscosity RVCM Blown Film ,2X5 ,&<r- 1 ,S92 0 1 i i i oO) Tappi Test Contamination Composite Screen Analysis .06 or less 710_________________ .15 | .20----- Mesh Weight 40 60 80 100 .Ml /3-2S ' IL.oZ % 0.0 l lo 3k Static Flow: if 0/ % Glassies 120 140 p.iz. Q-1S 3S. 0 I0.0 200 JAl 2U /c>/0 Avg. Microns Pan I.Q7 im Color L: ab CPA /u Technician: Ce VAB.0001193330 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 4 Date: 20 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date o*f Shipment: 17 May 91 FAX No. 302-836-5972 Product: 5265 Railcar No.: VIPX-45767 Order No.: 900738--007 Property Moisture, V. Test Method ABR --1A Analysis r ................ 0.06 Bulk Density, GM/CC ABR--2A * * ...................0.535 O GO Oo o Particle Size, 7. on ABR-3 40 60 100 120 140 200 PAN 0.7 15.0 24.1 30.1 19.8 17.5 2'8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A 0.031 0.66 0.471 0.65 0.076 0.66 0.073 0.66 1 2/ 5 3/ 5 2/ 4 3/ 4 Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193331 Vista Polymers Highway 25 Aberdeen 39730 RAILCAR ANALYSIS Load Date: 4-13.it Product: 5265 Time Logged In: I & 3o Logged Ship Date: Silo( s ): >~?Fc ^ 8 Q Car No .: 4-r 7L 7 Customer: Moisture Contamination A 1st I 2nd 1 *6(r 1 I Z. 1 LsuBulk Density 1 BD w/antistat CA CB B 1st 2nd 1st 2nd 1st 2pd *I -| -- 1 2- * I^0 i- t T</S~ 1_________ 1 ^X5~ | .1__________ 1D t *tS 1 1 Viscosity RVCM Mirrex Shipments ONLY Screen Analysis Mesh 40 Weight % O*. O <9 0< era 60 o, 37 80 7. V? /*> 100 tZM M-i 120 /xw 3(3, 1 140 nj 200 J. 7JT 7-5" Pan /,3g Zj S tatic Flow: 0 /7't Avg. Mi crons: / 'tT Color L: 1U'7 a / b ILL Technician: i<rJt VAB.0001193332 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 20 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 17 May 91 FAX No. 302-B36-5972 Product: 5305 Railcar No.: UTCX-46548 Order No.: 897918-05Q Property Test Method Analvsis Moisture, 7. ABR-1A 0.12 Bu1k Density, GM/CC ABR-2A 0.550 Particle Size, ABR-3 40 60 80 100 120 140 j 200 PAN 7. on 0.00 0.2 7.8 19.2 31.7 25.2 13.6 2.3 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.079 0.071 0.067 0.077 Inherent Viscosity ABR-10B 0.73 0.73 0.73 0.73 Contamination, Syntron, Blk/Brn ABR-5A 6/ 9 4/ 5 2/ 9 3/ 6 Made with decalcified water. All particles of contamination are less than ,07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193333 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Ship Date: Ft AX LCAR ANAL. YS X S Product: 5305 Car No. ; In: 0C-CO Logged In By: Si1o ( s ) : L 71 Customer: Moisture Contamination Syntron \ 1st 2nd C/\ 1st 2nd ClB I 1st 2nd I 1st 13 2nd , f 1_________ 1 ,/x. _________ | / /t _________ 1 / // Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 0. OO 0. 9 60 . o8 0-X 80 3.Ft 100 1,st ^ 120 /s'.sr 3f. 7 140 }?> X 200 /3.4 Pan A/S jl, 3 Static Flow: @ / /-V Color L: % Glassies: 1 Vo Avg. Microns a on~> b j.iQ CPA: l /Jt Technician: fIn ix VAB.0001193334 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 4- \ A V Date: 14 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 13 May 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: ACFX-41154 Order No.: 897918-056 Moisture, % Bulk Density, GM/CC Particle Size, % on ABR-1A ............................................... ABR-2A .................................................. 0.07 0.530 o CO ABR-3 40 60 100 120 140 200 PAN 0.00 0.4 16.6 25.5 30.2 17.4 7.4 2.5 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABjR-5A Made with decalcified water. All particles of contamination are less than .07mm* in size. This product was made with the new reactor rinse spray nozzle. I f/M Billy P. Sizemore ^ Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193335 Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR ANALYSIS MfX. Load Date = S- a -<71 Product: 5305 Time Logged In: \L 0 ^ Logged Car No.: Ship Date: Silo(s) Customer N^et-1 Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film .734 L .(M 2nd 1st 2nd I 1st 2nd I 1st 2nd ______ 1 ,07 1 ,o3 ,19.0 | 1 *< .129. /S9 Mesh 40 60 80 100 120 140 200 Pan Weight o./3 <3:3/ IQ'f- x 0.0 OH- &.SL tVt* 7.f- Static Flow: 0 &o L X Glassies: <1% Avg. Microns: Color L: a Alt> b CPA : /& Technician: VAB.0001193336 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 14 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 13 May 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX-46411 Order No.: 897918-057 1 Moisture, % Bulk Density, GM/CC Particle Size, % on ABR-1A ................................................. 0.07 ABR-2A ................................................. 0.549 ABR-3 40 60 80 100 120 140 200 PAN 0.00 5.1 27.4 25.3 22.7 12.1 5.6 1.8 BY COMPARTMENT Residual VCM, PPM ABGC-26 0.044 0.070 0.049 0.062 Inherent Viscosity ABR-10B Contamination, 0.74 0.74 0.73 0.73 Syntron, Blk/Brn AB4R-5A Made with decalcified water. 2/ 9 3/ 10 2/ 7 1/ 8 -- All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. Bil zemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193337 Vista Polymers Highway 25 Aberdeenj*%S 39730 Load Date: Time Ship Date: RAILCAR ANALYSIS 9/ Product Car No.: Contamination Syntron Method Wet Method Bulk Density BD w/antistat .SYo Viscosity RVCM Blown Film ,0W I 31 1 /, ,S<f3 1 .S~o Screen Analysis Mesh 40 Weight Dtp 6 % 0. o tic Flow: 0 60 80 100 120 /3.7/ /2>W j a.7.i/ A2.7 x Glassies l r/o 140 JS>J 200 2.7<? Pan AAvvgg.. MM icrons: Mr 7.7 Color L: Mj57 * O.S3 b .te/ CPA: /?/ Technician: C*Q ^ VAB.0001193338 Vista Vista Polymers A Division of P_ oYlyistma Cehermsical Company Highway 25 Post Office Box 91 Highway 25 P.O.Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 Aberdeen, MS 39730 Date: <?/ Customer: American Mirrex 13B9 School house Rd. New Castle, DE 19720 Attention: Lynne UJebb Date of Shipment: 9^ /Pfoy 7/ FAX No Produc t: Trai1er No.: Order No.: VBIA Proper tv Test Method Analysis Moisture, 7. ABR-iA * Bulk Density, GM/CC ABR-2A to Particle Size, 7. on ABR-3 40 60 j 80 100 j 120 140 | 200 PAN /fj \jtfj Af.Z JLA A, ? Residual VCM, PPM AB6C-26 < 1.0 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A This material was made with new clean wall technology. This material was made 4 with decalcified water. This product was made with the new reactor rinse spray nozzle. Lab upervisor/Lead Phone (601) 369-Bill VAB.0001193339 Dale S'- Customer Technician PVC BULK TRAILER ANALYSIS f Product 3ftTrailer Number / 0300 Particle Size Distribution: Screen Analysis Mesh Size 40 Grass Wt. Tare Nat Wt. H on Mesh D. .0 o 0.0 Screen Analysis Mesh Size Grass Wt. Tare Nat Wt H on Mesh 40 Min On Rotap shaker. 40 gins. Resin pius 1.0 ams. Csrto 100 120 140 200 Glassy Pan Pan. t/-*=r aol B,k I % -I IZJt PS. 2_ Min. On Rotap shaker 40 gms. Resin pius 1.0 gms. Cart) 60 100 120 140 200 IHSL 3. Glasay Pan Part. Remarks Star 20TA f Revised 1/12/07 \ Vista Polymers A Division of Vista Chemical Company Highway 25 . Port Offc* Box 91 . Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date Cus toner: American Mirrex 1309 School house Rd New Castle. DE 19720 Attention: Lynne Webb Date of Shipment: f FAX No. 302-B36-5972 Product: 5305 Trailer No. : . *72 Order No. : </ -0 3/ Propertv Moisture, % Test Method ABR-1A Analysis JA Bulk Density, GM/CC Partic1e Size, V. on ABR-2A ABR-3 1 40 1p1 80 1Pi 120 ~jPi 200 I PAN O,0 ,x | JO. 2_ ays /Vi' Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A < 1.0 .72 - .75 This material was made with new clean wall technology. This material was made with decalcified water. Laboratory Supervisor/Lead Phone (60X) 369-0111 VAB.0001193341 PVC BULK TRAILER ANALYSIS Date Customer Technician 7- ?