Document peD0Rw7b5OzK3dbK97BwdLDjD

3M SpecialtyMaterials 3M Center St.Paul,MN 55144-IOOQ_-:651733 1100 3M June 28,2000 FecEx, 18077182 FadEx Tracking Number for Customer VIA EXPRESS MAIL Dr.CharlesAuer Director Chemical ControlDivision OfficeOf PollutioPnreventionAnd Toxics UnitedStatesEnvironmentalProtectioAngency 401 M Street,Southwest Room 403 EastTower (MailCode 7405) Washington,D. C. 20460 RNI= 1-8077ji@@ FadEx Tracking Number for Customer 180 7 718 2 171= Fe&-X. FedEx TrackingN umber forCustomer o. Re: Dear Charlie: Information On PerfluorooctaneSulfonates Mixtures 3M has providedstudiespreviouslytotheAgency.on perfluorooctane sulfonate-s-includinCgAS numbers 1763-23-1(acid)2;9081-56-9(ammonium salt); 70225-14-8(DEA salt)2;795-39-3(potassium-sal2t9)4;57-72-5(lithiusmalt-)-as wellas on aqueous and/orsolventsolutionosfthesematerials.Pursuanttoour recent communications,3M isnow enclosinginformatioonn productsinwhich perfluorooctane sulfonatesare deliberatelaydded as an ingredienti,e.,perfluorooctanseulfonates mixtures.We are providintghisinformatioonn a voluntarybasisas partofour continuing discussionswithEPA regardingfluorochemistry. As indicatedinmy lettetro you dated May 11,2000, potassium perfluorooctanseulfonateisdeliberatelaydded to 3M's aqueous firefightinfgoam ("AFFF")products.The amount ofPFOS inbothcurrentand historicfaolrmulationosf theseproductshas been quitelow --generallayround 1 percent.Moreover,3M customersdilutAeFFF productssignificandtulryingenduse,andthus,theleveolf potassium perfluorooctanseulfonateinthefinalappliedproductwould be even lower. As these circumstancesindicates,tudiesand otherinformatioonn AFFF productshave limitedrelevance,ifany,tothe potentiahlazard profiloef perfluorooctane sulfonates.3M isprovidingtheAgency, thereforew,i.thbasichealthand environmental laboratorsytudieson theseAFFF products.With respecttotoxicologsytudies,3M is providingcopiesof alllaboratorsytudies,exceptthatwe are listinagcute studiesina bibliographyF.or environmentalstudiesw,e are providingcopiesofalllaboratorsytudies and a bibliographoyfpublishedliteratur3eM. iscontinuingitsfilereviewand will supplement theenclosed studiesas appropriate. CharlesAuer June 28,2000 Page 2 As you reviewstudiesw,e ask thatyou bear inmind a pointthatwe have made previouslwyithregardtotestsubstance identitaynd composition.Many ofthe studiesreferto thetestsubstanceonlyby a 3M productidentificatniuomnber witha "T", "L","FM","FC" orotherprefixA.lthoughanalysisofthetestsample has been included, where availablei,tisoftennotpossibletodeterminefrom thestudyreportitseltfhe identitoyfthe testsubstanceorcompositionofthetestsample. To assistininterpreting the studies,we have used 3M's productnumber recordstoprovidetestsubstance identitaynd compositioninformatio(ne.g.c,ompositionpercentages;solventcontent; puritygrade,etc.)nexttoeach studyname on the indexand/oron the studysummary. In some cases,theformulatioinnformatiocnomes from historicraelcordsaround thesame periodas thestudywas conducted;inothercases,onlycurrentproductformulation informatioinsavailableT.hus,theformulatioinnformatiopnrovidedmay not reflectthe preciseformulationofthe specifitcestsamplo. Moreover,itshouldbe recognizedthat productformulationshave evolvedoverthe years,and thus,some ofthetestsubstances do notconstitutceurrentproducts. 3M looksforwardtodiscussingthe enclosedinformatiownithyou and other EPA staff.Inthe meantime, pleasedo nothesitatetocontactme withany questions. Very trulyours Enclosures WilliamA. Weppner, Ph.D Directorof Environmental,Health,Safety And RegulatoryAffairs SpecialtyMaterialsMarkets 3M Bldg 236-lB-10 3M Center St.Paul,MN 55144 (651)733-6374(phone) (651)733-1958(fax) E-mail:waweppner@mmm.com AttachmenttsoLettetroC.AuerdiiieJdune28,2000 ToxicologiSctauldieasndOtherRelevant l[nformatioonnPFOS Mixtures PFOS Mixtures AcuteToxici Post 1976 Studies(Biblioi!rayobnyly) 1) FinalReport,PrimaryEye IrritatioSntudy - Rabbits,3M ReferenceNo. T- 1328, Biosearch,Inc.,Oct.18,1976. 2) FinalReport,PrimarySkinIrritatiSotnudy- Rabbits,3M ReferenceNo. T-1516, Biosearch,Inc.,June25, 1976. 3) FinalReport,PrimaryEye IrritatiSotnudy- Rabbits,3M ReferenceNo. T-1516, Biosearch,Inc.,June25, 1976. 4) FinalReport,Acute OralToxicity-Rats, 3M ReferenceNo. T-1516,Biosearch, Inc.,June 25, 1976. 5) FinalReport,PrimarySkinIrritatiSotnudy- Rabbits,3M ReferenceNo. T- 1639, Biosearch,Inc.,Nov. 22, 1976. 6) FinalReport,PrimaryEye IrritatiSotnudy- Rabbits,3M ReferenceNo. T-1639, Biosearch,Inc.,Nov. 22, 1976. 7) FinalReport,Acute OralToxicity- Rats,3M ReferenceNo. T-1639,Biosearch, Inc.,Nov. 22,1976. i 8) FinalReport,PrimarySkinIrritatioSntudy- Rabbits,3M ReferenceNo. T- 1943, Biosearch,Inc.,Sept.27, 1977. 9) FinalReport,PrimaryEye IrritatioSntudy- Rabbits,3M ReferenceNo. T- 1943, Biosearch,Inc.,Sept.27, 1977. 10) FinalRepor@ Acute OralToxicityinRats,3M ReferenceNo. T-1943,Biosearch, Inc.,Sept.27, 1977. 11) FinalReport,PrimarySkin IrritatiSotnudy- Rabbits,3M ReferenceNo. T-2080, Biosearch,Inc.,Mar. 2, 1978. 12) FinalReport,PrimaryEye IrritatiSotnudy- Rabbits,3M ReferenceNo. T-2080, Biosearch,Inc.,Mar. 2, 1978. . AttachmenttsoLettetroC.Auer dgfedJune28,2000 ToxicologiSctauldieasnd OtherRelevant kformationon PFOS Mixtures 13) FinalRepor@ Acute OralToxicity- Rats,3M ReferenceNo. T-2080,Biosearch, Inc.,Mar. 2, 1978. 14) FinalRepoM Acute OralToxicity- Rats,3M ReferenceNo. T-2226,Biosearch, Inc.,Aug. 7, 1978. 15) FinalReport,Primary SkinIrritatiSotnudy - Rabbits,3M ReferenceNo. T-2226, Bio'searchI,nc.,Aug. 7, 1978. 16) FinalReport,PrimaryEye IrritatiSotnudy- Rabbits,3M ReferenceNo. T-2226, Biosearch,Inc.,Aug. 7, 1978. 17) FinalRepoM PrimaryEye IrritatiSotnudy(Wash-out)- Rabbits,3M Reference No. T-2226,Biosearch,Inc.,Aug. 7, 1978. 18) FinalRepoM PrimaryEye IrritatiSotnudy- Rabbits,3M ReferenceNo. T-2226, Biosearch,Inc.,Sept.19,1978. 19) FinalReport,Acute OcularIrritatioTnestwith T-2278CoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 478EO272, Oct.11,1978. 20) FinalRepoM PrimarySkinIrritatiToenstwithT-2278CoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 478EO27 l-,Sept.29, 1978. 21) FinalReport,Acute OralToxicity- Rats,3M ReferenceNo. T-2278,Biosearch, Inc.,Sept.25, 1978. 22) FinalReport,Acute OcularIrritatiToenstwithT-287lCoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 0880EB0279, June 24, 1980. 23) FinalRepoM PrimarySkinIrritatiToenstwithT-287lCoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 0880EB0280, June 24, 1980. 24) FinalRepoM Primary SkinIrritatiToenstwithT-287 1CoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 0880EB0505, Nov. 12,1980. 25) FinalReport,Primary SkinIrritatiToenstwithT-287lCoC inAlbinoRabbits,. RikerLaboratoriesI,nc.,StudyNo. 0880EB0717, Mar. 3, 1981. AttachmenttsoLettetroC.AuerdatedJune28,2000 ToxicologiSctauldieasnd OtherRelevant Informatioonn PFOS Mixtures 26) FinalReport,FHSA Acute InhalatioTnoxicityEvaluationinRats,3M Reference No. T-2943CoC, InternationaRlesearchand Development CorporationJ,an.21, 1981. 27) FinalReport,Acute OralToxicity3,M ReferenceNo. T-3025,RaltechScientific Services,Inc.,StudyNo. 83673 1,NW. 10,198 1. 28) FinalReport,PrimaryDermal Irritatio3nM, ReferenceNo. T-3025,Raltech ScientifiScervicesI,nc.,StudyNo. 836731,Mar. 10,1981. 29) FinalReport,PrimaryEye Irritatio3nM, ReferenceNo. T-3025,Raltech ScientifiScervicesI,nc.,StudyNo. 83673 1,Mar. 10,1981. 30) FinalReport,Acute OcularIrritatiToenstwith T-3097CoC inAlbinoRabbits, Riker LaboratoriesI,nc.,StudyNo. 0881EB0227, Aug. 3, 1981. 31) FinalReport,Piimary SidnIrritatiToenstwith T-3097CoC inAlbinoRabbits, Riker LaboratoriesI,nc.,StudyNo. 088IEB0226, Sept.4, 1981. 32) FinalReport,Acute OralToxicityScreenwith T-3097CoC inAlbinoRats,Riker LaboratoriesI,nc.,Study No. 098 1AR0228, June 22, 1981. 33 FinalReport,Acute OcularIrritatiToenstwith T-309SCoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 088IEB0230, Oct.26, 1981. 34) FinalReport,Primary SkinIrritatiToenstwith T-3098CoC in,;klbinRoabbits, RikerLaboratoriesI,nc.,StudyNo. 088IEB0229, Aug. 28, 1981. 35) FinalReport,Acute OralToxicityScreenwith T-3098CoC inAlbinoRats,Riker LaboratoriesI,nc.,StudyNo. 098 1AR023 1,July 10,198 1. 36) FinalReport,Acute OcularIrritatiToenstwith T-3 154CoC inAlbinoRabbits, Riker LaboratoriesI,nc.,StudyNo. 0881EB03 74,Dec 7, 1981. 37) FinalReport,PrimarySldn IrritatiToenstwith T-3154CoC inAlbinoRabbits, RikerLaboratoriesI,nc.,StudyNo. 088 IEB0375, Nov. 16, 1981. 38) FinalReport,Acute OralToxicityScreenwith T-3154CoC inAlbinoRats,Riker LaboratoriesI,nc.,StudyNo. 0481AR0376, Dec. 1,1981. AttachmentstoLettertoC.Auer datedJune28,2000 ToxicologicSatludiesand OtherRelevant Informatioonn PFOS Mixtures 39) FinalReport,Acute OcularIrritatioTnestwith T-3194CoC in AlbinoRabbits, Riker LaboratoriesI,nc.,StudyNo. 