Document pXeEMNE3bqZorRQKdg7yKZmd

3M YrJean B.Sweeney Sh Spans 3M Environmental, Health and Sr 3M Center, do Bung 0224-05-33. November 9, 2009 mm RHD-0598-c037 3 room 3 AR278-393 GEDoiPcnAucFmtaeonnftPoRPlrolouostismosn6in4Pgr2e8CveAenntttei:ronSaenctdiTono8x0,) US. EPA 5; W12a0s0hiegninosny,iDaCn.is20A3v6e0n-u0e00N1W Ree TSE uSrCfaAce8(Wm ea)tSeurbsftraonDmtoitcahkleeRtiMsiFskEsFNiQosts.ii0cp3ep9:i8RS.iu3vl7efr3on-tRebuastedfarnodmC2a0r0b9oxAylnicsbyasseofdish and FO 30 i esuemtirngesthiosynt(ieCcMainannessduopotpalreePmelsnatpipernecvCiiooeursaosulurbAmTgiuesnsneic2oyn0s,(2Ma0nP0Cs6Aul)sfu.obnmy3ilMtaanlisdcpcoraonrvcbioedxirynnlg.ic eanney aSspoeeragreewncaortnettreysdrabepcyleiithvneegd3pfMrrooEgmnrhiamreocnMomnPedCnutcAatleadnLdabbyfrtinshateloaMryPl.CtTAehelfsorerePdpooocrlutsm2effnortsa dye: o Rts 2000. The Tolowig Summarizes ky aspects of he stte-dreted + The study was designedtoberepresentativeofth ntivty of Pool 2 fom Lock and + DHFdaoemrittNsoe.dst|2ud(yRR, MePno84eo7.6e)2 w14ta.os Fi camping was conduc dLiovcikdeadndntDoafmouNrod.is2ti(ncRtMre8a1c5h.e2s).. ted by the Minnesota Department These ae ofNatural generally Resources. res were apparenly collected ma le May carly June 2009 meme + e Water sr amplisnigtwtaosnncoiworsidiifnaotarecd.hbSyoutrhffheaecMePfowCuaArt.erres3aaMcmhpplrweoesvriwedeesdramapclocelodln.etcrtaTecdhteoorsne(JPwuaelcyree3, TFSaie meberbeudensdeksnietsevLraotcdaatrtiemod.n:1NbtouhmerongulaghluyLnoficoahct,iesonmaf1lo2ifmcouatchhbapsse,ecsomwmeorne carp + e For ameen aGiadvadofonthepufropotseasc,haepsp.roxTihmeatoetlayl 1nu0mbpeerrocfent ofshhecolflisehctseadmwpaless2a9n7d wai of th aes samp wr at wilh 3 + PnertMosrescufdonaotesCnH-dC1p3rfpoerrouoecraoncersbuolnyfloaneasm;idCeh, C6 nd C8 aStnuodsyerdeaClBs:re summarized in he following document hat have been copied to the Cp ONTAINS NO CBI 2851 HF 2 + AoemmrEixcccSeeollamfbploel,r,isnporgrroolyvvsiiHddieerTddehdi0tsoby33iMMethebbcyyMothPnheCeaAnMMPPtfCChoerAA,t,shasencnwitsoeerwdkdat""eMPriFsdCsasaRMgiPesnOseOPrLaotle22dJFbUiysLhtYhael2l009 + TT oShne aExooremee rinnteiadnopdtniaetldiornceooancthdeasaionarrpyiereevdnitoaiusfliyefdoarsah"eodU2M03-m0b6y955,t1hs"etutMdhyProCtocAuhhge.thrsrUiTcMtnha-helis8su.bs4jpcetaodfshtehtis, + oWanitieaErncsvraioimrspomalnmiianogniEoxnfceLSlaruberpofsrraicacsatedfosWhaetSRceetprpi(oSraostmatpmNelpoe.lsae,bsEo0Mcv9ioe-st.0seissspiopnpFdiliRuniogveorth--ePoMoPlC2:AJusluyrf2a0c0e9. + F3FheilEtPmoiitnlnieooCnoHnnmoetemdrnoogtleaAngaLaetbhneoseeryaCstoMolariyyciR2eer0dpe0odfr9to.mNPo.theeaEc0Mt9iIis:0os3Pin7sOs2Si,p.pFilrIuRonioutvrgheohircshbreSyeneptciohtcreitoMntAihn4neanl.eyssoTihtsiasof ierFoenemeneetnemdatiinnotnshmearrmMebasPeusCrssAfoinfritesphhirstetafmswepalmdiponlcgteusamE"xecScnoetrlstescspapenobsndoisIn"chgreoteosfa(rno1et0en%d"casebuobdvset)1.ocSofahmemppadlraeetasplit oSa oNamplnerreejsueelsctst.oSuawmimtashervIyerraelEpommrrat,apnp,mreepprnaotrvaeidldebLdyabbPoyarchaeteoArMnyaRPleCyptAio.cratlteNtoon.ddoeEcd0u9m1-0e03nd6to5c.tuhmOefnFitendothte, Various Study sampling locations. 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MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPIIRR. MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPIIRR. MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPII R. R. MMMIIISSSSSSIIISSSSSSIIIPPPPPPIIIAR... MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPII A A. MMIISSSSIISSSSIIPPPPII RR.. MMIISSSSIISSSSIIPPPPIIR.. MMIISSSSIISSSSIIPPPPII A. R. MMIISSSSIISSSSIIPPPPII RR.. MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPII R. R. MMIISSSSIISSSSIIPPPPII RR.. MMMIIISSSSSSIIISSSSSSIIIPPPPPPIIIRR.. MMIISSSSIISSSSIIPPPPII R. A. MMIISSSSIISSSSIIPPPPIIR.. MMMIIISSSSSSIIISSSSSSIIIPPPPPPIIIAR... MMIISSSSIISSSSIIPPPPII R. R. 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MMIISSSSIISSSSIIPPPPII RR.. alfish_format 2009 PoPoooll22 PPooooll 22 PoPoooll22 PPooooll 22 PPooooll22 PPooooll 22 PoPoooll22 PPooooll 22 PoPoooll22 Pool 2 PPooooll22 PoPoooll22 PPooooll22 PoPoooll22 PPooooll 22 PoPoooll22 PPooooll 22 PoPoooll22 PPooooll 22 PoPoooll22 PPooooll 22 PPooooll22 Pool2 PPooooll 22 PoPoooll22 PPooooll22 PPooooll22 Page? p.10 UM- 84 UUMM:- 88--44 UM-84 UUMM-- 88-44 UUMM--88.44 UUMM--8844 UM- 8-4 UUMM-:88.44 UUMM-- 88-44 UUMM--88.44 UUMM--88-34 UUMM--8833 UUMM--8833 UUMM--8833 UUMM--8833 UUMM--8833 MUM8-833 UUMM:-8833 UM-83 UUMM-- 88-34 UM- 8-4 UUMM-- 88-44 UM- 84 UUMM-: 88-44 UM-8.4 UUMM-- 88--44 UM- 84 UUMM-- 88-44 UUMM:- 88-44 uUMM--8811 009900229912 MMIISSSSIISSSSIIPPPPII RA.. 009900228034 MMIISSSSIISSSSIIPPPPII AA. 009900220956 MMIISSSSIISSSSIIPPPPII AA. 090297 MISSISSIPPIR alfish._format_2009 PoPoooll22 PPooooll22 PPooooll22 Pool2 p11 uUMm--88.11 UumM--88..11 UUMM--88-11 UM-8.1 Pages p.12 alfish_format 2009 CTY. "AREA." 2D0A0T4E0C83O1L'SSMPBE.C ' FISHID.. AFNILASTK .NOFISH 1L1GTH8INs WTLB 2200004400883311 SMB WHB FFIILLSSKK 41 11048s 2200005511000083 WWEE FFIILLSSKK 1 1 22172.55958940 2200005511000083 WWEE FFIILLSSKK 1 1 21795259910364 2200005511000033 CC FFIILLSSKK 1 1 22018665631544 2200005511000083 C C FIFILLSSKK 1 1 22420.14507954 2200005511000083 SMB FFIILLSSKK 1 1 2140.2430602425 2200005511000038 SSMMBB FFIILLSSKK 1 1 81606213461272 2200005511000033 SSMMBB FFIILLSSKK 1 1 81616.10421372 22000055110000338 SMB WHB FILSK FILSK 1 1 11022230602722 22000055110000388 WWHHBE FFIILLSSKK 1 1 1142556964933 2200005511000088 WHB WHE FFIILLSSKK 11194.94648086139 220000650180x0x8 CSHMCB FFIILLSSKK 1119202592173546 220000660088xxxx CCHHCC FIFLILSSKK 1 1 22172.55008046 2200006600880xx CHC CHC FFIILLSSKK 1 1 22529182452958 2200006600880xxx SSMMBB FFIILLSSKK 1 1 11255200864232 220000660088xxxx SMB SMB FFIILLSSKK 1 1 89..099746438788 220000660088xxxx BSGMSB FFIILLSSKK 1 1 97..00856161184 220000660088xxxx CBHGCS FFIILLSSKK 1 1 6.214062036632 220000660088xxxx CHC CHC FILSK FILSK 1 1 2257.5159060865 220000660088xxxx CCHHCC FFIILLSSKK 1 1 22501992618256 22000066008800xx SSMMBB FFIILLSSKK 1 1 68293979020183 220000660088xxxx SMB BGS FFIILLSSKK 1 1 58.774008165617 220000660088xxxx BGS CHC FFIILLSSKK 11 252.0940752142 220000660088xxxx CCHHCC FIFILLSSKK 1 1 22667377176955 220000660088xxxx CCHHCC FFIiLLSSKK 1 1 2246.4450606495 Pages 220000660088xx SSMMBB,, 220000680088:1 SBMGSB 220000880086x0x9 BBGGSS 2200008800660099 BBGGSS 2200008800660099 BBGGSS 2200008800660099 BKS SAG 2200008800660099 SSAMGB 2200008800660099 SSMMBB 2200008800660099 SSMMBB, 2200008800660099 WWEE 2200008800660099 WWEE 6622AAMM884444--8844 2200009900552288 FFWWDD. 62 62 RRMM 884444--8844 2200009900552288 FFWWDD 6622RRMM 884444--8844 2200009900552288 FFWWDD 6622 RRMM 884444--8844 2200009900552288 FFWWDD 6622 RRMM884444..8844 2200009900552288 FFWWDD. 6622RRMM884444..8844 2200009900552288 FFWWDD 6622 RRMM 884444.8844 2200009900552288 FFWWDD 6622 RRMM 884444..8844 2200009900552288 WWHHBB 6622 RFMM 884444..8844 2200009900552288 WWHHBE 6622 RRMM 884444--8844 2200009900552288 WWHHBB 6622 RRMM 884444-.8844 2200009900552288 WWHHEB 6622 RRMM 884444-.8844 2200009900552288 WWHHBE 6622 RRMM 884444.-8844 2200009900552288 WWHHBB 6622 RRMM 884444--8844 2200009900552288 WWHHEE 6622 RAMM 884444..8844 2200009900552288 WSMHBE alfish_format_2009 FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFiILSSKK FFIILSSKK FFiILLSSKK FIFLILSSKK FIFLILSSKK FIFLILSSKK FFiILSSKK FIFISLSKK FIFISLSKK Page 10 p13 1 1 88e6s14a1s7 1 1 595.41418881119 1 1 7s6a7r72010615 1 1 77.248830406155 1 1 67.649820931135 1 1 1113.3082536632 1 1 71687171106254 1 1 980e8s8t1a1187 1 1 88286576721678 1 1 22004477224444 1 1 91.34388851893 1 i 113380 1 1 11324 1 i 115402 1s 11 1310a 11 1102 no 1 1 t1ae 11 10128 1 1 11328 1 1 1123 1 1 112426 1 1 112282 11 11238s 1 1 1144s [TY 1 150 6622 RRMM 884444--8844 2200009900552288 SSMMBB 6622 RRMM 884444..8844 2200009900552288 SSMMBB 6622 AAMM 884444..8844 2200009900552288 SSMMBB 62 62 FAIMM 884444..8844 2200009900552288 SSMMBB 62 62 RAIMM 884444..8844 2200009900552288 SSMMBB 62 62 RAMM 884444..8844 2200009900552288 SSMMBB. 