Document pmZqG2jKzEo0yBpeXy2VbOVEB
FORM 5455-*
FILE
ANALYSIS FORM
a jj / ^pf*l
1 A/'AO
2
3 Ai-ao
4
5 A?~ AO
6
7 B>' frp
8
9 At- AO
to
11 bi-ao
12
13 At-AO
14
15 At-AO
16
1 Al-Ati
ei
19 Sf-AO
20
21 fa-fit?
22
23 01- AO
24
25 <5rA/At3/h*A5 tZ /
26
27 7
28
29 "3 30
31 * '
32
233
34
335 ----------------------------------------
11
I
f
in
j
36
m37 ------ .--------------------------------------------------------------------
7
38
39
) 41
4?
43 44
45
Sei&o l.l*T Tcrt/oo zxr SttSoo !}<
UM71 ClPZ
/mbH !.7171 U9em I.7UZ
13%*. 0.nn <1.511*
UH 0, Jt>of 9. Wit V s'
UMo
19575- 3t<
o.njt 1512V 3/*T
c.iwz 19129 3/5"
1X7*0 0. >bl 195,^ 3t<
HZ*g'S9J A//37
%*r
ma_ 0,1079 1.9312 s/r
7iSii o.iozz Wort US'
O./Ztxf %97p 3/5" Si7/J ft/ZW 9.9U1
mu. A. //S? 1.1992 nr
17,20 21-t/ 2-TaY
3z.n
2<Yi
,?&?r
HJ&.
Wa22 Yo,5t> 35,n>
____ 2L SO
cjoL V
-=: JUU /.71
-
x
50
<y/ V
- n.93
r 17 7
>
"COE FTDEN ITALN ATERI \LSU "T&l R0TE( ;tive< )RDH
m
OJLri 108977
-4*^ 7/wy
\)
*;wM:V v :. ^
tansr
EXTINCTION METHOD WORKSHEET
iXlt T -
V/' .`i-n?.
^tSn'4^f. * :' " :_W^ * ' <r$; ` ;
This method of calibrating the 3M Brand Organic Vapor Monitor No. 3500, 350? depends on adding a known mass of solvent or solvent mixture to a known volume
of air.
** The known amount of solvent Is determined by the change In weight of a syringe upon solvent Injection. The known volume of air comes from readings from a positive displacement flowmeter.
j- .,
'j4'wv
The solvent(s) are diffused through one of five aluminum columns. The small bore column Is #1 and Increasing bore sizes are numbers Z through 5.
Position
Monitor Meg, found
Diffuser Used _
AHfQVtet
ft/- too??-#'
jfe, 5
-6W
;
v '- - Blank
tntrr
rf2~*AOolr2 Al-riOo* 71
82- Aoe>
*?)2 - *tP <>2*r
Time
ZJLT Z'lO
Flowmeter (ft)(l)
jfy63.o~7 .saa,JL;z
Date of Test __ Solvent(s) ch rTemperature
Syringe Used ______________
Mean: Standard Deviation: Coefficient of Variation:
Syringe (gr)
Cowments
JA/jLoU-
.*.ZZ2J.
jk i CALCULATIONS:
FLOW RATE:
r*
af/ffrlruv\
*MILLIGRAMS* OF SOLVENT:
-?Ls-7 FtH H. 7Z
(METER)4 OF AIR:
.'.tjfv ''
CONCENTRATION:
f. 32 7 it ,, jPctZ
'*>>. r
EXPOSURE TIME:
,PPM:
31
-?*9 6>Sr
PPM-HOURS: /.?, 7^
3M 108978
/5c H
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
tC &^r<
087
TEMPI TIME1 RBTE TEMP2 T IME2 IH-J TEMP FIB TEMP BUM TEMP
270 30
S. 50 10.00 270 US
2.00
350 200 350 250 480 115
80
200 250 115
CHT SPB ZtKU BTTN 2T FIB SGNL
SLP SENS RREfi REJ FLOW fl FLOW B
0.30 10.0
9 B
0. 10
30.0 20.3
100 26.0
1(- f
DELETE CHANGE RUN 3 CHANGE RUN 0 3 CHANGE RUN 1 0 STOP
HP RUN # BOTTLE 1 BEEN
1
BUG^31^7y
RT
BRER
BREH
0.2S 3.36 0.46, 1 . 15"
392 11640
80940 t "1327'
0.416 12.344
35.333 1.407
BILi ,- Fi. fiC*.TOAR.5-1 1.0000 E+ 0 " rE 0 3
TIME 09:30:47
HP RUN # BOTTLE 2 BRER
2
RT AREA
0.28 0.37 0.46 1 . 15 ".i * --f? c
* 5i
pTi
416 1 1040 30440 1243000
506200
RUG''31-^79
BREfi
0.023 0.598 4.357 67.598 0.013 27.415
, .0
TIME 09:43:20
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 108979
088
HP R iJ H # BOTTLE 3
AF FP V
HUb
RT
AREA
AREA %
0 . 22 3 lL O 0 , -3 6 0.46 0.96 1.14
1 T "7
1.68 1,89 "* J
O^ 3.57 3.93 4.14 4.55 5,37 5.68
833 7 76 12340 84040 1356
82728 3342 3928 4271 909
7798 23950
2568 3485 7612
1296 1269
0. 344 kJ ^20 5.089 34.659 8.559 34.115 1.378 1.617
1.761 0.375 3.213 9,877
1.859 1.437 3. 139 8.534
0.523
OIL FACTOR: i. 0000 E9 0
aTHRT~ fr.Sfr 03,3*6
I ?1b 091 55 : 55
HP RUN # BOTTLE 4 AREA
4
AUG231^79
RT
AREA
AREA X
0.22 0.28 0.37 0.46 0.77 8.94 1 . 14 4i 7 0 1.68 1.89 2,22 iiii
3.58 3.93 4. 15 4.56 5.36
338 ' 770
12310 81760
3452 4277 79380 3261 ^71 7*0_ 1J 4919
759 6626
21548
1513 .2010 5315 . 244
0.368 0.331
5.290 35.136
1.483 1.838 34.113 1.401
1.600 2.114 0. a26 2.847 9 957 sllss
0.364 2.284
8. 105
BIL FACTOR: 1 .8800 E+ 0
TINE 10:08:29
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 108930
089
hR T. -0.0B3_
HP RIJN #
BOTTLE 5 HREfi
S
flUG''31 -79
ir~-x.
