Document qaOZmk1K7R7jooagBy7XKdbdj
R226 - 3546
ATTACHMENCT
italte Deoa0
000175
Ee LSORLEY)AY SaAlRih ie
`Nove1m1,b2e00r3
`MGEsP.laLsytnincHsall
2148North 2753" Road
Ottawa, IL 61250 Dear Lynn,
Ihave attaachcoepdyof the C8 report. Please letmeknowif Icanprovide any
additional information.
el Regards,
Tom Livese; Algoflon PTFETechnicalService
retitaid
000176
| EXYe&R E! Ren
|
Analytical Report
|
Fluorochemical Characterization of Wastewater Samples
Solvay Solexis PFOA Sampling 3/03
|
Exygen Research Laboratory Report No. L34300
|
Testing Laboratory
Exygen Research
St3a0te58CoRlelsegeea,rcPhAD1r6iv8e01
`Requester
`Warren H. Buck, PhD. Solvay Solexis 10 Leonard Lane
Thorofare, NJ 08086
RaEe BlTeer, usa
cerors
ia)
000177
i
1 Introduction LRaebsourattsoriaerse, Irnecp.o(rtdebda Efoxrygtehne Raensaelayrscihs)o(fExwyagleenr) fsraommpSloelsvaryecSeoilveeds.byThiCsenrterpeortAnparleysteinctasl resuls assigned to Exygen Researchstudy number L34300. `Speciic fluorochemical characterizaion by liquid chromatog/rtaapndhemy mass spectrometry (LCIMSIMS) was requested fralisamples. A single sample was receivedforanalysis. The samples were prepared and analyzed by LC/MS/MSfor the folowing ist of lorochemicals: Table 1: Target Analysis
2 Sample Receipt dTahteeswaamsplesuwppalsiesdu.bmTihteedsnamapplleastwiacsconrteacionenre,datonam/b1ie4n/t03t.eCmpheraaituorfec.usNioodsyamipnlfeorcmoaltlieocntioins presented in Atachment C.
3 Holding Times "T`shaemapnleasl.ytAiclaslammeptlheosdweurseedawnaalsyzveadliwdiattheidn a1g4adianyssatofmraexceiimptu.m holding me of 14 days in water
4 Methods - Analytical and Preparatory 4411.1 SLaOmpMleSPMreSparation for LOMSMS Analysis
Wreamtoevresarmespildeusalwcehlroeriinen.itSalodtrepahtaedsewietxhtr2a0ct0iounl(oSfPE2)50wamsgIuLsesdodtoiupmretphaiorseultfhaetesaSomlpulteiosnftoor LThGeMcSa/rtMiSdgaenawlayssise.ulAofdorwtiyt-hm4il0i%temraptohratnioonl:ofwastaerm.plTehWoaselutraatneswfearsreddistcoaardCerda. STPhEeccaarrtrtirdigdeg.e wbyasLOthMeSnIMelSu.tedTwhiitsh t1r0e0at%memnetthraensoull.tedAin5amnLeipgohrtlfoonldofcomnectehntarnaotliownasofctohlelesctaemdplfoersanprailoyrsitso analysis.
Pace20es
000178
UO/US/UD WEL 4b Lu ik 419448100
wee
wos
|
412 Sample Analysis by LOMSMS
|
A`aHnaolwyezet-tPhaecskaamrpdleHPe1x1a0c0tsH.PLAnCalsyyssitsemWacosuppleerdftoormaeMdicursionmgassselUelcttiemdaMreSactSiown amsoniutsoerdinfgo
(SRM). Samples were extracted on 3/26/03 and analyzed on 3/27/03 and 3/28/03. Raw
|
analytical data can be found in Attachment D.
i
5 Analysis
|
5.1 CAca6l-ipoboirnattcihaolenraitiofnorchureveawmapsouannadlyzofedraetrth,e TbenginCnainlg iofnthpeoratnsaywtcealrseeqpurereceata2n5d
50, 100, 250, 500, and 1000 ng/L (ppt), as perfluorooctancic acid (PFOA). The instrument
|
rWeeisgpwhoetnirnsoge,evtteehrresmuSisinotpehade,cyoA-ncncateeinrbtcrreaaptitiooannncwduarcsovrepirlesolatatteicdonfcocroeeefpafcitchiepano>tibn(0t.)9l6aUe2nsdi(nc7goelfif0ni.eca9ir6e5nr)te.gorfedsestieornmwiintahti1o/nx
|
---- Calibration standfoarMrSd/MsS analysis were prepared using the same SPEprocedureused
Fortra resus reported hrs, calbration teria wera mat.