088 IEB0564, Sept.18, 1982. 40) FinalReport,Acute OralToxicity,Primary Dermal IrritatioPnr,imary Eye Irritatior3@M Reference No. T-32 15,Hazleton Raltech,Inc.,Study No. 92489 1, Mar. 30,1982. 41) FinalReport,Acute Oral ToxicityScreen with T-33 54 inAlbino Rats,Riker LaboratoriesI,nc.,StudyNo. 0882AR061 1,Apr. 5, 1983. 42) FinalReport,Acute Oral ToxicityStudy,3M ReferenceNo. T-3558,Hazleton LaboratoriesAmerica, Inc.,StudyNo. 856443,May 31.,1984. - 43) FinalReport,Primary Eye Irritatio3nM, ReferenceNo. T-3558,Hazleton LaboratoriesAmerica, Inc.,StudyNo. 856443,May 31, 1984. 44) FinalReport,Primary Dermal Irritatio3nM, ReferenceNo. T-3558, Hazleton LaboratoriesAmerica, Inc.,StudyNo. 856443, May 31, 1984. 45) FinalReport,Acute Oral ToxicityScreenwith T-3601 in AlbinoRats,Riker LaboratoriesI,nc.,Study No. 0984AR0366, Aug. 30, 1984. 46) FinalReport,Acute OcularIrritatioTnestwith T-3601 inAlbino Rabbits,Riker Laboratories,Inc.,Study No. 0984EB03 64, Study No. Aug. 3 0, 1984. 47) FinalReport,Primary SkinIrritatioTnestwithT-3601 inAlbifioRabbits,Riker Laboratories,Inc.,Study No. 0984EB03 65,Aug. 8, 1984. 48) FinalReport,Acute Dermal ToxicityStudy with T-3601 inAlbino Rabbits,Riker Laboratories,Inc.,Study No. 0984ABO433, Oct.23, 1984. 49) FinalReport,Acute Oral Toxicity,3M ReferenceNo. T-3714, Hazleton LaboratoriesAmerica, Inc.,Study No. 50108150, Feb. 25, 1985. 50) FinalReport,Primary Eye Irritatio3nM, ReferenceNo. T-3714, Hazleton LaboratoriesAmerica, Inc.,Study No. 50108150, Feb. 25, 1985. SI) FinalReport,Primary Dermal Irritatio3nM, ReferenceNo. T-3714.,Hazleton LaboratoriesAmerica, Inc.,StudyNo. 50108150, Feb. 25, 1985. 1 AttachmentstoLettertoC.Auer datedJune 28,2000 ToxicologicSatludiesand OtherRelevant Informationon PFOS Mixtures 52) FinalReport,Acute Oral Toxicity,3M ReferenceNo. T-3715,Hazleton LaboratoriesAmerica, Inc.,Study No. 5010815 1,Feb. 27, 1985. 53) FinalReport,Primary Eye Irritatio3rM@ ReferenceNo. T-3715, Hazleton LaboratoriesAmerica, Inc.,Study No. 5010815 1,Feb. 27, 1985 54) FinalReport,Primary Dermal Irritatio3nM, ReferenceNo. T-3715, Hazleton LaboratoriesAmerica, Inc.,Study No. 5010815 1,Feb. 27, 1985 55) FinalReport,Acute Oral ToxicityStudy inRats,3M ReferenceNo. T-3 9 10, Hazleton LaboratoriesAmerica, Inc.,Study No. 60501972, Aug. 8,1986. 56) FinalReport,Primary Eye IrritatioSntudy inRabbits,3M ReferenceNo. T-39 10, Hazleton LaboratoriesAmerica, Inc.,StudyNo. 60501974, Aug. 6, 1986. 57) FinalReport,Primary Dermal Irritation/CorrosiSotnudy inRabbits,3M Reference No. T-39 10,Hazleton LaboratoriesAmerica, Inc.,Study No. 60501973, July11, 1986. 58) FinalReport,Acute Oral ToxicityStudy inRats,3M ReferenceNo. T-3 940, Hazleton LaboratoriesAmerica, Inc.,StudyNo. 60702815, Oct. 10, 1986. 59) FinalReport,Primary Eye IrritatioSntudy inRabbits,3M ReferenceNo. T-3940, Hazleton LaboratoriesAmerica, Inc.,StudyNo. 60702817, Sept.12,1986. 60) FinalReport,Primary Dermal Irritation/CorrosiSotnudy inRabbits,3M ReferenceNo. T-3 940,Hazleton LaboratoriesAmerica, Inc.,Study No. 60702816, Aug. 21, 1986. 61) FinalReport,Acute OralToxicityStudy inRats (OECD Guidelines)3,M ReferenceNo. T-4152, Hazleton LaboratoriesAmerica, Inc.,Study No. 80300664, May 31, 1988. 62) FinalReport,PrimaryEye Irritation/CorrosiSotnudy inRabbits(OECD Guidelines)3,M ReferenceNo. T-4152, HazletonLaboratoriesAmerica, Inc., Study No. 80300666, June 1,1988. 63) FinalReport,PrimaryDermal Irritation/CorrosiSotnudy inRabbits(OECD Guidelines)3,M ReferenceNo. T-4152, HazletonLaboratoriesAmerica, Inc., Study No. 80300665, May 26, 1988. AttachmentstoLettertoC.Auer datedJune 28,2000 ToxicologicSatludiesand OtherRelevant Informatioonn PFOS Mixtures 64) FinalReport,Acute OralToxicityStudy inRats (OECD Guidelines)3,M ReferenceNo. T-43 10,Hazleton LaboratoriesAmerica, Inc.,StudyNo. 90300747, June 16, 1989. 65) FinalReport,Primary Eye Irritation/CorrosiSotnudy inRabbits(OECD Guidelines),3M ReferenceNo. T-43 10,Hazleton LaboratoriesAmerica, Inc., Study No. 90300749, June 21, 1989. 66) FinalReport,Primary Dermal IrritatioDICorrosiSotnudy inRabbits(OECD Guidelines),3M ReferenceNo. T-43 10,Hazleton LaboratoriesAmerica, Inc., Study No. 903 00748, June 27, 1989. 67) FinalReport,Acute OralToxicityStudy inRats (OECD Guidelines)3,M ReferenceNo. T-431 1,Hazleton LaboratoriesAmerica, Inc.,StudyNo. 90300750, June 27, 1989. 68) FinalReport,Primary Eye Irritation/CorrosiSotnudy inRabbits(OECD Guidelines),3M ReferenceNo. T-431 1,Hazleton LaboratoriesAmerica, Inc., Study No. 90300752, June 21, 1989. 69) FinalReport,Primary Dermal Irritation/CorrosiSotnudy inRabbits(OECD Guidelines),3M ReferenceNo. T-43 11,Hazleton LaboratoriesAmerica, Inc., Study No. 903 0075 1,June 27, 1989. 70) FinalReport,Acute OralToxicityStudy inRats (OECD Guidelines)3,M ReferenceNo. T-5177, Hazleton LaboratoriesAmerica, Inc.,StudyNo. 00401930, May 30, 1990. 71) FinalReport,Primary Eye Initation/CorrosiSotnudy inRabbits(OECD Guidelines),3M ReferenceNo. T-5177, HazletonLaboratoriesAmerica, Inc., Study No. 0040193 2,May 3 1,1990. 72) FinalReport,Primary Dermal Irritation/CorrosiSotnudy inRabbits-(OECD Guidelines),3M ReferenceNo. T-5177, HazletonLaboratoriesAmerica, Inc., Study No. 0040193 1,May 31, 1990. 73) FinalReport,Acute OralToxicityStudy of T-5292 inRats (OECD Guidelines), HazletonWisconsin,StudyNo. 0 1102298,Jan.4, 1991. 74) FinalReport,Primary Eye Irritation/CorrosiSotnudy ofT-5292 inRabbits (OECD Guidelines)H,azleton Wisconsin,Study No. 01102301, Jan.17,1991. AttachmenttsoLettertoC.AuerdatedJune28,2000 ToxicologiSctauldieasnd OtherRelevant InformatioonnPFOS Mixtures 75) FinalReport,PrimaryDermal Irritation/CorrosSitoundyofT-5292 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 01102300,Dec. 27, 1990. 76) FinalReport,Acute Dermal ToxicityStudyofT-5292 inRabbits(OECD Guidelines)H,azeltonWisconsin,StudyNo. 0 1102299,Jan.14,199 1. 77) FinalReport,Acute OralToxicityStudyofT-5293 inRats(OECD Guidelines), Hazleton Wisconsin,Study No. 0 1102302,Jan.4, 1991. 78) FinalReport,PrimaryEye Irritation/CorrosSitoundyofT-5293 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 0 1102305,Jan.25, 1991. 79) FinalReport,PrimaryDermal Irritation/CorrosSitoundy ofT-5293 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 01102304,Dec. 27, 1990. 80) FinalReport,AcuteDermal ToxicityStudyofT-5293 inRabbits(OECD Guidelines)H,azeltonWisconsin,StudyNo. 01102303, Jan.14,1991. 81) FinalReport,Ac@te OralToxicityStudy ofT-5454 inRats (OECD Guidelines), HazletonWisconsin,Study No. 11103 011,Jan.15,1992. 82) FinalReport,PrimaryEye Irritation/CorrosSitoundyofT-5454 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 11103013,Jan.10,1992. 83) FinalReport,PrimaryDermal Irritation/CorrosSitoundyofT-5454 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 11103012,Jan.10,1992. 84) FinalReport,Acute OralToxicityStudyofT-5508 inRats(OECD Guidelines), HazletonWisconsin,StudyNo. 20203 02 1,Apr. 16,1992. 85) FinalReport,PrimaryEye Irritation/CorrosSitoundy ofT-5508 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 20203023,May 21, 1992. 86) FinalReport,PrimaryDermal Irritation/CorrosSitoundy ofT-5508 inRabbits (OECD Guidelines)H,azletonWisconsin,StudyNo. 20203022,Apr. 22, 1992. 97) FinalRepor@ Acute OralToxicityStudy ofT-5595 inRats(OECD Guidelines), HazletonWisconsin,StudyNo. 40102083, Apr. 13,1994. AttachmenttsoLettetroC.A uerdii'edJune28,2000 ToxicologicSatludiesand OtherRelevant Informationon PFOS Mixtures 88) FinalRepor@ Primary Eye Initation/CorrosioSntudy of T-5595 inRabbits (OECD Guidelines)H,azleton Wisconsin,Study No. 40102086, Apr. 7, 1994. 89) FinalReport,Primary Dermal Irritation/CorrosiSotnudy of T-5595 inRabbits (OECD Guidelines)H,azleton Wisconsin,Study No. 40102085, Mar. 23, 1994. 90) FinalReport,Acute Dermal ToxicityStudy of T-5595 inRabbits(OECD Guidelines)H,azeltonWisconsin, StudyNo. 40102084, Apr. 22, 1994. 91) FinalReport,Acute OralToxicityStudy of T-5678 inRats (OECD Guidelines), Hazleton Wisconsin,Study No. 30102536, Apr. 7, 1993. 92) FinalReport,Primary Eye Irritation/CorrosiSotnudy of T-5678 inRabbits (OECD Guidelines)H,azleton Wisconsin,StudyNo. 3010253 8,Mar. 16, 1993. 93) FinalReport,Primary Dermal Irritation/CorrosiSotnudy ofT-5678 inRabbits (OECD Guidelines)H,azleton Wisconsin,StudyNo. 30102537, Mar. 16,1993. 94) FinalReport,AcxiteOralToxicityStudy of T-5738 inRats (OECD Guidelines), Hazleton Wisconsin,Study No. 31202778, Mar. 14, 1994. 95) FinalReport,Primary Eye Irritation/CorrosiSotnudy of T-5 738 inRabbits (01@CD Guidelines)H,azleton Wisconsin,StudyNo. 3 1202780, Apr. 1,1994. 