Document pmoOD2dbdNQX9bXJ4Ybm9kq07
CG 01
CODE YE-721-D
<S>
( DATE )
< LOT ) Y
4448* LBS. ( EST WT )
PROCESSES < > YE-721-D (H)
APPROVED BY: FWP 11/08/82
COMTYP JOB NAME: 1YE721DMM
BLENDED BACK: CG
^
OUNDS)
NAME: MOLYBDATE RED
USE LBS
BTAIN FOR S-12 OBTAIN FOR S-34
OBTAIN FOR S-33
BTAIN FOR S-40 BTAIN FOR S-44
r sl
OBTAIN FOR S-47 ' y'l-- >#i w e j e $l in : o p t Rife,, mk
2W fI ^
' OPTR
MK
359 \J4\ WEIGH lS\ OPTR 'lldk, MK Jj_,
* OPTR
MK
9.7lfA T~___________
T T ___ %
68 600
12
195 350
61
I ACCT N-CODE | LBS
10B-A 4-A 3-A
32--D 3-A !
711-BD |
63 600 120
195 350
61
10-D
1509
423-D
243
RUN 10" (500 G) WATER INTO V-358
A RUN V-35? INTO V-351 & PUMP IN V-351
1 J ADJ TO 55" <260 G)
>SIFT IN N-108-A FROM S \u 4
Jr STIR 5 MIN it RECORD: f>H9 0)
ADJ TO PH 9.8-9.9 & RECORD: PH^JLife
ASSUME
50% 1i
ASSUME 66% \|
If5 | RUN INTO V-351 FROM BADGER METER 0PTR..3uK-~, MK,,_3__, 3-^
\j33J
JM'JS PUMP FROM V-351 TO V-358
10OOG
Xf WATER INTO V-358
I ADJ TO 74* < 33 G) AT 7-69#F
I A' RECORD: VO.L* _* & __..X*F
$,1
I
STIR 5 G/ML
hMIN<
:c GRD: PH.SJL<7.2-7.4) .<* *55-1 .058)
I NOTE IF G/ML GUT OF LIMITS FILL OUT CHECK
| LIST & ATTACH. TAKE 1 QT SAMPLE.
1 1
1 1
7-D 33-D
28-D
| ifei: I
I 'H
?V !2n RUN 2* <996 G) WATER INTO s I 1 RE6eRr-w^HS-^rrORAGE t a n k t o
| .A C^CIRCLE ONE : 4^2 41 411 420 424 025
CTTErFwfN-CU SUPV:
w"s''
| I *STORAGE TANK MUST CONTAIN AT LEAST 190
| | GAL: 402=39", 410=2", 411=38*, 420=20",
I j 424=20*, 425=25* | I ^STORAGE'TANNI MUST HAVE STIRRED AT LEAST
1 I 20 MIN SINCE LAST ADDITION OR ADJUSTMENT
| | *STORAGE TANK MUST BE ISOLATED UNTIL ALL I A PUMPING FOR THIS BATCH IS COMPLJ
j>2' I SET METER FOR 300 G & PUMP TO SV
0Vil2j982
LOT: EQUIP MENT
COMTYP JOB NAME: 01YE721DMM PAGE 02
BATE PRINTED;11/03/8;
USE N- ACCT LBS CODE LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP7~~~
CHECK PH 6 DENSITY* RECORD BELOW* IF NOT
IN RANGE^ STOP PUMPING 6 SEE SUPV.
* FH:_3tjG (2*2-3,7)
DENSITY:
G/ML <1.270-1.328)
IF S-23 OK ^HEN S-22 COMPLETE, RECORD
DENSITY ,,JJL G/HL ON TRAPPED SAMPLE
FROM END OF S-22 PUMPING.
USING DENSITY FROM S-24, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-22.
CIRCLE DENSITY & SETTING IN TABLE BELOW.
* TABLE #**#
I 1 G/ML SETTING 1 G/ML SETTING 1 G/ML SETTING
1 ! 1.270 1259 1 1.291 1146 1 1.312 1049
1 1 1<271 1253 1 1.292 1141 1 1.313 4045
1 1 lll72 1248 1 1.293 1136 1 1.314 1040
1 1 1.273 1242 1 1 .294 1131 1 1.315 1036
1 1 1.274 1236 1 1.295 1126 1 1.316 1032
1 1 1.275 1231 1 1.296 1121 I 1.317 4027
1 1 1 .276 1225 1 1.297 1116 1 1.318 1023
1 1 1 .277 1219 I 1 .298 1112 1 1.319 1019
1 t 1.278 1214 1 1.299 1107 I 1.320 1015
1 1 1.279 1208 1 1.300 1103 1 1.321 1010
1 1 1.280 1203 1 1.301 1098 1 1.322 1 006
i i 1.281 1198 1 1.302 1094 1 1.323 4 003
i i 1.282 1193 1 1,303 1 89 1 1.324
999
i i 1.283 1187 1 1 .304 1084 I 4.325
995
i i 1.284 i i 1.285
1182 1177
1 1 .305 1080 1 1.306 1076
f 1 X?A i"
994
i i 1.286 1171 1 1.307 1070 1 1.328
983
i i 1.287 1 f 66 1 1.308 1066 1 1,329
979
i i 1.288 1161 1 1.309 1061 I 1.330
975
! 1 1.289 1155 1 1.310 1057 1 1.331
971
i i 1.290 1151 1 1.311 1053 1 1.332
967
IP^SET METER 6 PUMP JJJBJLG (RECORD FROM TABLE)
