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PFOS 3M FLUOROCHEMICAL SUBMISSIONS February, 2002 - May, 2004 ENVIRONMENTAL STUDIES Click on Study Title to View Report Perfluorooctanesulfonate PAGE 1, 2, 3, 4, 5 Summary and Other Environmental and Health Assessment of Perfluorooctane Sulfonic Acid and Its Salts, 3M, August 20, 2003. [SubmittedAugust 25, 2003] 3M Lifetime Drinking Water Health Advisory for Perfluorooctanesulfonate, Revision Date: April 19, 2002. [Submitted July 16, 2002] Environmental Fate and Transport 1. Soil Absorption/Description Study a. Robust Summary, Soil Absorption/Desorption Study of Potassium Perfluorooctanesulfonate (PFOS), June 4, 2001. [Submitted July 16, 2002] b. Final Report, Soil Absorption/Desorption Study of Potassium Perfluorooctanesulfonate (PFOS), June 4, 2001, 3M Environmental Laboratory, Report No. E00-1311. [Submitted July 16, 2002] 2. Incineration Study a. Robust Summary, Laboratory-Scale Thermal Degradation of Perfluoro-Octanyl Sulfonate and Related Precursors, July 3, 2003. [Submitted July 9, 2003] b. Final Report, Laboratory-Scale Thermal Degradation of Perfluoro-Octanyl Sulfonate and Related Precursors, Environmental Sciences and Engineering Group, University of Dayton Research Institute, June 19, 2003. [Submitted July 9, 2003] Ecotoxicity 1. Final Report , PFOS: An Acute Toxicity Study with the Earthworm in an Artificial Soil Substrate, May 10, 2002, Wildlife International, Ltd., Project Number 454-111. [SubmittedJuly 16, 2002] 2. Perfluorooctanesulfonate, Potassium Salt (PFOS) Study a. Robust Summary, Perfluorooctanesulfonate, Potassium Salt (PFOS) Study, June 21, 2002. [Submitted July 16, 2002] b. Final Report, Perfluorooctanesulfonate, Potassium Salt (PFOS): A Flow-Through Bioconcentration Test with Bluegill (Lepomis macrochirus), June 21, 2002, Wildlife International, Ltd., Project Number 454A-134. [Submitted July 16, 2002] ENVIRONMENTAL STUDIES Click on Study Title to View Report Back to Menu PFOS Perfluorooctanesulfonate PAGE 1, 2, 3, 4, 5 3. Terrestrial Plant Toxicity Study a. Robust Summary, Toxicity to Terrestrial Plants, June 3, 2003. [Submitted July 9, 2003] b. Final Report, PFOS: A Toxicity Test to Determine the Effects of the Test Substance on Seedling Emergence of Seven Species of Plants, Wildlife International, Ltd. Project No. 454-110, May 30, 2003. [Submitted July 9, 2003] c. Analytical Laboratory Report, Analytical Method Validation for the Determination of Perfluorooctanesulfonate, Potassium Salt (PFOS) in Artificial Soil, Wildlife International, Ltd. Project No. 454C-120, May 27, 2003. [Submitted July 9, 2003] d. Analytical Laboratory Report, Analytical Method Validation for the Determination of Perfluorooctanesulfonate, Potassium Salt (PFOS) in Plant Tissues, Wildlife International, Ltd. Project No. 454C-125, October 22, 2001. [Submitted July 9, 2003] 4. Avian Studies a. TSCA 8(e) Notice of Draft Reports of Reproduction Studies of Northern Bobwhite and Mallard and PFOS [submittedFebruary 1, 2002] b. Mallard Duck Acute Study [SubmittedMay 11, 2004] i. Toxicological Summary, PFOS - Dietary Acute Mallard Study, March 23, 2004. ii. Final Report, PFOS: A Dietary LC50 Study with the Mallard, March 23, 2004. iii. Analytical Report, Laboratory Report Revision 1: Analytical Report of Data for PFOS Dietary LC50 Study with Mallards (Sera and Liver), March 19, 2001. c. Mallard Duck Pilot Study [SubmittedMay 