Document q2X4Y7JGvKVEykkK8z9myMdG
f'Z* 01 COPE *f&698-l>
TA
(' DATE )
K2L24., i LOT >
5527* UBS. < EST WT >
"fir
PROCESSES ( ) YE-698-D (T)
COHTYP JOB NAME:
APPROVED Y: FWP 10&5M2*:
01YE698DMT
BEENDED BACK : CG 01, PC 98/ :___________________
'WL
(CODE)
NAME: MOLYBDATE ORANGE
(LOT)
f ---(POUNDS)
u SeT T
7~a c c t
LBS | N-CODE | LBS
i- OBTAIN SODIUM SULFATE FOR S-13
84 ! 10S-A I 84
CALCULATE G SET ON BADGER METER FOR S-16
NITRIC ACID WEAK )
L_ %
S3.J
I
33-D |
60'
o b t a in s o d iu m c h l o r id e f o r s-33
734 | 4 --A i 734
I Ji&AIN. SODA ASH FOR S-37
146 1 3-A I 146
3BTAIN SODIUM SILICATE FOR S-39
237 j 32-D 1 237
{ SODA ASH FOR S-43
350 i 3-A 1 350
OBTAIN ANTIMONY TRIOXIDE FOR S-46
70 t 711-B j 70
WEIGH SODIUM CHROMATE INTO V-351 .. opTR://ir,,v
... f
OPDTTRD * __, MMUK______________%V |
-11j
WEIGH IN SODIUJMM MOLYBDATE SOLUTION
OPTR
wm&j; J-M,
Agzz\ 1
CPTR ______ MK _
T-__, ______ %J
10-D 423-D
Pti'N 1 0" (500 G) WATER INTO V-358
N V-359 INTO V-351 G PUMP IN V-351
l TO 55" (2600 G)
ET IN N-108-A FROM S 1
^
PIR 5 MIN G RECORD : :PH_/<2^_<9.'0-i 0*0)
i ADJ TO PH 9,8-9,9 G RECORD: PH_,_____
(CAUSTIC SODA SOLUTION)
ASSUME 50%
ASSUME 66%
N-33-B FROM S 2 USING BADGER METER
TO 66 * (3,12,1 G) AT 67-69*F
RECORD: VQLfefe.* ifeZ___ *F
I STIR 5 MIN G RECORD: PHjZizi7,4-7,6) G
i G/ML
. 080-1 ,G'8l>
i ! |
NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK i
LIST G ATTACH, TAKE 1 QT SAMPLE
|
1 ! :%ZrZ\
i i -r
7-D 33-D
I 1 885 i i | 303
l_Z___
I H9'*T RUM 20" (996 G) WATER INTO V- ** ] I RECORD N-41-D STORAGE TANK TO PUMP FROM, i Jk ' CIRCLE ONE: 402 41 411 420 424 425 i2r | CHECK WITH CU SUPV: 1 I ^STORAGE TANK MUST CONTAIN AT LEAST 2376 I 1 GAL: 402=49", 410*25", 411*43", 420=25", j j 424=25" 425=31" I f ^STORAGE'TANK MUST HAVE STIRRED AT LEAST
I I 20 MIN SINCE LAST ADDITION OR ADJUSTMENT I i ^STORAGE TANK MUST BE ISOLATED UNTIL ALL
PUMPING FOR THIS BATCH IS COMPLETE SET METER FOR 300 G G PUMP TO SV
OCT) 291982
I
' *i, /"
DU P050103056
1.0 TV &yi'& ME NT i .... .....i___ SV ! 22
3I CONTI
123 I I 124
CQMTYP JOB NAME 01YE698DMT PAGE 02
DATE PRINTED:10/15/82, USE I N~ IACCT LBS | CODE ! LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH & DENSITY. RECORD BELOW. IF NOT IN RANGE, STOP PUMPING 6 SEE SUPV.
* PH:(2.2-3.7) * DENSITY: _________ G/ML <i.270-1.323) IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD DENSITY G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING.