/ Co Product Silo km MOIST 1 CONT. Top | Bottom Top | Bottom iI GEL I Trailer Number. Order No. BULK DENSITY I 1 DRY | TIME I 1 COLOR | Lw vise FRONT ' - osP 1I L^ RVCM MIDDLE A= END I II I Particle Si/e Distribution Screen Analysis Mnh Size Gross Wt Tare Net Wt % on Mesh Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh Min On Rotap shaker. 49 gms. Resin plus t .0 gms. Carb Glassy 40 60 Pan Pari. Y00 120 140 200 o 40 ; ii 15.00 /2.2S- 73X 1.23 m3 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 GJaasy Part. Remarks Star 207A } Revised 1/12/67 VAB.0001193342 Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 / ( Date: 9 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX--45812 Date of Shipment: 7 May 91 Order No.: 897918-055 Propertv Test Method Analysis Moisture, V. ABR-1A **** 0.16 Bulk Density, GM/CC Particle Size, AABBRR-2-2AA ........................................................ 0.544 ABR-3 40 60 80 lOO 1120 140 200 j PAN 7. on 1.7 21.0 26.3 28.3 15.2 5.7 1.8 O O O| BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.092 0.141 0.029 0.101 Inherent Viscosity ABR-10B 0.73 0.73 0.73 0.72 Contamination, Syntron, Blk/Brn ABR-fSA Made with decalcified water. All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193343 Vista Polymers Load Date : 5 Time Ship Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS 4 ; Product: 5305 Car No. : M vS$ I Moisture Contamination Syntron 1st 2nd .of 1 I 1st 1 2nd 1 .07 I 1st | 2nd 1 -OL I 1st I___* / 2nd Mesh Weight x 40 o%a 0.0 60 A2 80 100 /OJH '/3*iS 9-t.O 2L.Z 120 /3StO 3*3 140 ?,&,*> 200 2= Si7 Pan Static Flow: Q/ Color L: 98 % Glassies: a 0.3 L. b Alio Avg. Microns : /SS.C CPA: n thi Technician: VAB.0001193344 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone(601)369-8111 Date: 6 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynne Nebb 19720 Date of Shipment: 2 May 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX-46556 Order No.: 897918-054 Property Test Method Analvsis Moisture, 7. ABR-1A * ................. * ............... .17 Bulk Density, GM/CC ABR-2A ..................................................... .530 Particle Size, V. on ABR-3 40 60 80 100 120 140 200 PAN 0.0 0.4 13.2 23.8 31.6 21.1 8.0 2.3 BY COMPARTMENT A CA CB B r is -- . Residual VCM, PPM ABGC-26 .058 .030 . 066 .069 Inherent Viscosity ABR-10B .73 .73 . 73 .72 Contamination, Syntron, Blk/Brn ABR-5A 4/6 5/5 6/4 4/7 Made with decalcified water. All particles of contamination are less than ,07mmZ in size. This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 f:,. r I :v :-i ir ' I i' VAB.0001193345 l/nr,i - .i ..................' f Vista Polymers Highway 25 Aberdeen) MS 39730. f RAILCAR ANALYSIS Load Dat Product: Time Logged In: Logged In Ship Date: Si1o ( s ) : Car No. Customer Ate 'NsML^ Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film A CA 1st 17 2nd 1st 1 /" 2nd CB 11st 2nd | 1st 1 . ^7 B 2nd Tappi Test Contamination Composite Screen Analysis Mesh Weight 40 * CO % .06 or less __ 7&> 1 .07-----------. 15 60 o. 80 >,,<? M. 100 M* 120 .20---------- 140 /0.5 &U 200 &o .60 Pan 7.&Static Flow: 0 L Color L: X Glassies: L?(* ab Avg. Microns: : ^*7 CPA Technician: 'RO-h VAB.0001193346 iI Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 6 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 2 May 91 FAX No Product: 5305 Railcar No.: VIPX-45864 + Order No.: 897918-053 Propertv Test Method Analvsis Moisture, */. ABR-1A .................................................... .23 Bulk Density, GM/CC ABR-2A ................................................ . 536 Particle Size, V. on ABR-3 40 60 80 lOO 120 140 200 PAN 0.0 0.4 11.6 21.3 30.6 22.7 10.8 2.6 BY COMPARTMENT CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-lOB Contamination, Syntron, Blk/Brn ABR-5A Made with decalcified water. All particles of contamination are less than ,07mm2 in size. V This product was made with the new reactor rinse spray nozzle. Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193347 Vista Polymers Highway 25 Aberdeen MS 39730 FfcAILOAR ANALYSIS Load Date: 30 9Y Product 5305 Car No.: Time Logged In: 6 Logged In By: j 1st j2nd .S3 L__ 1st // 2nd 1st .S3 2nd 1st Contamination Composite Screen Analysis Mesh Weight x 40 A a. 0 & s>( //.(* p(_3 Static Flow: 0 L % Glassies: <!% (O-B Avg. Microns: Color L: a AP7 b k* CPA: olO.O Technician: TZT-hHDL- VAB.0001193348 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 Dates 3 May 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynne Webb 19720 Date of Shipment: 1 May 91 FAX No Product: 5305 Railcar No.: ACFX-41167 Order No.: 897918-052 Property Test Method Ana 1ysis Moisture, 7. ABR-1A .................................................... .15 Bulk Density, GM/CC ABR-2A * *...................................... . 533 --o Particle Size, ABR-3 60 80 100 120 140 200 PAN 7. on o o 0.1 12.8 24.9 32.6 19.9 7.4 2.3 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 .016 .211 . 157 .026 Inherent Viscosity ABR-10B 4 Contamination, .73 .72 .74 .72 Syntron, Blk/Brn ABR-5iA & Made with decalcified water. 4/11 2/5 3/6 2/9 All particles of contamination are less than .07mm2 in size. This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193349 Vista Polymers 7 / / {*<: > i <' 7 7 ,/V * i' w Highway 25 Aberdeen, HS--39730 RAILCAR ANALYSIS & V* V :F fcfiX Load Date Product Car No>riI / Time Logged In: *ViJl&'c Logged In By k Ship Date: Silo(s ) : v / JJ Customer: k2 Moisture Contamination Syntron Method A 1st 2nd CA 1st 2nd i/ CB 1 st 2nd JO B 1st 2nd iL Mesh Weight % 40 @.OP QiO 60 0.0 7 ed. 80 6,39 /2'& 100 /a.J7 M9 120 }(p. 3 h> 3(3 . (p 140 ?.?*/ /f, 9 200 3.72. Pan A/3 A3 Static Flow: 0 /*7-S % Glassies: / /'0 Avg . Microns: /'4^ & Color L: a J33- b A 29 CPA: Technician: 1 0 VAB.0001193350 Vista Polymers Highway 25 Aberdeen MS 39730 I h RAILCAR ANALYSIS tTZA Load Date Product: 5305 Car No Time Logged In: Logged In By; Ship Date: d/Si ; 6>7XA 98 lo(s ) Customer: Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film Yr .725 .076 i .72/ .147 4- .7/f 724 .147 Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight Q.&O % .06 or less .07-----------. 15 60 JiJs. 80 100 _2Jz l7\i-- XJ, 120 /4.7f .20---------- 140 200 19.0 7. (e .60 Pan /. 2/ Static Flow: 0/ % Glassies: % Avg. Microns: J Color L: 3{ a b LM CPA: ician: Techn '/f - ^ < VAB.0001193351 1r Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 1 May 91 Customer: American Mirrex P. O. Box 728 New Castle, DE Attention: Lynne Nebb 19720 Date of Shipment: 29 Apr. 91 FAX No Product: 5305 Railcar No.: UTCX-46444 Order No.: 897918-051 Property Test Method Ana1vsis Moisture, 7. ABR-1A ** .11 Bulk Density, GM/CC ABR-2A * * * . 538 Particle Size, 7. on ABR-3 40 0.0 60 80 100 120 140 200 1 PAN m-`I0.1 12.3 23.2 21.3 8.9 2.6 BY COMPARTMENT CA Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-10B Con tamination, Syntron, Blk/Brn ABR--SA Made with decalcified water. All particles of contamination are less than .07mm* in size, This product was made with the new reactor rinse spray nozzle. Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193352 fr h Vista Polymers Highway 25 Aberdeeni MS 39730 Load Date: R.A ILCAR *7/ Product: 5305 A - Car No.: HLW'-l Time Logged In: 3 / JO______ Logged In By: Ship Date Silo ( s ) : b & ~ ?") 8 : C^L (Jh/AJut) Customer Moisture A I 1st 2nd j| *. Jj Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown CA 1st 2nd ; O'} CB \J B 1st 2nd ,0 ^ 1st * // 2nd Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % 0 >0 0 .06 or less %- 60 80 IZA ' .07-----------. 