6622 RRMM 884444..8844 2200009900552288 SSMMBB 62 62 RAMM 884444..8844 2200009900552268 C C 6622 RAMM 884444-.8844 2200009900552288 CC 6622 AAMM 884444..8844 2200009900552258 C 6622 AFMM 884444..8844 220000900552288 C C 6622 RAMM884444..8844 2200009900552288 C 6622 AAMM 884444..8844 2200009900552288 CC 6622 AAMM 884444..8844 2200009900552288 C 6622 AAMM 884444..8844 2200009900552288 BBGGSS 6622 AAMM 884346..8844 2200009900552289 BWGHSE 6622 RRMM 683366.-8844 2200009900552299 WWHHEE 6622 ARMM 883366..8844 2200009900552299 WWHHEE 6622 AAMM 663366..8844 2200009900552299 WWHHEE 6622 AAMM 663366-.8844 220000900552299 WWHHEE 6622 ARMM 663365.-8844 2200009900552299 WWHHEE 6622 AAMM 683366-.8844 220000900552299 WWHHEE 6622 AAMM 683366-.8844 2200009900552209 WWHHEE 6622 RRMM 883366..8844 2200008900552290 FFWWDD 6622 ARMM 883366..8844 2200009900552209 FFWWDD 6622 ARMM 883366.-8844 2200009900552299 FFWWDD alfish_format2009 FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FIFILLSSKK Page 11 pts 1 1 118378 1[I1T3]0 1a 11 113308 11115500 11181s4s 112u2z 1 i 0 23 1189 11 2wrr2 1 1 22336 1 1 2e0e 11119877 119273 1 1 2125a4 11 7515 1 1 n6.s1 11 21ss 1 o1u3s8 1112a 1130 10222 i1115002 22 1112an2a 11sne 11 1133s0 11112022 p15 alfish_format_2009 62 62 AM AM 836-84 836-84 20090529 20090529 FWD FWD 62 RAM 836-84 20090529 FWD 62 AM 836-84 20090529 FWD 62 62 RM AM 836-84 836-84 20090529 20090529 FWD FWD 62 62 RM RM 836-84 836-84 20090529 20090529 FWD FWD 62 62 RM RM 836-84 836.84 20090529 20000529 FWD SMB 62 62 RM RM 836-84 836-84 20090529 20090529 SMB. SMB. 62 RM 836-84 20090529 SMB. 62 RM 836-84 20090529 SMB. 62 62 RM RM 836-84 836-84 20090529 20090529 SMB. SMB. 62 RM 836-84 20090529 SMB. 62 RM 836-84 20090529 SMB. 62 62 RM RM 836-84 836-84 2200009900552299 SSMMBB.. 62 RM 836-84 20090529 SMB. 62 RM 836-84 20090529 SMB. 62 RM 836-84 20090529 SMB. 62 62 RM RM 836-84 836-84 20090529 20090529 SMB. BGS 62 RM 836-84 20090529 BGS 62 RM 836-84 20090529 BGS 62 RM 836-84 20090529 BGS 62 AM 836-84 20090529 BGS 62 RM 836-84 20090529 BGS 62 RM 836-84 20090529 BGS 62 AM 836-84 20090529 BGS 62 AM 836-84 20090529 BGS 62 62 AM AM 836-84 836-84 20090529 20090529 BGS BGS 62 AM 836-84 20090529 BGS 62 AM 836-84 20090529 BGS 62 RM 836-84 20090529 BGS 62 AM 836-84 20090529 BGS 62 AM 836-84 20090529 C 62 AM 836-84 20090529 C 62 AM 836-84 20090529 C 62 62 FM AM 836-84 836-84 20090529 20090529 C C 62 AM 836-84 20090529 C. 62 AM 836-84 20090529 C 62 AM 836.84 20090529 C 6622 RRMM 883366..8844 2200009900552299 CC 62 62 RM AM 836.84 836-84 20090529 20090529 C C 62 AM 836-84 20090529 C FiLSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FFIILLSSKK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK FILSK 1 126 1 122 11 amz2 1 163 1 182 1 169 1 138 1 22 1 138 1 138 11 0913 1 1a 1 108 1 100 11 11e222 11111300 1 102 1 126 1 18a 1 1a 11 5633 1 57 11 4593 1 65 11 6515 1 51 1 49 11 5555 1 59 1 51 1 5.1 11 212s8 1 201 1 tes 1 1208 1 1 a 220 1 ms or 1 isa 1 27 1 es Page 12 p.16 alfsh_format_2009 62 62 AM AM 883366--8844 2200009900552299 C C 6622 ARMM 883434.-58-41 2200009900552298 WFHWDB 6622 RAMM 883333..55--11 2200009900552299 WWHHBB 6622 RRMM 833.5. 833 5: 2200009900552299 WWHHBB|| 6622 RRMM 883333 55--11 2200009900552299 WWHHBB|| 6622 RRMM 883333 5-1 5: 2200009900552299 WWHHBB|| 6622 RRMM 883333 55--11 2200009900552299 WWHHBB|| 6622 RRMM 833.51 833 5-1 2200009900552299 WWHHBB|. 6622 RAMM883333 55--11 2200009900552299 WWHHBB.| 19 19 AAMM 882277--8632 2200009900660011 FFWWDD 19 19 AAMM 882277--8833 2200009900660011 FWD FWD 19 19 AAMM 882277--6622 2200009900660011 FFWWDD 19 19 AAMM 882277--8823 2200009900660011 FWD FWD 19 19 RRMM 882277--8833 2200008900660011 FFWWDD 19 19 RRMM 882277--8823 2200009900660011 FFWWDD 19 19 RRMM 882277--8833 2200009900660011 FFWWDD 19 19 RRMM 882277--8833 2200009900660011 SFMWBD 19 19 RRMM 882277--8823 2200009900660011 SSMMBB 19 19 RRMM 882277--8822 2200009900660011 SSMMBB 19 19 RRMM 882277--8832 2200009900660011 SSMMBB 19 19 RRMM 882277--8833 2200009900660011 SSMMBB 19 19 RRMM 882277--8832 2200009900660011 SSMMBB 19 19 RM RM 882277--8833 2200009900660011 SMB SMB 19 19 ARMM 882277--8832 2200009900660011 SSMMBB 6622 AAMM 883333..55--11 2200009900552288 C C 6622 AAMM 883333..55--11 2200009900552288 CC. FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFiILSSKK FFIILLSSKK FFIILSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIiLLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILSSKK FIFILLSSKK FFiILLSSKK 1 208 11 132017 1 1 113380 1 1 1a320 1 a2 1 1 113246 1 1 41328 1 1 113s8 1 1 113s0 1 1 1n2e2 1 1 1s 130 116d 1 1 11432a 11 12a62 1 122 1 1 113aa 2 1 1 113208 1 1 110380 1 1 194.04 1 1 114222 1 1 11100 11 10298 1180 11 12698 1 128 1 98 1 1 113042 11 181s02 1 1 222103 1 150 Page 13 p17 alfish_format_2009 62 62 AM AM 883333..5511 2200009900552288 C C 62 62 RAMM 883333..55-1 220000000552288 C C 6622 RRMM 88333.35.5: 2200009900552288 C C 6622 RRMM 88333355-+1 2200009900552288 C C 6622 ARMM 883333..55--11 2200009900552288 C C 19 19 AAMM 881155--6622 2200003900660011 BGS BGS 19 19 ARMM 881155--8822 2200000900660011 BBGGSS 19 19 RRMM 881155.-8822 2200009900660011 BBGGSS 19 19 ARMM 881155-.8822 2200009900660011 BBGGSS 19 19 AM AM 881155..6822 2200009900660011 BGS BGS 19 19 ARMM 881155--8622 2200009900660011 BBGGSS 19 19 ARMM 881155--6622 2200009800660011 BGS BGS 19 19 AAMM 881155--8822 2200009900660011 WBGHSB 19 19 RM RM 815-82 815-82 2200009900660011 WHE WHB 19 19 RRMM 881155..8822 2200009900660011 WWHHBB 19 19 RRMM 881155-.8822 2200009900660011 WWHHBB 19 19 ARMM881155.-8822 2200009900660011 WWHHBB| 19 19 AM AM 881155--6622 2200009900660011 WHB WHB 19 19 ARMM 881155--8622 2200009900660011 WWHHBB| 19 19 AAMM 881155.-6622 2200008900660011 WWHHBB 19 19 RRMM 881155--8622 2200009900660011 FFWWDD 19 19 RRMM 881155--8822 2200009900660011 FWD FWD 19 19 RRMM 881155--8822 2200009900660011 FFWWDD 19 19 RRMM 881155.-8822 2200009900660011 FFWWDD 19 19 RRMM81851.5-8822 2200009900660011 FFWWDD 19 19 RRMM 881155..8822 2200009900660011 FFWWDD FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFiILSSKK FFiILLSSKK FFIILLSSKK FIFILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIiLLSSKK FFIILLSSKK FIFILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FIFILLSSKK FFIILLSSKK 11 182s6 1 1 21520 1Ted193 1 1 212903 111s s 1 61 1 1 a399 1 69 1 1 5699 1 1 5657 1 a3 1 1 6579 1 1 5319 1 1 6573 1 1 1133as 11 121228 1 14s 1 1 1s 188 1 1 112262 1 a2 1 1 11406 1 1a 1 1 a1324 110 1 1 11as2 1108 1 1 1188a2 1 1 112820 1 1 1152a0 1 1 a1sa Page 14. p.18 alfish_format 2009 19 19 RM RM 881155-.8822 2200009900660011 FWD FWD. 19 19 ARMM 881155--8822 2200009900660011 SFWMDB. 19 19 ARMM 881155--8822 2200009900660011 SSMMBB 19 19 RRMM 881155--8822 2200009900660011 SSMMBB 19 19 ARMM 881155..6822 2200009900660011 SSMMBB 19 19 RRMM 881155--8822 2200009900660011 SSMMBB 19 19 RRMM 881155--8622 2200009900660011 SSMMBB 1199 RAMM 881155--8822 2200009900660011 SSMMBB 19 19 RRMM881155-.8822 2200009900660011 SSMMBB 62 62 RM RM 833.51 833 5: 2200009900552288 BGS BGS 6622 AAMM88333355--11 2200009900552288 BBGGSS 62 62 RM AM 833.51 833 5-1 2200009900552288 BGS BGS 62 62 AM AM 883333.55-:1 2200009900552288 BGS BGS 6622 AAMM 8833335.