11, 2004] i. Toxicological Summary, PFOS - Dietary Chronic Pilot Reproductive Study: Mallard, May 5, 2004. ii. Final Report, PFOS: A Pilot Reproduction Study with the Mallard, March 24, 2004. iii. Analytical Report, Extraction of Potassium Perfluorooctanesulfonate from Mallard Serum and Mallard Liver for Analysis Using HPLC-Electrospray/Mass Spectrometry (Mallard Pilot Study Samples), Centre Study No. 023-042, September 10, 2001. iv. Analytical Report, Extraction of Potassium Perfluorooctanesulfonate from Egg Membrane, Albumen, and Yolk for Analysis Using HPLC-Electrospray/Mass Spectrometry (Quail and Mallard Pilot Studies samples), Centre Study No. 023-063, September 10, 2001. ENVIRONMENTAL STUDIES Click on Study Title to View Report Back to Menu PFOS Perfluorooctanesulfonate PAGE 1, 2, 3, 4, 5 d. Mallard Duck Definitive Study [SubmittedMay 11, 2004] i. Toxicological Summary, PFOS - Dietary Chronic Definitive Reproductive Study: Mallard, May 5, 2004. ii. Final Report, PFOS: A Reproduction Study with the Mallard, March 24, 2004. iii. Analytical Report, Analytical Phase Report for PFOS: A Reproduction Study with the Mallard (Mallard Definitive Study Sera and Liver Analyses), 3M Environmental Laboratory Study # E01-1256, January 22, 2003. iv. Analytical Report, Extraction of Potassium Perfluorooctanesulfonate from Red Blood Cells and Serum for Analysis Using HPLC-Electrospray/Mass Spectrometry (Samples from Definitive Mallard and Quail Reproduction Studies), Exygen Study No. 023-070, June 12, 2003. v. Analytical Report, Analysis of Perfluorooctanesulfonate in Mallard and Quail Egg Yolk (Mallard and Quail Definitive Reproduction Study Eggs), Exygen Study No. 023-070, July 5, 2002. e. Northern Bobwhite Quail Acute Study [SubmittedMay 11, 2004] i. Toxicological Summary, PFOS - Dietary Acute Northern Bobwhite Study, May 5, 2004. ii. Final Report, PFOS: A Dietary LC50 Study with the Northern Bobwhite, Wildlife International, Ltd. Project No. 454-103, March 24, 2004. iii. Analytical Report, Laboratory Report Revision 1: Analytical Report of Data for PFOS Dietary LC50 Study in Northern Bobwhite (Sera and Liver), 3M Environmental Laboratory No. FACT-TOX-129, March 23, 2001. f. Northern Bobwhite Quail Pilot Study [SubmittedMay 11, 2004] i. Toxicological Summary, PFOS - Dietary Chronic Pilot Reproductive Study: Northern Bobwhite, May 5, 2004. ii. Final Report, PFOS: A Pilot Reproduction Study with the Northern Bobwhite, Wildlife International, Ltd. Project No. 454-104, March 24, 2004. iii. Analytical Report, Extraction of Potassium Perfluorooctanesulfonate from Quail Serum and Quail Liver for Analysis Using HPLC-Electrospray/Mass Spectrometry (Quail Pilot Study Samples), Centre Study No. 023-041, September 10, 2001. ENVIRONMENTAL STUDIES Click on Study Title to View Report Back to Menu PFOS Perfluorooctanesulfonate PAGE 1, 2, 3, 4, 5 g. Northern Bobwhite Quail Definitive Study [SubmittedMay 11, 2004] i. Toxicological Summary, PFOS - Dietary Chronic Definitive Reproductive Study: Northern Bobwhite, May 5, 2004. ii. Final Report, PFOS: A Reproduction Study with the Northern Bobwhite, Wildlife International, Ltd. Project No. 454-108, March 24, 2004. iii. Analytical Report, Analytical Phase Report for PFOS: A Reproduction Study with the Northern Bobwhite (Quail Definitive Study Sera and Liver Analyses), 3M Environmental Laboratory Study #E01-1245, April 18, 2003. 