15 .20---------- .60 100 Ji* A3.2 120 3U 140 200 Alt. 3 Al Pan A.C Static Flow: 0/ % Glassies: % Avg. Microns: a c olor L: /a b CPA: i Technician: VAB.0001193353 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: i May 91 Customer: American Mirrex P. Q. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 29 Apr. 91 FAX No Product: 5305 Railcar No.: UTCX-46419 Order No.: 897918-050 Propertv Test Method Analysis Moisture, 7. ABR-1A ...................................................... .08 Bu1k Density, GM/CC ABR-2A ******* .534 Particle Size, ABR-3 0 60 80 100 120 140 200 PAN 0 0 7. on 4 O 17.3 23.5 29.6 19.0 -- n : -i 7.6 2.4 BY COMPARTMENT Residual VCM, PPM ABGC-26 .070 . 147 .155 .147 Inherent Viscosity ABR-lOB .72 .72 .72 .72 Contamination, Syntron, Blk/Brn ABR-SA Made with decalcified water. 2/5 1/4 3/4 2/5 All particles of contamination are less than .07mm2 in size, This product was made with the new reactor rinse spray nozzle. Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193354 Vista Polymers Highway 25 J- i*v Aberdeen, MS 39730T & RAILCAR ANALYSIS pi. u Y Load Date: 3-1 - 7/ Product Car No.: Time Logged I n: Logged In By: Ship Date: Silo(s ) : Customer: Moisture Contamination Bulk Density BD w/antistat Viscosity RVCM A 1st 2nd 10 >(pl$ CA 1st 2nd 0. 5 f- CB 1 st 2nd , 0J j ii 55T/ .Lto? t I / O*\ B 1st 2nd & 3 Mirrex Shipments ONLY Tappi Test Contamination Composite .06 or less % Screen Analysis Mesh 40 Weight % S .60 60 C-ltfo.! 80 3. 4 7 Static Flow: 0 / f?i / .07---------- .15 .20---------- .60 100 120 140 200 Pan /If. V?.3 X6 4- IL.V . 2.. S' Avg. Microns: AJ & / Color L: %k3S a b Technician: rt VAB.0001193355 +* CERTIFICATE OF ANALYSIS Date: 3-18-91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3-15-91 FAX No. 302-836-5972 Product: 5265 Railcar No.: PL.WX-44376 Order No.: 900738-005 Property Test Method Ana Iysis Moisture, 7. ABR--1A ******************* 0.05 Bulk Density, GM/CC ABR-2A .......................................................... 0.553 Particle Size, 7. on ABR --3 40 0.00 60 0.1 80 1 100 120 140 200 - - ---- .. PAN 7.4 ' 17.2 29.3 26.4 16.8 2.8 BY COMPARTMENT Residual VCM, PPM ABGC-26 Inherent Viscosity ABR--10B Contamination, Syntron, Blk/Brn ABR-5A A 0.084 0.67 CA 0.124 0.67 CB B 1 ................................................... -- 0.082 0.121 ' 0.67 0.67 ' Eh i- O -........................................-- - 3/ 7 5/ 11 . 3/ 9 -- H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 1 r: I : I- VAB.0001193356 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-009*' Phone (601) 369-8111 rv A J Date: Customer: ZS- fyr. 9/ American Mirrex P. 0. Box New Castle. DE 19720 Attention: Lynne UJebb Date of Shipment: JZS /for. FAX No. 302-836-5972 VIS1A Product: 5305 Trailer No. Order No.: Propertv Moisture, 7. Test Method ABR-1A 4 Analvsis * Bulk Density, 6M/CC ABR--2A * + * * i Particle Size ABR-3 40 Mesh M. 200 Mesh Pan LJt Residual VCM, PPM ABGC-26 Inaerent Viscositv ABR-10B < 1.0 0.71-0.74 Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193357 PVC BULK TRAILER ANALYSIS Date Customer IDf KX Technician ~T^ ^-3 Product Trailer NumHBr T 7^ lime Order MOIST Hotlotn i FRONT CON'T. Bottom GEL l BULK DENSITY I * . >W a DRY 1 TIME 11 |1 1 1 COLOR 1 J A *0 1 ^ |. 3^\ Vise 1 RVCM jficu) \c( | /1 o * < I II I MIDDLE A- END I * i i i i. A- Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt H on Mesh Screen Analysis 40 &-O Mesh Size Gross Wt Tare Net Wt H on Mesh 40 "aJO BtoA/fe *< Min On Rotap shaker. 40 gins. Resin plus 1.0 gms. Carb 60 100 120 140 200 Glassy Pan Part. &SZ DAL. MALE.. /ML. HALL U.f8 &7A. DA /OS 2c/-0 ,A0 22.. 0 Min. On Rotap shaker 40 gms. Resin plus 1.0 gms. CarO Pan 60 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/67 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone {601)369-8111 Aj * Da te: Customer XS fyr. V American Mirrex P. 0. Box 728 New Castle- DE Attention: Lynne Webb 19720 Date of Shipment FAX No. 302-836-5972 VIS1A Product: 5305 Trailer No. T-2XAZ' Order No.: Propertv Moisture, 7. Bulk Density, GM/CC Partic1e Size Test Method ABR--1A * ABR--2A ABR--3 40 Mesh _____ad Residual VCM, PPM ABGC-26 Ingerent Viscosity ABR--10B Analvsis >Ab lJ2L 200 Mesh __ lA.Q Pan /7 < 1.0 0.71-0.74 Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193359 </- a /Date q rhCustomer Technician {PVC BULK TRAILER ANALYSIS / f Product Silo___ ^3 c<s r- ,m gTrailer Number. Time. ;63 Panicle Size Distribution ''&/2> Bf****- 6 /f :reen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. H on Mesh &oS_ 0-0 Screen Analysis Mesh Size Grose Wt Tere Net Wt H on Mesh 40 Min On Aotap shaker. 40 gms. Resin |phis 1.0 gims. Carb 60 ---- 80 100 -- - - -- 120 . -- ..----- 140 --------- 200 Glassy Pen Part. 0LZ- M 5.Ct 0'2 > 1 q-cf 2lA 33 V 23-c! J0-O ILL Min. On Rotap shaker 40 gms. Resin plus 1.0 gms. Carb Glassy Pan Part. 60 100 120 140 200 Remarks Star 207A Revised 1/12/07 1! I' Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 ^ - Phone (601) 369-8111 ' CERTIFICATE OF ANALYSIS Date: 17 Apr. 91 Customer: American Mirrex P. O. Box 728 New Castle, DE 19720 Attention: Lynne Webb Date of Shipment: 16 Apr. 91 s Product: 5305 Railcar No.: UTCX-46513 Order No.: 897918-048 Propertv Moisture, '/ Test Method Analysis ABR--1A ***** 0.17 Bulk Density, GM/CC Particle Size, '/. on ABR-2A .............0.530 ABR-3 | 40 60 80 lOO 120 140 200 PAN 0.00 0.3 13.3 24.5 30.7 19.7 9.0 2.5 BY COMPARTMENT A CA CB Residual VCM, PPM ABGC--26 Inherent Viscosity ABR-lOB 0.016 0.73 0.078 0.73 0.063 0.73 0.075 0.72 Contamination, Syntron, Blk/Brn ABR--5A 2/ 5 4/ 13 4/ 5 2/ 7 Made with decalcified water. All particles of contamination are less than ,07mm2 in size, This product was made with the new reactor rinse spray nozzle. Laboratory Supervisor/Lead Phone (601) 369--8111 VAB.0001193361 Vista Polymers Highway 25 Aberdeen* MS 39730 PVC RAILCAR \ fr- ANALYSIS 'V KTC-X. Load Date: Product: 5305 Car No.: Time Logged In: &3QO Ship Date : /b SiXo(s ) : Logged In By: 67 2-680 Customer /6 flwAjuf) Contamination Syntron Method Screen Analysis Mesh 40 Weigh t % > QO 6.6 60 03 80 13.3 100 Static Flow: O L S3 X Glassies: Color L: >& b A7 120 140 200 Pan *tS<- t &7 !*13 33 : JMIAvg. Microns: CPA nA Technician: VAB.0001193362 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-009 Phone (601) 369-8111 , r A Date: 16 Apr. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynne Webb 19720 Date of Shipment: 15 Apr. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: UTCX-46420 Order No.: 897918-046 Mo i s tu re q. y. Bulk Density, GH/CC Particle Size, % on ABR-1A ABR-3 0 . 16 0.529 40 0.0 0 60 0. 1 80 10 0 8. 1 120 140 2 0 0 PAN 30.9 rn/ J oj* 13.2 2.7 r--- CO CO BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0 . 135 0.115 0.056 0.048 Inherent Viscosity ABR-10B 0.73 0.73 0.73 0.74 C ontamina tio n, S y n 1r o n , B 3 k / E r n A B R - 5 A Made with ieca 1 cif ied water . 3/ 9 4/ 8 2/ 14 3/ 12 ----------------- 1 All partic1es of c o n tami n a t i o n are less than .07mm2 in size, T his produ c t was made with the new reactor rinse spray nozzle. r a t o v y S. \ p _* r v i P h c 11 e \ 6 0 1 ! 36 9-8113 VAB.0001193363 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date : 4-? Ft AX LCAR Product ANALYSTS itrtK Car No* : 4-L4-ZG Time In: 0 A Ship Date A / r /K^ ^nCfe^ Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film A 1st 2nd . /& CA 1st 2nd ^ /O CB 1 st 2nd /Q B 1 st 2nd ,// Tappi Test Contamination Composite Screen Analysis .06 or less i/ Yu Mesh Weight % 40 - D 0,0 60 >. V i5 0,1 80 t-1 .07----- --- .15 .20----- -- . 