-511 2200009900552288 BBGGSS 62 62 RM RM 883333..551: 2200009900552288 BGS BGS 6622 RRMM 88333355-1: 2200009900552288 BBGGSS 6622 ARAMM 883333.55--11 2200009900552288 BGS C 62 19 ARMM 883135.-58-21 2200009900650218 C C 19 19 RM RM 815-82 815.82 2200009900660011 C C 19 19 ARMM 881155.-8622 2200009000660011 C C 19 19 RM AM 881155--8822 2200009900660011 C C 19 19 RAMM 881155--8622 2200009900660011 C C 19 19 RRMM 881155--6622 2200009800660011 C C 19 19 ARMM 881155--8822 2200009900660011 C C 19 19 RRMM 881155.-8822 2200009900660011 C C 6622 ARMM 884444--8844 2200009900552288 BBGGSS FFIILSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FIFILLSSKK FFIILLSSKK FFIILLSSKK FFIILSSKK FFIILLSSKK FFIILLSSKK FIFILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FIFILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FFIILLSSKK FIFISLSKK FFIILLSSKK FFIILLSSKK 1 1e2 1 1 1a32a 11 110130 1 1s 1 1 18 108 1 1 115370 [IT 1110 100 1183 1 us 1 1 18078 1 108 1 1 5553 1 1 5513 1 1 5513 1 51 1 1 6635 11 4599 1 1 5555 1 1 5617 1 220 11 181s8 1 1 210899 11 182s01 11 113943 1 111830 1 1 189 180 118s 1 1 2a123 1 208 1 1 3a19 Page 15 p.19 alfish_format_2009 6622 FRMM 884444-.8844 2200009900552288 BBGGSS 6622 RAMM 884444.-8844 2200009900552288 BBGGSS 6622 RAMM 884444--8844 2200009900552288 BBGGSS 62 RM 844-84 20090528 BGS FFIILLSSKK FFIILLSSKK FFIILLSSKK FILSK 1 39 11 3397 1 1 a317 1 1 a3n7 Page 16 WIKG "UAT 31207759 311.2253 1m 22451%6 45.617755 0285 00.215625 00.310335 00.241156 0.047481 005261695 2633 2485 175 1.2755 00.649524 00116728 00..116565 0.202852 25 325 3s 0.0633 0.175 00.107655 00752 32255 325 2 7 LONG p.20 alfish_format_2009 "TAGE" ~~ SEX: /LIPRCT.. PEOAPREPFOACODRFOSPPE 00.643513 K K 915005 7m 00.568618 K K 181.138 3 OF 0614 K 755 2F 7 OF 00559318 K K 415850 4a Mm 5 OF 05162042 K 247 735 5 0M 6F 0065098 K K 412705 6 5 0Fm 005661095 K K 6266.94 am aF 00,569067 K K 31637 5 0M aF 00569115 KK 112528 4F 2F 00,567089 K K 51160 aF 2F 0.60065 KK 214002 iF 4F 061.0127 K 1883660 F 060055KK 2a9774 0055KK 420324 0055KK 9".n0r8 00997428 819788 0.08.5769 53129 0.904 a5 NR 23 05KNR 825043 05K 92 0055KK 65168 05K 107 NNRR 151809 NNRR 1372009 0622 NR 658027 1.0156 K 21876 117314 77a42 Page 17 p21 alfsh_format_2009 00125784 NNRR 5125000 0o2o1n4 0069 NNRR 833814 NR 330 00..119434 33 MFm o0s4t 22446KK 61052 0.011631 33 MOmF 00s4 224423KK a1577 0.01209023 35mM 051 0 224581KK 122 00384766 s7 omOF 23208 224493KK 36321 00110438 a5 uF 004%7 224387KK w38s0 00.118672 55 MOmF 00x57 223458KK 111280 01..123674 +5s mOMF 016817 224489KK 218463 0013.151999 5as uF 072168 224459KK w69s5 0033744 55 u9 11075 249245K Kibpion 728405 00550059 021 5 OF 5J 217889 6 Mom 224328 0 w12o8 248 KPoo. on o0s57%1 S7 oMM07o8w a25e KKauit. $m3n9 o1.s00t6 06 MF051587 224486KeRUL . m53 00334989 54 FF220596 22408 KdAeTtE 1T5a7 00.341033 0538 5 mM 3 OF oe 108 5 mos 22458 KKoooTe 77 a 26 KUT ow 00.340919 0229 63 mMM os4t2a dow om 22448 Ru"niyf 280989 ae KE es 00541192 4s mFo 17a8s 2a3s KKEalRmi 8T5oS o0s5e25 +5 oFm a2s4e 2a4e4s KKEiTnO ewosn 0763 F 383 243 3 51s 00.544499 0.434 33 3 MFFo3t2o38r56 223099 24 KKEohEmLeEEn 9s0e6d ws 00464186 34 0F M Z108 a2s4s KKemEer e7r 00680619 64 oFm amas 224666 KRioseoi: weese 0078645s o7mmM o12o1 224a5 Mwwi . sat2 Page 18 00636678 0527 001..740207762 003857638 01.800253 1.189 0o5r4e8 20037542 11.178716 24329638 11..494870 21.476670 21.180863 21.168980 0719 0.160 00.0074s9 00..444806 00376620 00831492 000.46734%34 00279709 0239 00.341802 000.333769883 00.449062 00230219 alfish_format 2009 57 m0Mm oomr 5 0M 07 694 MFFooss0s.56 7smOF o1w 77 MFon129 9 0M 156 75 3s OFFF oa00m383 6 M732 955M0FM em6ds0s5 7M as 56 Momm 237682 6Ss M M am6 56 0MM me467 57mM 453198 4J 0.86 7F 05 53 M mM os0.63 33 F F am302 s Fam 43 MoF a1s2s7 2 F 088 i5 F F am1.01 23 FOF 20255m 6F 2F 2m 278 23 MFn1.01 443 0FF 2211143 55 MF 12152 2som4 oanm 2204 KK 248 Kooi. 222424038 KRoIAniL 22m3 KK 4 22304 KKooi 248 Ku 22438% KKoioo 22438 5K.giST 223176 KWEC 2214 KKEEF 22213K 5Ki"r 22236 Koifem 221165 KKhionn 25246K i 24 KET 2.44 x ik 22458 KH oe o 22444 KKAERLE 224a9 KKjiULoE 243 Ko 25 Ko | 2244 K KoOoT 226080 KKioyou. 25 244 KKoOoi 224a2 CKaoh)o 226485 24 KK oa i 223499 JeeSY 220a RKOiUETr p22 82685 172 20130917 8a2s 4s9.23 356 114346 23614 412273 2a9a 1113s6 M68a6 2392 7.02201 142 175 111449 775a8 srr 779572 593 9el4e7 7150 631 7s s46.8r 03 7119 a10m4 asiess Page 19 =0400 00331560 0073535 01..340824 0561 00648095 00176540 00.3179s6 0292 o06di2e 0054733 00521536 oo0s3teses 0o006s82 0000423 0000.000085s91t99 000.00068418 000047s6 02.306565 1502 11.4730940 1922 1073 22442575 c11o.6e09233 2.488 1.538 p23 alfsh_format 2009 E--1 4 OF 2 208 64mM42262 224%4 8FE M 211418 224448 95 0FM os277 224m3 5 F 16 246 64amMt1 22346 27 OFF ozti 22434% 2AEM 054 236 3 om or 24 7OFm o08m 2d4m5 53 3 0MFMm oso0s8m1 224299 201 56 M Moosdt 224493 64 F Foose 222s5 i3 FoF o0ms 223m7 33 4OF 01x37 225:1 46MMos042 S5 oh0 oisnt 223489 2s4w6 i$3 FmF 065 om I22358 3somFosoe 222384 73 MOF 2osms 22402 5 OF eo 2a 655MMMa2s42s805 224395 25 5 Mm 325 245 66 M F ae263 22438 T5Ss om0F m saise 2b210e95 6M 804 249 5M 12 238 -K Ko 36 KKooillu e27289 & S#ET3 7s1e8a KKuiiliit a38m8 KKKeEivoT 64d 194 KKLohEl a1226 PE 308 tes gKeooni 1w4e9 KKiiloH 250066 KKeEgE f2ast KfKWEaiELiel a23ss:s KoWoAL a25e9 RKeAfLoEl 4s5sa KRKfieeEl hEo a3a0n3 wessr EKKoaAisE S09 ars KKioo o 38% s KRTER ases KKiEeEsL 192 aa fKeonit. 21e214 Ko 181 RKOE.T 111317 K BlEaC S sa16sw6 REEe 108 RSF 107 Page 20 p2e allfish_format_2009 21.877025 66 F F1a5r7 22a3m Ke uoa12m9 00381105 45 M0 2037 224448 KKooo 41035 ose7 4 F 3m 245 Ko sie 00643395 45 0FM 111357 224484 KKWoL e7s2s os06t167 35 MF 210503 224444 KKon o 713a9 o0s54t1 i4 MFam219 22404KKio %s0e2 00850997 54 FF2o6s8 223s Kkoomeu o07t4e8 35 ooFm a1y9 2283 KKSlEE a0ss 00535629 $3 FM22l0m a2e5 KKoil emsee 0430 3 OF 1.99 237 KEE 101 0459 5 F 055 249 Wis 108 00.922957 0.495 48 5s MF 007s7 Foss 22458 25 KKoSO g ae1ss3a7 o05t37 66 FFooss 2250 KROiAu saries 00338533 44 MFooe x 224a4 KKioo 427 00447587 5s F Fo os s 226a KKoo o owam 00434385 55 OF F o076 2244 kK.Koo 51750 0o4z0s0 53MFositm a24e Ke rwida 005130 2 F4 oos0es 22338 KoKiot eass 0432 5 Mm 036 24 Koi 526 00269793 74 OF F o053 221088 RKEoTE s2068 0358 4 F 027 238 fr 279 00225315 08% 33mM03043 IE om 222148 KKEiFTlE a48s ms kin ms 0.269 3 OF os 245 KET 703 os0.14415 0229 55 0MM om033 3 Fos 22403 gikos: 609 2% Kod an 00255650 63 F 4 oxos 2230 KKii.. 4239 01352070 35MMosass 22458 KeSwihkh dseeo 22.127088 oss2 6 MM23488 4 Fos 225a ae bKhi,b 7 102 Coan Page21 p25 alfish_format 2009 i PY ow on Eee ow 21.733749 75 MF05a7s 224468 KKio 57220 02842512 47MF20a0 224a8 KKoisooo 7189 11.862824 s5s MFaiemr 22489 saes 2109 6 M54 23 Kio 573 1.1.068529 54mF 562 118 248 25 KK' 0o0u0 230 906 00.099658 45 MM043527 224484 KK.o- ol 2a316 0021 2 4 om 25 Si wa 0039 FE 086 244 Hoe 002 000..011743784 66iFMM03 00747 222444658 K Kii oo 336718 as1 001018s0 6fomM 0om% 2a4m9o gKoio 99 a 000.100373191 2F 46 FF 0o9m8 22 22159 RKeiE lkli: Yawssi 000000246073 2533OF0 0o8m 224466 a4 KKKEvEhEneE ea9sm10ao 00501849 54 MFoimr 22658 KKooot. a56s8 00.358399 0394 42 3 mFFM a: 227235 224495 239 KSEod 8e7s.s4 ow 00668144 5iFFam42 22m5 F_ m 0.363 3M 342 24 THE 4 006.2203 3 5 mFMf 119123 22e5 RiKDA e1i6s 00.27304 52 FF252367 223486 KoKheiir T1e2s8 0535 4am 105 248 Kish om 0645 4F 298 25 Koo eat 0621 6F 3.06 24 KEE te 00.531919 oo F5R Mis072 6 F 1s 921432896 BEKiMiE:tWt284s90a8r 00357150 53 mFM 09o1s e91s9 "ESuhia 1a0t00 00749310 85 FFos171 2t4e2s EKOiRnG ss0w2 00.334654 0788 a i8 FmFam1i7a6 s2omr EKWEO: o2i1e0 17s Blade aso 0.669 6 F 124 276 B hy 632 0714 6F 0.41 246 KEK 298 Page 22 0868 00.765804 00357427 00423923 00.441396 00388520 0032630 0911 00280806 00233018 00.006499 00.005408 00006483 00.01i226 00080759 00005128 00101683 20.200467 11660333 2120 01..959542 11..451917 00780%0 1015 1.450 0815 01.473524 21091108 00000270 p.2s alfish_format 2009 6 F om 787 401 56 FJ 171962 224383 KoKia o 264726 35 FF o0.a44 226409 RtTl 7w8e5 3+ F F osom 22057 Koo. 456%1 5 oOmF 0044 22459 KK 2259 $8 FFosom a2m3 mK aw m61r2 s3 omFozom 2a3m gKiU wasm s Fost 248 Koo 77 237 a MMFozo0e3r 22489 KK 248 K. 952815 200 3 101 24 Keno 183 5FE mM o03m4 224466 Kaom0 1m9a5 33 F OF os047 3 ow aw 22446 am RKKFOTE s7s39 ay T3 oeFosom o25m1 ogKoon m14e3 55 mmMM 0i3t%e 2265 K KO 7 s2s04a 4 Fos 2 mM oss 224688 KK.i of aat6e 4aMozoz 224347 KKoioo. 