Document ppxqQoRwreBkkK0odj39pnaqk
\ji1l
To: T. H. Huffman
From: Dote:
D. C. Skokna July 27, 1990
Subject:
ABERDEEN MONTHLY PROGRESS REPORT JUNE, 1990
Safety
There were no reported injuries in June. At month's end Aberdeen plant employees had worked 4013 days (5,340,396 manhours) since the last lost time injury.
June
X,T,p.
PVC Production, MM Lbs. Reactor Stream Factor, % Resin Quality, % Prime VCM Efficiency, Lbs./Lb. Flexible Compound Production, MM Lbs. Flexible Compound Quality, % Prime Rigid Compound Production, MM Lbs. Rigid Compound Quality, % Prime Plasticizer Production, MM Lbs. Plasticizer Quality, % Prime Energy Use, (EUI, %) Fixed Cost Variance, $M Variable Cost Efficiency Variance, $M
37.4 92.0 98.9 C.97642
5.8 98.5
4.6 99.8
1.4 85.6
< 3.2>
< 12.0>
40.7
336.5 88.4 97.3
1.0013 54.4 98.3 44.3 99.6 13.6 87.1
< 7.7>
215.3 594.0
Operations
Six railcars of low calcium 5305 were produced for Klockner. Installation of the permanent clean wall system began and will complete in August.
Some 56 hours of Line I time were used for Plenex Polymers development. Rates in the ridgid compound unit were adversely affected by screener problems (136 hours of downtime).
VAB.0001190036
T. H. Huffman 7/27/90 Aberdeen Monthly Progress Report - June, 1990 Page 2
Variable costs were favorable In the resin and compound units. Good efficiencies and low offgrade rates in these units and favorable product mixes caused the good results. Offsetting these variances was an unfavorable (high use of raw materials) variance in the plasticizer unit. A process change made earlier may be the cause of the inefficiency.
1. 100% of the plant's natural teams met during June.
2. Overall, natural team scores for the 3rd quarter are up 46% from the previous quarter; an average score of 7.3 points.
3. The plant's estimated Q-Scorecard results as of June 1 are 10.3.
4. The Vinyl "B" Shift Natural Team made its management presentation. They recommended improved blend tank sparger design that benefits the environment, improves safety and quality, and reduces energy consumption.
5. AT&T (a compound customer) presented us their 5 Star Rating (the highest) as a result of our semi-annual vendor rating.
------------------------
D. C. Skokna Plant Superintendent
rah
Hous ton
J. D. Burns
X
R. T. Ferrell
X
T. H. Huffman
C. J. Matson
D. F. Harman
H. R. FI amine r
R. R. Smith
B. J. Bean
R. H. Gerlach
R. D. Gamblin
W. L. McClain
J. P. Stokes
Aus tin
R. L. Poe
X
H. J. Hall
Oklahoma City
H. D. Garrison
LCVCM Plant
R. A. Conrad
LCCP Plant
J. Friend
LCLAB Plant
J. W. Ware
X
Baltimore
L. R. Bauer
X
Hammond
J. Pavao
X
Blane
C. R. Miller
Premiere
P. L. Foote
Aberdeen
RWS/DCS (File Copy), TJA, JBA, JEB, JME, SCH, MRK, JEL, DAM, RBN, JEN, JDO, REP, BLT
X X X X X X X X X X
X X X X
X X
'H*'
1
VAB.0001190038
f
SAFETY - B. L. Trego
First Aid OSHA Recordable
Total Injuries
Number of Restricted Workday Cases Number of Lost Workday Cases
June
0
0
Fiscal
3
0
Fiscal
2
0
Vinyl Operations Compound Operations Maintenance Laboratory Receiving/Warehouse Office
Totals
Injuries by Type
Cuts and Abrasions Eye Injuries Burns Bruises Strains/Sprains Stings Other
Totals
Lost Workday Cases Days Lost
Last lost time injury - 7/5/79
Days since -
4013
Employee hours since - 5,340,396
On June 30, 1990, the employees of the Aberdeen plant completed 4013 days with no lost time injury.