60 100 f.ft 120 /S'ef Zo.l 140 /2-&Z 1^.2 200 6 /3 .i? Pan / 3_r Static Flow: O / c>, 3 % Glassies: / UiCVa Avg. Microns : JJMJ. Color L: ^ a f>, 2 b /J/ CPA: / ^ c? Technician: /n, 7 <? 7 ^ T)L t In r1-- ? !***> l 4.- . i, . . t 1 p- -M- - i -- -'t VAB.0001193364 *t Vislo Potymnrs A Division of Vislo Chemical Company Highway 25 Post Omen Box 91 CERTIFICATE OF ANALYSIS v Adardoon, Mississippi 39730-0091 Phonn (601) 369-8111 , ' A- h >v Date: 10 Apr. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attentions Lynne Webb Date of Shipment: 8 Apr. 91 VIS1AFAX No. 302-836-5972 Products 5305 Railcar No.: UTCX-46519 Order No.: 897918--044 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Particle Size, ABR-3 I 40 60 7. on 0.00 O o Analvsis tilt 0.06 0.521 lOO 120 | 140 200 PAN 8.9 21.0 30.3 13.0 1.1 BY COMPARTMENT A CA B Residual VCM, PPM ABGC-26 0.010 0.057 0.080 0.097 Inherent Viscosity ABR-10B Contamination, 0.74 0.73 0.72 0.73 Syntron, Blk/Brn ABR-5A Made with decalcified water 2/ 4 1/ 6 2/ 5 3/ 10 All particles of contamination are less than ,07mm2 in size. i ii f 1J Bil Laboratory Supervisor/Lead l Phone (601) 369-8111 * 4 VAB.0001193365 T Vista Polymers Highway 25 Aberdeen, MS 39730 ANALYSXS #TX Load Date: 4-Z-..1L Product: Car No Time Logged In: *<.X & o Logged In By: > Ship Date: JL Silo(s): - 3 oy V Customer Ai nJ o T A 1 st 2nd Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat 2V 7 SU Viscosity RVCM .nan Blown Film CA 1st 2nd 1 CB 1st 2nd .0 s' B 1st 2nd 1* o C // <? L -5?3 ) C' .736 .72Z Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight 0, 6 0 X o.. 6 0 .06 or less Vi 60 OrOX V.(j 80 3 97 !. ? .07----------.15 .20---------- .60 100 foSo > 120 .1312 Jo. J 140 13. $ C 7 200 6. 9? _&.0 Pan &. sy // Static Flow: G / /P J X Glassies: ^:/ ?$> Avg. Microns: 93>.i Color L: 9 ter a b LT7 CPA: /9< 6 Technician: fa, VAB.0001193366 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 Pate: 16 Apr. 91 (Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynne Webb 19720 Date of Shipment: 15 Apr. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45778 Order No.: 897918-047 r> Mo i s ture Bulk Density, GH/OC Particle Size, % on ABB--1A ................................................. ABB-2 A ................................................ 0.17 0.526 ABB-3 40 0.0 0 60 0.1 80 10 0 120 140 2 0 0 PAN 7.9 18.5 30. 1 26.2 14.3 2.9 BY COMPARTMENT Residual VCM, PPM ABGC-26 0.048 0.048 0.069 0.055 Inherent Viscosity ABB-1OB 0.72 0.73 0.73 0.72 Con ta min a tion, Syntron, Blk/Brn ABF-5A o/ q 3/ 5 7/ 4 3/ 7 Made with decalcified water. All particles of contamination are less than .07mm* in size, 4 This product was made with the new reactor rinse spray nozzle. Laborstory Sopervisor-L- Phone 6 01 ) 369-8111 VAB.0001193367 _*** ***. Vista Polymers Highway 25 Aberdeen. MS^~3$730 RAILCAR ANALYSIS pir/K Load Date: tf-#' V Product: 5305 Car No.: Time Logged In: ^>6 Ship Date Logged In By: O&fl:Customer fklMjh -4r 0 Moisture Contamination Syntron Method /5ft 1st I 2nd .of 1 1st o-S' 2nd 1st .n 2nd 1st 2nd os' Tappi Test Contamination Composite .06 or less --J!z Screen Analysis Mesh 40 60 80 Weight .60 3.9b % 04 0. / 7.9 .07 ----- .15 .20----- -- .60 100 l 120 /S.of a 140 13. *9 6. 2. 200 Ms Pan Static Flow: O / 8-C> % Glassies: Avg. Microns: / Color L: a b JJZ, CPA: /2 Technician: VAB.0001193368 CERTIFICATE OF ANALYSIS Date: 3-19-91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3-18-91 FAX No. 302-036-5972 Product: 5305 Railcar No.: UTCX-46579 Order No.: 897918-038 Propertv Test Method Ana1vsis Moisture, 7. ABR--1A *** 0.22 Bulk Density, GM/CC ABR--2A ******************* 0.530 03 O Particle Size, 7. on ABR-3 40 .. 60 100 120 140 0.00 0.1 4.7 14.6 37.6 ......- 200 PAN 14.1 2.5 BY COMPARTMENT A CA CB B (N 1*0 N 1 O Residual VCM, PPM ABGC-26 0.051 0.068 0.044 0.068 Inherent Viscosity ABR-10B 0.73 0.73 0.73 Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. 2/ 6 5/ 9 * 3/ 8 4/ 9 All particles of contamination are less than ,07mm2 in size. H.D. Lucas Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193369 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: /-hi i Product 5305 Car No. :. uzil Time Logged In: //& Ship Date:.3 -9/-rf Silo( s ) : Logged In By: ~"7cT & Customer: . Moisture Contamination Syntron Method A 1st 2nd CA 1st 2nd *12 CB 1st 2nd lOI B 1st 2nd , at Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight 0,60 % 0*0 .06 or less 60 0< O 7 Oj 80 033 .07 .15 .20 .60 100 7.29 rtk 120 ]Zl 3*7, & 140 !*Jt aL4 200 7.o(> /*/,! Pan Static Flow: 0 /?. 7 % Glassies jC/% Avg. Microns: J??'7 Color L: 99.0(* a 0.2? b A 6^ CPA: 7 Technician: (f[Q 0 ^ VAB.0001193370 I p d ' Vista Polymers Highway P.O.Box 91 Aberdeen, MS 39730 CERTIFICATE OF ANALYSIS Date: 3-19-91 Customer: American Mirrex 1389 Schoolhou se Rd. New Castle, DE 19720 Attention: Lynn Ulebb Date of Shipment: 3-18-91 FAX No. 302-836-5972 Product: 5305 Railcar No ACFX-41136 Order No.: 897918-037 Propertv Test Method Analysis Moisture, 7. Bulk Density, GM/CC ABR-1A ABR-2A + *- + + + + ** + + + * + + ** .08 Particle Size, 7. on ABR-3 40 0.0 60 0.1 80 100 120 140 200 PAN 8.5 18.5 37.3 22.4 11.1 2.1 BY COMPARTMENT Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A A . 146 .73 CA CB .028 .72 .074 . 73 B .217 .73 3/7 2/8 3/6 2/6 This material was made with decalcified water. All particles of contamination are less than .07 mm2 in size H. D. Lucas T fcnpav VAB.0001193371 Vista Polymers Highway 25 Aberdeen, MS 39730 /{CF-'f. Load Date: Time Logged In: I Ship Date Product: 5305 Car No.: Logged In By: Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film I , 726 $01 1 G?f\ Screen Analysis Mesh 40 Weight % 0 *0 (3 Static Flow: Color L: 60 0-6 4 A 80 y.j?r IS 100 Hr 120 If.1/? 31.3 140 //.jj 200 //-/ Pan /.dC -LI-- % Glassies Avg. Microns: /.y ab CPA: Technician: j VAB.0001193372 Phone (601) 369-8111 x t' _ Y Vista Polymers s h. Highway 25 P.O.Box 91 Aberdeen, MS 39730 CERTIFICATE OF ANALYSIS Date: 3-19-91 Customer: American Mirrex 1389 School house Rd. New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3--18--91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX--45794 Order No.: 897918--036 Property Test Method Ana1vsis Moisture, V. ABR--1A ** .30 Bulk Density, GM/CC Particle Size, * 7. on ABR--2A *** .530 ABR-3 O o 40 60 80 100 120 140 200 | PAN 0.7 8.8 20.3 40.3 19.2 8.6 2.1 . BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B S4on - .054 .72 .060 .72 .060 .73 .060 .72 4/6 5/7 2/5 3/7 This material was made with decalcified water. All particles of contamination are less than .07 mm2 in size. t-* **(*. r - 1r s +. - r. v , + VAB.0001193373 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date Product: /S3QTime Logged In: Ship Date: 3 / silo ( s ) : Car No.: d In Bv: 0 : kUhtUAj, \C^tL Customer 2V79/ V 03 G Moisture Contamination Syntron Method A 1st 2nd CA 1st 2nd CB 1st 2nd / i.J-o B 1st 2nd /t> Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % &0 *06 dr less .07---------- .15 .20---------- .60 60 * 0.3H .7 80 v- if i-i 100 120 Jo.39 ^as__ 4-o 3 140 <?.L6 n.i 200 H.3X y.L Pan l.*3 S. ( Static Flow: y.( Color L : 111 * Glassies3 ^ / 7* Avg. Microns: a b 4>7 CPA: 2. f>* if Technician: VAB.0001193374 i. 1 Vista Polymers -Highway 25 P.O.Box 91 Aberdeen, MS 39730 CERTIFICATE OF ANALYSIS Date: 3-22-91 Customer: American Mirrex 1389 School house Rd. New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3-l-91 FAX No. 302-836-5972 - \ A Product: 5305 Railcar No.: VIPX-45849 Order No.: 897918-039 Prooe|rty Test Method ,t Analvsis Moisture, 7. ABR--1A * ........................ .07 Bulk Density, GM/CC ABR-2A ................. **** t .537 Particle Size, ABR-3 7. on BY COMPARTMENT Residual VCM, PPM ABGC-26 A .075 CA CB .085 i .076 B ------- -- .090 . . Inherent Viscosity ABR-10B .73 .73 .73 .73 Contamination, Syntron, Blk/Brn H ABR-5A v ... . 5/9 - V 9/7 - 6/14 5/9 This material was made with decalcified water. All particles of contamination are than .07* mm2 in size. H. D. Lucas * ,- * * ,i VI. * VAB.0001193375 .***. 1 ,1 Vista ' ' F - - - i-'V.h y*-*. ,-rv- A^<: ***rs*ic- * * _-;A- " .... r i + b J* r * l; **tt Polymers H1 ghva '* iI K 4 ;' V-V;A`' "-i: -A H. .. .,:L :1 ' ;J- . i% 5 'flfifc.' : * 1 l I1 'll ..k r 1t.t :nii ^ ' ! . i- 1: -> ,*#*+ ; "fi > MS 397 "i'v I. ': E>VC RA X LCAR | H ' *. ANALYS X S M 1 Load Data: Product 5305 Car No: Tine Logged In: > L/j> o Ship Date Silo(s) Logged In By: ia . > iP ,/ V , ii ' - Customer .f / / Y Contaaination Syntron Method Screen Analysis Mesh 40 Weight X 0,0 Static Plow: 60 80 100 120 7. iC 0,2 Si 15.2 $L X Glassies: t?e 140 /J.7-Q 211 200 Avg Microns: Color L: IX. X* bm CPA: Pan /4 Technician: VAB.0001193376 Laboratory Supervisor/Lead Vista Polymers Highway 25 P.O.Box 91 Aberdeen, MS 39730 CERTIFICATE OF ANALYSIS Date: 3-22-91 Customer: American Mirrex 1389 School house Rd. New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3-21--91 FAX No. 302-036-5972 Product: 5305 Railcar No.: PLCX-43086 Order No.: 097918-040 Property Test Method Analysis Moisture, 7. ABR--1A * . 12 Bulk Density, GM/CC ABR--2A ** . 528 Particle Size, * X on ABR-3 O * o 40 i 60 80 100 120 140 200 PAN 0.2 4.6 14.4 39.3 27.8 11.9 1.8 BY COMPARTMENT Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A A .001 .73 2/6 CA .153 .73 3/2 CB .113 B 1 n " 1 -- .001 .73 .73 2/8 3/5 This material was made with decalcified water. All particles of contamination are less than .07 mmz in size. H. D. Lucas Laboratory Supervisor/Lead VAB.0001193377 Vista Polymers Highway 25 Aberdeen, MS 39730 RAX Li CAR Load Date: /^-/S * Product: Car Time Logged In: J?36Q 3Ship Date : Silo(s ) : Logged In By: L?3, Uf Customer Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film A 1st 2nd .to Z. 725 061 CA 1 st 2nd *o(& ,sn mtmmm 776 IS3 AVJD CB 1 st 2nd *o6 S3 9 B 1st 2nd .12. .S3 ? 72.1 Screen Analysis Mesh 40 Weight % O-QQ 0-6 60 . IP 80 100 120 140 200 1-20 IlSS 133)0 97 /. IL Static Flow: 0 / % Glassies: 1% Avg. Microns: Color L; ?9cC a0 b AL* CPA: ?v.-\ Pan J1 Technician: T wrnmm^ MM VAB.0001193378 Vis> ta' ur Polymers Highway 25 P.O.Box 91 Aberdeen, MS 39730 Date: 3-22-91 Customer: American Mirrex 1389 School house Rd. New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3-21-91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45308 Order No.: 897918-041 Property Test Method Moisture, 7. ABR-1A + Bulk Density, GM/CC ABR-2A Particle Size, ABR-3 7. on Analysis ++++++>++++++++ . 12 40 0.0 60 0.4 80 100 120 | 140 200 PAN . 9.0 17.7 36.0 23.8 11.2 1.9 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A .069 .72 3/5 .079 .72 1 2/8 .059 .72 3/9 .095 .72 i 4/10 This material was made with decalcified water. All particles of contamination are less than .07 nun2 in size. H. D. Lucas VAB.0001193379 Vista Polymers Highway 25 Aberdeent MS 39730 RAILCAR ANALYSIS Load Date : Product 5305 Car No. : Time Logged In: Ship Date: ?>'U Silo(s): Logged In By: Customer i/7/Z & Moisture Contamination Syntron Method 1st 2nd 1st / /<X. 2nd 1st / /A 2nd 1st 2nd Screen Analysis Mesh 40 Weight x oo 60 <2_/ >. 80 4. S'A 9.0 100 fO, 7 120 O 140 <3<% 200 &.Lt //,fl Pan A9_ Static Flow: 0 / *7,^ X Glassies: 1% Avg. Microns: /3t. <7 Color L: a 0 b CPA: /7IO* ^ Technician: VAB.0001193380 Vista Polymers Highway 25 P.O.Box 91 Aberdeen, MS 39730 CERTIFICATE OF ANALYSIS Date: 3-12-91 Customer: American Mirrex 1389 School house Rd. New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 3-11-91 FAX No. 302-836-5972 Product: 5305 a Railcar No.: VIPX-45748 Order No.: 897918-035 Property Test Method Analysis Moisture, 7. ABR-1A * * * *.............********** . 16 Bulk Density, GM/CC ABR-2A ************ ................... .535 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN V. on 0.3 3.2 11.2 34.2 29.6 18.7 GO (N O o BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A .077 .72 .068 .72 .060 .72 .069 .72 2/16 4/19 2/11 2/18 This material was made with decalcified water. All particles of contamination are less than .07 mm2 in size. H. D. Lucas VAB.0001193381 Vista Polymers Highway 25 Aberdeen. MS 39730 RAILCAR ANALYS Load Date: fh3o^jo Time Logged In: 0 Ship Date: Product 5305 Car No . : feV Logged In By; M Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film 0 A 1st 2nd / <? CA 1st 2nd o CB 1st 2nd 4 /(S' O B 1st 2nd >// Tappi Test Contamination Composite Screen Analysis Mesh Weight 40 0*00 %& .06 or less y,<* 60 0 /3 6-2 80 hS l. 7. .07---------- .15 .20---------- .60 100 120 If,2. 140 200 Pan t,3& I &. *7 2 5 Static Flow: O / b,/h Color L: % Glassies: \*U Avg . Microns: t a 0. 12 b Ml CPA o ? Technician: T> * ^ VAB.0001193382 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Lth I 1r I CATE-vn ***- i OF ANALYSIS Date s 3 -12-91 Customers Arnerican M1rrex P. 0. Box 728 New Castle. DE 19720 Attention; Lynn Webb VKIAFAX No. 3O2 -S36-5972 P r o cl u c t s Railcar No.: PLCX-42984 Da te a f S h:i. pmen t s 3--11--91 Order No.: 897918-033 ............................................................................................ ... ......................................................................... . i Mewmsms--sm--i in>* hw Property It4f H "i H*4**4M1 f44#*IM fe Jl I *1 Moistures. 7. Test 4*> ** I*t Method 144*44 feW * *4 441* Bl ^ .*+*-**** WI ABR-1A Analysis O 09V* H J / Bu 1 k D e n s i t y , GM / CC P a r t i c 1 e S i ze /m onti ABR-2A + + + + + ff + 4> + t + + + t + + +* O . b 3 4 ABR--3 WtllHMIMK 4I > Mfl B M* 4* te* iieHH nri kf|*tlt**tMU*>*fe44*4fefefe**|fe*4MllNH* 40 60 80 <** ***I4*4*4***444*44feei ifi#4peen<P hmil P4W44^**itM*tl*4 10 0 120 *44 P^4< tee putti *ttSW**H4HHfe*U*t*l*iS*4 I 4lfeH><lifefeMt *fefefefefe*W* ( H44IM1 rf4414M*H444 14 0 9 o ns.f IH feil Hit*. I*Hip PAN 4 f MfMfeHUIttftSMS* i#* nf e***W*fe fe*fe<*fep*e** fe***4 0.00 iH*ll**ia*itii*4tf **# ******-p*M4**#r il**i*iitM**Mtf *-** * fePfefe*41f44i* 141 fe+l fe o r'\ **lf+ >44tt*tn>*t>ni4H 1*4H 11 *** ^***** ie* tl Wt^Pttfa*4*i*Bi 4i t|_fe el 4|i *** **. 1'We '*, it |H. 4IM > >tt *i I1HNI 111 1*1 PM4**4t*i*fe.rtH*MPPf f*4feVtf***i j!H*tW4 i*P*I1**** 1 H*> T+4t+4*te*4 OO ,, 18.9 2 m *fetfefW I ttlfefelitm |* *i w* P-et+ee********* tttHffet * 4 ten >*Mfet*t*I4eatf bi**Htiitiasfet**t*4M C*t**pee kd |efe>.|*eietfeHe*ppfe>fefe4e**e* !!* M*44*i4hi.mw*n*i*tH*t**fe*M**ft*t4W***P*iimfHW4"*it*M.>fe>feMPPiMMi< Hifeit 14* HHt*el*l*inw*ti i****** ii*t*ti* .................................... *eet -- feife* w\(,l* BY C0MPARTMEN1 H444** l*4*44*> *4. 1t*m.Hmi aw****-* *4 . + ** 14#* HfeWI M'l l P ' A i*ifetH|tnfeMi|ttt**H*mtPf< 1144 I4***44*ttnnn * H|*tt IPttHlW CA CB KtlVfelMWfe MlKt niitiwi <4tt41 ttl H 14tHI*W*****Pf*tWt44tH H*fefei fefefe *****! l44feH**H4feM I444*tt * 4 i B 4 4 MHpiHifemPii i**fei lPnlM*l*H*Pl fe i *Hife*** Residual VCM. PPM ABGC-26 Inherent Viscosity ABR--10B Con t am i ri a t i on 0.07 5 0.031 0 099 . i4tVtt.fe.ife i 1 tHtttMl*1t**mil44*44M4fe*4i 4 1***1 **** I4IM P 4* I44I44IHI tPttff -- l|flt**l*4tHlt.lH.tai .nl.l mb#* O7 *Hf m >r *fwf f ) r> t) 7 m / 4tfb . i tee >Hi*IH4lMT4*44*4tlW 4||lw*l44t4MMtl nMltliMpUPMlfefi 0.076 i i.ptB...1f uii4!4Ht444*ii4iilii -7 < ***-***-*' El y n t r o n , B1 k / B r n ABR-5A Made wi t h dec a 1 c .i. f i ed water o / 1 b j 0 / 18 44 44 44444 .4 441*444444 444pat | ut.4 ****** **** p*i IptllM *4 ** **| * - H *Mp*.pap*l*fetl 1/ 6 -- *; / J*W J* 6 All particles of contamination are less than . 