92060 6 Mom 3 OF 101 23 243 KEKTUC m3 10s 6 Mass 248 Koo ess 55 0FM 6 Mm 377429 397 24922439KKiKLtiTl sasses 120 65 M0mM 5 OF 332214 079 21a223i0i5KiEii 1s34e0 om 25 wFm 220676 22234 kii i o87n4 5FYOF 0m7o7 2zae m19e6 5F 326 226K id 586 4M 254 243K 17 3 6 F 162982 221323 Kifoetoy a8769 66FE MF 0.N95 no 22251aasKi C10 Kribio 168me [I N20 K 105 Page 23 p27 alfsh_format 2009 0001281 J J NNo 22d5 KKiidnai. seamt G00o001163 T 1 vuSNNN 246 a25m kK KAi EnL 831 m11s5 0013 1 N 248 KIT 139 0.009 1J N 249K A 18.1 Page 24 p28 alfsh_format2009 'PEOSCODPFOSCMMT /;PRBSPPE'PEBSCOD PFHSFPEPRHSCODPFOSAPPIPFOSAGO MPCAMiss R Pool2-SMB #1 fillet L7474-38 (A) 33.1 MPCAMiss R Pool2 -SMB #2 fillet L7474-39 (A) 5.04 MMMPPPCCCAAAMiLLs8B6s611R66-P2.o52oW6lE2W-2-1EWB #2, #3, #4, #5- fillet composite L7474-40 (A) 454 MMPPCCAA LLeB61166..2278WW4EE3 MMMPPPCCCAAA LLL8B86G6111666.-.6870CCaaarrrppp---132 MMMPPPCCGAAA LLL68865G111666.-.912C09aCSraMprB-p-4-15 MMMPPPCCCAAA LLL88855G111666...3332105SSMMMBBB---432 MMMPPPCCCAAA LLLBBB6GG111666...233034W5SBMM-BB1--56 MMPPCCAA LL88661166..2221WWB8-.32 MMMPPPCCCAAA LLL8B8666111666-..122134SWWMBBB--u45falo 3aMMCChhaamnneell ccaasshh 76 0055KK KK 33MMGChhaammnneell ccaatsshh 9& 0055KK KK 3S3MMMSSCmmhaaallniinmmeooluucttahhtfbibsaahssss1021 0055KK 05K KK K S33MMMSSSmmmaaalllimmmooouuuttthhh bbbaaassssss 543 0055KK 05K KK K 33MMBBlluueeggiill ssuunnffiisshh 76 [05KSS K K 33MMGChhaamnnneell ccaasthh 1176 0055KK K K S3MMCGhhaanmnneell ccaattficshh 1198 0055KK KK 33MMGShmaamlnmeolucthasbhas20&s 0055KK KK 33MMSSmmaallimmoouutthh bbaasss7s8 0055KK KK 3SMMBBlluueeggiill ssuunnffiisshh 1143 0055KK KK SSMMCChhaannnneell ccaatitshh 2276 0055KK KK 3SMMCChhaannnneell ccaatftishh 2206 0055KK KK 3MChannel cath 30 05K K Page 25 alfsh_format_2009 `3aMMSSmmaalliimmoouutthh bbaassss 910 20335K K K 33MMBSlmuaelgiimlosuutnhfibsahs2s011 0055KK K K A3MxBylsuLeTgIi3l1s1u-nf1i3sRh 21 40851KK K AAxxyyssLL1111331111--1145 RR 448933KK AAxdyssLL1111331111--1176 A R 485 K 4.95 K AAxxyyssLL111B31111--S12RR 459083KK AAxxyyssLL1111331111:-67 RR 485K 495K AAAxxxyyysssLLL111111333111111---981RR0R 447849KK 4.95 K m AAxAxyxyysssLLL11111333111111---1121RRR(A) 449983KK 49K AXAAxxYyySss_LLL11111323191141-5-4:8R22 498 K 49849KK AAXXYYSSL11122994455.2234 48K 476 K AAAXXXYYYSSS_LL1111222909444555-222567 44335 K K 5K AAXXYYSS_L11220044552298 (A) 448983 K K AAXXYYSSLL1122994465--130 4499KK AAAXXXYYYSSS_LLL1112229949644:55256 4955 KK 49K AAXXYYSSLL1122993445-176 4a385 K K AAXXYYSSLL1122993344--1178 495 K aK AAAXXXYYYSSS___LLL111222099333444---212190 4858 KK 49K AAXXYYSSLL1122093344-2228(A) a48m5 K K AAXXYYSSL1112299334-4190 478K 485 K AAXXYYSSLL1122993344--1112 a4s3KK AAXXYYSSLL1122993344--1143 44993 3KK AAXXYYSS_LL1122993314--1152 4499KK Page 2s p.29 324.149K6 53708544 238521K 249K 538079 237K 1880 918865J 3234294K 2824 2429.45 K K 242 K 223488 K K 22465KK 224446 K K 248 K 245 K 22458 K K 245 K 22448 K K 248 K 226555 26.9427 227483 K 243 243 K 22445 K K 254764 K 224455 K K alfish_format_2009 AXAYXSY_SLL121023013-113-(1A4) 4a888 K K AAXXYYSSLL1122993311--1165 444965 K K AAAXXXYYYSSSLLL11122992330113--11187-1(A9) 443%5 K K 478 K AAXXYYSS_LL1122993311--2210 448877 K K AAXXYYSSL[1122903312-282 483 K 495 K AAXXYYSSL1122903322-910 a49r5 K K AAXXYYSS_LL1122998126--1117 493 K 478 K AAXXYYSS_LL1122991166--1189 4a73KK AAAXXXYYYSSS_LL1111222999111766-:212103 448237KK 469K AXAYXSY_SLL1122901176-2124(A) 452442KK AAXXYYSS_L1112299116:62248 4a73KK AAAXXXYYYSSSL11111222909111766-221655 4259 KK 493K AAXXYYSSTLL1I2290146B-2175 (A) 4a888KK AAXXYYSSLL1122994488--1176 458KK AAAXXXYYYSSSLLL111222099333333---111876(A) 488 K 4a988 K K AAXXYYSSL11122993333-2109 4% K 485 K AAXXYYSS 1111229033332212 5K as K AAXXYYSSL11122993333-2234 4a985 K K AAXXYYSS 1111229933332256 as5s KK AAAXXXYYYSSS_LL1111222999333444--222879 488 K 448833 K K AAXXYYSSL11122904354-3150 49K 493 K K AAXXYYSSLL1122994455:-1176 a8 K 478 K AAXXYYSSL[1122994455-1189 a4s%s K K AXYSL12945-20 am K Page 27 5.30 224444 K K 222438 K K 224498 K K 223349 K K 220324 K K 224488 K K 27.4169 K 223379 K K 22116 4KK 242K 223251KK 229276 K K 221156 K K 25246KK 22444 K K 25K 224446 K K 232339 249 K 25493 K 62854K 271 21483 K 302 234028 K 384 22446 4KK 224399 K K 223493 K K alfish_format2009 AAAXXXYYSYS_S_LLL111222999444566:.:222165 448%8 K K 476K AAXXYYSS__LL1122994466-:2287 a4385 K K K AAXXYYSS_LL1122904465-820 448758 K K AAAXXXYYYSSS_LL111122299934415-5-31900 498 K 4i6897 3KK AAXXYYSSLL112290332-212 488 K ar K AAXXYYSS_L1112290332:243 4a9 KK AAXXYYSSL1112299332:256 498K 483 K AAXXYYSSLL1122993312-273 4a592 K K AXAXYYSS_LL1122993311--2245 443588 K K AAXXYYSSLL1122993311--2276 463K 4% K AAAXXXYYYSSS__LLL111222099343118:-:22889 44855KK 503 K AAAXXXYYYSSS_LL111122299494848-8-11910 a4ra7KK 508 K L AAAXXXYYYSSS__LLL111222999444777---111534 4a78 KK 498 K AAAXXXYYYSSS_LLL111222999444777---111867 44993 5KK a7 K AAXXYYSSLL1122994477--1290 4853 KK AAXXYYSS_LL1122994477:-2212 448572 K K E AAXXYYSS_LL1122991477--1263 483 K a8 KE AAXXYYSSLL1122991177--1187 4a88 KK AAXXYYSSLL1122991177-:1290 45% KK AAAXXXYYYSSSLLL111222099111777---222312(A) aas9 K K 493 K K AAXXYYSS__LL1122991177--2245 439K 469 K AAXXYYSSLL1122091177--2267 48 K as K AXYSL12917:28 478K Page 28 p31 224464 K K 224048 KK 224483 K K 223406 K K 223446 K K 244 K 22336 K K 224498 K K 224425 K K 222469 K K 229 K 223419 K K 243 K 225215 K K 223387 K K 251 K 22338 K K 224496 K K 248 K 223318 K K 25 K 232668 K 242 K 22444 KE K 22439 K K 22455 K K 23 K 224169 K K 22439 K K 249 K 238 K aliish_format 2009 K AAXXYYSS_LL1122991177:-2390 4a885 K K AAAXXXYYYSSSLLL111222909843363---131100(A) 488 K 44359KK AAAXXXYYYSSS_LL1111222099333333-111234 448988 K K 48 K AAXXYYSSL11122993333-1257 488 K a8 K AAXXYYSS 1111229933332280 4% K ams K AAXXYYSSLL1122993343--130 49K 485 K AAXXYYSSLL112200343-423 (A) 4a875 K K AAAXXXYYYSSS_LLL11122299943354-4-154 ar5s KK 4% K AAXAXYXYSYS_SLLL111222909444566:--21154 5K 45% KK AAXXYYSSLL1122994466--1176 4855 KK AAXXYYSS L11122994466-1189 448888 K K AAAXXXYYYSSS__LLL111222999444666::.222120 44989KK as K AAXXYYSSLL1122904466:2234 (A) 4a881 K K AXAYXSY_SLL112924954-543. 