The major topics for June safety meetings were CPR and Respirator Training.
S
j'
/
VAB.0001190039
SAFETY - Continued
David C. Sheffield of International Loss Control Institute, conducted a plant-wide safety audit during the week of June 25, 1990. A report of the findings is expected from ILCI during July.
Routine dosimetry results for the month were:
Chemical
<_________________________
Number
VCM Lead Total Particulates
77 98.72 18 94.74
7 100.0
1 1 0
Both overexposures were benefit of respiratory protection.
Percent
1.28 5.26
0.0
latery Class
Department
No injuries reported during June.
Description
m MR MM
T
VAB.0001190040
f
ABERDEEN CHEMICAL PLANT INJURIES
(Twelve Month Running Totals) 40
35
30
Z8
20
15
10
5
0
J'ffJF MAMJJASONQJ'
MAMJ JASON QJ*
MAMJJASON QJ'9QF MAMJ
TOTAL INJURIES
o OSHA RECORDABLE
*
VAB.0001190041
T. J. Arbeiter
Q3FY90 Natural Team scores are in! The Aberdeen Plant team activity resulted in an average score of 7.3 points, up 46% from the previous quarter. Our Natural Teams and facilitators deserve great credit for the accomplishment. These "points" represent a lot of good work done by our teams.
The Vinyl "B" Shift Natural Team made a presentation to management on June 20th. The team recommended changes to sparger design aimed at benefiting the environment, improving safety and the quality of our products, and reducing energy consumption.
The Aberdeen Q-Scorecard score as of June 1st is 10.3. Our progress by line item is as follows:
Item
1990 Card Submission 1991 Card Submission Average Natural Team Score Safety Cost Control Quality Waste Minimization Linkage
Score
i-
10 10* 10 12 12 10* 13
4
* Assumed
VAB.0001190042
P
pwmwmmm
D. C. Skokna
PVC Flexible Compound Rigid Compound Plasticizer
$74.0 38.9 11.3
( 83.5) $ 40.7
($65.5) ( 21.4) ( 1.6)
.... MJfc
($ 44.1)
$ 8.5 17.5 9.7
-C39.il
$( 3.4)
PVC -
$74.0M favorable. VCM consumption was below budget, and product mix was favorable. Offgrade production was 70% below budgeted levels.
$38.9M favorable. Raw material use was slightly above budget ($20.1M) , product mix was $49.3M favorable, and variance due to offgrade was $10.6M favorable. Millscrap production was 62% below budget.
$11.3M favorable. Operation was essentially at budget.
$83.5M unfavorable. Raw material use was significantly above budget. Investigation indicates that a switch to soda ash neutralization (done to reduce the amount of BOD going to the wastewater system) may be the cause of this month's and recent month's inefficiencies. To evaluate further, use of caustic has been resumed.
$44.1M unfavorable
- Alfol 610*Alcohols - 610P to Flexible Compound - VCM - AllOther PricesVariances
Total
M
$ 31.9 . 28.9
( 68.9) ( 36.0') ($ 44.1)
Fixed Cost Variances - $12.0M unfavorable
- Payroll and Benefits - MM&C - Miscellaneous - TI&D - Clearances
Total
$ 24.2 42.5 62.5
( 137.2)
( 4.0)
($ 12.0)
VAB.0001190043
* mmm
u
COST VARIANCES - Continued Payroll and Benefits - Payroll was essentially at budget while benefits
clearances were $179M favorable. M. M. & C. - Activity was below budgeted levels. Miscellaneous - Most items in this group were favorable; the most favorable
item was ''packaging supplies'' - $26.2M favorable. T.I. & D. - An unexpected city tax clearance caused this category to be
significantly unfavorable. We are trying to determine why this happened.
jr
VAB.0001190044
VINYL - J. D. Olson, J. M. Vlnoskl
The Vinyl Department had no first aid or OSHA recordable injuries during the month of June.