07 mm2 in s i. z e H.D. Lucas Laboratory **+* i i 4*44*444*444.44444* ****** * + * **! 44*1*1 M PI PI H44I44 H 14*41 E3u perv .i so r / L e ad Phone (60.1) i** VAB.0001193383 >1 4* > ;ERT IFI CATE ANALYSI Da te 2 Customer M. +*-|+ 1 X hi i r re /% >r ,l*,i FAX No It * + f-4-r i H. D L u c a s / '*-'** * I J La bora tory WMHfffir*' . ....................................................... S u p e r v i. s o r /1.... e a d Phone (&U.1) 3 6>c? -- B 1.1.1 VAB.0001193384 Vista Polymers Highway 25 Aberdeen. MS 39730 RAILCAR ANALYST Load Date: Time Logged In: Ship Date: Product: Car No. : Logged In By: : UxAAJLKL Contamination Syntron Method Bulk Density BD w/antistat Viscosity RVCM Blown Film J2L J2- JtL ML /g/ / L i i o <N Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight OcrO % Go .06 or less z* 60 9 0.68 @r\ 80 t'W 3.1 .07----- -- .15 100 3.32 //.x 120 140 /C.LO 33, S' 30-0 ----- .60 200 Pan Ig5 A-S- / 7-7Static Flow: O % Glassies: Z )% Avg. Microns: JJif. A Color L: a O.Tl b }(oO CPA: Jo*) Technician: Tf, v- Sfs VAB.0001193385 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, MHPpi 39730-0091 Phone (601) 369-8111 Date; 8 March 91 Customers American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 7 March 91 FAX No. 302--836--5972 Product: 5305 Railcar No.: GACX-73400 Order No.: 897918--024 Property Test Method Analysis Moisture, V. ABR-1A 17 Bulk Density, GM / CC ABR-2A Particle Size, 7. on ABR-3 40 1 0.0 60 0.3 80 100 120 140 200 PAN 4.8 13.0 35.2| 29.6 15.1 2.6 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than .07mm2 in size. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193386 -1 Vista Polymers Highway 25 * Aberdeen, MS 39730 Load Date: Time Logged Ship Date: Product: 5305 Car No.: Silo(s): Logged In By: Customer : ihjwY Im A5o THcftl-- Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film A 1st 2nd ir JS2. CA 1st 2nd CB 1st 2nd ofT B 1st 2nd *4* Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight X 0^ O .06 60 *2. 80 eL&. 100 fc,e> 120 (75* .20 .60 140 200 Pan Loo 2 Static Flow: o ,7? X Glassies: Avg. Microns te%/ Color L: a $31 b LJ2J2. CPA: Technician: + h- h * ...... 1 in a VAB.0001193387 T* Vista Polymers A Division of Visto Chemical Compony Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39/30-009T Phone (601) 369-8111 Date: 6 March 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 4 March 91 VIS1AFAX No. 302-836-5972 Product: 5265 Railcar No.: UTCX-46396 Order No.: 900738-004 Proper tv Test Method Ana lysis Moisture, '/. ABR-1A ttttttttttttttttt*! 0.13 Bulk Density, GM/CC ABR-2A 0.531 Particle Size, ABR-3 40 6* O 80 100 120 140 200 PAN */. o n 0.00 i 0.3 7.8 17.3 39.4 23.0 9.9 2.3 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Con tarnina tion, Syntron, Blk/Brn ABR-5A 0.065 0.67 0.070 0.66 0.062 0.66 0.060 0.66 2/ 5 ........ . i 2/ 10 i 1/ 3 4/ 6 Labor atory Supervisor/Lead Phone (601) 369-8111 VAB.00011$3388 Vista Polymers Higlwr 2fT Aberdeen, MS 39730 Load Date: Time Logged Ship Date: RAILCAR ANALYSIS VTCX Produc t: Cor No .zJdfkllk IJOD Logged In By: Silo(s): Customer: Moisture 1st 2nd 1 *st 2nd I 1st 2nd 1st 2nd P J3___1 >7 I 1 ,0-2- Contamination Bulk Density ~"z 1 ssc, 1 12 | /o 1 .3$ | 1 J___ BD w/antistat Viscosity RVCM Mirrex Shipments ONLY Screen Analysis Mesh 40 Weight % 0*0 60 J3 .7 80 Static Flow: Color L: 100 120 140 3M Avg. Microns O, b /To 200 Pan [A3 Technician VAB.0001193389 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 Date: 6 March 91 Customer: American Mirrex P. 0. Box 728 Mew Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 4 March 91 FAX No. 302-836-5972 Product: 5305 Railcar Mo.: VIPX-45765 Order No.: 897918-029 Property Test Method Analvsis Moisture, 7. ABR-1A ................................. * 0.13 Bu1k Density, GM/CC ABR --2A ............... O . 519 Particle Size, V. on ABR-3 40 60 80 ICO 120 140 200 PAN 0.0 0 0.3 O 0 14.5 40.2 28.1 11.6 1.5 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.061 0.086 0.061 0.064 Inherent Viscosity ABR-10B 0.73 0.72 0.72 0.73 Con tamination, Syntron, Blk/Brn ABR--5A 4/ 8 3/ 9 7/ 11 3/ 10 Made with decalcified water. All particles of contamination are less than .07mm2 in size. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193390 Vista Polymers Highway 25 Aberdeen. MS 39730 RAILCAR ANALYSI Load Date I* Product: KLZ%r Car No.: Time Logged In: Ship Date: Silo(s) Logged In By: &2. : jLLwaAfl6Sf Customer 1st 2nd 1st 2nd 1st 2nd 1st 2nd Moisture Contamination Syntron Method 6? .0-3 Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film ./>&/ Tappi Test Contamination Composite Screen Analysis Mesh Weight X 40 e>, co o.o *06 or less 60 -J- 6.3 80 13o .07 . 15 .20 .60 100 120 &S3 140 l<ko6 200 Pan -M Static Flow: a 3.3 % Glassies Avg. Microns: /3/.^ Color L: a <*-^5 b A&? CPA: Technician: VAB.0001193391 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Adendeen, Mississippi 39730>0091 Phone (601) 369-8111 Date: 6 March 91 Customer: American Mirrex P. D. Box 728 New Castle, DE Attention: Lynn Webb 19720 Date of Shipment: 4 March 91 FAX No. 302-B36-5972 Product: 5305 Railcar No.: VIPX-45760 Order No.: 897918-030 Pr oper ty Test Method Ana lysis Moisture, 7. ABR-1A ................................................... 0.22 Bu1k Density , GM/CC Particle Size, 7. on ABR-2A * *...........*...................... 0.525 ABR-3 O oO 40 60 80 lOO 120 140 200 PAN 0.2 6.7 16.7 38.6 24.4 11.7 1.7 BY COMPARTMENT A CA CB B Residua 1 VCM, PPM ABGC-26 0.215 0.083 0.075 0.050 In heren t Viscosity ABR-10B 0.72 0.72 0.72 0.72 Con t am ina t ion , Syntron, B1k/Brn ABR-5A 3/ 7 2/11 6/ 13 2/ 10 Made with decalcified water. All particles of contamination are less than .07mm2 in size. Laboratory Supervisor/Lead Phone (601) 369-8111 t VAB.0001193392 Vista Polymers Highway 25 Aberdeen* MS 3ST730 Load Date: Time Ship Date: RAILCAR ANALYSX : 4S7C& Contamination Syntron Method Tappi Test Contamination Composite .06 or less Screen Analysis Mesh Weight % 40 h-QO O'O 60 .a JL 80 33? 6.7 .07 100 $.23 Static Flow ^ / 7*7 X Glassies: . 15 .20 . 60 120 itsz Wo 140 200 Pan j9.a/ S. XT' , fT LLA Avg . Microns: /3t h Color L: r lb b L3f CPA: iTechn lcian: 6^7 VAB.0001193393 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 25 Feb. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE Attention: Lynn Ulebb 19720 Date of Shipment: 22 Feb. 91 FAX No. 302-836-5972 Product: 5305 Hai lcar No. : VIPX--45747 Order No.: 897918--023 Proper ty Moisture, 7. Test Method ABR--1A Ana lysis ............................... 0.08 Bu1k Density, GM/CC Particle Size, 7. on ABR--2A * ............... * **** 0.533 ABR-3 40 60 80 lOO 120 140 200 PAN 0.00 0.1 4.4 14.4 38.9 26.4 13.8 2.1 .. ...... BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination are less than .07mm2 in size. Laboratory Supervisor/Lead Phone (601) 369-8111 .I VAB.0001193394 Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR ANALYSIS Load Date: I u Product: 5305 Car No . 