44%78KK AAXXYYSS_LL1122993311--12 487 K as K AXAYXSY_SLL1122993311--43 442667 K K AAXAXYXYSYS_SLL111122299393131-.1576 4487KK 437K AAXXYYSSL11122993311-89 44529KK AAXXYYSSLL1122993311--1110 aas2s K K AAXAXYXYSYS_SLLL111222999333222::-222978 478 K 4a7s8s K K AAAXXXYYYSSS__LLL11122299913162:6-6730 4955 KK 5K AAXXYYSSLL1122991166:89 495K 4% K Page 29 p.32 224339 K K 224448 K K 22741 4KE 297 E 23444 E K 450277 42 327345 22564 32775K 249 K 22458 K K 25 K 243 K 22454 K K 244 K 224459 K K 2244KK 22494KK PES 22384KK 213 K 223348 K K 224 K 222168 K K 245 K 223463 K K 239 K 223393 K K 22458 K K 22458 K K 249 K AAAXXXYYYSSS___LLL111222999111666---111102 AAXXAYYXSSY__SLLL11122299911661--611534(A) AAXXYYSS__LL1122991166--116 AAAXXXYYYSS_S_LL11122200941186-6123 AAXXYYSS 112200448823 AAXXYYSS (112200448854 AAXXYYSS 11112200448876 AAXXYYSS 1111220044772254 AAXXYYSS_L11122004477-2267 AAXXYYSS 1111220044772289 AAXXYYSSL111220044773310 (A) AAXXYYSS 1111226933442254 AAXXYYSS 11122093384126 AAXXYYSS 11112200333323 AAXXYYSS_L1112260335354 AAXXYYSS 11112200333367 AAXXYYSS11112200333398 AAXXYYSS 11112200334476 AAXXYYSS 11112200344683 AAXXYYSSL11122004466-45 AAXXYYSS 11112200446667 AAXXYYSS 11112200446698 AAAXXXYYYSSSL11111222000444666111210(A) + AAXXYYSS_L1122004456-4113 alfishformat 2009 449935 K K 449955 K K 4958 KK a4975 K K 4955 KK a58 KK a4g9e3 K K 449s5 K K 449488 K K a4349 K K 4953 KK 4a983 K K 4593KK 498 K 4a978KK 4858 KK a4881 K K 4583KK 44798 3KK 4955 KK 448988 K K 4a985 K K 4a995 K K 448933KK 44978 6KK 449853 K K 493 K Page 30 p.33 224468 K K 224488 K K 22459 KK 223488 K K 32.4489 K 5235 E K 224486 K K 224458 K K 222%0 E K 225179 K 12353 K 214363 K 22456 K K 226528 27428 E K 2254 K K 237759 E E 250426 K E 22927 E 361882 223428 K 412783 02832 K 246 K 223489 KK 83 E 62365 K d alfish_format 2009 AAXXYYSSL1112299454-51123(A) 49K 465 K AAXXYYSSL11122994352-2104 a43s5 KK AAXXYYSSLL1122993322::2212 44998 3KK AAXXYYSSL1122093322:2243 (A) 4598KK E AAAXXXYYYSSS_LLL111222999333222-::122256 5K 44699 3KK AAXXYYSS_LL1122903322--1134 aas7s K K AAXXYYSSL112290322-1156 (A) 493 K 498 K AAAXXXYYYSSS_LLL111222999333222---111789 44955 K K as K AAXXYYSS_LL1122994488--1132 44933KK AXAXYYSS__LL1122994487--114 449838 K K AAXXYYSSLL1122994477:-32 498K 503 K AAAXXXYYSYS_SLLL111222990444777---465. (A) a5n KK 498 K AAXXYYSSL11122994477.87. 495 K 495 K AAXAXXYYYSSS__LL111122299044477-7-11910 4a8r8s K K 478 K AAXXYYSSLL1122991467--41.2 448955 K K AAXXYYSS_LL1122901176-:25 498474KK AAXXYYSS_LL1122991177-:43 (A) 449486KK AAXXYYSS_LL121921971:756 448891KK AAXXYYSSLL1122991177--87 444687KK AXAYXSY_SLL1122991177-:190 448883KK AAXXYYSS_LL1122991177--1112 452K 4.85 K AAXXYYSSL11122991166:2298 44625 0KK AXAYXSY_SLL1122091176--130 a249KK AAXXYYSSLL1133114488:20 4958 KK Page 31 p34 661 224458 K 385 28895 157162 252 E 234765 K 689053 476 430079 272 228436 K 224466 K K 224489 K K 225317 K K 226436 K 224488 K K 620367 K 223493 K K 22448 9KK 223479KK 428366K 24K 323354K 224442KK 222463KK 22132 K K 221245KK 22459 K K AXYS 1131483 AXYSL13148-4. AXYSL131485 AXYSL131486 AXYSL131487 AXYSL131488 AXYS1131489 alfish_format_2009 5K 4% K 43K 5K 515K 495K 4K p.35 25K 249 K 248 K 25K 258 K 248 K 249 K Page 32 p.36 alfish_format 2009 PFPGAPPEPFPeACOI PFDAPPB 297 PFDACOD PFURAPPE 24 PFUACO! PFDOAPPE 473 PFDOACOI PFHXAPPE 0558 242 a 223 163 253 162 065 0767 Page 33 p.37 alfish_format2009 24K 24K 264 369 24 246K 263 246K 2.46 K 246 242K 383 3 242K 242 243K 248K 78 248K 474 248K 25 248K 243 248 251K 251K 251K 251K 251 249K 243K 249K 243K 249K 243K 249K 243K 249 243 248K 248K 248K 248K 248 237K 244 237K 237K 237 235K 248K 329 248 345 2.48 308 248K 235 248 246 K 321 332 289 245 249K 249K 249K 249K 249 245K 249K 245K 249K 245K 249K 245K 249K 245 249 245 K 245K 245 K 2.45 K 245 249 K 242 K 249 K 242 K 249 K 242 K 249 K 242 K 249 242 288 K 238 K 238 K 238 K 238 248 K 292 248 K 248 K 248 246 K 246 K 246 K 246 K 248 25 K 246 K 25K 246 K 25K 246 K 25K 246 K 25 248 244 K 244 K 244 K 244 K 244 248 K 248 K 248 K 248 K 248 245 K 245 K 245 K 245 K 245 25 K 25K 25 K 25K 25 248 K 245 K 248 K 245 K 248 K 245 K 248 K 245 K 248 245 24K 24K 24K 24K 24 248 K 298 248 K 248 K 248 248 K 23 K 292 254 248 K 23 K 248 K 23 K 248 236 25 K 246 K 25K 244 K 25K 244 K 25K 244 K 25 244 245 K 243 K 669 321 437 243 K 27 243 K 245 243 239 K 367 238 K 239 K 239 239 K 243 K 263 271 239 K 243 K 239 K 243 K 239 243 22454KK 226889 24K 243 24 245 K 245 K 245 248 K 248 K 329 248 K 248 K 248 K 246 K 246 K 246 246 245 K 317 245 K 245 K 245 245 K 245 K 245 K 245 K 245 Page34 244 K 244 K 248 K 223 K 248 K 249 K 239K 234 K 234 K 222 K 248 K 248 K 23 K 246 K 239K 237 K 216 K 214 K 242 K 235K 221K 226 K 237 K 216 K 215 K 25 K 246K 24 K 244 K 25K 206 K 248 K 24K 249 K 249 K 243 K 25K 24K 24K 248 K 243 K 25K 244 K 202 K 242 K 245 K 246 K 248K 239 K 249 K 243 K 2% K 278 244 K 248 K 258 248 K 249 K 239 K 231 K 231 K 202 K 248 K 248 K 236 K 248 K 239 K 237 K 216 K 214 K 282K 235K 221K 226 K 266 216 K 215 K 25K 246K 24K 244 K 25K 246 K 252 271 333 381 243 K 25K 352 324 345 299 25K 244 K 32 242 K 245 K 248 K 244K 239K 219 K 243 K 239 K alfish_format 2009 384 244K 248 K 223 K 248 K 249 K 239 K 234 K 234K 212 K 248 K 248 K 23 K 245 K 239 K 237 K 216 K 214 K 202K 235K 221K 226 K 297 K 216 K 215 K 25 K 246K 24K 244 K 25 K 246 K 244 K 24K 67 249 K 243 K 25K 24K 241 248 K 243 K 416 244 K 438 202 K 245 K 246 K 244 K 239 K 249 K 243 K 239 K Page3s 224444 KK 248 K 223 K 248 K 249 K 239 K 234 K 234 K 242 K 248 K 248 K 23 K 246 K 239 K 237 K 216 K 214 K 242K 235K 221K 226 K 237 K 216 K 215 K 25K 246K 24K 244 K 25K 248 K 244 K 24K 208 249 K 22435KK 24K 24K 248 K 243 K 118 244 K 9.44 282 K 245 K 246 K 244 K 239 K 249 K 243 K 230 K p.38 224444 248 223 248 249 239 234 231 222 248 248 236 246 239 237 216 214 242 235 221 228 247 216 215 25 248 24 244 25 2.46 2.44 24 249 249 22453 24 24 248 243 25 244 242 242 245 246 2.44 239 249 243 239 246 K 223484 K K 244 K 224438 K K 224369 K K 234 K 224446 K K 22336 K K 224498 K K 242 K 224256 K K 222499 K K 223419 K K 243 K 225215 K K 223387 K K 225319 K K 224398 K K 224486 K K 238 K 231 K 22256 K K 228324 K K 22444 KE K 224%9 K K 22455 K K 22436 K K 221395 K K 224499 K K 238 K 248 K 223484 K K 244 K 224483 K K 224369 K K 234 K 224446 K K P23ESK 224498 K K 242 K 224256 K K 222499 K K 223419 K K 243 K 225215 K K 223378 K K 225319 K K 223489 K K 224486 K K 238 231 K 22353 K 333915 22444 KE K 22439 K K 22455KK 22438 K K 223159 K K 224499 K K 238 K alfish_format_2009 246 K 244 K 224348 K K 224438 K K 224369 K K 284 K 224146 K K 23 K 22438 K K 224492 K K 224256 K K 222499 K K 231K 224439 K K 225 K 225317 KK 238 K 225319 K K 224398 K K 224486 K K 238 K 22315KK 226 K 513 282 24 KK E 244 K 224%9 K K 22455 K K 2263 K K 223159 K K 224499 K K 288 K Page 36 224446 K K 224348 K K 224483 K K 224369 K K 223446 K K 22438 K K 22438 K K 249 K 224425 K K 226 K 222499 K K 231 K 224493 K K 225 K 225317 KK 225318 K K 239 K 224398 K K 224468 K K 223318 K K 22265KK 2442 K 22444 KE K 224396 K K 22455KK 22463KK 221395 K K 224499 K K 238 K p.39 224446 22.3484 224438 223496 223446 223464 224386 249 224452 226 222499 231 224493 225 225317 225318 239 224398 224468 223318 22256 204 242 22444 224396 22455 22436 223159 224499 238 223493 K K 224488 K K 224445 K K 224449 K K 22444KK 249 K 224557 K K 223473 K K 22435KK 224397 K K 25K 248 K 22453 K K 25 K 224444 K K 249 K 22454KK 2244KK 249 K 228347 K K 24K 221331 K K 238 K 221284 K K 226 K 224435 K K 23 K 223339 KK 22395KK 248 K 22458 K K 249 K 223493 K K 324148 K 224445 K K 224449 K K 22524K 249 K 223475 K K 323423 K 327453 K 237K a25119 22925K 22453 KK 224446 K K 268 22554K 22494K 249 K 224371 K 24K 223143 K K 238 K 221284 K K PES 230443 K 236 K 22339 KK 239 K 22458 K K 22458 K K as alfish_format 2009 224339 K K 224448 K K 224445 K K 224489 K K 22444KK 249 K 224357 K K 228473 K K 243 K 25 K 224397 K K 25K 22485KK 243 K 25 K 224464 K K 249 K 22454KK 2244KK 249 K 223547 K K 24K 223143 K K 238 K 221284 K K 226 K 224633 K 23 K 223393 K K 22395KK 22485KK 248 K 249 K Page 37 223493 K K 224448 K K 224445 K K 224449 K K 22444KK 249 K 224357 K K 223473 K K 22435KK 224397 K K 22458 K K 22835KK 25K 224444 K K 249 K 22454KK 2244KK 249 K 223917 K K 24K 223143 K K 238 K 222108 K K 226 K 224435 K K 22339 K K 223393 K K 22485KK 22485KK 249 K p.40 223493 224448 224445 224449 244 24 22.3479 245 223473 243 22357 249 22.458 22453 22454 