|
52 xBEtxltrraaanccitkoisonnbbllaannkkssshWoeurlodprnoopahraevdeaannydatanragleytzaendaWliyttehsepverryeextasrlaocertiaobnnobvtaetcthheofcosncaemntpraltieoTnsh.oef
ho low-level calbraton standard. Forthese samthpeextlracteionbsla,nkswere complart,
|
oInvseircuamlebnrtatbiaonnksstainntdahred,foarnmdofafctlreaknnmoewthhaingohl-lseovlevlesnatmwpelerse.alsAogaainna,lhyzeedblaafnekrsesvheroyudhingoht
|
hSaamvpeleasnyprtaasragneitecanhaalryetetsheprIonssetnrtumeanttbolraanbkosaverethcoomlpolwadrotv.al calbraton standard. For the
53 Surrogates `Surrogate spikes are not a component of the LC/MS/MS analytical method.
55 Duplicates ATthaecshammepnlteA.was analyzed in duplicate. Resuls ara given along with the sample results in
56 MLialbiowraatterorwaysCsopnitkerdowlihSaPmFpOlAeals50 and500 nL. with each exiracton set. All laboratory control samples shoved racovaries between70and 130%.
6 Data Summary
Please seoAtichment Afor a cetaled lstng of the analytical esuls. Al resuls are reported
in (nglL) parts per trilion as PFOA.
raceaoes 000179
7 Data/Sample Retention
`SaacmhploensccarleadlisopoAsTecdhWofedoonenmroenttihoavfatebretheedreapoarnt dis ihsasrudedcoupnylersespoothsearwriesessopreecidfiied.atAall
folders maintained by Exygen.
8 Attachments
81 Aachen A Rests
82 Attachment B: Chain of Custody 83 Attachment C: LC/MS/MS RawAnalytical Data
9 Signatures
.
Paul Gomnoly Tears Loader, LYS
John. FancyV,i rac
25 Banse Date 3
Other Lab Mambers Contig o Data Karen Smith
pacers 000180
Exygen re ResReaErchSEARCH raven Ress.
a Pes
Analytical Resiits Solvay Solexis Wastewater Sampling 3/03
Solvay SolexisSaiple Identification
PFOA (nglL)
00330088533 (oratory duplicate)
7745010000
Limit of Detection (LOD) for the procdure is appoximely 10 nglL
Limit of Quaniaton (LOG) or ihe pracodure is 50 ng
ND - Compound not detected
NG - Compound detected at level Batwasn the LOD and LOQ. Results not quantifiable.
ND<LOD <NQ <LOG
REE8 ERs Bihan, usa
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RESnEARCH SStsattReCeolulghe,DPAiv16801 PoFmasx 184126237121150800
SAMPLE TRANSFER SHEET
Protocol Number:
NA
Exygen Study Number:____ L34300
Cows| ow |.
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Samples moved om Hn
Samples rewmed tof _____e Duwn i) g fg Comments:
SampleCsualsaItndtoilssdDaties/Tzaime December 19, 20026
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PhoFnaer:: 881144-.227321-.11053890
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Comments: 100, of250mp.sod entivassed olsnpls lrspin isst0Av03u/2c6/:03
Analysis Summary: `pDua Sget:_1B26idg0na 3BSHV)
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LC/MS/MS SYSTEM AND OPERATING CONDITIONS
`Sponsor Protocol No:NA
ExygenStudy No: L34300
Instcument:
Micromass Quattro Ultima (LOMS/MS Unit #7)
Computer
IBM Intellitation M Pro
Software:
`MWiicnrdoomwasssXPLiPmriotfeeds:siMonaasls:LVyemrxsi4o.n0 5.1: Service Pack I
HPLCEquipment:
HewHlePttQuPaatckPaurmdp.(HP) Series 1100HP Vacuum Degasser
HP Autosamplec
HP Column Oven
HPLCColumn: G(enJeOsNiEsSCC-H,R5OcMmAxT2O.G1mRAmPHidY.:x4Ppactt(NEo.xyFKgSeI9Dn6:2E7)24)
Mobile Phase (A):
Mobile Phase (B):
2mM AmmAo cetatneini TypeuIWamter
Methanol
fe 110?