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21. CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
* **# TABLE
i 1 G/ML SETTING
1 ! 1 .270 1673
1 1 i .271
1670
1 1 1 .272 1663
1 1 i .273 1656
1 1 1 .274 1649
1 1 1 .275 1641
1 1 1 .276 1634
1 1 1 .277 1627
1 1 1 .279 i 620
I 1 1 .279 1614
1 1 1 .280 1607
i 1 1 .281
1600
1 I 1 .282 1593
1 i 1 .283 1586
i 1 1 .284 1580
i i 1 .285 1573
} 1 1 .286 1566
i ! 1 .286 1566
1 f 1 .287 1559
1 1 1 .288 1553
i ! 1 .289 1546
1 1 1 .290 1540
G/ML SETTING 1 G/ML
1 .291
1534
1 1.312
1 .292
1527
1 1.313
1 .293 1521
} 1.314
1 .294 1515
1 1.315
1 .295 1509
I 1.316
1 .296 1503
1 1.317
1 .297 1 497 1 1.313
1 .298 1490 j 1.319
1 .299 . 1484 1 1.320
i .300 1478 i 1.321
1 .301
i 473
1 1.322
1 .302 1467 1 1.323
1 .303 1 461
1 1.324
1 .304 1 455 1 i.325
1 .305 1449 1 1.326
1 .306 1 444
! 1.327
1 .307 1 433 1 1.329
1.307 1 433 i 1.328
1 .308 1432 1 1.329
1 .309
1427
1 1.330
1 .31 O 1 421
} 1.331
1 .31 1
1415
1 1.332
SETTING 1410 1404 1399
1394 1388 1383 1378 1372 1367
1362 1357 1351 1346 1341 i 336
1331 1 326 1326 1543 1537 1 532
1526
|25|
II 1I 1261 II 127} 128} II 1I 12?I I I
1301
SET METER PUMP ________G (RECORD FROM TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS
ADJ LEAD NITRATE TO 76* (3625 G) AT 67-6?*F.
RECORD: *F
STIR 5 MIN & RECORD PH: _ __ (2.2-3.7)
IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 667.
& RECORD PH:______
ASSUME 5051
NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING
RECORD: ________G/ML (1.143-1.144) IF OUT OF SPEC
FILL OwwUT CHECK LISTi w& nAT* T\ AnCulHl*.
.
STIR AT 67-6?F FOR S-31. TAKE 1 QT SAMPLE.
41 -D } 5110 57-A I I
33-D } 7-D |
\
DUP050103057
? L-...' Xt
r~ jfvj t t u **!*
%
COMTYP JOB NAME: 01YE698DMT PAGE 0:
DATE PRINTED : 1 0/45/.$2. .... 1 USE I.. . M- 1ACCT
'`LOT: _ ^QUIP 'jMENTI
4r--- *5*
COMTYP JOB NAME: 01YE693DMT PAGE 02 AT APPROX 100. G WHILE CONTINUING TO PUMP,
DfTBs|RifE^i i LBS I CpDE I LBS
^`5 1 1 CHECK PH & DENSITY. RECORD BELOW..IF NOT
4JEONTJ I IN RANGE,, STOP PUMPING^ SEE SUP9.
1 * PH:
(2.2-3.71
* DENSITY:
G/ML (1.270-1 .328T :-
IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
i DENSITY________ G/ML ON TRAPPED SAMPLE. :
1 FROM END OF S-21 PUMPING. v
. ;' '
"
2^Kt3SING DENSITY FROM S-23, FIND METER SETTING FOR - I SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
! ACCOUNTS FOR 30 G ALREADY PUMPED IN S-21.
I CIRCLE DENSITY & SETTING IN TABLE BELOW.
|
} $$$ TABLE!
$6
1 1 G/ML SETTING | ' G/ML SETTING i G/ML SETTINGj
i 1 1.270 1644
i 1 .291
1504
i 1 .312 1382 i
' i ! 1.271
1637
| 1 .292 1487
I i .313 1376 |
i | 1.272 1630 f 1 .293 1491 j 1.314 1371 i
1 1 1.273 1623 i 1 .294 1485 i 1 .315 1367 |
- j- 1 1.274 1616 | 1 .295 1479 | 1... 31 6 ;,.-4'361 1
| | 1.275 1609 j 1 .296 1473 f 1 .31 7 1356 |
] 1 1.276 1602 I 1 .297 1467 i 1 .318. 1351 1
i I 1.277 1595 1 1 .298 1461
I i .319, 1345- .1
! 1 1.278 i 588 i 1 .299 1455 I i: 3.20 1340. !
1 I 1 .279 1582 i 1.300 1443 | .1.321' 1335 1
- i i 1.280 1575 I 1 .301 1444 ' | t. 322 , * 1330 |
1 .1 1.281 1568 i 1 .302 1438 I 1-. 32-3 ' : -1324/;' -]
:yv | | 1.282 1562 I 1 .303 1432 | i .324- 131 -9 EL
- i 1 1-283 1555 j 1 .304 1426 1 i ii25` - 1315 I
I 1 1.284 1549 | /i 1305"""
i 1 .326V '1310 i
/ i | 1 .285 1542 |
1416 . 1 1-.327 1305 ,]
- : 1 I 1.286 1535 | 1 .30? 1410 | 1 .328 1 30' " I-
i |1.287 1528 ] 1 .308 1404 |- 1.329
1 | 1.238 1522 | 1 .39 1399 i T .33 1290
1 i 1.289
1515
1 1 .310
1393
I 1 .331
1285 i
1 ! 1.290
151G
i i .311
138? j 1.332 1280 |
'S 1
1
T.:
iaS-kSET METER & PUMP i?io G (RECORD. FROM TABLE)
i
1 FLUSH LINE WITH WATER INTO SV FOR APPROX IMA TEL. Y
!- i 30 SE C0NDS
/ i 2>t^ADJ L EAD NITRATE TO 3625 G. (76"-2 42/245 & 74.5"
247) AT 67-dSUf-f
| .T^RECORD:
& ICE CONSUMED .(330S/BLOCK)
STIR 5 MIN & RECORD pH:
(2.2-3.?)