244 224459 24 2244 228479 234 24 223143 222348 218 224256 243 223369 223339 22458 22458 594 224468 K K 248 K 224498 K K 25 K 223488 K K 22458 K K 22445KK 224448 K K 224458 K K 224294 K K 22129 K K 22456 K K 246 K 24 K 22456 K K 224495 K K 223494 K K 2254KK 2245 K K 282 K 23 K 224488 K K 22458 K K 224498 K K 224484 K K 224492 K K 224469 K K 223488 K K 282 K 246 K 224468 K K as24t8 K 249 K 25 K 224388 K K 329418 K 22445KK 224446 K K 244752 K 62.3166 233189 K 2575 123456 K 22465KK 224495 K K 225494 K 42.394K 24K 22759 K 238 K 364585 339424 238324 381583 214426 K 325419 K 22318 K 483 347 alfish_format 2009 224486 K K 224488 K K 249 K 25 K 223488 K K 826498 K 244 K 22458 K K 224485 K K 37.9345 224 K 22129 K K 22056 K K 284162 K 25K 224459 K K 224359 K K 244 K 2264K 24 K 22452 K K 243186 K 248 K 22544KK 827 3544 248 K 829882 K 224469 K K 213188 K 242 K 295 Page38 224468 K K 224488 K K 22495KK 223488 K K 22485KK 22445KK 244 K 224465 KK 244685 K 220 K 22129 K K 22456 K K 228466 K 22465KK 249 K 223495 K K 248 K 2254KK 24 K 22452 K K 223988 K 22485KK 72.4341 K 330822 248 K 627422 K 224469 K K 29338 K 242 K 246 K p41 224488 224488 22459 223488 22458 244 22.454 224465 224489 224 22129 22.456 22446 22458 2.49 224359 244 2254 24 22452 22.3486 2.48 22454 249 224484 248 224492 224469 223488 242 248 228435 K K 224498 K K 224496 K K 22459 K K 22355 K K 246 K 224937 K K 246 K 224498 K K 22484KK 224486 K K 224446 KK 225419 K K 237 K 22456 K K 224488 K K 244 K 223397 K K 224483 K K 249237KK 222439KK 22345KK 222344KK 224424KK 222463KK 221323 K K 221245KK 22459 K K 253313 K 240723 425527 24845 42255 K 248 K 231473 K 246 K 239492 275 26 423456 K 234082 K 324093 K 251337 K 246 K 224488 K K 248 K 223997 K K 224483 K K 321237K 82.4449K 22345KK 324334K 224472K 222463KK 221323 K K 252245K 22459 K K alfish_format2009 224553 K 301 349026 326 237992 32375K 246 K 433268 246 K 354085 234383 K 288 224468 K K 224449 K K 265 237 K 23486 K 224488 K K 244 K 223397 K K 224483 K K 249237KK 326449K 22345KK 24324K 224442KK 222463KK 223132 K K 222415KK 22459 K K Page 39 224656 K 248 K 230419 K 374 229937 4.2095K 234467 K 266 234867 K 258 224928 K 246 K 224466 K K 224494 K K 225317 K K 22456 K K 248 K 224448 K K 223379 K K 224483 K K 242397KK 222479K 22345KK 82.4394K 224424KK 222463KK 221323 K K 221245KK 22459 K K p.42 223435 248 224499 246 22459 22355 22.3476 243 22.4496 248 248 22446 224468 22.4494 225317 22458 2.48 224448 223397 22.4438 249 223479 223 235 22244 223444 242 224236 221323 221245 22459 25 K 224496 K K 22556 K K 224489 K K 25 K 224496 K K 22585KK 225459 K alfish_format 2009 22459 K K 246 K 22558 K K 224498 KK 22459 K K 22465KK 258 K 224498 KK p.43 22459 22456 258 224489 Page 40 p44 alfish_format 2009 PFHXACOI K PFHpAPPE 0.491 PFHPACOI K PFNA0P.4P9B5 PFNACOD K PFHXSPPEPFHXSCOI 206K PFBAPPB PFBACOD K K 0.087035KK 0507668KK 512234KK Page a1 p.45 alfish_format 2009 K 24K 24K 481K 24K K 246K 246K 493K 246K K 242K 242K 483K 242K KK 224438KK 224438KK 44.9855KK 224438KK K 251K 251K 503K 251K 249K 249K 4.98 K 249K K 243K 243K 485K 243K K 248K 248K 4.95 K 248K K 237K 237K 474K 237K K 235K 235K 469K 235K K 248K 248K 495K 248 K K 246K 246 K 493K 2.4K6 K 249K 249K 498K 249K KK 224495KK 224495KK 44998KK 224459KK K 2.45 K 2.45 K 49K 245K K 249 K 249 K a9 K 249 K K 242 K 242 K 483 K 282 K K 238 K 238 K a7 K 238 K K 208 K 248 K 495 K 218 K K 246 K 248 K 493 K 248 K K 25 K 25 K 5K 25 K K 246 K 246 K 493 K 246 K K 240 K 244 K 488 K 244 K K 248 K 248 K 495 K 248 K K 245 K 245 K 4s K 245 K KK 22458 KK 22458 KK 4955 KK 22458 KK K 245 K 245 K 49 K 245 K K 24K 24K as K 24 K K 248 K 248 K 495 K 248 K K 248 K 248 K 495 K 248 K K 238 K 236 K a2 K 236 K KK 22450 KK 22454 KK a5s KK 22454 KK K 245 K 245 K a9 K 245 K K 243 K 243 K 485 K 243 K K 239 K 239 K 478 K 239 K K 239 K 239 K 478K 239 K K 243 K 243 K 485 K 213 K KK 22454KK 24K 245 K a8 K 49K 24 K 245 K K K 224468 KK 224466 KK a4993 KK 224466 KK K K 245 K 245 K 245 K 245 K 49K 49K 245 K 245 K Page 42 p46 alfish_format_2009 K K 224444 K K 224444 K K 4a8s8 K K 224444 K K K K 222438 K K 222438 K K a4945 K K 222438 K K K K 224198 K K 224498 K K 449985 K K 224498 K K KK 223349 KK 223349 KK 446778 KK 223349 KK K 234 K 234K 467 K 234 K K K 224882 K K 224282 K K 4a985 K K 224282 K K K K 224%8 K K 22438 K K a49n5 K K 223468 K K K K 223496 K K 223196 K K a49m5 K K 223196 K K K K 237K 216 K 221367 K K 4a73KK 221367 K K K K 22104 2KK 224124KK a4287 K K 220124 K K K K 222315KK 222315KK 114629KK 222315KK K K 22236 7KK 222567 K K aas7e K K 223276 K K K K 221165 K K 216K 215 K 4a329KK 221156 K K K K 25246 K K 25246KK 549K3K 25246KK KK 22440 KK 22404KK 4ag8 KK 22444 KK K K 22456 K K 22456 K K 4953 KK 22456 K K K K 22444KK 22404KK a4888 K K 22444KK K 249K 249 K 4% K 249 K K K 224439 K K 224439 K K 448%5 K K 224493 K K K K 2254KK 2245KK 5K a8 K 2245 KK E K K 22484KK 22484KK 4a895KK 22448 K K K K 243 K 25 K 22435KK 4855 KK 243 K 25 K K K 222424 K K 228428 K K 448838 K K 224424 K K K K 224152 K K 224425 K K 44833KK 224425 K K KK 22446 4KK 22446 4KK 44983 8KK 246 K 244 K K K 224399 K K 22349 9KK 4a798KK 224399KK K K 223453 K K 243K 2% K 447885KK 224339 K K Page 43 p47 alfish_format_2009 K K 224464 K K 224464 K K 483K 488 K 246 K 244 K K K 238 K 244 K 238 K 244 K 447868KK 223484 K K K K 224483 K K 224483 K K 495 K 485 K 248 K 243 K K K 224369 K K 223496 K K 4a973 K K 224369 K K K K 234 K 216 K 238 K 246 K 446973KK 223146 K K K K 22434 K K 22434 KK a4828 KK 22438 KK K K 23 K 248 K 23 K 248 K ar K 495 K 23 K 248 K K K 224429 K K 224892 K K 498K 48 K 224429 K K K K 245 K 226 K 245 K 226 K 49K 452 K 224256 K K K K 249 K 229 K 249 K 229 K 498K 459 K 249 K 229 K K K 223419 K K 231K 249 K 463K 4% K 223419 K K K K 224235 K K 222435 K K a4ss5KK 243 K 225 K K K 251 K 237 K 251 K 237 K 503 K a7 K 225317 K K K K 225318 K K 225318 K K 457083 K K 22531 K K K K 239 K 238 K 239 K 238 K 447786KK 223398 K K K K 249 K 246 K 249 K 246 K 449938KK 224469 K K K K 248 K 238 K 248 K 238 K 443756 K K 224388 K K K K 22315KK 231 K 25 K 463K 5K 231 K 25 K K K 223216 K K 222364 K K 4a627 K K 223264 K K KK E 22442 KK E 22142 KK E 4a881 KK E 22442 KK E K K 22430 K K 244 K 23 K 4a88 KK 284 K 23 K K K 22495KK 22495KK 4958 KK 249 K 25 K K K 245 K 23 K 245 K 23 K as K as K 245 K 23 K KK 22416 9KK 224169 KK 44933 9KK 224169 K K K K 223459 K K 223459 K K 4a689 K K 223459 Ki, Ko K K 249 K 238 K 249 K 238 K 44978 6KK 249 K 238 K Pagedd p.48 alfish_format 2009 K 239 K 239 K 478K 239 K K K 224483 K K 224443 K K 44885 8KK 224443 K K K K 224458 K K 224458 K K 44935KK 224458 K K K 244 K 244 K 488K 244 K K K 224449 K K 224449 K K a4%8 K K 224489 K K K K 22454KK 22444KK aas8s K K 22484KK K K 223479 K K 223479 K K a47% K K 223479 K K K 245 K 245 K as K 245 K K K 223473 K K 223473 K K aas7s K K 223473 K K K K 22435KK 22435KK 485 K 5K 243 K 25 KE K K 224597 K K 225479 K K a4r9s8 K K 223479 K K K 25K 25K 5K 25K K K 22485KK 248 K 25 K 45% KK 22485KK K K 22435KK 22435KK 4855 KK 243 K 25 K K K 224444 K K 224444 K K 448888 K K 224444 K K K 249 K 249 K 4% K 249 K K K 22454KK 245 K 24 K a48s K K 22454KK K K 2244KK 2244KK aa8s K K 2244KK K K 223479 K K 223479 K K a47% K K 223479 K K K K 22344KK 22344KK 487K ag K 22344KK K K 213K 231 K 22133 0KK 4a627 K K 223143 K K K K 222308 K K 223280 K K aa87 K K 222868 K K K 218 K 218 K 437K 218 K K K 224256 K K 224256 K K 44529KK 224256 K K K K 224%3 K K 22433 K K aas2s K K 22433 K K K 239 K 239K 478K 239 K K K 22339 K K 223393 K K aa75 K K 22339 K K K K 22485KK 22485KK 45% KK 22485KK K K 22485KK 22485KK 4955 KK 22485KK ase 491 498 K 267 Page 45. p.49 alfish_format 2009 K K 246 K 248 K 246 K 248 K 449935 K K 224468 