4Z7A1 Time Logged In: !d'3 Ship Date : X A Silo(s): Logged In By: L7i Customer Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film (3> 1st 2nd , 0b i/ 1st 2nd | 1st . Db 2nd A */<-$rt /y - 1st 2nd P-5- 3 Tappi Test Contamination Composite .06 or less _____ rX________________ Screen Analysis .07---------- .15 .20---------- Mesh Weitfht V 40 A. Cf 60 p ^ . o 3'.... . OJ 80 J?. 2 0 100 7/1 /f 4- 120 140 /?- yy. I* 15^0 200 kJl .60 Pan lt>3 Z,/ Static Flow: O I. 27 % Glassiesl * :/ Avg. MMicrons: Color L: b CPA: tZ-3 ,/ Technician: % ft. U> VAB.0001193395 VAB.OOOl193396 TO: mmuiiiiv Communication FROM DATE SUBJECT: John Olson Jim Edwards March 8, 1991 Wet RC# GACX 73381 at AMC American Mirrex's Lynne Webb sent a wet resin sample from the top of compartment CA of the subject 5305 railcar. Please refer to the attached note* We then requested for the CSX Terminal to send us top and bottom samples from all four compartments. These samples showed the top of CA and the bottom of CB were wet. Please refer to the attached analysis sheet. The lab retain samples for this car were dry. We recommended that both CA and CB compartments be returned to the plant. Please research the production of this car of 5305 so we can understand how this material passed our Quality Control. cc: RWS,DCS,JRW,BPS,AEB,LDH,DEK 6im Edwards Chief Plant Chemist VAB.0001193397 mm mmm VAB.0001193398 Railcars Car No. TYPE SILO NO. TIME/BY SAMPLEO BY TIME SAMPLEO TESTED BY SHIPPING SAMPLE LOG Comp. ORIGINAL INFO. T/B Moist. Screens 40 200 Pan Bulk UJL RESAMPLE RESULTS DATE 3-08-9/ Revised 243 V AB.OOOt193399 Vista PolynMn A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Adeideen. Mississippi 39730-0091 Phone (601) 369-8111 i* tA Da te: 25 Feb. 91 Customer American liirrey. P. 0. Box New Castle, DE Attention: Lynn Webb 19720 Date of Shipment: 22 Feb. 91 FAX No. 302-836-597 VEJ* Product: 5305 Railcar No.: GACX-73381 Order No.: 897918-034 Proper ty Test Method Ana 1vsis Mo3 sture, 7. ABR-1A 0.06 Bu1k Density , GN/CC Par ticle Size, ABR-2A ABR-3 0.525 00 1,00 120 140 | 200 PAN */. on 0.00 0.5 i .9 111. 5 36.7 28.8 16.8 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.056 0.054 0.055 0.054 Inherent Viscosity ABR-10B 0.72 0.72 0.72 0.72 Con taminatlon, Syntron. Blk/Brn ABR-5A 3/ 9 4/ 8 3/ 6 4/ 10 Made i')i th decalcified water All particles of contamination are less than .07mm2 m size. LaLoratcry Supervlsor/Lead Phone (601) 369-8111 VAB.0001193400 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 i' \ Date: 25 Feb. 91 Customer: American Mirrex P. O. Box 728 New Castle, DE Attention: Lynn Ulebb 19720 Date of Shipment: 22 Feb. 91 VKt\FAX No. 302-836-5972 Product: 5305 Railcar No.: GACX-73381 Order No.: 897918-034 Property Test Method Ana 1vsis Moisture, '/. ABR--1A * * 0.06 Bulk Density, GM/CC Particle Si2e, ABR-2A ABR-3 0.525 40 60 80 100 120 140 j 200 PAN V. on 0. OO 0.5 2.9 11.5 36.7 2B.8 16.8 2.8 i BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.056 0.054 0.055 0.054 Inherent Viscosity ABR-10B 0.72 0.72 0.72 0.72 Con tamina tion, Syntron, Blk/Brn ABR-5A Made with decalcified water. 3/ 9 4/ 8 3/ 6 4/ lO fe All particles of contamination are less than ,07mmz in size. Laboratory Supervisor/Lead P hone (601) 369--8111 VAB.0001193401 Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR Load Date : tw Ir Product ANALYSIS gy&X Car No.: 7AS U Time Logged In: OL0& Ship Date: 1 $/ Silo(s): Logged In By: Cjo (o%~> : AjAMjUf Customer Moisture Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film A 1st 2nd , o4 S3! six . >S~l CA 1st 2nd , -3T .7/fT i CB 1st 2nd / fa P/(. B 1st 2nd ( Jtit Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight 0*0 O % 06 or less 60 D*2r3 ,J> 80 .07---------- .15 .20---------- .60 100 120 140 200 Pan IL6. 3LTt 2M t6J JI.P Static Flow: 0 / 4nX3 % Glassies: Avg. Microns: /*- Color L: a OZ,9 b / L3 CPA: Technician: A'3 JrR.tf 1 VAB.0001193402 Vista Polymers A Division ol Vista Chomioal Company Highway 25 PostOmc* Box 91 CERTIFICATE OF ANALYSIS T* V Adoftfcon, Mississippi 39730-0091 Phono (601) 369-8111 f lh \ Date: 21 Feb. 91 Customer: American Mirrex P. 0. Box New Castle, DE 19720 Attention: Lynn hlebb Date of Shipment: 18 Feb. 91 VISIAFAX No. 302-836-5972 Products 5305 Railcar No.: VIPX-45B66 Order No.: 897918-031 Property Test Method Analysis Moisture, V. ABR-1A * 0.07 Bulk Density, GM/CC ABR-2A 0.537 Particle Size, ABR-3 40 1 60 80 100 120 140 200 PAN *i 7. on 0.00 0.3 7.3 18.8 19.1 14.2 2.4 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.019 0.016 0.003 0.001 :'.V 1<* -. * I* Inherent Viscosity ABR--10B 0.73 0.73 0.73 0.73 L `1I Contamination, Syntron, Blk/Brn ABR-5A * '" 2/ 5 3/ 7 2/ 5 2/ 8 * iT Made with mixed calcified water i t ->:1 All particles of contamination are less than -07mm* in size. *. - .< --- Ai *' ' f*.^ - " . V ' '*j^ 4 'v 1 .1 * 54 i .\ ":`4 -rA1 Bil Laboratory Supervisor/Lead Phone <601) 369-8111 VAB.000119340& Vista Polymers Load Date: Tine Ship Date^ Highway 25 Aberdeen* MS 39730 (t railcar analysis yjr/'A Product:! 5305 437 t Contamination Syntron Method Wet Method Mesh Bulk Density w/antistat Viscosity RVCM Blown Film 727 . iI L 72 ?| 1- sy/ 1. Screen Analysis Mesh 40 Weight X 60 0-/3 3 80 7J 100 jM 120 /Q-y/ 140 7-5Y /%/ Static Flow: p/7.7 Avg. Microns: Color L: 77. p */ a b CPA: 200 Pan 7-/2 /v.2 -4 Technician: k VAB.0001193404 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Omen Box 91 CERTIFICATE OF ANALYSIS Adonfeon, Mississippi 397304)091 Phono (601) 369-8111 / & Date: 21 Feb. 91 Customer: American Mirrex P. O. Box 72B New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 18 Feb. 91 VKI\FAX No. 302-836-5972 P roduct: 5305 Railcar No.: ACFX-41170 Order No.: 897918--032 Propertv Test Method Analysis Moisture, 7. ABR-1A * * * * ............................. * * 0.03 Bulk Density, GM/CC Particle Size, ABR-2A ................................................... 0.540 ABR-3 | 40 60 1 80 I100 [l20 I 140 j j 200 [pan| 7. on 0.00 0.4| 7.3 16.4 32.6 21.7 19.1 1 2>5I BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC--26 Inherent Viscosity ABR--lOB Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water. All particles of contamination less than .07mm2 in size. Laboratory Supervisor/Lead Phone (601) 369-8111 p VAB.0001193405 Vista Polymers Highway 25 Aberdeen. MS :3973JD 4 b RAILCAR ANALYSIS V* Load Date: /3 6 Product: 5305 Time Ship Date: Car No. Contamination Syntron Method Screen Analysis Mesh Weight % 40 0 06 <S O 60 llX 80 100 120 140 I Static Flow: 6 / .6? Avg. Microns: Color L: a g- * b CPA: fl.& % Glassies: i% 200 Pan 2S Technician: VAB.0001193406 Vista Polymers A Division of Vista Chwnical Company Highway 25 Post OfRc Box 91 CERTIFICATE OF ANALYSIS Aderd--n, Mississippi 39730-0091 Phono (601) 369-8111 14 Feb. 91 Customer: American Mirrex P. 0. Box New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 12 Feb. 91 VBC\FAX No. 302-036-5972 Products 5265 Railcar No.: UTCX-46510 Order No.: 900738-002 Property Test Method Analysis Moisture, V. ABR-1A 0.12 Bulk Density, GM/CC ABR-2A 0.535 Particle Size, ABR-3 40 60 80 100 120 1140 |200 PAN 7. on 0.00 0.2 8.5 J18.0 39.4 22.4 j 9.2 2.3 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 .Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A 0.059 0 66 0.069 0.66 0.069 0.66 0.070 0.66 2/ 8 1/ 5 2/ 8 1/ 6 Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193407 Vista Polymers Highway 25 Aberdeen * MS RAILCAR ANALYSIS urcX Load Date: Product: 5265 Car N Time Logged In: >/3 Q Logged In By: Ship Date: Silo(s): Moisture Contamination 1st 1 2nd 4 <0t> Bulk Density BD w/antistat Viscosity RVCM 1 Mirrex Shipments ONLY 2nd l8t 2nd 1st 2nd Screen Analysis Mesh 40 Weight L&2. % QiA 60 sUL 80 4, *7 Static Flow: 0 t%7 Color L : 100 oz 120 19 39.4 140 UiZ / 22.4 200 9.2> Pan Ln anAvg. Microns: a M b L22 Technician: *H*P"*"fM 9' mmmm * >W> i. VAB.0001193408 p i . i mmfm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office .Box 91 CERTIFICATE OF ANALYSIS Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 14 Feb. 91 Customer: American Mirrex P. 0. Box 728 New Cast1e, DE 19720 Attention: Lynn Webb Date of Shipment: 11 Feb. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: VIPX-45850 Order No.: 897918-028 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Particle Size, ABR-3 7. on Ana 1vsis * 0.18 40 60 | 80 100 120 140 J200 jpAN 0.00 0.3 13.5 23.7 37.9 14.4 8.6 1.6 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.099 0.006 0.019 0.104 Inherent Viscosity ABR-10B 0.73 0.74 0.74 0.73 Contamination, Syntron, Blk/Brn ABR-5A 12/ 4 9/ 5 10/ 4 9/ 6 Made with non-decalcified water. All particles of contamination are less than .07mm2 in size. Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193409 Vista Polyaers Highway 25 Aberdeen# MS 3^730, RAILCAR ANALYSIS Load Oate:. to '21 -7g Product: 5305 Car No. Time Logged In: Ship Date JL SiJLot s ) Logged In By: Customer yjfK 4 Moisture Contamination Syntron Method Wet Method Mesh Bulk Density w/antistat Viscosity RVCM Blown Film 1st 2nd ,n 1 1st jr 1 2nd I 1st 1 ,/r I 2nd I 1st | , /4. 1 2nd l __________1 CT0 . 715*? 1__________ ,0/1 __________ __________ Screen Analysis Mesh 40 60 80 100 120 140 Weight 0.00 ,/r 6. 77 MH. /%/r 7.22 X o.o ,3 )3,r 22. 7 27,1 Static Flow: 0 / 7,1 Avg. Microns Color L: ^ a .43 b A 47 CPA n. i X Glassies: </% 200 Pan A6 Technician VAB.0001193410 Vista Polymers Date: Highway 25 Aberdeen* MS 39730 RAILCAR ANALY3XS * - / Product: Ship At Moisture Contamina t ion 1st 2nd 1st 2nd 1st 2nd 1st 2nd _____________ 2 Bulk Density BD w/antistat Viscosity RVCM Screen Analysis Mesh 40 Weight ,oo 0.0 60 A 2- Static Flow: 80 337 63 100 *7. (0$ /ry 120 if.? 140 ;o,so 2/, C> 200 /S.f Avg. Microns /JZ7 Pan AtO 3 .4 Color L ^4,00 f.S h / Technician: VAB.0001193411 CERTIFICATE OF ANALYSIS \ Dates 30 Jan. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynn UJebbb Date of Shipment: 28 Jan. 91 FAX No. 302-836-5972 Product: 5265 Railcar No.: UTCX--46584 Order No.: 900738-001 Property Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Analysis * 0.19 0.543 Particle Size, 7. on ABR-3 40 0.00 60 0.2 80 6.7 100 15.4 120 38.7 140 200 PAN .... 21.6 13.8 3.6 ........................................... BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 Inherent Viscosity ABR-10B Contamination, Syntron, Blk/Brn ABR-5A 0.082 0.66 0.082 0.66 0.080 0.66 0.081 0.66 1/ 3 6/ 4 3/ 4 2/ 5 Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193412 Vista Polymers Highway 25 Aberdeen, MS 3973 Load Date: RAILCAR ANALYSX S P/.CA Product 5305 Car No* : &6 & Time Logged In: 1*2^0 O Ship Date: Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film mi / js-wt Tappi Test Contamination Composite Screen Analysis Mesh Weight 40 oa0 X Oja o 06 or less UA r7--__--_-. _ _ i1oC .20---------- .60 60 2>,/3 .3 80 3.0<o Aj-- 100 f./L /<f-3 120 m? 3%;s~ 140 / 3 7 200 K.3l Pan 0JS t. 7 Static Flow: 0/ y.i X Glassies: Color L: _jUL1M a ^-^7 b Avg. Microns: CPA: A ^Techniicciiaan: an mmmmfrn 'r y r1 VAB.0001193413 `F* iS T CERTIFICATE OF ANALYSIS Date: 5 Feb. 91 Customer: American Mirrex P. 0. Box 728 New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 4 Feb. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: PLCX--46860 Order No.: 897918-027 t Property Test Method Analysis Moisture, V. ABR-1A * 0.08 Bulk Density, GM/CC ABR-2A 0.545 Particle Size, V. on ABR-3 40 0.00 60 0.3 80 100 120 140 200 PAN ............................................-............................... 6.1 ^3 3 38.5 25.9 11.2 1.7 BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.026 0.724 0.053 0.048 Inherent Viscosity ABR-10B Contamination, 0.73 . 0.72 0.73 0.72 Syntron, Blk/Brn ABR-5A 2/ 3 3/ 5 2/ 4 3/ 8 Made with decalcified water. All particles of contamination are less than .07mm2 in size. Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193414 ./ Vista Polymers Highway 25 r* Aberdeen* MS 39730 Load Date t 1 RAILCAR ANALYSIS //CK Product: 5305 Car Mo. : W C C/ Tine Looggggeeda Iinn:: Qi lyOO 7^/tfl Si Ship Date Silois): Logged In By: <r t 7 U gf Customer: JtASKi Contamination \W\Syntron Method j Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film 711. , /eb jJ !\ 7? I . ^f2-| i - 7z^ 1 *1 || 1 '/? t . 710 | a/s" - 773 . oss t Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % y.f o 0.VV .06 or less 7 60 o,/ 0.2. 80 .07----------.15 r- .20---------- .60 100 LkU. 120 17. & 7 140 ILLS'. 200 'S:?. L Pan ?? Up Static Flow: 0 / 7*? X Glassies: w T't Avg. Microns: /SJ/?, *0 Color L: ab CPA: ZjQyU Technician: 4- Kjf VAB.0001193415 b -i Vista Polymers Highway 25 P.O.Box 91 Aberdeen, MS 39730 CERTIFICATE OF ANALYSIS Date: l. Customers 5 Feb. 91 American Mirrex P. 0. Box 728 New Castle, DE 19720 Attentions Lynn Webb Date of Shipment: 4 Feb. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: PLCX-42664 Order No.: 897918--026 Propertv Test Method Moisture, 7. ABR-1A Bulk Density, GM/CC ABR-2A Ana1vsis ................................. 0.05 ........................................ 0.542 Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193416 1 CERTIFICATE OF ANALYSIS Date: 5 Feb. 91 Customer: American Mirrex P. O. Box 728 New Castle, DE 19720 Attention: Lynn UJebb Date of Shipment: 4 Feb. 91 FAX No. 302-836-5972 Product: 5305 Railcar No.: PLCX--42664 Order No.: 897918--026 Propertv Test Method Ana1vsis Moisture, 7. ABR--1A *** 0.05 Bulk Density, GM/CC ABR-2A * 0,542 Particle Size, 7. on ABR-3 40 0.00 60 0.2 80 100 120 140 200 PAN 8.2 18.1 38.5 23.4 10.0 JL v BY COMPARTMENT A CA CB B Residual VCM, PPM ABGC-26 0.106 0.042 0.062 0.055 Inherent Viscosity ABR-10B 0.72 0.72 0.72 0.72 Contamination, Syntron, Blk/Brn ABR--5A 2/ 8 3/ 7 1/ 7 2/ 5 Made with decalcified water All particles of contaminat ion are less than .07mmz in size. Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193417 \V * VAB. 0^01193418 tMiMVBiPMWM 1T 9 Vista Polymers Highway 25 H i Aberdeen MS 39730 PVC RAILCAR ANALYSX Load Date: Time Ship Date: \ Contamination Syntron Method Wet Method Bulk Density BD w/antistat Viscosity RVCM Blown Film Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight x 6o a- 60 80 100 120 140 200 Pan MJ. 7,n n.Li J.?/ 0.7/ s. c.<\ IS-J 42A ASA. iJ _L_ Static Flow: n % Glassies: Color L: 99, /UsT' a b 7A7D Avg. Microns: CPA: ijp.f Technician: 4 4- fi.M VAB.0001193419 CERTIFICATE OF ANALYSIS Date: 5 Feb- 91 Customer: American Mirrex P. O. Box 728 New Castle, DE 19720 Attention: Lynn Webb Date of Shipment: 4 Feb. 91 FAX No. 302--836--5972 Product: 5305 Railcar No.: ACFX-41145 Order No.: 897918-025 Property Test Method AnalYfei5 Moisture, 7. ABR-1A ................................................... 0.06 Bulk Density, GM/CC ABR-2A *..............******** 0.543 Particle Size, ABR-3 40 60 80 100 120 140 200 PAN 7. on 0.00 0.5 6.9 15.8 42.2 25.4 7.8 1.4 BY COMPARTMENT A CA CB B Residual VCM, PPM AB6C-26 0.064 0.060 0.070 0.051 Inherent Viscosity ABR-10B 0.73 0.73 0.72 0.73 Contamination, Syntron, Blk/Brn ABR--5A Made with decalcified water 7/ 17 8/ 16 1 5/ 11 1 6/ 13 All particles of contamination are less than .07mm2 in size. Billy P. Sizemore Laboratory Supervisor/Lead Phone (601) 369-8111 VAB.0001193420