96) FinalReport,Primary Dermal Irritation/CorrosiSotnudy ofT-573 8 inRabbits (OECD Guidelines)H,azletonWisconsin, StudyNo. 31202779, Mar. 21, 1994. 97) FinalReport,Acute OralToxicityStudy ofT-5739 inRats (OECD Guidelines), Hazleton Wisconsin, Study No. 3 120278 1,Mar. 11,1994. 98) FinalReport,Primary Eye Irritation/CorrosiSotnudy of T-573 9 inRabbits (OECD Guidelines)H,azletonWisconsin, StudyNo. 31202783, Apr. 13,1994. 99) FinalReport,Primary Dermal Irritation/CorrosiSotnudy of T-5739 inRabbits (OECD Guidelines)H,azletonWisconsin, StudyNo. 31202782, Mar. 23, 1994. 100) FinalReport,AcuteOralToxicitSytudyofT-5801inRats(OECD Guidelines), Hazleton Wisconsin,Study No. 31202784, Mar. 14, 1994. Attachments to Letterto C Auer dated June 28,2000 ToxicologicalStudiesand Other Relevant Information on PFOS Mixtures 101) FinalReport,PrimaryEye Irritation/CorrosSitoundy ofT-5801 inRabbits (OECD Guidelines)H,azleton Wisconsin,Study No. 31202786, Apr. 8, 1994. 102) FinalReport,Primary Dermal Irritation/CorrosiSotnudy ofT-5801 inRabbits (OECD Guidelines)H,azleton Wisconsin,StudyNo. 3 120278 5,Mar. 23, 1994. 103) FinalReport,Primary Eye Irritation/CorrosiSotnudy of T-6016 inRabbits (OECD Guidelines)H,azletonWisconsin, StudyNo. HWI 40901956, Dec. 2, 1994. 104) FinalReport,Acute Dermal ToxicityStudy inRabbits,3M ReferenceNo. T6076, Stillmeadow Inc.,Study No. 1635-94 Jan.5, 1995. 105) FinalReport,Primary Eye IrritatioSntudy inRabbits,3M ReferenceNo. T-6076, Stillmeadow Inc.,Study No. 1636-94,Jan.3, 1995. 106) FinalReport,Primary Dermal IrritatioSntudy inRabbits,3M ReferenceNo. T6076, Stillmeadow Inc.,Study No. 1637-94,Jan.5, 1995. 107) FinalReport,Acute Oral ToxicityinRats,3M ReferenceNo. T-6076, Stillmeadow Inc.,StudyNo. 1634-94,Dec. 21, 1994. 108) FinalReport,Assessment of Acute Oral Toxicitywith T-6587 intheRat, NOTOX, ProjectNo. 180811, Sept.14, 1996. 109) FinalReport,Acute Eye Irritation/CorrosiSotnudy with T-65@7 intheRabbit, NOTOX, ProjectNo. 180833, Sept.14, 1996. 110) FinalReport,Primary Skin Irritation/CorrosiSotnudy with T-6587 intheRabbit (4-hourSemi-OcclusiveApplication)N,OTOY,..,ProjectNo. 180822, Sept.14, 1996. 111) FinalReport,Primary Eye Irritation/CorrosiSotnudy of T-6650 inRabbits (OECD Guidelines)C,ovance LaboratoriesInc.,ProjectNo. 70405313, June 19, 1997. 112) FinalReport,Primary Dermal Irritation/CorrosiSotnudy of T-6650 inRabbits (OECD Guidelines)C,ovance LaboratoriesInc.,ProjectNo. 70405312, June 19, 1997. AttachmentstoLettertoC.Auer datedJune 28,2000 ToxicologicSatludiesand OtherRelevant Informatioonn PFOS Mixtures 113) FinalReport,Dermal SensitizatioSntudy of T-6650 inGuinea Pigs Maximization Test (EC Guidelines)C,ovanc'e LaboratoriesInc.,ProjectNo. 70405314, July24, 1997. 114) FinalReport,Acute OralToxicityStudy of T-6650 inRats (OECD Guidelines), Coming Hazleton Inc.,ProjectNo. CHW 60903120, Dec. 17, 1996. 115) FinalReport,Primary Eye Irritation/CorrosiSotnudy ofT-7130.1 inRabbits (OECD Guidelines)C,ovance LaboratoriesInc.,ProjectNo. 90300106,May 11, 1999. 116) FinalReport,Primary Eye Irritation/CorrosiSotnudy of T-713 1.1inRabbits (OECD Guidelines)C,ovance LaboratoriesInc.,ProjectNo. 90300107, Apr. 29, 1999. 117) FinalReport,Dermal SensitizatioSntudy.qfT-5679 in Guinea Pigs Maximization Test (EC Guidelines)H,azeltonWisconsin,ProjectNo. 212022562, Mar. 29, 1993. 118) FinalRepor@ Dermal SensitizatioSntudy of T-5680 in Guinea PigsMaximization Test (EC Guidelines)H,azeltonWisconsin,ProjectNo. 212022563, Mar. 29, 1993. 119) FinalReport,Dermal SensitizatioSntudy of T-5681 inGuinea Pigs Maximization Test (EC Guidelines)H,azeltonWisconsin,ProjectNo. 212022564, Mar. 29, 1993. 120) FinalReport,Acute OralToxicity,Acute Dermal Toxicity,PrimaryDermal Toxicity,Primary Eye Irritatio3nM, ReferenceNo. T-3 65 1,Hazelton LaboratoriesAmerica, Inc.,Dec. 3, 1984. 121) FinalReport,Primary Eye IrritatioSntudy inRabbits,3M ReferenceNo. T-4026, Hazelton LaboratoriesAmerica, Inc.,Mar. 2, 1987. 122) FinalReport,Primary Dermal IrritatioSntudy inRabbits,3M ReferenceNo. T4026, Hazelton LaboratoriesAmerica, Inc.,Mar. 6, 1987. 123) FinalRepor@ Primary Oral ToxicityStudy inRats,3M ReferenceNo. T-4026, Hazelton LaboratoriesAmerica, Inc.,Mar. 24, 1987. Attachments to Letterto C Auer dated June 28,2000 ToxicologicalStudiesand Other Relevant information on PFOS Mixtures 124) FinalReport,Acute OcularIrritatiToenstwithT-2849CoC in AlbinoRabbits, Riker LaboratoriesI,nc.,Study No. 0880EB0165, Apr. 7,1980. 125) FinalReport,Primary Skin IrritatioTnestwith T-2849CoC inAlbino Rabbits, Riker LaboratoriesI,nc.,Study No. 0880EB0166, Apr. 16, 1980. 126) FinalReport,Acute OralToxicityScreenwith T-2849CoC inAlbino Rats,Riker Laboratories,Inc.,Study No. 0880EBO 167,May 1,1980. Pre-1976 Studies(biblioi!raphoynly) 127) Report toMinnesota Mining and Manufacturing Company, Acute Toxicity Studieson FC- 194,Lot 3,Acute Oral Toxicity- Albino Rats,Eye IrritatioTnest - AlbinoRabbits,Eye IrritatioTnest- Albino Rabbits,3M ReferenceNo. T4933, IndustriaBlio-TestLaboratoriesI,nc.,Feb. 14, 1966. 128) Report toMinnesota Mining and Manufacturing Company, Acute Toxicity Studieson L-2265, Acute OralToxicity- Albino Rats,Eye IrritatioSntudy Albino Rabbits,SkinIrritatioSntudy - Albino Rabbits,3M ReferenceNo. T493 6,FC- 195,LifestreamLaboratories,ProjectNo. 1264, July7, 1969. 129) 130) Report toMinnesota Mining and Manufacturing Company, Acute Toxicity Studieson L-2542, Lot 2,Acute Oral Toxicity- Albino Rats,Eye IrritatioSntudy - AlbinoRabbits,SkinIrritatioSntudy - Albino Rabbits,3M ReferenceNo. T493 9,FC- 196,LifestreamLaboratories,ProjectNo. 1369,Jan.27, 1970. i Report toMinnesota Mining and Manufacturing Company, Acute Toxicity Studieson L- 1872,Acute Oral Toxicity- AlbinoRats,Eye IrritatioSntudy Albino Rabbits,Skin IrritatioSntudy - Albino Rabbits,3M ReferenceNo. T5022,LifestreamLaboratoriesP,rojectNo. 763,Apr. 1, 1968. 131) FinalReport,Acute OralToxicity- Rats,3M ReferenceNo. T-289,Biosearcb, Inc.,Feb. 24, 1971. 132) FinalReport,Primary Skin IrritatioSntudy- Rabbits,3M ReferenceNo. T-36 1, Biosear-chI,nc.,Study No. Dec. 9, 197 1. 133) FinalReport,Primary Eye IrritatioSntudy - Rabbits,3M Reference No. T-3 6 1, Biosearch,Inc.,Dec. 9, 1971. AttachmenttsoLettetroC.AuerdatedJune28,2000 ToxicologiSctauldieasndOtherRelevant InformatioonnPFOS Mixtures 134) FinaRleportA,cuteOralToxici-tRyats,3M ReferencNeo.T-361B,iosearch, Inc.,StudyNo. Dec. 9, 1971. 135) FinalReport,PrimarySkinIrritatiSotnudy- Rabbits,3M ReferenceNo. T-567, Biosearch,Inc.,Feb. 18,1974. 136) FinalReport,PrimaryEye IrritatiSotnudy- Rabbits,3M ReferenceNo. T-567, Biosearch,Inc.,Study No. Feb. 18, 1974. 137) FinalReport,Acute OralToxicity- Rats,3M ReferenceNo. T-567,Biosearch, Inc.,Feb. 18,1974. 138) Report,OralLDio, 3M ReferenceNo. T-676,WARF InstitutIenc.,Project No. 3070098, July2, 1973. 139) Report,Eye IrritatiSotnudy,3M ReferenceNo. T-676,WARF InstitutIenc., ProjectNo. 3070098, July2, 1973. 140) Report,SkinIrrititiSotnudy,3M ReferenceNo. T-676,WARF InstitutIenc., ProjectNo. 3070098, July2, 1973. 141) Report,OralLD5o, 3M ReferenceNo. T-1049,WARF InstitutIenc.P,roject - No. 4071932, Aug. 1, 1974. - 142) Report,Eye IrritatiSotnudy,3M ReferenceNo. T-1049,WARF 1 InstitutIenc., ProjectNo. 4071932, Aug. 1,1974. 143) Report,SkinIrritatiSotnudy,3M ReferenceNo. T-1049,WARF InstitutIenc., ProjectNo. 4071932, Aug. 1,1974. 144) Report,Acute OralLD50, 3M Reference No. T- 1118,WARF InstitutIenc., ProjectNo. 4102872,Nov. 20, 1974. 145) Report,Eye IrritatiSotnudy,3M ReferenceNo. T-1118,WARE InstitutIenc., ProjectNo. 4102872,Nov. 20, 1974. 146) Report,gldnIrritatiSotnudy,3M ReferenceNo. T-1119,WARP InstitutIenc., ProjectNo. 4102872,Nov. 20, 1974. Attachments to Letterto C. Auer dated June 28,2000 ToxicologicalStudiesand Other Relevant Information on PFOS Mixtures 147) Report,Acute OralLD50 (male& female),3.M ReferenceNo. T-1207,WARF InstitutIenc.,ProjectNo. 503 0800, Apr. 11, 1975. 148) Repor@ Eye IrritatioSntudy,3M ReferenceNo. T-1207, WARF InstitutIenc., ProjectNo. 5030800, Apr. 11, 1975. 149) Report,Skin IrritatioSntudy,3M ReferenceNo. T-1207, WARF InstitutIenc., ProjectNo. 5030800, Apr. 11, 1975. 150) FinalReport,Primary Skin IrritatioSntudy - Rabbits,3M ReferenceNo. T-1328, Biosearch,Inc.,Oct.6. 1975. 151) FinalReport,Primary Eye IrritatioSntudy - Rabbits,3M ReferenceNo. T-1328, Biosearch,Inc.,StudyNo. Oct.6, 1975. 152) FinalReport,Acute Oral Toxicity- Rats.R-eferenceNo. T-1328,Biosearch,Inc., Study No. Oct.6, 1975 153) FinalReport,Primary Skin IrritatioSntudy,3M ReferenceNo. T-269, Biosearch, Inc.,Oct. 1,1970. 