K K K KK 248 K 224498 KK 248 K 224489 KK 495K 449%5 K K 224488 K K 249 K K K 25K 238 K 22385KK 5K a7 K 25K 238 K K K 218 K 25 K 22485KK 4595KK 248 K 25 K K K 248 K 244 K 28 K 244 K 443858 K K 224484 K K K K 25K 244 K 22451 K K 4858 KK 22458 K K K K 246 K 245 K 248 K 245 K 44939KK 224465 K K K K 224489 K K 224489 K K 44995 8KK 224498 K K K K 220 K 22 K 220 K 22 K 448K 441 K 226 K 22 K K K 22195KK 219 K 25 K 4539KK 219 K 25 K K K 246 K 246 K 246 K 246 K 44933KK 246 K 246 K K K 2245KK 2254KK as K 5s K 2245KK K K 245 K 249 K 246 K 249 K 449983 K K 22469 K K K K 223459 K K 224359 K K 44789KK 223405 K K K K K 22445KK 24K 244 K 2254KK 4588KK as K 244 K 2254KK K K 2245KK 2254KK a58 KK 2245KK K K 220328 K K 223428 K K 44788KK 242 K 238 K K K 224458 K K 221468 K K 483K 4% K 224486 K K K K 22454 K K 22445KK 4858 KK 22454 K K K K 224498 K K 224498 KK a4s9s8 KK 234888 K K K 224484 K K 224488 K K 44898 5KK 224448 K K K K 224429 K K 224429 K K 74.382 3K 328022 K K K 224496 K K 224496 K K 45%5 K 224496 K K K K 238 K 248 K 238 K 248 K 476K 727 E 22388 K K K K 228426 K K 224428 K K 640343 E K 327486 K Pagea6 p.50 alfshformat2009 K K 223435 K K 228435 K K 43K 465 K 245 K 283 K K K 22489 K K 224198 K K 449%5 K K 227498 K K K 224496 K K 224469 K K 44398 3KK 224496 K K K K 25K 249 K 25K 249 K 5K 498 K 25K 249 K K K 22355 K K 22355KK 4859 KK 22355 K K K K 246 K 237 K 246 K 237 K 483K 47s K 224367 K K K K 224436 K K 224463 K K 4489s 3KK 224436 K K K K 249 K 248 K 249 K 248 K 449985 K K 224489 K K K K 22484KK 22484KK 435 K as K 22484KK K K 246 K 246 K 246 K 246 K 449933 K K 224486 K K K K 22446 4KK 224446 K K 493K 488 K 224446 K K K K 225419 K K 224519 K K 540338 K K 225419 K K K K 22375KK 22357KK ar5s KK 257 K 25 K K K 246 K 248 K 248 K 248 K 449935KK 248 K 248 K K K 224448 K K 224448 K K 44985 8KK 224484 K K K K 223379 K K 223379 K K aa7m K K 223397 K K K K 243 K 248 K 243 K 248 K 485 K 495 K 243 K 248 K K K 249237KK 249287KK 498474KK 249237KK K K 222439KK 222439KK 446968K 620419K K K 235K 24K 235K 24K 446891KK 235K 24K K K 223244KK 223244KK 4as687K 210344K K K 224442KK 224442KK 448883KK 224424KK K K 222463KK 224236KK 448552KK 224236KK K K 221323 K K 221323 K K 442605 K K 221323 K K K K 222415KK 2212.45 KK a249KK 221245KK K K 22459 K K 22459 K K 4358 KK 22459 K K Page 47 p.51 alfish_format_2009 K K 25 K 249 K 25 K 224496 K K 5K 44998 3KK 25 K 224496 K K K K K 246 25 K K 258 K 22558 K K 5155 KK 495 K 22558 K K 248 K K K 224489 K K 224489 KK as K 249 K Page 48 p.52 alfish format2009 DOWLKNUANAME ALT_NAME Page 49 p.53 alfish_format 2009 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-: 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-:8-81-)1) FRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll22 (U8-M1) R-M (UM- 8-1) RM 884444--884477.55 MMIISSSSIISSSSIIPPPPII A. R. PPooool2l2 ((UUMM-- 88--11)) ARMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-: 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88.-11)) RRMM 884444--884477..55 MMIISSSSIISSSISPIPPIPRRI.. PPooo22lo((UUlMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-: 88--11)) ARMM 884444--884477..55 MMIISSSSIISSSISPIPPIPRIR.. PPoool22o((UUlMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 2 2 ((UUMM-- 8-1) 8-1) RM AM 884444--884477.55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--11)) ARMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII A. R. PPooool2l2 ((UUMM-- 88--11)) RRMM 884444--884477.55 MMIISSSSIISSSSIIPPPPII A. R. Pool Pool 2 2 ((UUMM-- 88--11)) FM RM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--11)) RRMM 884444--884477..55 Page 50 p54 alfish_format_2009 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--11)) ARMM 884444--884477.55 MMIISSSSIISSSSIIPPPPII RR.. PPooooll 2 2 ((UUMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88--11)) FAMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--11)) ARMM 884444--884477..55 MMIISSSSIISSSSIPIPPIPRIR.. PPoool22o((UUlMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 8-1) 8-1) FM AM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-: 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 8-1) 8-1) FM RM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM: (UM- 88--11)) RM RM 884444--884477.55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-: 88--11)) RRMM 884444--884477.55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM-- 88--11)) ARMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM(UM- 8-1) 8-1) AM RM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--11)) RRMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. PPooooll 22 ((UUMM-- 88--11)) AAMM 884444--884477.55 MMIISSSSIISSSSIIPPPPII R. R. Pool 2 Pool 2 (UM- 8-1) (UM- 8:2) RAMM 884346--884473.5 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-: 88::22)) RAMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88::22)) RM AM 883366--884433 MMIISSSSIISSSSIIPPPPII A. A. PPooool2l2 ((UUMM-- 8:2) 8:2) AM AM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 ((UUMM-- 88:-22)) RM RM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88::22)) AAMM 883366--884433 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 8-2) 8:2) RM RM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. Pool 2 Pool 2 ((UUMM-- 88::22)) ARMM 883366-.884433 MMIISSSSIISSSSIIPPPPII A. R_ PPooooll 2 2 ((UUMM-- 88::22)) AAMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88::22)) RRMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88::22)) AAMM 883366--884433 Page 51 p.55 alfish_format 2009 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM(UM- 8:2) 8:2) AM RM 883366--884433 MMIISSSSIISSSSIIPPPPII RR.. PPooool2l2 ((UUMM-- 88-:22)) RAMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. Pool Pool 2 2 (UM(UM- 8:2) 8-2) AM AM 883366--884433 MMIISSSSIISSSSIIPPPPII AR.. PPooooll 2 2 ((UUMM-- 88-:22)) AM AM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM(UM- 8:2) 8:2) RM RM 883366--884433 MMIISSSSIISSSSIIPPPPII A. A. PPooool2l2 ((UUMM-- 88::22)) AAMM 38366--884433 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 88::22)) AAMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88:-22)) RRMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. Poo2l (UM- 8:2) Pool 2 (UM- 8:2) RAMM 883366--884433 MMIISSSSIISSSSIIPPPPII RA.. PPooooll 2 2 ((UUMM-- 88:-22)) AM AM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUNM-- 88::22)) RRMM 883366--884433 MMIISSSSIISSSSIIPPPPII A. A. Pool 2 (UMPoo2l (UM- 8:2) 8:2) RAMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 2 2 ((UUMM-- 88-:22)) AAMM 883366-.884433 MMIISSSSIISSSSIIPPPPII A. R. Pool Pool 2 2 (UM(UM- 8:2) 8:2) RM RM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88::22)) RRMM 883366.-884433 MMIISSSSIISSSSIIPPPPII A. A. Pool Pool 2 2 (UM(UM- 8:2) 8-2) AM AM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 2 2 ((UUMM-- 88::22)) ARMM 883366--884433 MMIISSSSIISSSSIIPPPPII RA.. PPooooll 2 2 ((UUMM-- 88::22)) RM RM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 2 2 ((UUMM-- 88-:22)) AAMM 883366--884433 MMIISSSSIISSSSIIPPPPII A. A. Pool Pool 2 2 (UM(UM- 8:2) 8-2) AM AM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88-:22)) RRMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. Pool 2 Pool 2 (UM- 8:2) (UM- 8-2) ARMM 883366-.884433 MMIISSSSIISSSSIIPPPPII A. A. PPooooll 2 2 ((UUMM-- 88-:22)) AAMM 883366--884433 MMIISSSSIISSSSIIPPPPII RR.. PPooooll 22 ((UUMM-- 88-:22)) AAMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM-- 88::22)) RRMM 883356--884433 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 2 2 ((UUMM-- 88--22)) RAMM 883366--884433 Page 52 p.56 alfish._format_2009 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 22 ((UUMM-- 88--22)) ARMM 883366--884433 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88-:13)) RRMM 884343-.854873.45 MMIISSSSIISSSSIIPPPPII A. R. Pool Pool 2 2 ((UUMM-- 88--33)) RM RM 8833335.