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EKxayrgenenRiRsehsaearch 3Ph0o5n8eR:e(s8e1a4r)c2h7D2r-i1v0e,39StFatAeXC:ol(l8e1g4e), 2P3A1-115688001
NOTE: The next 3 pages are computer generated printouts from the masslynx software program. The pages contain the instrument settings used for the analysis of this data set.
All Handwriten Peak ID's by: MY idethor
000193
Experiment Report
FiSloe:nate: Prived:
cBALiymasslynxifCTlhEuuoNrrTosRcdhEaeKymaiMcraaerlncs.hsp2r(7oK,\a2arc0eqn0u9Rdib1s\hp4ef1)o3a.3e9xp Reason Update sovent deioy Thursday, March 27,2003 1430.03 Hue ls
| Page 1
| |
NaCrmeaetion Time
TDhefua2ul7tNEixrpe2r0i0m3en1t4:13:39
|
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Printed:
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Thursday, March 27, 2003 14:50:56
HP1100 LC Pump Initial Conditions
solavrents cBoy or
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P1100 LC Pump Gradient Timetable
The gradient Timetable contains 10
Tine 0.00a ssono
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HP1100 LC pump External Eveat Timetable
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TTnii0mt.ei0a0l
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P1100 Autosampler Initial Conditions
DEDjrreaacwwtSPopSsepicetdeidon(41(/nmm)in)
2200000..020
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000195
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CAl:\MassLynTxhfulrusodraoychMearmcihca2l7,s.2P0R0O3\1C6Q:U0D1B:\08PFOA Tune.IPR BRyosson 'nCewENtTuRnEeKfiaerens (Karen Risha) Thursday, March 27, 2003 1455717 [Fn
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printed: Friday,March 28,2970:109A3M
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Page 1 of 1
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ExygenEFReEseaErch,:058 Research rive taT e ColegT e, P-A 16R 801, Data acauakeed an LOVSHSE7 eeon 000197
S`QtuuadnytiNtoy.1SLa3m4p30l0e,RDeaptoarStet0326038 SOLVAY-, ExtDate:03/26/03, Analystk Risha SDantaotsweet: ALC:\WMasFsrUiydmafyu,oMroacrhcehmi2c6,al2s00p3ro\8:00372:60083A8MSOLVAY.qid
RByeason PCroEceNssiTngREW(KaarreneRinshsa) Printes:__ Friday, March 28, 2003 8:07:13AM
nRDaiitano ,dZESAGEE--SE&
Page 10119 EE
| CMaeltihboradt:ioCn::W2a8ssMLayrni20f0u3or0o8:c4h5e:m1i9cals.PROMethDBIPFOA 032503,mdb28Mar2003 08:18:18
DNaatmeo::270-3M2a6r0-3280300301 DTeismcer:ip2t1i:o2n3::5X8C031703.0,0 gl Standard
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Exygen Research, 3058 Research Drive, State College, PA 16801, Data acquired on LCMSMSH?
000198
are `Study No.:L34300, Data Set:0326038 SOLVAY,ExtDate:03/26/03, AnalystK Risha
E Bet Ge ob rorsi LAY 1
BRyeason PCrEoNcTesRsEiKngarens (Karen Risha)
fBweEoyenmasercOscSosntn ehyevernso =or Description: XC031703-1, 26ng/L Standard
sta3gs
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640 6.57 675
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Datstet CVassLymsfuoprroolc28h0e38mSOiLcVAaYl.s
Signature:
printed:
AFRBtyeraosno,nMaPrFrrCciohEdcaNe2yTs,5RsMiE2anK0gra0cr3h.e32n80s,7(:2K10a30rA3enM9:R0i7s:h0a8)AM
TDNiaamtmeees::220137276a1023780.033003
Description: XC031703:2, 80 ng. Standard
PC-rhoinnaT s snes oniza)
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en Research, 3058 Research Dre, tae Colege, PA 16301, Dataaacequiredon LONSMSHT
000200
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RByeason PCrEoNcTesRsEiWnagrens (Karen Rishe) inlod: Friday, March 28, 2008 :07:13 AM
taom:e:270-3M2a6r0-32B0-033004 me: 22:13:54
escription: XC031703-3, 100 ng/L Standard
~
22063013786-3330.0140S0mmogothS(mMnna.n2xr3d)
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`Ygen Research, 3058 Research Drive, Sate Collage, PA 16801, Data acquired on LMSMSH?