154) FinalReport,Primary Eye IrritatioSntudy,3M ReferenceNo. T-269, Biosearch, Inc.,Oct. 1,1970. Attachments toLetterto C. Auer dated June 28,2000 ToxicologicaSltudiesand Other Relevant Informationon PFOS Mixtures Genotoxicity 1) FinalReportI,nVitrMoicrobiologiMcuatlageniciAtsysaysofThree3M Company Compounds, 3M ReferenceNos. T-213 6 [FC-206],T-213 8,T-2140, SRI InternationaPlr,ojectNo. LSC 4442-16,Apr. 1978. 2) FinalRepor@ InVitroMicrobiologicaMlutagenicityAssays of3M Company's Compound T-365 1,SRI InternationaPlr,ojectNo. LSC-3145, Feb. 1985. PFOS Mixtures FC-1 85F Acronyms: cc8l7-19,Lab Request Number: 7544 Physical/ChemicaPlroperties Title None available Laboratoryor Completion Author Date Type EnvironmentalFateand Transport Title Ready biodegradabiloiftFyC-185F (BOD/COD) Laboratory or Author 3M Env.Lab Completion Date 2/24/82 Type Robustsummary, laboratordyata summary EcotoxicitEylements Title AquaticToxicitTyesgng: FC-185F (cc8l7-19L)1-2303LR 7544 (FatheadMinnow) Laboratory or Author 3M Env.Lab Acute toxicitoyfFC-185F toactivatesdludgemixedliquor 3M Env.Lab Completion Date 2/l/82 1/28/82 Type Robustsummary, technicarleport summary Robustsummary, copiesofdata sheets FC-200 Summary Reports Title Laboratory or Author Completion Date Summary foswork perrormedfortheGerman Government Agency forMilitarTyechnologyand Procurementon fire lextinguishifnogam compounds frommultiplceompanies Dr.H. Hellmann,D. Muller 10/12/77, 3/7/80 Type Robustsummary, Technical Awareness Report,finarleport FC-201 Acronyms: Lab Request Number: 2563 Physical/ChemicaPlropordes Title None available EnvironmentalFateand Transport Title Ready biodegradabiloiftFyC-201 (BOD/COD) EcotoxicitEylements TFitle Laboratory or Completion Author Date Type Laboratory or Author 3M Env.Lab Completion Date 1128/75 Type Robustsummary, copiesofdata. summary sheets Laboratory or Au Completion Date Type lacute statictoxicitoyfFC-201 tofatheadminnow 3M Env.Lab 1/11/75 Robust summary, copiesofdata sheets FC-201AF Acronyms: Lab Request Numbers: N3281, N3747, L-13652 Physical/Chemical Properties N2964, Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabilitoyfFC-201AF (BOD/COD) Ready biodegradabilitoyfFC-201AF (BODICOD) Laboratory or Author MDS Environmental ServicesLimited, London, Ontario, Canada Pace Analytical Services,Golden Valley,MN Completion Date 5124195 2/6/96 Type Robust summary, summary report Robust summary, laboratory summary report,copies ofdata sheets EcotoxicityElements Title Acute staticrenewal toxicitoyf FC-201 AF tofathead minnow Acute toxicitoyf FC-201AF to green algae,Selenastrum capricomutum Growth InhibitioTnest with the Marine Alga Skeletonema costatum - FC-201 AF LightWater Brand AFFF Acute ToxicityTest with the Marine Copepod Acartiatonsa FC-201 AF LightWater Brand AFFF Acute ToxicitySediment Test withtheMarine Amphipod Corophium volutator- FC-201 AF LightWater Brand AFFF Laboratory or Author 3M Env. Lab 3M Env. Lab RF Rogaland Research, Stavanger,Norway RF Rogaland Research, Stavanger, Norway RF Rogaland Research, Stavanger, Norway Acute stabctoxicitoyfFC-201AF toDaphnia magna Acute toxicitoyf FC-201AF toMicrotax 3M Env. Lab 3M Env. Lab lacute toxicitoyf FC-201AF toactivatedsludge mixed liquor 3M Env. Lab Completion Date 10/20195 1/7/96 115/00 115/00 1/5/00 8131/95 1212195 9114/95 Type Robust summary, copies ofdata sheets Robust summary, copies of data sheets Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Robust summary, copy ofdata sheet Robust summary, laboratory report,copies ofdata sheets Robust summary, copies of datei-@ sheets FC-201F Acronyms: Lab Request Number: K1792 Physical/Chemical Properties Title None available Laboratory or Author Completion Date Type 2 EnvironmentalFateand Transport Title ,Ready biodegradabilitoyfFC-201 F (BOD/COD) Laboratoroyr Completion Author Date Hygiene Institutfeor the Ruhr District, Gelsenkirchen, Germany 9113/93 Type Robust summary, English language summary, German language report EcotoxicityElements Title Acute Toxicityof FC-201 F to Fathead Minnow (Pimephales promelas) FurtherInvestigatioonn the Acute Toxicityof FC-201 F to Fathead Minnow (Pimephales promelas) Acute Toxicityof FC-201 F to Daphnia magna Laboratoryor Author Ascl Corporation, Duluth,MN Asci Corporation, Duluth,MN Asci Corporabon, Duluth,MN Completion Date 8/24/92 10/5/92 8/21/92 Type Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Microbialinhibitio(ndehydrogenase activityo)fFC-201 F Hygiene Institutfeor the Ruhr District, Gelsenkirchen,' Germany 9/13/93 Robust summary, English language summary, German language report lacutetoxicittyofish(Leuciscusidus) Hygiene Institutfeor the Ruhr District, Gelsenkirchen, Germany 1 9/13/93 Robust summary, English language summary, German 1 language report FC-201 F-X Acronyms: Lab Request Number: Kl 126 PhysicaUChomical Properfies Title None available Laboratoryor Completion Author Date Type Environmental Fate and Transport Title Ready biodegradabilitoyfFC-201 F-X (BOD/COD) Laboratoryor Author Pace Incorporated, Minneapolis,MN Completion Date 2/17/92 Type Robust summary, laboratory summary report EcotaxicityElements Title Laboratoryor Author Acute toxicitoyf FC-201 F-X to Microtox 3M Env. Lab lacute toxicitoyfFC-201 F-X toactivatedsludgemixed liquol 3M Env. Lab Completion Date 4/17/92 3/23/92 Type Robust summary, copies ofdata sh eets Robust summary, copies ofdata sheets 3 FC-203 Acronyms: VWI 60390, Sample #5729, Sample 7902, 3M Sample B, Lab Request Numbers 1940,2002,2009,2034,2036,2093,2103, 4971, 4971 S, 5360A, 5541 S, 8483, 9611, H2864-9, J1608-8, J2176-5 Physical/Chemical Properges Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Summary of biodegradabilittyestsof FC-203 (BOD/COD) Laboratoryor Author 3M Env. Lab Completion Date 1973-1980 Type Robust summary, copies of data sheets OECD Biodegradation Testing on FC-600 and FC-203 3M Env. Lab Repeat OECD Biodegradation Test on FC-600 and FC-203 3M Env. Lab Modified OECD FC-600 Screening Test on FC-203, FC-203A, and Ready biodegradabilitoyf FC-203 (BOD/COD) 3M Env. Lab Pace Incorporated, Minneapolis, MN 4118/83 6/16/83 7/9/84 8/13/91 Robust summary, Technical Report Summary Robust summary, Technical Report Summary. Robust summary, Technical Report Summary, selected copies of data sheets Robust summary, finalreport Ecotaxicity Elements Title Laboratoryor Author Completion Date Acute toxicitoyf FC-203 to rainbow trout ute toxicitoyf LightWater" to bluegil(lLel2omis macmc-w U"S 3M Env. Lab Bionomics, Inc. Wareham, MA Unknown September, 1972 Summary of acute statictoxicittyestsof FC-203 to bluegill Acute Toxicityof3M Samples (A and B) to the Water Flea (Dapbnia magna and Scud (Gammarus fas6iatus - robust summary forDaphnia magna Acute Toxicityof3M Samples (A and B) to the Water Flea (Dgp@ magna and Scud (Gammarus fasciatus - robust summary forGammatus fasciatus summary of microbialinhibitio(ndehydrogenase activity) testson FC-203 AlgicidafActivityof Two Samples Labeled "A" and "B" 3M Env. Lab Bionomics, Inc. Wareham, MA Bionomics, Inc. Wareham, MA 3M Env. Lab IndustrialBio-Test Laboratories. Northbrook, IL 1973-1974 December, 1973 December, 1973 - 1973-1974 1/23/74 lacute statictoxicitoyf FC-203 to rainbow trout 3M Env. Lab 2/23174 Type Robust summary, copy of data sheet Robust summary, finalreport Robust summary, copies of data - sheets Robust summary, finalreport Robust summary, finalreport Robust summary, copies of data sheets Robust summary, finalreport Robust summary, copies of data sheets 4 Acute toxicitoyf3M Company's sample 7902 tograss shrimp (a-al-a-emo-net-pegs-Q@loj EG&G Bionomics Marine Research Laboratory, Pensacola, FL Acute Toxicityof7902 totheCommon Mummichog (fundulvseterocli=) EG&G Bionomics Marine Research Laboratory, Pensacola, FL Acute Toxicityof3M Company's Sample 7902 toembryoslarvaeofeasternoysters(CLa-aaQA=YiL@ EG&G Bionomics Marine Research Laboratory, Pensacola, FL Acute toxicitoyfSample #5729 toembryo-larvaeofeastern oysters(glassoalLr--aemaim@, EG&G Bionomics Marine Research Laboratory, Pensacola, FL StaticAcute Toxicityof FC 203 to theAlga,Selenastrum capticomutum Acute toxicitoyfFC-203 withoutTolybrazole(VWI 60390) to Microtox EnviroSystems DivisionResource Analysts,Inc., Hampton, NH 3M Env. Lab StaticAcute Toxicityof FC 203 to the Daphnid,Dal?hnia magna Acute ToxicitySediment Test withthe Marine Amphipod Corophium volutator EnviroSystems DivisionResource Analysts,Inc., Hampton, NH RF Rogaland Research, Stavanger, Norway Acute ToxicityTest withthe Marine Copepod Acartiatonsa RF Rogaland Research, Stavanger, Norway Growth InhibitioTnest withthe Marine Alga Skeletonema costatum RF Rogaland Research, Stavanger, Norway August, 1979 Robust summary, finalreport August, 1979 Robusts-ummary, finalreport August, 1979 Robust