The monthly safety meeting topic was "Plant Emergency Action Guidelines".
1. Six railcars of decalcified 5305 resin were produced and shipped to Klockner in June. Resin calcium levels were reduced to about 10% of normal. Additional June production of decalcified resin will be held for Klockner's July order of six railcars.
2. Work began in June of the permanent BUS-80 system. Installation will be completed by mid-August.
3. The resin raw materials in the 744 account were valued at $334.6M.
- Production, Mrt -Daily Rate, M Lbs./C.D. - Capacity Utilization Factor, % - Total Reactor Charges - Charges/C.D. - Reactor Stream Factor, % - Rotary Dryer Stream Factor (#4-#8), - Fluid Bed Dryer Stream Factor, % - Resin Quality, % Prime
%
June
37.4 1246.7
102.3 870.0
24.0 92.0 89.2 97.6 98.9
336.5 1232.6
101.1 7898.0
28.9 88.4 80.5 92.3 97.3
Hours
Operational downtime (recovery scheduling conflicts, New Module rinse/charge water conflicts, waiting for Q.C. data before charging, 0-ring leaks, no place to dump, rinsing chem wash tanks power outage).
405.5
Maintenance downtime (sewer valve replacement on 741, condenser drilling on 500, condenser jacket acid cleaning on 300 and 400, hydro blasting and condenser drilling on 745).
170.5
VAB.0001190045
VINYL - Continued
Drver Downtime
Reactor limited production.
Operational downtime (centrifuge plugs dryer cleaning, and flameouts).
Maintenance downtime (#4 resin hopper repairs, activator, baghouse, centrifuge, and exhauster maintenance, screw conveyor repairs).
% of Total 41.2 22.9
35.9
Number "6A" cooling tower east cell was shutdown during the month for repairs to its drive shaft and three of its blades. The fan shaft broke causing damage to three of the fan blades.
The north recovery condenser and both sub coolers in the Old Reactor Unit were shutdown during the month for >leaning. The tube sides were drilled and the shells were acid cleaned on each.
Reactor 600 was shutdown for relief valve changes during the month. The new relief valves were installed as part of the Low Molecular Weight Resin project.
The "A" recovery compressor was shutdown during the month for repairs. The bearings and seals were replaced.
Reactor 745 was shutdown during the month for condenser drilling and hydroblasting as part of the contamination control program.
The Number 7 dust collector was shutdown during the month to replace the screw feeder on the dryer discharge. The screw shaft had broken on the screw feeder.
Reactor 500 was shutdown during the month for condenser drilling because of cooling control problems.
The motor on the #4 dryer exhauster was replaced during the month because of bad bearings and windings.
There was one major valve changed out in the Reactor area during the month.
*
mm
VAB.0001190046
T
COMPOUND - J. E. Nickerson, K. G. Akins
The compound department worked without injury in June. The topic of the monthly safety meetings was respirator training.
General
Continued formulation testing for PLENEX polymers consumed 56 hours on Line I. UL testing on different jacket/insulation combinations and constructions continues. Line V operated 12 days in June. Line V was down for 34 hours for a pelletizer clutch repair.
Rigid compound rates were adversely affected by problems with the Gump screeners in June. Maintenance required on the screeners as well as rescreening several railcars of material caused 136 hours of downtime in June.
Plasticizer rates were also reduced by reprocessing "cloudy"
plasticizer. It is suspected that the "cloudiness" is caused by
monoester and/or filtering agent.
Several tests including
additional filtration, water washing, and return to caustic
neutralization are underway to solve the problem.
Operating Davs
Line I
30
Line III
30
Line V
12
Total
% Prime
Capacity Utilization Factor
Downtime
Production (M Lbs.) !&nh AVg,/Pay Fiscal Y.T.D.