000201
rere pepe------------------ `SQauayntiNto.y1 3Sa4m5p0l0e,RDeaptoartSet0326035 SOLVAY, ExtDste:03126103, Analyst KRisha DoSataswewt e CAUiWasslFyrnirdiauy.orMochaemricl2ce0p0rh3o9l002372.650083A8,MSOLVAY qd : printed:___ BRFryeiadasyo,nMaCPrrcEohNcTe2sR6sE,iWn2ag0r0e3ns97(:K1a3rAeMn Risha)
NDaatmee::270-3M2a6r0-3280:033005 TDiesmcer:ip2t2i:o3n0::4X3C031703-4, 250 nglL Standard
PcSsFozO6r0Ai38a:,3085aSnmooklSiannd2ar)d o
PiTroioes
Page5 oi 19 !:
Rot carsoasmiissain.d
| ' Lo Tee Te he ik 4k 4k seE sk 8% |E8%Tr 7% TThe 800in
Exygen Research, 3058 Research Drv, Sate College, PA 16801, Data acquired on LOMSMSHT
000202
GCQuaentySaLm3p5l0e,RaDpiorStoL0326098 SOLVAY, EXLORG032603, Anabyst sha DBotaseot RCay:WassLyndfroenr2c5c2h0e03mi0a7.l0p8ArSM0O3L2V6A0Y3iBd Prtod._ BRFyasosodn aP(CrEoyNs2Ts5aRe,E5s\M0gK0a3raen7rs.(1Kc9aArehnMRisha)
TNDiaammteee::2702.24067051332810.033008
Deiplon XCO31703.5,508nl. Standard
SpCprsaonE ncS SrooE nnzy
(abiron
TTT mea |i i]
i
|
wert creistye:s
" . ETT TI TI1 E TTR TR TTR he ke a apTee rm
Exygen Research, 3058 Research Die tte Colege, PA 1880, Data sid on LCMSNSHT
000203
a QuantiNtey S3a4m3p0l0e,RDepaorSteL0326038 SOLVAY,ExtDate 03126103,Analyst Rishe PageTol1s DSatwaseet CABiyMassLyFmrdifClduaoEyrMoNchToerRrriEca(Klc2ea0.er0pher9ronlRe200i73ns2.sh60s0a83)A,8 MSOLVAY.qd Ported: RFreiadsayo.nMaPrrcohce2s8s,i2n0g03 3:07:19AM
`DNaatem:e:270-3M2a6r0-3280-033007 TDiesmcer:i2p3t:io0n4::1X7CO3703-6, 1000ng Standard SPTEsF2OAeA0T30,3000m0 9o8sSc)ars =
fesiirsotas
nko enlsaimzeeln5:
i ol Tyr nar
I I I EEE creEpSema
Exygon Research, 3055 Research Dive, Stale College, PA 18801, Data acquired an LCMSHSET
000204
santify Sample Report
-
dy No.1.34300, Data Set:0326038 SOLVAY,ExtDate:03/26/03, Analyst Risha
Page 8 of 19 !
oBn i
ws !
sy il "rw
51077
148 [| 190 2
43 401
!
Here
|
iy
ol
|
1en Research, 3058 Research Drive, State College, PA 16801, Data acquiredon LCMSMS#7
000205 ii
iS tu No 3430R 0, Data Set0325038 SOLVAY, ExtDate 03/26/03, Anala yst Risha man ||
dJogtraset.ce ALCMasslFyrneViyo,rMochaemicral2sc0p0r3oh$0032726.003888ASMOLVAY qd By CENTREW(KaarreneRinshsa)
: ;
vinted: FRreiadsayo,nMaPrrcohce2s8,si2n0g03 907:19 AM
|!