summary, finalreport July,1980 Robust summary, finalreport June,1991 7/19/91 Robust summary, finalreport Robust summary, summary sheet,', copies ofdata sheets 8/9/91 1/6100 1/6/00 1/6/00 Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Summary Reports Title Laboratoryor Completion Author Date Investigationosftoxiceffectsand biologicadlegradabilitoyf foam extinguishingagents inthewaste water EnvironmentalEffectsofLIGHT WATER Brand AFFF and Components - Robust summary forFC-203 EnvironmentalEffectsofLIGHT WATER Brand AFFF and Components - Robust summary forVWI 60390 (FC-203 withouttolyltriazole Ekkehard lsing 3M Env. Lab 3M Env. Lab 3/29/90 411/91 4/l/91 Type Abbreviated robustsummary, summary reportfrom German Army Robust summary, Technical Report Summary Robust summary, Technical Report Summary FC-203A Acronyms: FC-203 NF,.Lab Request Numbers: 2543, 2563, 9611, Physical/Chemical Properties 5 Title None available Laboratory or Completion Author Date Type EnvironmentalFate and Transport Title Ready biodegradabiliotfyFC-203A (BOD/COD) degradationof"LightWatee'ProductsinOECD Test - 6/80 EffectofBiodegradatioonn Foaming of"LightWater" Products. ModifiedOECD ScreeningTestof FC-203,FC-203A, and FC-600 Laboratory or Author 3M Env. Lab Completion Date 1/28175 3M Env. Lab 6/30180 3M Env. Lab 8/6/80 3M Env. Lab 7/9/84 Type Robust summary, datasummary. pages Robust summary, Technical ReportSummary Robust summary, lettereport, copiesofdata sheets Robust summary, Technical ReportSummary EcatoxicityElements Title Acute toxicitoyfFC-203A tofatheadminnow Laboratory or Author Completion Date 3M Env. Lab 1111/75 Type Robust summary, copy ofraw data FC-203C Acronyms: L-5440, 81-1/8 Lab Request Numbers; 6811 S, 7038, 7736, 7737, 7738, 7903,7625 Physical/ChemicalProperties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabili(tByOD/COD) ofFC-203C Laboratory or Author Numerous Completion Date 1981-1982 Type Robust summary ofseveral studiesc,opiesofdata sheets EcotoxicitEylements Title Acute Toxicitoyf81-1/8toFathead Minnow (Pimephales 2 Lom e La-2) Acute Toxicitoyfa SurfactanStolution(81-1/8t)othe Mummichog Fundulusheteroclituisna Flow-through System. Laboratory or Author EG&G Bionomics, Wareham, MA EG&G Bionomics' Marine research Laboratory, Pensacola,FL Completion Date October,1981 October,1981 AlgalAssay: BottleTest(AA:BT),ToxicitTyestingFC-203C 3M Env. Lab 6/12/81 Acute toxicitoyf FC-203C toDaphnia magna 3M Env. Lab 7/6181 Type Robust summary, finalreport Robust summary, finalreport Robust summary, Technical Report Summary Robust summary, datasummary 6 Acute toxicitoyf FC-203C toactivatedsludge mixed liquor 3M Env. Lab 71 1/81 Robust summary, copies ofdata sheets FC-203CE Acronyms: Lab Request Numbers: H1480-1, H1480-3, J1884-1 PhysiceitChomicalProperties G1358-1, Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) & TOC ofFG-203CE Ready biodegradabili(tOyECD 301E) ofFC-203CE-T Laboratory or Author Completion Date Type Pace Laboratories, lnc,.Minneapolis,M 3M Env.Lab 5/12189 Robust summary, finalreport -7bust 6/23/89 summary, copiesofdata sheets EcataxicityElements Title Laboratory or Author Acute statictoxicitoyf FC-203CE toDaphnia magna' Acute stafic-renewatloxicitoyfFC-203CE tofathead minnow Acute toxicitoyf FC-203CE to green algae,Selenastrum capricomutum ToxicityofFC-203CE to activatedsludge mixed liquor 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab ToxicityofFC-203CE toMicrotox 3M Env. Lab Toxicityof FC-203CE Toxicityof FC-203CE mixed liquor toactivatedsludge mixed liquor + andfoamer to activatedsludge 3M Env. Lab 3M Env. Lab StaticAcute ToxicityofFC-203CE tothe Daphnid,Daphnia magna EnviroSystems DivisionResource Analysts,Inc., Hampton, NH StaticAcute Toxicityof FC-203CE capticomutum EnviroSystems DivisionResource to theAlga,Selenastrum Analysts,Inc., I Hampton, NH Completion Date 5/13/89 5/15/89 5/28/89 6/16/89 3/19/90 3/19/90 June, 1991 July,1991 Type Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, copy of data sheets Robust summary, finalreport Robust summary, finalreport Summary Reports Title EnvironmentalEffectsofLIGHT WATER Brand AFFF and components - Robust summary forFC-203CE Laboratory or Author 3M Env. Lab Completion Date 4/l/91 Type Robust summary, Technical Report Summary 7 FC-203CF Acronyms: FC-203CF-X, Lab Request Numbers: J1884-3,J1885-1, K1905-1,N2977, Wl 127, Physical/Chemical Properties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabiliotfy FC-203CF (BOD/COD) Laboratory or Author Pace Incorporated, Minneapolis,MN Completion Date 7/2/91 Type Robust summary, finalreport EcotoxicityElements Title Stabc Acute ToxicityofFC-203CF totheFathead Minnow, Pimephales promelas StaticAcute ToxicityofFC-203CF tothe Daphnid, Daphnia magna Laboratory or Author EnviroSystems DivisionResource Analysts,Inc. Hampton, NH' EnviroSystems DivisionResource Analysts,Inc. Hampton, NH Completion Date June, 1991 July,1991 Acute toxicitoyfFC-203CF toMicrotox Stabc Acute Toxicityof FC-203CF to theAlga,Selenastrum capticomutum Acute toxicitoyfFC-203CF-X toactvated sludge mixed liquor Acute toxicitoyfFC-203CF-X tonitrifyibnagcteria(ISOIDIS Method 9509) Acute toxicitoyfFC-203GF-A tonitrityibnagcteria (NitroseedTmMethod) Acute ToxicityofFC-203CF to Fathead Minnow (Pimephales promelas) 3M Env. Lab EnviroSystems DivisionResource Analysts,Inc. Hampton, NH 3M Env. Lab 3M Env. Lab 3M Env. Lab ASci Corporation, Duluth,MN 7119/91 August, 1991 6/26/92 8/24195 8124195 2122199 Type Robust summary, finalreport Robust summary, finalreport Robust summary, copiesofdata sheets Robust summary, finalreport Robust summary, copies ofdata sheets Robust summary, copiesofdata sheets Robust summary, copiesofdata sheets Robust summary, finalreport FC-203FC Acronyms: Lab Request Number: Rl 335 Physical/ChemicalProperties Title None available Environmental Fate and Transport ititle Laboratory or Author Completion Date Laboratory or 'A Completion Date Type Type 8 Rl 335 BOD Report for3M Company AScl Corporation, Duluth,Mn September, 1997 Robust summary, finalreport EcotoxicityElements Title ToxicityofFC-203FC toMicrotox ToxicityofFC-203FC toactivatedsludge mixed liquor AcuteToxiciotfyRl335 toDaphniamagna GrowthinhibitioofnR1335 forGreen Alga(Selenastrum r-apricomutum) AcutestatitcoxcityofFC-203FC tofatheadminnow Tc-uteToxicitoyfRl335 toFatheadMinnow (Pimephales promelas) Laboratory or Author Completion Date 3M Env. Lab 3117/97 3M Env. Lab ASci Corporation, DuluthM,N ASci Corporation, Duluth,MN 3/24/97 4/l/97 417/97 3M Env.Lab ASci Corporation, Duluth,MN 4118197 6/26/97 Type Robust summary, copies ofdata sheets Robustsummary, copiesofdata sheets Robustsummary, finarleport Robustsummary,finalreport Robustsummary, copiesofdata s eets Robustsummary,finalreport FC-203S Acronyms: Physical/ChemicaPlroperties Title None available EnvironmentalFateand Transport Title None available EcotoxicitEylements Title .AcutetoxicitoyfFC-203S toRainbow Trout Laboratory or Completion Author Date Type Laboratory or Completion Author Date Type Laboratory or Completion Author Date Type ABC Laboratories, Columbia,MO 12/2188 Robustsummary, summary letter, finarleportmissingfirs5tpages. FC-206 Acronyms: L3243, Sample C Number-. 2577 Physical/ChemicaPlroperties Lab Request Title None available EnvironmentalFate and Transport IT!tle Laboratoryor Author Completion Date Laboratory or I Completion Date I Type Type 9 Ready biodegradabilitoyfFC-206 (BOD/COD) 3M Env. Lab Ready biodegradabilitoyfFC-206 (BOD/COD) Biodegradationof "LIGHT WATER" Products inOECD 6/80 .Effectofdegradauon on foaming of FC-206 Test - 3M Env. Lab 3M Env. Lab 3M Env. Lab 1/16/75 6/30/76 6/30180 8/6180 Robust summary, results summary Robust summary, results summary Robust summary, Technical ReportSummary Robust summary, lettereport Ecotoxicity Elements Title Summary ofmicrobialinhibitio(ndehydrogenase actvity) testson FC-206 Laboratory or Author 3M Env. Lab Acute statictoxicitoyf FC-206 tofatheadminnow 3M Env. Lab Acute statictoxicitoyf FC-206 torainbow trout Acute ToxicityofSample C toMummichog (Fundulus heteroclitusG)r,ass Shrimp (Palaemonetes vula6risand FiddlerCrab (LLcapuciiiato-rRobust summary for mummichog Acute ToxicftyofSample C to Mummichog (Fundulus heteroclitu,sGrass Shrimp (Palaemonetes Yuloarisand FiddlerCrab (Ucg;?uailator- Robust summary forgrass shrimp Acute ToxicityofSample C to Mummichog (Fundulus heteroclitusG)r,ass Shrimp (Palaemonates vulaarisand FiddlerCrab (U-qapucillato-rRobust summary forfiddler crab Acute ToxicityofSample C toAtlantiOcyster (Crassostree ykginkg) Acute ToxicityofSample C toWater Flea(Daphni maan ) and Scud (Gimmarus fasciatus.