1932
64
3489
116
-Aift 5839
216
98.5
.735
17869 31137
5437 54443
98 .774
Hours
- Product Changes * PLENEX Polymer Testing - Miscellaneous Maintenance - Quality Problems & Control
92 56 30
4
- Product Changes Miscellaneous Maintenance - Quality Problems & Control - Dicer Problems & Maintenance
Line V
- Werner & Pfleiderer Maintenance - Quality Problems & Control - Product Changes - Miscellaneous Maintenance
73 19 15
9
34 33 n 11
VAB.0001190047
COMPOUND - Continued
Operating
,
Month
Rigid Compound
30.5
% Prime
Capacity Utilization Factor
5412 99.8 .909
177
Dp.wptjffiq
Hours
- Screener Maintenance & Product Rescreening
- Product Changes - Miscellaneous Maintenance - Quality Problems & Control - Welex Maintenance
136 64 73 42 22
Operating __Pavs
Month
Plasticizer
29.5
% Prime
Capacity Utilization Factor
1434 85.6 .652
X,.L.P.
39493 99.6 .827
Fiscal Y.T.D. 13600 87.1
r- i
. 708
Key Maintenance Work - J. B. Autrey, J. B. Hegwood
The vacuum jets on Plasticizer Reactor R-l w< for cleaning during the month due to an calcium carbonate build ud.
removed
The #7 air compressor was shutdown during the month for repairs. The valves and wipes were replaced due to wear.
The #1 welex was shutdown during the month for repairs because the motor was kicking out on high amps. An IRD analysis was run on the motor and the welex bearings and it was determined that the jack shaft had a bad bearing that was causing the motor to pull high amps. The jack shaft and motor were replaced and the welex was put back in service.
The Line I "A" blender was shutdown during the month for repairs because of a failing bearing in its gearbox. The gearbox was replaced with a spare and the blender put back in service.
- Several repairs were made to the VCM unloading compressors
during the month. Numbers 1, 2, 3, 4, and 5 compressors were
shutdown for repairs. Numbers 1, 2, 4, and 5 were shutdown
and rebuilt because of blown gaskets. Number 3 compressor has a broken crank case and shaft. It was sent back to the factory for repairs.
VAB.0001190048
W MMMMnHPVPWHWlWPVWiMVffWVMHVMMMNMMMMMpMPi
ENGINEERING - R. E. Polk, S. C. Hillman, M. R. Kane * GENERAL
5305 Decalcified Resin
Production of decalcified 5305 resin continued using the temporary system in the New Module. Enough resin was produced in June to satisfy Klockner's requirements for the month of July.
Evaluation of the technology options for removal of calcium was
completed.
Ion exchange has been chosen over membrane separation
because of the relative economics. A Class "A" design will be issued
by the beginning of August.
Batch Water
Improvement of the batch water stripper performance has occurred during the last two months. Most of the improvement is due to monitoring the system. Recommendations to further improve the stripper reliability include standardizing the operating procedure and some minor maintenance and capital modifications.
The AFE request for the TC Compliance Project was submitted for approval. This project provides the implementation of EVC
containment from the Batch Watch Strippers.
A Hazard and Operability Study (HAZOPS) has been completed on this project. A consultant from Stone and Webster Engineering led a team of operations, maintenance, and engineering personnel through the review of P&I diagrams for the project. Representatives from PED and the Oklahoma City Plant also participated to learn HAZOPS techniques. PED is preparing the HAZOPS report from the study.
Production Model Building
Production Model Building began last month. The production models will be used as a part of OASIS to provide more accurate product cost accounting. The production models will include not only the current IPA items (utilities and raw materials) but also the activities which were recommended by Price-Waterhouse in their activity-based cost accounting evaluation.
VAB.0001190049
ENGINEERING - Continued
h
Economics were identified for the justification of a method to produce compound samples at Aberdeen. The cost of having samples produced at Premiere and filane and the cost of the excess material when samples are produced at Aberdeen justifies further work. A design basis is being identified with a Class "A" design expected by September.