altaem:e:270-3M2a6r0-3280-033009
i i
J"eIsmcer:i2p3t:i3o7n::401105020 Control
[i
3F126o0600n3280.C3o0n0o9rStn 26) -
1 . olf 19J0im gon 2Maza310
le RNG d2a3sm5e0leneg3s0.s |
spa ass 538 aes pee
oss 700 218 re
17o4
" TR TR he ak ve Rak i Sk Sk em ak 7h 14remay in
+y9en Research, 3058 Research Dive, State College, PA 16801, Data acquired on LCMSMS#7
000206
SQuayriNfey S3a7m5p0le0TDopaoarSto0325038 SOLVAY,EDe026/03,Anast Risha
DSattaasuerte, Printed
CBiylMassLFynrxaCfyluE.orNMaacTheenRmi2Ec6a,(Kl2ks0.aa8pr3rreon9\oR00i3n7s2h06se08)3A8 SOLVAY gid. RFeraesyo.nMarPcrhov2e5s,ai2n0g03 97:18 AM
TNDiaamtmeee:::227053:M62a46r:02z36o89010 Sescrpton; 0106020 Spk A, 50 nglL
>SShF2oar3010 Sine)
prionn
fo
0
Fags 10018
i}i iI!i| I [EdmT eesms
x
"8 ou
rr nar
A
aA TE
CETTTR iR ake ake ake ak aw iE ER ek eh eh 7% TE ab .
i|
genReseach, 3058Research Dive, StasColege, PA 16501, DatsaconLiOMSMdSHT
000207
`QSutaundtyiNfoy.SLa34m5p0l0e,RDeaptoarStet0326038 SOLVAY,ExtDate:03/28103, Analyst Risha
SDiagtnaasteurte: Printed:
ABCLiyWasslymFCriEifdNuaTyo,RrEoMcKaharecrmhoin2c6sa,l(2sK0ap0rr3eonl90:i03s72h:6a008)38AMSOLVAY.cld FRreiadasyo,nMaPrrcohc2e8s,si2n0g03 8:07:19AM
DNaatmee::280-3M2a6r0-3280-033011 DTeismcer:ip0t0i:o1n1::102106020 Spk B, 500 ngiL
PS0i3Ot2e6oA0s3o83s0p1e1, Ssmocotnnbinzz)
pSroen
poy
Ed
FPagetiors ;| i!
i ; enoMeu1l5m07te60s0s0.8
TTR TTR E| R TER TR Tk ak Wk em ek Ge 700 750 abi
Exygen Research, 3058 Research Drive, Sate College, PA 16801, Data acauired on LCMSHS#7
000208
WJSQuEanStnifyESample -- eEReportcm eryinhdsi =iof-- nnEr ensnis,for 2... cob
g -- s =T B=unEEor 52
1 1
Page 120f 19
HwEy
000209
QuSatundtyifNyo.SLa3m4p30l0e,RDeaptoartSet:0326038 SOLVAY,ExtDate:0326/03, AnalystK Risha
SDaotnassteutr:e: Printed:
ACLiMisssLFryindfalyo,rMoachrecmhi2c8a,l2s0p0r3ol9.00372.50083A8MSOLVAY.qld RByeason _CPErNocTeRssEiKhagrens (Keren Rishe) Friday, March 28, 2003 9.07:19AM
DaNtaeme::280-3M2a6r0-3280-033013 TDiemsecr:i0p0t:i4o4n::4L734300-1 Rep, DF=100
0PR 3F2O60A3e 83013SSrohan 20)
we
To
aan
TTRT aemoris
peels.