- Robust summary for Daphnia magna Acute ToxicityofSample C toWater Flea(Daphni mean ) and Scud (Gammerus fasciatus.- Robust summary for Scud 3M Env. Lab Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Bionomics EG&G, Wareham, MA Acute statictoxicitoyf FC-206 tofathead minnow Acute statictoxicitoyf FC-206 amended tosoiltofathead minnow lacpte flow-throughtoxicitoyfFC-206 tobluegilslunfish 3M Env. Lab 3M Env. Lab 3M Env. Lab Completion -Date 1973-1974 2/15/74 4/5174 May, 1974 May, 1974 May, 1974 July,1974 August, 1974 August, 1974 6/19/76 11/6/76 11/11/78 Type Robust summary, copy ofdata sheet Robust summary, copies ofdata sheets Robust summary, copy ofdata sheet Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport Robust summary, copy ofdata sheet Robust summary, copiesof data sheets. Robust summary, copy of data shee Summary Reports Title Laboratory or Author investigationosftoxiceffectsand biologicadlegradabilitoyf foam extinguishingagents inthewaste water Ekkehard Ising Completion Date 3/29/90 Type Abbreviated robustsummary, summary reportfrom German Army Summary forwork performed fortheGerman Government Agency forMilitarTyechnology and Procurement on fire extinguishinfgoam compounds from multiplecompanies Dr.H. Hellmann, D. Robust summary, Technical Muller 10/12/77, 3/7/80 Awareness Report,finalreport 10 -7 FC-206A Acronyms: Physical/ChemicalProperties Title None available Laboratoryor Completion Author Date Type Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) of FC-206A Laboratoryor Author 3M Env. Lab Completion Date 11/10/78 Type Robust summary, copies ofdata sheets EcotoxicityElements Title FC-206A cc 785-22:Results ofAquatic 96-hr.LC50 Tests (bluegislulnfish)' Laboratoryor Author 3M Env. Lab Acute statictoxicitoyf FC-206A tofatheadminnow 3M Env. Lab Acute flow-throughtoxicitoyfFC-206A tofatheadminnow 3M Env. Lab Acute toxicitoyfFC-206A toDaphnia magna 3M Env. Lab Microbialinhibiotn (dehydrogenase activitoyf) Fc- 06A 3M Env. Lab Acute toxicitoyfFC-206A toactivatedsludgemixed liquor 3M Env. Lab Completion Date 11/2178 7114179 7/21/79 7/14179 11/29/79 818179 Type Robust summary, Technical Report Summary Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdatasheets FC-206C Acronyms:L-5439,81-2/8,Lab Request Numbers; 6812S, 7625,7736, 7737,7738, 7903, PhysicallChomicalProperties Title None available Environmental Fate and Transport Title Ready biodegradabili(tByOD/COD) of FC-206C Laboratoryor Completion Author Date Type 7@ 1 Laboratoryor Author Numerous Completion Date 1981-1982 Type Robust s. ummary ofseveral studies,copies ofdata sheets EcotoxicityElements Title Laboratoryor Author Acute toxicitoyfFC-206C toactivatedsludgemixed liquor 3M Env. Lab Completion Date 7/1181 Type Robust summary, copies ofdata sheets Acute Toxicityof81-2/8to Fathead Minnow (Pimephales alomelas) Acute Toxicityofa SurfactanfSolutiontotheMummichog (Fundulusheteroclituisna Flow-throughSystem. (FC206C) E(3&G Bionomics, Wareham, MA October, 1981 EG&G Bionomics, Pensacola, FL September, 1981 [AlgalAssay: BottleTest (AA:BT),ToxicityTestingFC-206d 3M Env. Lab 6/23181 Robust summary, finalreport Robust summary, finalreport Robust summary, Technical Report summary FC-206CE Acronyms: Lab Request Numberts: G1358-2, J1884-2, H1480-2, H1480-4 PhysicallChemical Properties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) of FC-206CE Ready biodegradabilit(yOECD 301 E) ofFC-.206CE Laboratory or Author Completion Date Type Pace Laboratories, Inc,Minneapolis,MN 3M Env. Lab 5/12189 6123/89 Robust summary, finalreport Robust summary, copies ofdata sheet EcotoxicityElements Title Acute statictoxicitoyfFC-206CE toDaphnia rnagna Laboratory or Author Completion Date 3M Env. Lab 416189 Acute statictoxicitoyfFC-206CE toDaphnia magna testatic-renewatloxicitoyrFC-206CE tofathead minnow Acute toxicitoyf FC-206CE togreen algae,Selenasttvm capticomutum 3M Env. Lab 3M Env. Lab 3M Env. Lab 5/13189 5/15/89 5/28/89 Acute toxicitoyf FC-206CE to Microtox 3M Env. Lab 6116189 Acute toxicitoyfFC-206CE to activatedsludgemixed liquor 3M Env. Lab 6123/89 Acute toxicitoyfFC-206CE ute toxicitoyfFC-206CE mixed liquor toactivatedsludgemixed liquor + antifoamertoactivatedsludge 3M Env. Lab 3M Env. Lab StaticAcute Toxicityof FC-206CE magna to the Daphnid, Daphnia EnviroSystems Divisionof Resource Analysts Inc., Hampton, NH StaticAcute Toxicityof FC-206CE capticomutum EnviroSystems Divisionof Resource to theAlga,Selenastrum Analysts Inc., Hampton, NH 3123/90 3/23/90 June, 1991 July,1991 Type Robust summary, copy of data sheet Robust summary, copies ofdata sheets Robust summary, copies ofdata" sheets Robust summary, copies ofdata sheets I.' Robust summary, copies ofdata' sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets . Fobust summary, copies of data_, sheets Robust summary, finalreport Robust summary, finalreport 12 Surnmery Reports Title Environmental EffectsofLIGHT WATER Brand AFFF and components - Robust summary forFC-206CE Laboratory or Author 3M Env. Lab Completion Date 4/1/91 Type Robust summary, Technical Report Summary FC-206CF Acronyms: FC-206CF-X Lab Request Numbers: J1884-4, J1885-2, K1905 Physical/ChemicaPlroperties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabilitoyf FC-206CF (BOD/COD) Laboratory or Author Pace Incorporated, Minneapolis,MN Completion Date 7/2191 Type Robust summary, finalreport EcotoxicityElements StaticAcute ToxicityofFC 206CF tothe Fathead Minnow, Pimephales promelas staticAcute Toxicityof FC-206CF to the Daphnid, Daphnia magna EnviroSystems DivisionResource Analysts,Inc., Hampton, NH EnviroSystems DivisionResource Analysts,Inc., Hampton, NH June, 1991 June, 1991 Acute toxicitoyfFC-206CF toMicrotox staticAcute Toxicityof FC 206CF to theAlga,Selenastrum capticomutum Acute toxicitoyfFC-206CF-X toactivatedsludge mixed liquor 3M Env. Lab EnviroSystems DivisionResource Analysts,.Inc., Hampton, NH 3M Env. Lab -1 7/19/91 August, 1991 6126/92 Robust summary, finalreport Robust summary, finalreport Robust summary, copies ofdata sheets Robust summary, finalreport Robust summary, copies ofdata isheets FC-600 Acronyms: 3M-1 Lab Request Numbers: 2874,8483,8873,8875,9063,9595, Physical/ChemicaPlroperties Title None available Environmental Fate and Transport Laboratory or Author Completion Date Type 13 Title isummary ofready biodegradabilitsytudieson FC-600 Laboratoryor Completion Author Date Type 3M Env. Lab 8/15/75,10/27/82, Abbreviated robustsummary,,-* 4/18183,7/9/84, copies ofdata sheets,Technical 10/4/88, Report Summaries Ecatoxicity Elements Title Acute statictoxicitoyfFC-600 tofatheadminnow Acute statictoxicitoyf FC-600 tobluegilslunfish Laboratoryor Author 3M Env. Lab 3M Env. Lab Completion Date 8129/75 8/29/75 Type Robust summary, copiesofdttasheets Robust summary, copiesofdata sheets Acute statictoxicitoyf FC-600 to Daphnia magna -firsotf 3 studiesofeffluentfrom an FC-600-exposed SCAS reactor Acute statictoxicitoyf FC-600 to Daphnia magna - second of3 studiesofeffluentfrom an FC-600-exposed SCAS reactor(treaterdeactorafter4-hours oftreatment) 3M Env.Lab 3M Env.Lab 8/10/77 Robust summary, copies ofdata sheets 8/10/77 Robust summary, copies ofdata sheets Acute statictoxicitoyf FC-600 to Daphnia magna -thirdof 3 studiesofeffluenftrom an FC-600-exposed SCAS reactor(blankcontrolreactorafter4-hoursof treatment) 3M Env. Lab Acute toxicitoyfFC-600 toactivatedsludge mixed liquor Acute toxicitoyfFC-600 (fromAntwerp,Belgium)to activatedsludge mixed liquor Range-findingstudy ofacute toxicitoyfFC-600 (US) to fathead minnow Range-findingstudy ofacute toxicitoyfFC-600 (Belgium)to fathead minnow Range-findingstudy ofacute toxicitoyfFC-600 (US) to fathead minnow Range-findingstudy ofacute toxicitoyfFC-600 (Belgium)to fathead minnow Dynamic Acute Toxicityof3M-1 to Fathead Minnows (EimeRL@LE -aplomelis) 3M Env.Lah 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab AnalyticaBlio- Chemistry Laboratories,Inc. Columbia, MO AquaticToxicityTesfing:FC-600 (Belgium-AFFF)LR 9595 3M Env. Lab 8/10/77 2/l/83 2/1/83 2/10/83 2/10/83 2/10/83 2/10/83 Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets Robust summary, copies ofdata sheets 3/29/83 7/21/83 Robust summary, finareport Robust summary, Technical Report Summary FX-601 Acronyms: Lab Request Number: B1684 PhysicaVChomical Properties Tftle None available Environmental Fate and Transport Labora.toroyr Completion Author Date Type 14 Title None avialble Laboratoryor Completion Author Date Type EcotoxicityElements Title Acute statictoxicitoyf FX-601 tofatheadminnow lacutetoxicitoyfFX-601 toactivatedsludge mixed liquor Laboratoryor Author 3M Env. Lab 3M Env. Lab Completion Date 6/15/84 6/20184 Type Robust summary, copies of