Boiler Feedwater Tank Replacement
The boiler feedwater tank has been condemned. This project will use an existing tank to replace the condemned tank. The tank will be lined with placite and located next to the existing boiler feedwater tank.
VAB.0001190050
F. G. Jeanson
Water
All wastewater discharge parameters were met for the month of June.
Results were received from the State on our NPDES inspection. We were in full compliance.
Waste
Waste shipments for the month included:
One bulk load of lead bags was shipped to CWM in Emelle, Alabama.
Two bulk loads of stormwater solids were shipped to CWM in Emelle, Alabama.
Thirteen drums of stabilizer spill were shipped to TES in LaPorte,
Texas.
The Louisiana House and Senate have both passed a bill that would increase for hazardous wadst'es disposed of in their state and would ban
Mississippi from disposing of hazardous waste in Louisiana starting January 1, 1991. This bill is very similar to the one Alabama passed.
Superfund
A draft order was received from the State this month to do a remedial investigation of the superfund sites. Comments were gathered from legal, Joe Ledvina and Conoco. These comments were communicated to the State in a meeting held in Jackson.
Our comments were incorporated into the order and the State reissued the draft order for our review. We gave our final comments to the State. The final order is expected the first part of July.
DuPont Environmental Remediation Services (DERS) was in the plant this month to do a geophysical survey of the superfund sites.
Two other contractors contacted the plant about pond 2 resin removal this month. We are considering these options.
The modeling study was reviewed by the State. The risk calculated from the fenceline concentrations determined in the modeling study was greater than the State's internal guidelines. A meeting was held with the State to discuss the results of the modeling study and determine what action needed to be done in order for us to get a construction permit for the VCSM Project.
VAB.0001190051
ENVIRONMENTAL - Continued
Air - Continued
We presented an option to reduce total emissions even though we will increase production by combining two projects. The VCSM Project and the Steam Stripping Optimization Project will be done in parallel; thus producing a net reduction in emissions. The State agreed with this option and wrote a draft construction permit. This permit was reviewed and sent back to the State. The State Permit Board will review this permit in the first part of July.
A construction permit should be granted the first part of July for the VCSM Project. However, our current operating air permit expires in March, 1991. The State plans to address the high risk associated with our fenceline concentrations at this time.
The NESHAP's quarterly report was completed and issued to the State.
SARA
The 1989 313 emissions were completed and issued to the EPA and the State. Ten chemicals were reported this year. A summary of the emissions is attached.
ffl3C$UftfiePUg
I attended waste minimization conference held by the Mississippi Technical Assurance Program.
The dust collectors sold to Louisiana Chemical Equipment Company were tested for asbestos. Twenty samples were taken and no asbestos was found.
I attended the DOT training held in Houston by the Corporate Environmental Department.
I participated in an environmental audit of the Oklahoma City Plant this month.
* pi
wm
wmm mm
rnmmmmmmmmmmmmmmmmmmmmmmm
VAB.0001190052
AIR
WATER
FUG.
STACK
LAND
OFFSITE
S ECOND TOTAL OFFSITE OFFSITE
ANTIMONY
00
0 0 1386(1) 2(2) 1(7)
BARIUM
00
00
24(1)
335(4)
2(2)
BISPHENOL AO
0
Di-N-Octyl Phthalate
0
0
335 0 5232(3) 732(7)
HYDROCLHORIC 0 ACID
296
00
0
LEAD
07
0 0 5233(1) 26(2) 8(7)
METHANOL
1-499 1-499
00
0
PHTHALIC
00
ANHYDRIDE
0 0 6072(5)
SULFURIC ACID 0
0
0 0 20970(8)
VCM(6)
3016
73196*
6
0
0
0 0
0 0
0 0 0 0
1389 * 361 *
5964 *
5267 * 0 6072 20970 0
(1) Empty Bags (Sent to Chem. Waste Management, Emelle, AL) (2) Floor Sweep (Sent to Chem. Waste Management, Emelle, AL)
(3) Filter Cake (Sent to Chem. Waste Management, Emelle, AL) (4) Stabilizer Spill (Sent to Chem. Waste Management, Emelle, AL) (5) PA Spill (Sent to Chem. Waste Management, Emelle, AL)
(6) Fugitive emissions were calculated using correlation factors developed
from a bagging study done at this plant) (7) API Sludge (Sent to Chem Waste Management, Emelle, AL)
(8) Sulfuric acid contaminated dirt from Acid Dike Replacement Project (Sent
to Chem. Waste Management, Emelle, AL)
A Represents a reduction from 1988 emissions reported.