T ?
o
0.37 S. 46 1.15 2.76 3.57
HkEh
484 11750 79880 1235000
339 50-9100
hRES %
0.026 B. 64@ 4. 349 67.246 0.018 27.728
DIL FACTOR: 1.0000 E+ 0
TINE 10:21:04
HP RUN # BOTTLE 6 AREA 'A
RT HP:Efi
3.22 0.28 0.37 0.46 0.78 0.96 1 . 14 1.38
1.63
1.89
2.82 3.57 3.92 4. 13 4.55 5.39 5.68
863
773 12030 82260
4171 1389
73840 3438 3599 3949 390 6592
22390 2246 2891 6344 1150 1284
HUG^31.-'79
hREh y.
0.367 0.329 5.105 34.994 1.774 0.591 33.539 1.463 1.531 1.680 0.379 2.884 9.525 0.955 1.230 2.699 0.439 0.546
DIL FfiCTOR: 1.0000 E+ 0
14
HREfi
BUG-'31^79
TIME 10:33:39
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 108981
TINE 10:46:13
090
--------
hKtM
Ti K ti n --
0.22 0.28 S.37 0.46 0.74 0.96 1.14 1.37 1.69 1.39 y - -? o o9
3.58 3.93 4.14 4.35 5.39 5.67
892 790 12150 32100 3364 1529 37300 3593 4270 4677 O "? fL_
8394 24420
2371 3173 7266 1 133 1 481
0.356 0.316 4.355 32.813 1.344 0.611 34.333 1.433 i > / yb 1.369 0.334 3.554 9.753 0.947 1.268 2.903 0,455 8 - 592
L FACTOR: 1.0000 E+ 0
START-
i
HP RUN #
BOTTLE 3 AREA ms.
S
AUG-'31 ,'79
RT
AREA
AREA *1
0.23 0.37 0.46 1.15 2.75 3.57
437 11260 80520 1292000
362 511500
0.026 0.594 4.'247 63.139 0.019 26.97 6
DIL FACTOR: 1,0000 E + 0
TEMP":
14
TIMt 10:53:4^
.HP RUN #
9
BOTTLE.rr.i.'
'^6,
flRER'^T'mai
HUG . * -v
0.22 0.23 0.36 0.46 0.76 0.96 1.14 , 1.37 1.63
>-l-yAREA 6' ^AREA i5*
* ' Iff, '
V';,
914 318 11318 32900 4242 1314 37540 3821 4352
.369 0.331 4.772 33.495 1.714 0.531 35,369 1,544 1,758
T I ME 11:07:53
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 10S982
091
T* Tl
7 ^ 5--J ^
-_!= * -_j f _Q
4.14 4.56 5 7? 5.66
7330 24430
1753 2216 5972
960
177Q i
L FRCTOR: 1.0000 t~*~ 0
0.382 3.164 q , 895 0] 710
0.895
2.413
,1 -7 i"i i" a _ *_ *_=
0.315
START
14
HP RUN *
BOTTLE 10 HREh
10
HUG'31 79
R.T
i~j r> 0
E_' .
_
0.28
0.37
0.48
0.96
1.14
1.37
1.68
1 . S3
2.22
", ~T "l
tC. <_> lL.
3.58
3.93
4.14
4.56
5.39
5.56
HKhh
843 7 68 11850 83360 1352 83860 3018 3700 3922 775 6820 22750 1717 2253 5312 941 1024
HRER *;
0.358 3.326 5.037 35.645 0,575 35.645 1,233 1.573 1,667 0.329 2,399 9.670 0.730 0.958 2.470 0.400 0.435
DIL FRC-TOR: 1.0.000 E+ 0
TEMPI 1 1 5 ^ ROTE 0 3
TIME 11:20:28
CONFIDENTIAL MATERIAL SUBJECT TO PROTECTIVE ORDER
3M 108983