data. sheets. Robust summary, copies of data sheets. FC-602 Acronyms: FC-602-X,FC-602-ATC, Lab Request Number: F 1151 Physical/Chemical Properties Title None available Laboratoryor Completion Author Date Type Environmental Fate and Transport Title ,Ready biodegradabilit(yBOD/COD) ofFC-602 Laboratoryor Completion Author Date Pace Laboratories, Inc.Minneapolis,MN 314/88 Type Robust summary, finalreport EcotoxicityElements Title Laboratoryor Author ToxicityofFC-602 to Microtox 3M Env. Lab Acute statictoxicitoyfFC-602-X toDaphnia magna 3M Env. Lab Acute statictoxicitoyfFC-602-X tofathead minnow Acute ToxicityTest with the Marine Copepod Acaiffatonsa (FC-602) Growth InhibitioTnest with the Marine Alga Skeletonema costatum FC-602) Acute ToxicitySediment Test withthe Marine Amphipod Corophium volutator(FC-602) 3M Env. Lab RF Rogaland Research, Stavanger,Norway RF Rogaland Research, Stavanger, Norway RF Rogaland Research, Stavanger, Norway Completion -Date 1/28/88 3/17/88 3/25/88 117100 117/00 - 117/00 Type Robust summary, copies ofdata i sheets Robust summary, copies ofdata sheets Robust summary, copies of data.,.. sheets Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport FC-603EF Acronyms: Lab RequestNumber: P2581 Physical/ChemicalProperties 15 Title None available Laboratoroyr Completion Author Date Type EnvironmentalFateand Transport Title Ready biodegradabilit(yBOD/COD) ofFC-603EF Laboratoryor Author 3M Env. Lab Completion Date Type Robustsummary,copiesofdata Dec., 1996 sheets Ecotoxicity Elements Title Acute toxicitoyf FC-603EF to the Golden Orfe (Leuciscus idus) Acute toxicitoyf FC-603EF to the alga,Sconedesmus subspicatus Acute toxicitoyfFC-603EF toDaphnia magna Bacteriad]ehydrogenase activitoyfFC-603EF by the TTC method Toxicityof FC-603EF toactivatedsludge Laboratory or Author Hygiene-Insdtutdes Ruhrgebiets, Gelsenkirchen, Germany Hygiene-Insfitudtes Ruhrgebiets, Gelsenkirchen, Germany Hygiene-institudtes Ruhrgebiets, Gelsenkirchen, Germany Hygiene-insbtutdes Ruhrgebiets, Gelsenkirchen, Germany Hygiene-InsUtutdes Ruhrgebiets, Gelsenkirchen, Germany Completion Date 9/26/96 9/26/96 9/26/96 9/26196 9/26/96 Toxicityof FC-603EF toMicrotox 3M Env. Lab Toxicityof FC-603EF toactivatedsludge mixed liquor Acute ToxicityofFC-603EF, LightWater (TM) ATC 3% ARAFFF toDaphnia magna 3M Env. Lab ASci Corporation, Duluth,MN 10/22/96 10/23/96 11/7/96 Type Robust summary, Finalreportin the German language Robust summary, Finalreportin the German language Robust summary, Finalreportin the German language Robust summary, Finalreportin the German language Robust summary, Finalreportin the German language Robust summary, laboratory summary report,copies ofdata sheets Robust summary, copies of data- sheets Robust summary, finalreport Growth InhibitionfFC-603EF, LightWater (TM) ATC 3%, AR-AFFF toGreen Alga (Selenastrumcaprfcomutum) Acute Toxicityof FC-603EF, LightWater (TM) ATC 3% ARAFFF toFathead Minnow (Pimephalespromelas) Growth InhibitioTnest with the Marine Alga Skeletonema costatum - FC-603EF Acute ToxicityTest withthe Marine Copepod Acartfatonsa FC-603EF Acute ToxicitySediment Testwiththe Marine Amphipod Corophium volutator- FC-603EF ASci Corporation, Duluth,MN AScl Corporation, Duluth,MN RF Rogaland Research, Stavanger,Norway RF Rogaland Research, Stavanger,Norway RF Rogaland Research, Stavanger,Norway 11/22196 1/28/97 1114/00 1/14/00 1114/00 Robust summary, finalreport, Robust summary, finalreport. Robust summary, finalreport Robust summary, finalreport Robust summary, finalreport. 16 FC-603F Acronyms: Lab Request Number: M1655 Physical/Chemical Properties Title None available Environmental Fate and Transport Title Ready biodegradabilit(ySOD/COD) ofFC-603F Laboratory or Author Completion Date Type 7 Laboratory or Author Pace Inc., Minneapolis,MN Completion Date 5/10/94 Type Robust summaries, summary reports EcotoxicityElements Title Acute statictoxicitoyf FC-603F tofatheadminnow uto stabc toxicitoyf FC-603F to Selenastrum caprfcomutum Laboratory or Author Completion Date 3M Env. Lab 5/27/94 3M Env.Lab 10113195 Acute statitcoxicitoyf FC-603F toDaphnia magna 3M Env. Lab 5127/94 Toxicityof FC-603F to Microtox 3M Env, Lab 5/20/94 lacute toxicitoyfFC-603F toactivatedsludge mixed liquor 3M Env. Lab 5/10/94 Type Robust summary, copy ofdata sheets Robust summary, copy of data sheets Robust summary, copy ofdata sheets Robust summary, copy ofdata sheets Robust summary, copy ofdata sheets FC-780 Acronyms: Physleal/Chomical Properties Title None available Laboratory or Auth or Completion Date Type Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) ofFC-780 Laboratory or Author Completion Date Numerous 4/23/82 Type Robust summaries, summary reports EcotoxicityElements Title Laboratoryor Author - Completion Date Type Acute toxicittyo Mummichog (EgodulU bg!eLo-c-rLLug) Naval Research Laboratory,Fire Supression Section, Washington, D.C. 6/11/82 Robust summary, summary report 17 FC-780B Acronyms: 7901, Sample 1-3,AFFF r-, Lab Request Numbers: 4461, 4653, 4673, 5598, 62llS7685 Physical/ChemicalProperties Title None available Environmental Fate and Transport Title Ready biodegradabilitoyfFC-780B (BOD/COD) ady biodegradabiliotfyFC-780B (AFFF C) (OECD Closed BoftleTest) EcotoxicityElements Title 780B (lot788-20): ResultsofAquaflc96 Hr.LC50 Tests teToxicityof7901 tothe Common Mummichog (EunAulgabelerogritus) Dynamic 96-Hour Acute Toxicityof3M Sample 1-3 to Fathead Minnows (ELmepbal-esprgme-Lqo Laboratory or Completion Au Date Type Laboratory or Author Completion Date Numerous Numerous 3M Env. Lab 11128/80 Type Abbreviated robustsummary, copies ofdata sheets Robust summary, copies ofdata sheets Laboratory or Completion Author Date 3M Env. Lab EG&G Bionomics, Wareham, MA AnalyticaBlio Chemistry Laboratories,Inc. Columbia, MO 11/15/78 April,1979 9/29/80 Type Robust summary, Technical Report Summary Robust summary, finalreport Robust summary, finalreport FC-783 Acronyms: 3M sample no.6, Lab Request Number: 4896 Physical/ChemicalProperties Title None available Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) ofFC-783 EcotoxicityElements Title Acute Toxicityof3M Sample No. 6 toBluegilSlunfish (LgRmk MAC-LoshLrU-Si Laboratory or Completion Autt Date Type Laboratory or Author 3M Env. Lab Completion Date 6/8/79 Type Robust summary, copies ofdata,. sheets Laboratory or Author AnalyticalBio Chemistry Laboratories,Inc., Columbia, MO Completion Date 6/19/79 Type Robust summary, finalreport 18 lacutetoxicitoyfFC-783 toactivatesdludgemixed liquor 3M Env. Lab 6/4/79 Robust summary, copiesofdata sheets FC-787 Acronyms: FC-787-X. Lab Request Numbers: H1608,HI6091 Physical/ChemicalProperties Title None available Laboratoryor Author Completion Date F ---Type EnvironmentalFate and Transport Title ,Ready biodegradabiliotfyFC-787 (BOD/COD) EcotoxicitEylements Title Acute toxicitoyfFC-787 toMicrotox StaticAcute ToxicitoyfFC-787 tothe Daphnid,Daphnia magna FlowThrough AcuteToxicityofFc-787to theFathead Minnow, Pimephales promelas Laboratoryor Completion Author Date Type Serco Laboratories,9/28/90,10/13/90, St Paul,MN 11/2190 Robust summary, finarleport Laboratoryor Author 3M Env. Lab EnviraSystems DivisionResource Analysts,Inc., Hampton, NH EnviroSystems DivisionResource Analysts,Inc., Hampton, NH Completion Date 8/16/90 9/4190 9120/90 Type Robust summary, copiesofdata sheets Robust summary, finalreport Robust summary, finarleport FC-3003 Acronyms: Lab Request Number: R1331 Physical/ChemicalProperties Title None available EnvironmentalFate and Transport Title RI 331 BOD Reportfor3M Company EcotoxicitEylements Title Toxicitoyf FC-3003 toMicrotox 19 Laboratoryor Completion Auttor Date Type Laboratoryor Author AScl Corporation, Duluth,MN Completion Date August,1997 Type Robust summary, finarleport Laboratoryor Author 3M Env. Lab Completion Date 3/13197 Type Robust summary, copiesofdata sheets ToxicitoyfFC-3003 toactivatedsludgemixed liquor Acute ToxicitoyfR1331 toDaphnia magna Growth InhibitionfRI 331 forGreen alga(Selenastrum capricomutum) Acute statitcoxicitoyf FC-3003 tofatheadminnow uteToxicitoyfR1331 toFatheadMinnow (Pimephales promelas) 3M Env. Lab AScl Corporation, Duluth,MN AScl Corporation, Duluth,MN 3M Env. Lab AScl Corporation, Duluth,MN 3/21/97 3/27/97 4/3/97 4118197 6/26/97 Robust summary, copiesofdata sheets Robust summary, finalreport Robust summary, finalreport Robust summary and copiesof data sheets Robust summary, finalreport FC-3017 Acronyms: Lab Request Numbers: N3188, N3688 Physical/ChemicalProperties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Biodegradafloonf"LightWater"ProductsinOECD 6/80 Test - N3688 BOD Reportfor3M Company Laboratory