5. Bluegill Study [SubmittedMay 11, 2004] a. Robust Summary, Acute Toxicity to Bluegill Sunfish, 3M, April 14, 2004. b. Analytical Report, 96-Hour Static Bluegill Toxicity Test: Aquatic Toxicity Data Sheet (FC-95), 3M, May 27, 1978. Analytical Purity Revisions to Ecotox Studies 1. Summary Table, PFOS Ecotoxicological Testing Results Comparison of Effect Concentrations Calculated Using Different Sample Purity, May 2004 [SubmittedMay 11, 2004] 2. Addenda to Previously Submitted Reports Revised to Reflect the Most Recent PFOS Purity Analyses [SubmittedMay 11, 2004] Letter to Susan Beach from Kurt R. Drottar, Wildlife International, Ltd., September 27, 2001, enclosing: a. Addendum, PFOS: A 96-Hour Static Acute Toxicity Test with the Saltwater Mysid (Mysidopsis bahia), Wildlife International, Ltd. Project No. 454A-101, September 27, 2000 [Addendum to AR226-0095]. b. Addendum, PFOS: A 96-Hour Static Acute Toxicity Test with the Fathead Minnow (Pimephales promelas), Wildlife International, Ltd. Project No. 454A-102, September 27, 2000 [Addendum to AR226-0083]. c. Addendum, PFOS: A 96-Hour Toxicity Test with the Freshwater Alga (Selenastrum capricornutum), Wildlife International, Ltd. Project No. 454A-103A, September 27, 2000 [Addendum to AR226-0085]. d. Addendum, PFOS: A 48-Hour Static Acute Toxicity Test with the Cladoceran (Daphnia magna), Wildlife International, Ltd. Project No. 454A-104, September 27, 2000 [Addendum to AR2260087]. ENVIRONMENTAL STUDIES Click on Study Title to View Report Back to Menu PFOS Perfluorooctanesulfonate PAGE 1, 2, 3, 4, 5 2. Addenda to Previously Submitted Reports cont. e. Addendum, PFOS: A 96-Hour Static Acute Toxicity Test with the Freshwater Mussel (Unio complamatus), Wildlife International, Ltd. Project No. 454A-105, September 27, 2000 [Addendum to AR226-0091]. f. Addendum, PFOS: A 96-Hour Shell Deposition Test with the Eastern Oyster (Crassostrea virginica), Wildlife International, Ltd. Project No. 454A-106, September 27, 2000 [Addendum to AR226-0089]. g. Addendum, PFOS, A Flow-Through Life-Cycle Toxicity Test with the Saltwater Mysid (Mysidopsis bahia), Wildlife International, Ltd. Project No. 454A-107, September 27, 2000 [Addendum to AR226-0101]. h. Addendum, PFOS: An Early Life-Stage Toxicity Test with the Fathead Minnow (Pimephales promelas), Wildlife International, Ltd. Project No. 454A-108, September 27, 2000 [Addendum to AR226-0097]. i. Addendum, PFOS: A Semi-Static Life-Cycle Toxicity Test with the Cladoceran (Daphnia magna), Wildlife International, Ltd. Project No. 454A-109, September 27, 2000 [Addendum to AR226-0099]. Letter to Susan Beach from Raymond L. Van Hoven, Wildlife International, Ltd., November 27, 2000, enclosing: a. Addendum, Non-GLP Study: Determination of the Solubility of PFOS in Wildlife International, Ltd. Freshwater, Freshwater Algal Medium, and Saltwater, Wildlife International, Ltd. Project No. 454C-101-1, November 27, 2000 [Not previously submitted to the AR226 docket]. b. Addendum, Determination of the Water Solubility of PFOS by the Shake Flask Method, Wildlife International, Ltd. Project No. 454C-107, November 27, 2000 [Addendum to AR226-0052]. Letter to Susan Beach from Edward C. Schaefer, Wildlife International, Ltd., December 1, 2000, enclosing: a. Addendum, PFOS: An Activated Sludge, Respiration Inhibition Test, Wildlife International, Ltd. Project No. 454E-101, December 1, 2000 [Addendum to AR226-0093].