Document ppgqLBkRm124mgYrJBJnQyyOw
S.V.
C.v. 1 05,1 1 06
D.V.
317, 32Z Ji23
CG 46 CODF d-S20-D FKG
JAN 1 8 1982
<"5St e"T"
(LD1 NUMBER'
LIT. *r. r5l>3* IBS.
PROCESSES < ) YT-B20-D (D>
APPROVED BY EWK 10/21/81
riFFD FY JMH STA^ARD HRS. 8.8
TIME
F'REf AF iTICN HUES _ ______ _______ _____________ ZEferc^__________________________________ Safct^fe^o*fc___
________________ \j)eLJ&
EQUIP MENT
NAME: DALAMAR YELLOW - R
PREP 1
I 1 OBTAIN 3-NITR0-4-AMIN0ANIS0LE FOR S6 OBTAIN ACETOACET ORTHO ANISIDIDE FOR S22
I CLEAN, DRESS, CLOSE 24* CLARIF PRESS -I 15 FRAMES
I
DV i RUN 17* (595 G) WATER INTO `V_JL<L2__
2 WEIGH IN HYDROCHLORIC ACID FROM V-324
U" M---~f_____
L^rT DUMP IN FROM SI 3-NITR0-4-AMIN0ANIS0LE
I
LOT,
* 100%
3 .
i _,,5bs;x_^ ______ _____________j s &A-
131&:
1 USE I LBS
N-CODE
396-C 46-C
t
mm i
\'vl
liilteiB
spiili*
i___ a I S&tlQ1 -- L:L:iLiiw I_______
Hi
3 ItrO
ACC7 LBS
559 , ayf
I_______ l_______
i>r 1i
I___
STIR 10 MIN OR LONGER TO WET
I
ADJ TO 33' (1155G) AT 28-32*' F (ICE)
1 0X330
57-A
SIPHON IN SODIUM NITRITE IN 12-15 MfN
M__f,,_____ ,
___ %
STIR 30 MIN AT 28-32 DEG F MAINTAINING
I /5ijS\*S` 725-A
+ CR, + KI FOR S 12
I
RECORD: TI ME STARTJMJML&I CR___ 1 (+),
I
Kl^jfe.^*.) '
1
NOTE:
i
(1) IF CR-, KI-, ADD 20* 'AS IS' INCREMENTS|
HYDROCHLORIC ACID
ASSUME 32% |,,_ ___I 28-D
RECORD: CR______ ( + ), KI______ ( + )
1
I
(2) IF CR+, KI-, ADD 20* 'AS IS' INCREMENTS!
I
SODIUM NITRITE
ASSUME 33% !__
RECORD: CR______( + ), KI______ ( + )
|
I 725-A I
S ZJltJP
495
d a t e riiiN n-:i
*>
USE ACCT 1
PAGE 2 OF 3 CG 46 CODE YT-820-D <D) LBS fililllllil LE.S
Lj '^iISC
-j^r SLURRY
IN
40
GAL
WATER
IN
DRUM
6
PRECOAT
I-
^pppi
ULARIF PRESS WITH BICALITE, FILTER AID
ni-u i
DV "wHiN~S~10''sTlR^c6HPLEfI7'~5DHp""lN~ACTivAfiD-
4 J*sA CARBON JMP IN DICALITE, FILTER AID
15 1 13 -B 1 15 10 777-A |
STIR 30 MIN AT 28-32 DEG F MAINTAINING + CR, + Kl FOR S 20
'll57-A |___
RECORD: TIME ^TAftTYij&t
CR.,_2I_< + >
. Kl_ife_._<+> '
-
NOTE:
(1) IF CR--', KI-, ADD 204= * AS IS' INCREMENTS
1
I
HYDROCHLORIC ACID
ASSUME32% _____1 2B-D i___
RECORD: CR ,,._<*>, *KI_____ ( + )
(2) IF CR+, KI-, ADD 24= 'AS IS' INCREMENTS
I
SODIUM NITRITE
ASSUME33%
, I 725-A I___ _
RECORD: CR___ ^<+> , KI_______ ( + )
CV jeP7 *r On ""T0*~7?70*"g 7"w at er '"in t :o ""v ZZZ??Z"&~_ "" I
5 INSTALL TEMP CHART
_. L I . '
POUR IN SODIUM HYDROXIDE
___ , TIl IAx ! /.Gl A-
ADJ TO 40* <3880 G) AT 66-70 DEG F
| 3X33
CLOSE STACK DAMPER
l5n STIR FOR S 22
I i
>
7-D 1 562 57-A I
~Dv'
6
h. JjtfB f
WHEN S 14 STIR COMPLETE, TEST DV & RECORD
CR_jL_ < +) , i< I
+ > TEMP : 5JL_ < 28-32 F)
NOTE:
<1> IF CR-, KI-, ADD 20# 'AS IS' INCREMENTS
HYDROCHLORIC ACID
ASSUME 32%
RECORD: CR___._,,< + >, KI______< + >
(2) IF CR+, KI-, ADD 204= 'AS IS* INCREMENTS
SODIUM NITRITE
- ASSUME 33%
RECORD: CR______(+), KI__< < + >
TURN ON V-^SMr AGITATOR, CHOP & ADD ICE
THEN TURN OFF AGITATOR.