Upww
mm
m
VAB.0001190053
*
WASTE production vs GOAL 89 it 90
ALL WASTES EXCEPT WASTEWATER
LBS WASTE/M LB PRODUCTION
Dc--88
Mor--89
Jon--89
S#p-89
D#c-89
1988 ACTUAL
o 3 MO. ROLLING AVG.
+ 1990 GOAL
Mar-90
Jun-90
WASTEWATER DISCHARGE VS. GOAL
1989FY -- 1990FY
MM LBS WASTEWATER/MO.
Dpc-88
Mor-69
Jun-89
a lOM ACTUAL
- 3 MO. ROLLING AM6.
Spp-89
D#<-89
+ lOOO COAL
Mor-90
Jun-90
VAB.0001190054
wmnmi
mmmmmmmmmmmmmmmmmmmrnm
immm
w
D. A. Moore
June. 1990
A. Unadjusted EUI
<3.1%>
B. Adjusted EUI
<3.2%>
C. BTU/Lb. Product
2545.0
D. Total Energy Consumption MMM BTU 125.50
< 7.5%>
< 7.7%>
2640.0 1181.93
III.
There were seven energy related Items completed in June, 1990. Six of these items were steam leak repairs. The remaining one was steam trap repairs.
No. 1 No. 2 No. 3
Combustion Efficiency % June. 90 Fiscal Y.T.D.
83.3% 83.2% 83.0%
83.4% 83.3% 83.0%
*
VAB.0001190055
BTU/LB
VAB.0001190056
ABERDEEN ENERGY CONSUMPTION
BTU/LB
MONTHLY
MONTH
-------- 12 MONTH AVERAGE
Carina Cook, New Hire
Robert Wil liens from Lab Trainee to Head Building Attendant.
Jerry JenJcins from Head Building Attendant to Compound Operator
i
Mitchell Bishop bid from General Helper to Lab Trainee. Brskin Morgan promoted from Yard "B" Operator to Yard "A"
operator
None
None
None
VAB.0001190057
Aberdeen* Mississippi
Salaried Employees Hourly Emolovees
* **
Total Employees
Employees (Hourly) New Employees Terminations
DEPARTMENTS Warehouse ' Gen. Plant Maintenance Laboratory Compound Vinyl
^
Plasticizer
PAR 16 13 41 24 40 33
_________ ____
5
80* 172 252
JUNE* 1990______________ MONTHLY PERSONNEL REPORT
Minority Employees
Z
Hourly Total
0
Hourly Min. Hired
0
0
Z Min. Hired
Q
Hourly Min. Term.
Q
Z Min. Term.
q
ft EMPLOYEES MIN. EMP. % MIN. NEW HIRES YTD TERM. YTD TURNOVER YTD
15 16
41 24 24
38
33 10
5 40
fe
Number of Applicants:
Month ________Q
Year to Date
APPLICANT BREAKDOWN:
0 Minority
q
% Minority 0
:t Female o % Female
n 0
* This total includes 2 Co-op Students and 2 Summer Process Engineers.
Hires (Hourly):
Month 0 Year to Date Q
Terminations (Hourly):
Month
0
Year to Date Q
Overall Turnover
0
Projected Annual Turnover 0
VAB.0001190058
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VAB.0001190059
ppm
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mPMPPIIVMfWMMMMli
VAB.0001190060
- D. A. Barclay
Safety There were no safety Instances this month.