| i 1
I 33QX. j
41- D I 5110 .1
.57- A 1.
| j *%** USE TI TRIMETER TO ADJUST N-41--D PH ****
|
128+^IF NECESSARY ADJ Tp PH 3.0-3.1
ASSUME 66% |
1 I, & RECORD PH: _.___krT
ASSUME 50% 1
] OTE: DILUTE.N-7-B 10:1 WITH WATER BEFORE ADDING]
33-----i 7.
1291 RECpRD:
(1.143-1.144) IF OUT OF SPEC!
il l o u t c h H!k LIST S= .ATTACH.
1
STIR AT S7-69*F..F0Ri S-31;:.' TAKE 1 T SAMPLE.
|
l|pS" DU P050103058
tmii*r
flENT I
__
r
I
COMTYP JOB NAME:' 1YE698DMT
PAGE 03
DATE PRINTED : 1 0/J 5/82
USE
N- ACCT
LBS
CCDE I LBS
s.:5v""~ rii*" i''o b t a in 7 5t s a mp l Is o f s -i & s-3 s o l u t io n s
5 -r
CDN'T!
G TITRATE TWICE NOTIFY SUPV IF ML N-iO-D IS NOT IN RANGE
7.1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0.1 ML N-10-D (IF YES, FLUSH ALL
EQUIPMENT & REPEAT TITRATIONS)- DO NOT
PROCEED IF N-iO-D TITRATION IS OUT OF RANGE
ADJUST V-3.543 FOR A TITRATION PH OF 4 0 TO ErgOj
t,FRO FINAL IN-LINE TITRATION, RECORD LOWEST*"
1 P #_4- KU n --10--d
i
._i 33-D I
7-D
1 i WHEN S-31 TITRATION OK , STRIKE V-358 THRU
|
.SV I
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
|
6 } 1 16-18 MIN RECORD^ START
^7/D , TOTAL MIN,,_A_;___
I i
NOTF>^STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS |
BUBBLES APPEAR IN SIGHT GLASSES
|
IMMEDIATELY DUMP IN N-4-A FROM S 3 S SET TIMER |
OR 15 MINUTES
1
JNJRl^G S 33, WASH IN V-3,
2 MIN^^RECQRD PHJ
1.8-2.5)
TBXS,^nl__<MUST EE + )
! STIR TOTAL OF 15 MIN FFROM S-33 G
j RECORD: TEMP_J>4__F <67-73*F)
35^L DUMP N-3-A FROM S-4 3#"'CsTlR 3 MIN
3^-T POUR IN N-3.2-D FROM S-5
4^L.STIR 2 MIN
4V'TT RUN IN LIQUID ALUM USING BADGER METER
4Tfpr STIR 3 MIN & FLUSH ALUM LINE WITH WATER
4^f DUMP IN N-3 FROM S-6
m I STIR 4 MIN FOR S-48
`'
5-DI 367
i 43 | RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW
39 i
J CONTROL PANEL
MK
JJL- 2
_! 28-D | 105
IL
MK_____ ______________%
_! 28-D i______
\*riT\ DURING S-44 SIFT N-711-B FROM S~7 INTO V-39
I WITH AGITATOR ON IN 1-2 MIN
147"^[ SSTIR 1-2 MIN TO MILKY SOLUTION
i
SV i/U'HEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
8 I | SOLUTION GRADUALLY OVER 5.MIN PERIOD INTO SV
i ! WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
I \ UNTIL FOAM SUBSIDES. |4rTjUJMP IN BLANC FIXE N
i
33 I 128-A| 33
!5nWHEN SCHEDULED, DUMP IN BLEND BACKLISTED ON j
|
i | TOP OF PAGE 1
"
||
I I RECORD: CODE______ LOT_______________, ______J
|
1510-STIR 2 MIN
-
1j
1 52j^ RECORD : PH__Jl L_T. < 5.8-6. )
1i
I^T IF NECESSARY, ADJ TO PH 5.8-6.
ASSUME 5% |_
_J 7-D 1____
!1
& RECORD: PH-__r=r,,____ ASSUME
154^1 FLOOD TO 153" (7298 G) S STOP AGITATOR
66Z | ___ ,_| 33-D1____
|I
I
\\
^
. I1
ART
-
^glR
II
---- '
-
- jj
DUP050103059