or Author Completion Date 3M Env.Lab AScl Corporation, Duluth,MN 6/30/80 April1,996 Type Robust summary, technicalreporf. summary Robust summary, finalreport EcotoxicityElements Title Laboratory or Author Completion Date Acute toxicitoyfFC-3017 to Microtox 3M Env.Lab 9/26195 Acute statircenewaltoxicitoyf FC-3017 tofatheadminnow 3M Env.Lab 9/29/95 Acute toxicitoyfFC-3017 to activatesdludgemixed liquor Acute Toxicitoyf FC-3017 toDaphnia magna 3M Env. Lab ASci Corporation, Duluth,MN 9/29195 12123/95 lacutetoxicitoyfFC-3017 to Selenastrumcapricomutum 3M Env.Lab 1/16/96 Type Robust summary, copiesofdata sheets Robust summary, copiesofdata sheets Robust summary, copiesofdata sheets Robust summary, finalreport Robust summary, laboratory summary report,copiesofdata sheets Summary Reports Title Laboratory or Author Completion Date Summary forwork performedforthe German Government ,Agency forMilitarTyechnologyand Procurementon fire extinguishinfgoam compounds frommultiplceompanies Dr.H. Hellmann,D. Muller 10/12/77 Type Robust summary, Technical Awareness Report,finalrepo@-I FC-3031 20 Acronyms: Lab Request Number: N3188 Physical/ChemicalProperties Title None available Environmental Fate and Transport Title None available EcotoxicityElements Title Acute stabctoxicitoyfFC-3031 tofatheadminnow Laboratoryor Completion Author Date Type Laboratoryor Completion Author Date Type Laboratoryor Author 3M Env. Lab Completion Date 8/14/76 Type Robust summary, copies of data sheets FC-3041 Acronyms: Lab Request Number: 6508S Physical/ChemicalProperties Title None available Laborat* or-- Completion Autt Date Type Environmental Fate and Transport Title Laboratoryor Completion Author Date Ready biodegradabilit(yBOD/COD) ofFC-3041 3M Env. Lab 315/81 lnvestigabonforthe Eco-toxicologicaElvaluationofthe Fluoro-surfactanBtase FC-3041. Aerobic Degradation. Partf Fraunhofer Institute for Environmental Chemistry and Eco- toxicology, Schmallenberg, Germany December, 1993 Investigatiofnorthe Eco-toxicologicaElvaluationofthe Fluoro-surfactanBtase FC-3041. Anaerobic Degradation. Part g Fraunhofer Institute for Environmental Chemistry and Eco- toxicology, Schmallenberg, Germany December, 1993 EcatoxicityElements Title Laboratoryor Completion Author Date Acute statictoxicitoyfFC-3041 tofatheadminnow 3M Env. Lab 2/13/81 cutestatictoxicitoyfFC-3041 toDaphnia magna 3M Env. Lab 2/13/81 Acute toxicitoyfFC-3041 to activatedsludge mixed liquor 3M Env. Lab 316/81 Type Robust summary, copies ofdata sheets Robust summary, finalreport Robust summary, finalreport A Type Robust summary and copies of data sheets Robust summary and copies of data sheets Robust summary and copies of data sheets 21 FC-3052 Acronyms: Lab Request Number: W2039-2 Physical/Chemical Properties Title None available Environmental Fate and Transport Title None available EcotoxicityElements Title Acute ToxicityofFC-3062 to Rainbow Trout (Oncorhynchus mykiss) Laboratory or Author Completion Date Laboratory or Author Completion Date Type Type Laboratory or Author AScl Corporation, Duluth,MN Completion Date 7/19/99 Type Robust summary, finalreport FC-3072 Acronyms: Lab Request: M3597 PhysicallChomical Properties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title None available Laboratory or Author Completio D altefeI nj Type EcotoxicityElements Laboratory or Completion Title Author AcuteToxicitoyfFC-3072toFatheadMinnow (Pimephales AScl Corporation. Promelas) DuluthM,N Date 3/20/95 Acute statictoxicitoyfFC-3072 toDaphnia magna 3M Env. Lab 3/23/95 Acute toxicitoyfFC-3072 toMicrotox ,Acute toxicitoyf FC-3072 toactivatedsludge mixed liquor 3M Env.Lab 3M Env. Lab 3115/95 3/20/95 Type Robust summary, finalreport Robust summary, copy ofdata sheet Robust summary, copy of laboratorysummary report,copies ofraw data sheets Robust summary, copiesofdata sheets FX-3103 Acronyms: Lab Request Number: PhysicaUChemical Properties Cl I11-1 22 Title None available Laboratoryor Author Completion Date F Type Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) ofFX-3103 Laboratoryor Author 3M Env. Lab Completion Date 4/18185 Type Robust summary, laboratorydata summary Ecotoxicity Elements Title Laboratoryor Completion Author Date Acute statictoxicitoyf FX-3103 tofatheadminnow ute stabc toxicitoyf FX-3103 to Selenastrum capricomutum 3M Env. Lab 3M Env. Lab 2/8185 2123/85 Acute statictoxicitoyfFX-3103 toDaphnia magna 3M Env. Lab 2/8/85 ToxicityofFX-3103 to Microtox 3M Env. Lab 2/5/85 Acute toxicitoyfFX-3103 toactivatedsludge mixed liquor 3M Env. Lab 2/20/85 Type Robust summary, copy ofdata sheets Robust summary, copy of data sheets obust summary, copy ofdata sheets Robust summary, copy ofdata sheets Robust summary, copy ofdata sheets FX-3104 Acronyms: Lab Request Number: Cl 111-2 Physical/ChemicalProperties Title None available Laboratoryor Completion Author Date Type Environmental Fate and Transport Title Ready biodegradabilit(yBODICOD) ofFX-3104 Laboratoryor Author 3M Env. Lab Completion Date 4118185 Type Robust summary, laboratorydata summary EcotoxicityElements Title Acute statictoxicitoyfFX-3104 tofatheadminnow Tr-tte stabc toxicitoyf FX-3104 to Selenastrum capricomutum Acute statictoxicitoyfFX-3104 toDaphnia magna ToxicityofFX-3104 toMicrot6x Acute toxicitoyf FX-3104 to activatedsludge mixed liquor Laboratoryor Author 3M Env, Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab Completion Date 2/8/85 2/23/85 218/85 2/6/85 2/20/85 Type Robust summary, copies ofdata sheets Robust summary, copies of data sheets Robust summary, copies ofdata, sheets Robust summary, copies ofdata sheets Robust summary, copiesof data sheets 23 FX-3106 Acronyms: Lab Request: C2282 Physical/ChemicalProperties Title None available Laboratory or Author Completion Date Type Environmental Fate and Transport Title Ready biodegradabilit(yBOD/COD) of FX-3106 Laboratory or Author Completion Date 3M Env. Lab 11/26/85 Type Robust summary, copiesof data sheets EcotaxicityElements Title Acute staticrenewal toxicitoyfFX-3106 tofathead minnow IToxicitoyfFX-3106 to Microtox Laboratory or Author 3M Env. Lab 3M Env. Lab Completion Date 11/2185 10/28/85 Type Robust summary, copiesofdata sheets. Robust summary, copiesofdata sheets. L-4647 Acronyms: Lab Request Number: Physical/ChemicalProperties 5623S Title None available Environmental Fate and Transport Title Ready biodegradabili(tByOD/COD) ofL4647 EcatoxicityElements Title Acute statictoxicitoyfL4647 tofatheadminnow Laboratory or Author Completion Date Type Laboratory or Author Completion Date 3M Env. Lab 5121/80 Type i@o-bustsummary, copies of data sheets Laboratory or Author Completion Date 3M Env. Lab 6/28180 Type Robust summary, copiesof data sheets. Miscellaneous Studies Title Summary forfoaming studiesdone on vairousAFFF products Laboratory or Author 3M Env. Lab Completion Date 8/15/79,6118/81, 3/15/82,3/16/90, 8119/92,1/27/94, 3/20/95 Type Abbreviated robustsummary, reports,copies ofdata sheets. 24 AttachmenttsoLettertoC.Aue-r'dat6e/d28/00 BibliograpohfyPublisheLditeratuirne3M'sPossession RelatetdoPFOS Mixtures I A Review ofFireFightingFoams toIdentifPyrioritiefsorEQS Development.R&D Note 339,ResearchContractorW:Rc plc,Environment Agency,UY, 1994. 2. Ansul Company. FinalReport:EnvironmentallyImproved AFFF. Department of Defense TechnicalInformationCenterNOO 173-76-C-0295,December 13,1997. 3. Bass,C.M. SoiltreatmentofAFFF: MicrotoxtoxicitmyonitorevaluationP:hase 1. Naval CivilEngineeringLaboratory.TM No. 80-54-14.Sept.1980. 4. Bass,C.M. The fateand effectosfaqueousfilmformingfoam (AFFF) asitpasses througha sand,soilo,r activatecdarbonbiofiltewrithappendiceson highperformance liquidchromatographyand theBechman Microtoxtoxicitmyonitorapplicationtso AFFF: Ph.D.DissertatioUnn,iversityofOklahoma (1982). 5. Chan, D.B. Toxic substanceD:isposalof wastewatercontainingaqueousfilmforming foam (AFFF) -A summary ofprogresstodateon developmentofallAFFF treatment processes.TMNO. M-54-80-10,CivilEngineeringLaboratoryN,aval Construction BattalioCnenter,Aug. 1980, 6. Chen, Guoqing and Farhang Shadman. Removal of Trace Surfactanftrom Ultrapure Water Through UV 1?hotolysiasnd PhotocatalytiOcxidation.Chemical & Environmental EngineeringDepartment,Universityof Arizona,Tucson,Arizona85721. 7. Howell,R.D.,and E.E. Tucker.Removal ofsurfactantfsrom fireextinguishinfgoam. American EnvironmentalLaboratory12 (1996)10. 8. Moody, C.A. and J.A.Field.DeterminationofPerfluorocarboxylatiensGroundwater Impactedby Fire-FightinAgctivityE,nvironmentalScience& Technology,Vol.33,No. 16,(1999),pp.2800-2806. 9. Saam, R. and P.Rakowski. Firefightinsgchoolwastetreatmentstudy.Naval Civil EngineeringLaboratory.TM No. 54-79-14.June,1979.