2X330
PUMP DV THRU CLARIF PRESS INTO DV
MAINTAINING TEMP AT 28-32 DEG.F
^/
RECORD: TIME START JL'JiR-f'ri TOTAL
i
1
!
57-A 2S-D 725-A 57~A i JaS
. 'I DUMP ACETOACET ORTHO ANISIDIDE INTO CV
ti cFRoOmM* S2
LOT
4=100%
%
| t\SjJstL2$.'-jf
JJTJ&
46-C 1 1547
R 10 MEN TO DISSOLVE
'
STACK DAMPER
IN ACETIC ACID UNDERSURFACE IN 20-25 j . ~ i
s - mj A_____, ,,4A?-/. /All-1
5 MIN & RECORD: PH,, JT.J*,,..<5.8"6 .3) |
"`'^SARY, ADJ TO PH 5-8-6,3 6 RECORD 5
5.8-6.3) SODIUM HYDROXIDE ASSUME50% I _rr=
ACETIC ACID
ASSUME70% | ;J1'
30-D | 871 I
7-D 30- D
DUP050110603
Ufllfc. l-'KlNItU: 1/12/82 MAKH'fG .INSTRUCTIONS BATCH UNIT
USE "n -c q d e' ACCT
'PAGE 3 OF 3 'CG 46 CODE YT-920-D (D> LBS
LBS
{ WHEN S 21 CLARTF COMPLETE, WASH DV (S 4)
LINES, PUMP & PRESS FOR 20 MIN OR TO A -CR
J TEST ON A SAMPLE Qr TOTAL PRESS EFFLUENT,1
I WHICHEVER COMES FIRST. COLLECT WASHINGS
IN DV (S 21 )
',
37 I STIR 5 MIN & RECORD: TEMP^.jiL-C28-32F) &
NECESSARY, ADJ TO 28-32#F. RECORD*F
Jr I WEIGH SULFAMIC ACID IN RUBBER BUCKET 6 WASH
\ INTO DV
31 i STIR 5 MIN 6 RECORD: KI_jfc___ (-)
32 I IF NECESSARY, -ADJ TO -KI (SULFAMIC/ACID)
I AND RECORD
RECORD: VOL
1 `5
57-A 395-D 395-D
15
MISC 9
CV 10
?IGM SODIUM HYDROXIDE IN DRUMS.FOR S41
DISSOLVE IGEPAL CO-630 IN 20 GAL WATER IN DRUMS FOR S43
JHEN S 33 COMPLETE, ADJ CV TO 43" (4197 G)
J^AT 80-84 DEG F
5<1 CHECK ACCURACY: HT_j5j&___DEG F t*
S*
RECORDERDEG F
m I IMMEDIATELY RUN IN DV THRU UNDERSURFACE
\\ DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV
I AT ,80-84*F.
.
^
^KRECORD: TIME START^^M., TOTAL KINJ&3____
37 I S*fR 10 MIN. DISCONNECT TRANSFER LINE AT CV IMMEDIATELY
RECORD: DIAZG___'T_.__(-> > BASE__ZfT__,,( + ) >
PH_.*(LA<4.3--4.7> NOTE: (1) IF DIAZO + ,
BASE -, it PH BELOW 4.3:
(A) ADJ TO PH 4.3-4.7 SODUIM HYDROXIDE
ASSUME 50%
(B) RECORD: PH_____ __
I (2) IF DIAZO +,BASE - 6 PH ABOVE 4.3 ADD 8*1
100% N-7-D SODIUM HYDROXIDE ASSUME 50% TO A 55G DRUM. ADJ WITH WATER TO +/-25G
ADD 20* 100% M-46-C' AND STIR TO DISSOLVE, POUR IN CV AND STIR 10 MIN.
REPEAT ABOVE AS NECESSARY TO - DIAZO,
+ BASE
OUR IN N-7-D SODIUM HYDROXIDE FROM S34 &
STIR 5 MIN.
* i RECORD PH^Jl ?_(7.1-9.0) & IF NECESSARY ADJ
V I^PH 7.1-9.0
SODIUM HYDROXIDE ASSUME 50%
CORD: PH^fe- HYDROCHLORIC ACID ASSUME 32%
HP IN N-979-D FROM S 35
HEAT TO 2O0-204 DEG F IN 58-62 MIN ^F^MfTIR 30 MIN AT 200-204 DEG F
yf RECORD: TIME START_/_'_^/____
Y I FPLOOD TO 94 * (9174 G) AND STOP AGITATOR
I START
f in
OF'TR
:J:z
>rD 979-D
337 50
7-D 7-D 46-C
7-D WM-
28-D
DUP050110604
DUP050110605