t I FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
50 SECONDS
___ .
AM_LEAD NITRATE TO 3244 G <68*-242/243 6(66,5L?
^ 24AT 67^69F
----------
1I 41-D
, Rec o r d : _j l __ *f & ic e c o n s u med <330#/b l o c k > 330X_ I 57-A
L2T STIR 5 MIN & RECORD PH :
(2.2-3.7)
**** USE TITRIMETER TO ADJUST N-41-D PH ****
IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 66%
u
l
l
i 1 33-D
. & RECORD PH : A./--.
ASSUME 50%
IDTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING
1 7-D
1-301 RECORD:
G/ML, (1.128-1.129) IF OUT OF SPEC
t X FILL OUT CHECK LIST 6 ATTACH.
I>n I STIR AT 67-69*F FOR S-33. TAKE 1 QT SAMPLE.
4094
DUP050059735
COMTYP JOB NAME: 01YE721DMM PAGE 03
DATE PRINTED:11 /08/82
USE | N-
USE
LBS | CODE LBS
OBTAIN 1 QT SAMPLES OF S-19 & S-31 SOLUTIONS i & TITRATE TWICE I NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
I 9.5-9*9 OR IF THE TWO TITRATIONS DIFFER BY
I MORE THAN 0*10 ML N-10-D (IF YES, FLUSH ALL i | EQUIPMENT 4, REPEAT TITRATIONS) . DO NOT
I I PROCEED IF N-10-D TITRATION IS OUT OF RANGE
! I ADJUST V-358 FOR A TITRATION PH OF 1 *QQ .ffH'HQO I | FROM FINAL IN-LINE TITRATION, RECORD LOWEST I I PH ---------- 4, ML N-10-D-----------
33-D 7-D
*wW I -/ I
_________________.____ _______ ...________
SV !^3 I WHEN S-32 TITRATION OK, STRIKE V-358 THRU BOTH
6 | ! UNDERSURFACE DJO'R||UTORS INTO SV IN**44~46 MIN I I RECORD: START f!MF1 TOTAL MIN__JfX__ I | J&IOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
I A 4, BUBBLES APPEAR IN SIGHT GLASSES
I IMMEDIATELY DUMP IN N-4-A FROM S 2 4. SET TIMER I > FOR 15 MINUTES
DURING S 34, WASH IN V-358
1^6 1 STIR 2 MIN 4, RECORD PH__/c2,,_( 1 *7-1 .8)
f A PBXS,_j A___(MUST BE + )
WP7 ! .STIR TOTAL OF 15 MIN FROM S-34 4. of RECORD : TEMP *//___ F <67-73F>
4 DUMP N-3-A FROM S-3 STIR 3 MIN
J POUR IN N-32-D FROM S-4
.! STIR 2 MIN
RUN IN LIQUID ALUM USING BADGER METER
>*,r.*'*>*JS,. TDUTMRP
3 MIN 4, FLUSH ALUM IN N-3 FROM S-5
LINE
WITH
WATER
604 115-D 302
| STIR 4 MIN FOR S-49
P 390
7
RUN IN HYDROCHLORIC ACID USING WEIGHT 4, FLOW *
I CONTROL PANEL
MK 3__ ,
V MK______, _______ 1%
! DURING S-45 SIFT N-711-B FROM S-6 INTO V-3.90
WITH AGITATOR ON IN 1-2 MIN
| STIR 1-2 MIN TO MILKY SOLUTION
28-D 28-D
90
SV I WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B
8 SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES.
A DUMP IN BLANC FIXE N
5-1' I WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP OF PAGE 1
RECORD: CODE, LOT____________ _____, _*
J- STIR 20 MIN * ^
#i'# RECORD: PH_(5 * 8-6.0 >
IF NECESSARY, ADJ TO PH ,5.8-6*0
ASSUME 50%
4. RECORD: PH-____ ..
ASSUME 66%
| FLOOD TO 153' <7298 G> 4, STOP AGITATOR
275
7-D 33-D
STAR! biMi
|p^
URTR,
Li. J- yL.J
DUP050059736