rie
Th 1k TE 2h 2% 360 3% AB 4% sl oo sL m 600 6s 780 750 | 40
Exygen Research, 2058 Research Dive, State Colege, PA 16801, Data acquiroend LCMSWIS#7
000210
`Guaniify SLam5p2le0RDepmorSt 250 SOLVEAxY, tetazeos, Aras
DSaoasmate fGe aFsaytarr 2o00pn8rGS0Zo7S0083mSOLiVAYc44
inet: BFBydraasa(BeCrEeN3Tc5R,oE2Kn0ar0e8ns97(K1ar9en0Risha)
oaem:Zata52)6ar0e2308038014
Despin:XCASYTOS.1, 25ng Standard
S rSio"aataE n sE m. e
fio)n
"Page tol 19
rs tJpegEe
pr
os
RS
B 2 O L. SEE 63A 16.44 88A 1
ET E e T TRE TR TR
Sorgen Ress, 205 Research re,SseClg, PA1851, Ds acqred on LOSS
000211
I --TE vay a
J `Quantitfy San mple R2eportSucs2003 souvay, eat nz space SDhantaatsuerte: ABCLy:asCFsriEdtayNy, MTnarRdchEi26Ku,(G2oar0p0ertr5neo\e$R003i7cn2.n60hsa083)Ae8NSmOLiVcAYlisd Printed: FiRkedsasyo,nM_aPrcrhoc2e6s,t2i0g03 3:07:19an
| DamDetnsece:risp2to8i.ronai:rs2X0G003317012, 50 ng. Standard
EParnoiansors 20)
ron
-
i
---- "
Page 15 or 75
-
Mot chums. alanis
2 rsr TEe T m TR STARnannak
1 a . ose Vogo A1h7ao ah RRTOR ER TTR
Xygen Research, 3058 Research Drive, State College, PA 16801, Data acquired on LCMSMS#7
000212
SQStuiuaS dnytiNtoy:SL3a4m3p0l0e,RDeap-- toartSet0325038 S-- OLVAY,ExtDale 0-- 3/2603, Analyst-- Risha -- Fae 180115
DSiaotnaasleutr:e: ACBLy:tfasCFsEiLdNyaTymR,rEMtWaharrocerhno2sc8(,hK2e0am0ri3ec5n.aR0ii7ssh0pa8)rAoSMlO0L3V2A5Y0q3l8d
Printed: FRreialdasyo,nMearPcrohnc2e6s,sd i2n0g09w 9:07:1s 9AM
TDNaiatrmee:::20801.:33a24r6:0520308033016
Description: XCO31703-3, 100ng.Standard
PScrsEosRAS3,otsosmmeonnSgienr2a) -
frionn
Mot cpharme:
5
Jr
J
| [2 1 booTres
ae
ak
ae
ak
ak
eke
ke
TER oerR
Po, TER TTr R TRt min
a rn scm, venience 000213 |
A
ue
SEN Quantify 0 SampleShReport
a asnso sovvar
exomessas
oar
TE
rn ----------
Signature:
Pinte
AFB8toroyn,viSCFrriEdhagIyo,TiMaaEirenchn0287,c:2100a0309r:07s:08 AM
DaDPeirsc:rip2ti3onXerCsUS12750tgi3S.ta4nda,rd
1 s TPironans soning
"Tw
=
reining
Page 17 of 19
hagawrcBa a
1
1 Lr
:
TT TE TT a r TE e
Exygen Research, 3058 Research Driv, State College, PA 16601, Data acquired on LCMSMSHT
000214
| QStuuadnytiNfoy:LS3a4m3p0l0e,RDeaptoarStet0325038 SOLVAY,ExtDate:0312603, Analy--st isha DSantaatsuerte: AGBL:yMasslyFrnCiediEahyu,NoMrTaorcRchehEm2i6cK,(a2Ksa0apr0rre9onle9R0.i30ns27.h60s0a3)A8 SOLVAY.qd Printed: FRreiadasyo,nMarPcrohc2e6ss,i2n0g03 507-19AM
DaNtaem:e2:60-3M2a6r0-3280-033018
TDiemscer:ip0t2i:o0n8::2X6CO31703-6, 500 nglL. Standard
XP0-C2Fa6Oa0IA3T8G.33,1820S0nmgoo.nSgainn20d)
Frion
Ed
"Page 180 18
MRM h2laSinaeeeosn.s
wee TRIS
ak ak
aR he eee
TT TTR
|
`gen Research, 3058 Research Drive, State College, PA 18801, Data acquired on LCMSMS#7
|
i
1
000215 |
SGGtuvuadnytiN-- toy-SSLaa3m4mp3lp00e,R-- eDaptoLaUr. tS4eY0F-- 3A2A603H8ASVOEL-- SVIAVYL,YExtDa-- te 03280h3-- i,dAnsyst-- Risa -- TT -- ---- --Pa-- g-- e Tao-- s
SDaatausette. : ABCy:WaFCsrEiNdsaTyR.lEMWayracrmhon2f6s,o(3K0rpa0ro8elon0S073cRB2i5hs0)3eA5nSOiLVcAYagsia
Printed: RFreiadasyo.nMaa rPcrohce28s,si2n0g03 37:19An
NTaDiamtmeee:::2008243:022a55r:0132580.033019
Description: XCO39703., 1000 nglL Standard
pA3ir2i1o0na3e03,18oSkomSsa)
frionn
Meters raRmsoss.
EA
Sani
"|
ECE IEI i
: ra ores a PSR in
9en Research, 3058 Research Die, Sst College, PA 16301, Data acquired on LOMSMSHT
000216