Cost Savings Savings due to competitive bidding were $8,620 for June, and $100,039 for FY1990. Savings due to prompt payment discounts were $1,645 for June, and $17,977 for FY1990. Savings due to using excess materials (AFE and work order stores) was $17,090 for FY1990.
Warehouse - Finished Goods Inventory Slow moving and off'grade inventories are still a major concern approximately 35% of total packaged inventories.
tir.aT;figj.c
Joe Lutz, U.E.&C., r>.inducted VMS training during June. Jack Little met with Price'Waterhouse to discuss activity based cost accounting. Mickey McGee (EDS) and Gerald Burzynski visited the plant to oversee VMS implementation. Employee Development VMS training held during the entire month of June. Meetings Various meetings and training sessions for VMS.
VAB.0001190061
m In
Immmmm tun
MUM
HlciOn n fMMCTS
MHtU
pnuc 11,211,1$!
139,511
MTI
ipi/hc UOU8K
1,090,111 141,750
0 0
umu mmmm
imtWMHM
* v`i
OUlMItU
HUM - Hcum
1.SII.IH MM.ttl
1M2I 1,115,510
111,119 9 0
1,207,951 119,499
0 0
00
l.m.isi 0
0 0
0 9
i.in.u0i
usneun
*
mu
lunnn vr
1T0.I2I Ml,l
0
IN 11,019,009 1,021,120
unit
1i1nSiu. u comm uwrnncmisonm
uiua 141 2100 2
C0STOIII COIVOI rim C1II1II
42 47 94 1 12 04
rciu jin
195
49
$7
TTI
PIUIC irr/ifc mum
lM.Ml.Ul 1.UI.IH
iii.,nhii..hiiii
1.NMN 0
11,HUM MSI,111 U,III,IN 1,111,111
9 0
51,010 0 0
20,141,720 1,IN,111
i.iss,in nun
0 0
9 0
1 Mii.iii 0 129.205
1,304,200 2,275,010 MiMii
hi,in,in 111.111,141 s.iii.ns
TOTAL
230
20
39 I
295
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inn mom
puifiatn
mU TTI
PICU6II:
Mlllt Kill nmuimom
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1,321 113 217 21
1,N1
243 11 10
9
270
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11 07
3 9
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529 39
141 33
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1 1
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*
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VAB. OOO1190062
J. M. Edwards, Jr.
A. Safety - There were no safety incidents in the Laboratory during
June.
The monthly safety meeting topic was respirator and
breathing apparatus training taught by Bruce Trego.
B. Customer Contacts - There was one customer contact during June.
Jim Edwards, accompanied by Mark Washington, visited AT&T Network Systems in Omaha, Nebraska. Two recent contamination complaints were discussed and the packaging of the boxed material was discussed. Cheryl Cincetti presented us with a full Five-Star Rating for our semi annual vendor rating grade for the end of 1989.
/
6/14 Vvcom, Scranton. PA
Vycom reported "white streaks" while making gray sheeting. It is suspected that the problem could be from undispersed Ti02 or line scale in the dryblend. Jerry Janes is investigating. The product is RP-421 WHT
110
6/28 Formtech. Stow. OH
Formtech reported finding metal contamination
in RP-91 WHT 110 bulk trailers.
The
contaminate was ground ferrous magnetic metal
the size of color concentrate particles. No
metal contamination was found in the retains
from the suspected shipment lots.
06/29 Madison Cable Corn.. Worcester. MA
Gordon Snyder at Blane reported that Madison Cable's screens were clogging up on 1 1/2 to 2 hours with white fines using 384 FR NAT. Austin R&D analyzed the white contamination and found it to be very high in aluminum concentration. The aluminum trihydrate used in the compound was Aluchem AC 712K (lots V0289-00286, 0131 and 766870).
