Document pe8LDbJ3NEyMn2M97KbX5kgD6

From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: October 9, 1990 To: Mr. William H. Cooper PPG Industries Chemicals Division P.0. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA04888 Sample location: PPGHC Cooling Tower Sludge (B) Collected by: PREJEAN Collection date: 09/07/90 Time: 13:15 Laboratory submittal date: 09/13/90 Time: 19:00 Received by: RLH Validated by: RLH Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 09/20/90 Time started: 11:45 Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 09/27/90 Time started: 09:00 Parameter: TCLP Volatile Organics Method reference: EPA 624 Result: see appended report Date started: 09/30/90 Time started: 20:33 Date finished: 09/21/90 Analyst: MJF Date finished: 10/08/90 Analyst: JSC Date finished: 09/30/90 Analyst: BB SL 0A6066 Mr. William H. Cooper Page: 2 October 9, 1990 Sample I.D. AA04888 (continued) Parameter: TCLP Semi-Volatiles Method reference: EPA 625 Result: see appended report Date started: 09/28/90 Time started: 02:43 Date finished: 09/28/90 Analyst: BB Parameter: Selected Volatile Organics Method reference: SW846-8240 Result: see appended report Date started: 10/02/90 Time started: 21:56 Date finished: Analyst: BB 10/02/90 Parameter: Semi--Volatile Organics Method reference: SW846-8270 Result: see appended report Date started: 10/02/90 Time started: 23:23 Date finished: 10/02/90 Analyst: BB Parameter: pH Method reference: EPA 150.1 Result: 7.9 SU Date started: 09/14/90 Time started: 15:00 MDL or sensitivity: 0.00 Date finished: 09/14/90 Analyst: KEL Data for TCLP Volatile Organics ug/L Component Name Benzene Carbon Tetrachloride Chlorobenzene Chloroform l,2-Dichloroethane 1,l-Dichloroethene Methyl Ethyl Ketone Tetrachloroethene Trichloroethene Vinyl Chloride Pyridine Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det 33 11 Not Det Not Det Component MDL 10 10 10 10 10 10 10 10 10 10 500 SL 046067 Mr: William h. Cooper Page: 3 October 9, 1990 Sample I.D. AA04888 (continued) Data for TCLP Semi-Volatiles ug/L Component Name l,4-Dichlorobenzene Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4-Dinitrotoluene Hexachlorobenzene Cresols, total 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol Pentachlorophenol Concentration Not Det Not Det NOt Det Not Det NOt Det NOt Det NOt Det Not Det Not Det NOt Det Compon nt MDL 10 10 10 10 10 10 20 10 50 50 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Lead, TCLP Mercury, TCLP Selenium, TCLP Silver, TCLP Concentration Not Det 2.9 .03 Not Det .04 Not Det .025 Not Det Compoi .005 .1 .01 . 03 .04 .005 .005 .03 Data for Selected Volatile Organics mg/Kg Component Name Concentration Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride 1.1- Dichloroethene 1.1- Dichloroethane trans-1,2-Dichloroethene Chloroform 1.2- Dichloroethane Trace 42 190 Not Det Not Det Not Det Not Det Not Det Not Det 110 Component MDL 10 10 10 10 5 5 5 5 5 5 SL 046068 Mr; William H. Cooper Page: 4 October 9, 1990 Sample I.D. AA04888 (continued) Data for Selected Volatile Organics (continued) Component Name Concentration 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1.2- Dichloropropane t-l,3-Dichloropropene Trichloroethene Dibromochloromethane 1.1.2- Trichloroethane Benzene c-l,3-Dichloropropene Bromoform Tetrachloroethene 1.1.2.2- Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Xylene, total c-i,2-Dichloroethene 1.1.1.2- Tetrachloroethane Not Det Not Det Not Det Not Det Not Det 110 Not Det 36 Not Det Not Det Not Det 1200 12 5 Not Det Not Det Not Det 350 Not Det Component MDL 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 Data for Semi-Volatile Organics ug/Kg Component Name Phenol bis(2-Chloroethyl) Ether 2-Chlorophenol 1.3- Dichlorobenzene 1.4- Dichlorobenzene 1,2-Dichlorobenzene bis(2-Chloroisopropyl) Ether N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2.4- Dimethylphenol bis(2-Chloroethoxy) Methane 2.4- Dichlorophenol 1.2.4- Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro-3-methylphenol Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 SL 046069 Mr. william H. Cooper Page: 5 October 9, 1990 Sample I.D. AA04888 (continued) Data for Semi-Volatile organics (continued) Component Name Concentration Hexachlorocyclopentadiene 2.4.6- Trichlorophenol 2-Chloronaphthalene Dimethyl Phthalate Ac naphthylene Acenaphthene 2.4- Dinitrophenol 4-Nitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenylether Fluorene 4.6- Dinitro-2-methylphenol N-Nitrosodiphenylamine 4-Bromophenylphenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene bis(2-Ethylhexyl) Phthalate Chrysene Di-n-octyl Phthalate Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(l,2,3-c,d)pyrene Dibenzo(a,h)anthracene Benzo(g,h,ijperylene Benzidine alpha-BHC beta-BHC delta-BHC gamma-BHC Heptachlor Aldrin Heptachlor Epoxide Endosulfan I Dieldrin 4,4'-DDE Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 860 Not Det Trace Not Det Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Compon nt MDL 300 300 300 300 300 300 1500 1500 300 300 300 300 300 1500 300 300 300 1500 300 300 300 300 300 300 600 300 300 300 300 300 300 300 300 300 300 2400 300 300 300 300 300 300 300 300 300 300 SI, 046070 Mr. William H. Cooper Pag : 6 October 9, 1990 Sample I.D. AA04888 (continued) Data for Semi-Volatile Organics (continued) Component Name Concentration Endrin Endosulfan II 4,4'-DDD Endosulfan Sulfate 4,4'-DDT Methoxychlor Endrin Aldehyde alpha-Chlordane gamma-Chlordane Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 l,2-Diphenylhydrazine N-Nitrosodimethylamine Comments: Reference Lab Report No. R1461. Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det I1* Compon nt MDL 300 300 300 300 300 300 300 300 300 600 300 300 300 300 300 600 600 300 300 If there are any questions regarding this data, please call. SL 046071