D. Requests for Corrective Action
There were no requests for corrective action during the month of June.
Dayton Extruded
Product RP-151 WHT 145
Reason Color
mrnrnmmmm
PP
2 R/C
VAB.0001190063
LABORATORY - Continued
F RVCM Summary
The following is a summary of residual VCM results on in-
process samples.
None of the reactor daily averages
exceeded 400 ppm RVCM during the month of June, 1990.
Reactor Slurries
________Drier
5265
5305
Number of Samples Average RVCM, ppm
865 124
22 0.214
80 0.243
The following is a summary of the residual VCM analysis of shipment samples for the month of June, 1990.
Product
5265 5305 5385 5395 5415 Dry Blend Debox Pond
Average RVCM. ppm
33 0.063 93 0.103 54 0.311
9 0.043 60 0.034 54 0.065
8 0.199 4 0 603
(based on dryer "regulars")
mi
Bulk Density Inherent Viscosity
(vs. 0.715 - 0.744) L Color A Color B Color % on Pan
(vs. 2%, max.) % thru 140 Mesh Drytime Mets I.R.
(vs. 95% of control) Hard Particles, (% > 10) Average particle size,
microns
1.60 4.33
11.67 6.67 5.33 0.52
--
0.39
--
*----- *---""-
139
5305
1.07 1.67 0.83 3.17 7.33 2.33 1.28
0.69
-- -- --
--*-
136
5?85
1.67 0.50
4.00
2.17 0.83
--
0.91 1.67
--
-----37.5
161
5395
0.11 0.26
13.00
2.50 0.88 *--* 0.63 0.89 2.99
----
0
145
5415
1.23 0.89
6.67
6.33 2.67 0.17 3.33 2.00 3.46 1.85 2.3
172
VAB.0001190064
Continued
Hardness Color Hard Particles Heat Stability Contamination Dicing Cross Contamination
Totals
unwary
47.0 <0.77>
12.0 <0.20>
59.0 <0.97>
Rejections M Lbs. (%)
39.5 9.8
88.0
<0.65> <0.16> <1.45>
10.2 16.8 U.4 178.7
<0.17> <0.17> <Qt ZU> <2.95>
Summary
Torque Rheometry Color
Total
3.3
11.1
<0.07>
<9.IZ>
<0.24>
1. The program to extract data from the resin shipment database for importing into letters of analysis is complete. A list is being prepared on the letters that will need to be converted using PFS Write to accept the data.
2. After a floppy disk failure of an often used program, a complete backup was made of all important disks managing lab data.
3. Dave Cox met with Witco and Vista R & D representatives to discuss wax properties, wax QC and calcium stearate specifications.
4. Dave Cox examined and evaluated an on-line particle size tester marketed by Lazentech. The instrument failed to reproduce the data and could not tell the difference between resins of different
Another precision test was done on the Sintech tensile and elongation tester. The results still indicate an assignable cause
6. Work was started (process flow written) to check raw material Certificates of Analysis against specifications and quarantine of non-complying materials.
7. The RVCM headspace analyzer failed once due to a black carbon dust
buildup on the circuit boards.
VAB.0001190065
LABORATORY - Continued
8. The Inherent Viscosity analyzer pneumatic mechanism was repaired twice in June. Major work and downtime on this instrument is likely to be needed soon.
The Brabender computer went out during a power outage. It was out
h
for repairs for two weeks and still was out at the end of the month. The Caulter Counter particle size analyzer computer was used during this time which has delayed testing Austin R & D autoclave resin besides slurry samples from the plant.
10. Jim Edwards was trained in Houston to implement the Customer Needs Response Program. This program was activated 06/29/90.
11. The lab worked with Price Waterhouse personnel in determining resources and costs associated in analyzing each individual resin, compound, dryblend, and plasticizer product.
12. All 6 laboratory natural teams met once during the month of June.
i,j* J-
*
VAB.0001190066