-5883344 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 8:3) 8:3) RRMM 883333..55--883344 MMIISSSSIISSSSIIPPPP1I RR.. PPooooll 22 ((UUMM-- 88.-33)) RRMM 883333..55883344 MMIISSSSIISSSSIIPPPPII A. R. Pool Pool 2 2 ((UUMM-- 88-:33)) RM RM 8833335.-5883344 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88-:33)) RM AM 883333..55883344 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88-:33)) RRMM 883333.55-883344 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 8-3) 8:3) RM RM 883333.55--883344 MMIISSSSIISSSSIIPPPPII R. A PPooooll 22 ((UUMM-- 88:-33)) AAMM 882277--883300 MMIISSSSIISSSSIIPPPPII A. A. Pool Pool 2 2 (UM(UM- 8:3) 8:3) AM AM 882277--883300 MMIISSSSIISSSSIIPPPP1I R. A. PPooooll 2 2 ((UUNM-- 88::33)) ARMM 882277--883300 MMIISSSSIISSSSIIPPPPII A. A. PPooooll 2 2 ((UUMM-- 8:3) 8:3) AM AM 882277--883300 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88:-33)) RRMM 882277--883300 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 22 ((UUMM-- 88::33)) RRMM 882277--883300 MMIISSSSIISSSSIIPPPPII A. R. Pool Pool 2 2 (UM(UM- 8:3) 8:3) AM AM 882277--883300 MMIISSSSIISSSSIIPPPPII R_ R. PPooooll 2 2 ((UUMM-- 88.:33)) RRMM 882277--883300 MMIISSSSIISSSSIIPPPPII R. R. Pool 2 Pool 2 (UM(UM- 8:3) 8:3) RAMM 882277--883300 MMIISSSSIISSSSIIPPPPII A. A. PPooooll 2 2 ((UUMM-- 88::33)) AAMM 882277--883300 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-: 88::33)) RRMM 882277--883300 MMIISSSSIISSSSIIPPPPII AA.. PPooooll 2 2 ((UUMM-- 88-:33)) AM RM 882277--883300 MMIISSSSIISSSSIIPPPPII RA.. PPooooll 2 2 ((UUMM-- 88::33)) AM AM 882277--883300 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88-:33)) RRMM 882277--883300 MMIISSSSIISSSSIIPPPPII A. A. PPooool2l2 ((UUMM-- 88-:33)) AAMM 882277--883300 MMIISSSSIISSSSIIPPPPII RA.. PPooooll 2 2 ((UUMM-- 88-.33)) AAMM 883333.55-883344 MMIISSSSIISSSSIIPPPPII RR.. PPooooll 2 2 ((UUMN-- 88:.33)) RM RM 883333.55-883344 Page 53 p57 alfish_format 2009 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 8:3) 8:3) RM RM 883333..55-883344 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88::33)) RRMM 883333..55-883344 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 8-3) 8-3) RM RM 883333..55-883344 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88:-33)) RRMM 883333..55--883344 MMIISSSSIISSSSIIPPPPII R. A. PPooooll 2 2 ((UUMM-- 8:3) 8:3) AM AM 883333..55883344 MMIISSSSIISSSSIIPPPPII 8. R. PPooool2l2 ((UUMM-- 8-4) 8-4) ARMM881155--682200 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 ((UUMM-- 88--44)) AM RM 881155.-682200 MMIISSSSIISSSSIIPPPPII R. R. PPoolo22((UUoMM--8l8--44)) RAMM 881155--862200 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM(UM- 8-4) 8-4) RM AM 881155.-882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIPIPPIPAIA.. PPoool22o((UUlMM-- 88--44)) RAM8M1851-5-882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--44)) AAMM881155--882200 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM(UM- 8-4) 8-4) AM RM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM-- 88--44)) ARMM 881155..882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM:- 8-4) 8-4) AM RM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM-- 88--44)) RRMM 881155-.682200 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--44)) RRMM 8B1155--862200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. A. Poo2l Pool 2 (UM(UM- 8-4) 8-4) AM RM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM:- 8-4) 8-4) AM RM 881155--882200 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88--44)) AAMM 881155--882200 MMIISSSSIISSSSIIPPPPII RR._ PPooooll 22 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--44)) ARMM 8B1155--862200 Page 54 p.58 aliish_format 2009 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 22 ((UUMM-- 88--44)) RAMM 881155-.682200 MMIISSSSIISSSSIIPPPPII A. A. PPooooll 2 2 ((UUMM-- 88--44)) AAMM 881155--882200 MMIISSSSIISSSISPIPPIPRIR.. P Poolo22((UUoMM--8l8--44)) ARMM81851-5-682200 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 88-.44)) ARMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88--44)) RRMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM: (UM- 8-4) 8-4) AM RM 881155--882200 MMIISSSSIISSSSIPIPPIPRIR.. PPoool22o((UUlMM-- 88--44)) RAMM 881155.-882200 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 ((UUMM-- 88--44)) AM RM 881155--882200 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88--44)) AAMM881155--862200 MMIISSSSIISSSSIIPPPPIIR.. PPooooll 2 2 ((UUMM-- 88-:33)) RRMM 883333.55-883344 MMIISSSSIISSSSIIPPPPII RR.. PPooooll 22 ((UUMM-- 88:-33)) RRMM 883333..55883344 MMIISSSSIISSSSIIPPPPII R_ R. Pool Pool 2 2 ((UUMM-- 88::33)) AM RM 88333355--883344 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88::33)) RRMM 883333..55883344 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 (UM(UM- 8:3) 8:3) RM RM 883333.55--883344 MMIISSSSIISSSSIIPPPPII A. R. PPooool2l2 ((UUMM-- 88::33)) FRMM 883333..55883344 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMN-- 8-3) 8:3) RM AM 883333..55-883344 MMIISSSSIISSSSIIPPPPII R. R. PPooool2l2 ((UUMM-- 88::33)) ARMM 883333..55883344 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 88--34)) RRMM 881353-.8528034 MMIISSSSIISSSSIIPPPPII R. A. Pool Pool 2 (UM- 8-4) 2 (UM- 8-4) AM RM 881155.-882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. Poo2l Pool 2 ((UUMM-- 88--44)) AM AM 881155..882200 MMIISSSSIISSSSIIPPPPII A. R. PPooooll 2 2 ((UUMM-- 88:-44)) RAMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 8-4) 8-4) AM AM 881155--882200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--44)) ARMM 881155--882200 MMIISSSSIISSSSIIPPPPII R. A. PPooool2l2 ((UUMM-- 88--44)) RAMM 881155--862200 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--11)) RAMM 884444-.884477..55 Page ss 5.59 allish format 2009 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--11)) AAMM 884444--884477..55 MMIISSSSIISSSSIIPPPPII R. R. Pool Pool 2 2 (UM(UM- 8-1) 8-1) RM AM 884444--884477.55 MMIISSSSIISSSSIIPPPPII R. R. PPooooll 2 2 ((UUMM-- 88--11)) RRMM 884444::884477..55 MISSISSIPPI R. Pool 2 (UM- 8-1) RM B44-847.5 Pages p.60 squaamlpiflieed samPpFlCes (coded as "E" for estimated) 009900016232 PFA ALL 009900114319 PPFFOOSSAA 090142 PFOSA 009900115917 PPFFBOASA 090203 090215 PPFFOOSSAA 009900222109 PPFFOOSSAA 009900222223 PPFFOOSSAA 090227 090229 PPFFOOAA 090281 090233 PPFFOOAA 009900223364 PPFFOOAA, PFHxS, PFOSA 009900223477 PPFFOOAS,, PPFFHOXSSA p61 1 ENVIRONERNeTrALorLiGtoBOERuATnOoRsY Final Report FluorochemiMciaslsiCshsairpapciteRriivzeart--ioPnooofl Surface Water 2; July 2009 Samples, Laboratory Request Number: E09-0365 75.S8e-1k54P:h3asDeetEexrmaiMcnetaottnihooandnodfRHPeieqgfuhuioPrreeirmnfeaonlmetda:nAcc3iedMLs,iMAecdotnhCoholvdso,mEAaTmlSiod-ge8rsa-,p1ha5yn4ld.MS3asuslSrpleecstoimn eWtayl'aby meee eeE em----R--e--Dpr oto-rAeugutste12,20t 06 mereee Testing Laboratory. --ST-- 3M EHS Operations 3M EnBvuiilrdoinnmgen2t6a0l-5LNa-b1or7atory Maplewood, MN 56144-1000 Requester Gary Hohenstein 3M Building 224-5W-03 Saint Paul, MN 55144-1000 Phone: (651) 737-3570 aa TE heatesE tiang onpeitledeohveeiroioonimnpnao1mn5ee:0nesTtceshweonfrgqT50us1n50iir0rnsgomananndesCosfawliIniEinC L 17a02m52aa005n"b GSIanansnac.dcaosr3da5cn 0evi Contiicats #2052.01 once p62 ENVIRONME"NRTeAbOLRLTANBGOER0A0T0O3R85Y 3M Environmental Laboratory 3aMM PErnivnicriopanlmeAnntaallytLiacbaorIanvteosrtyigMaatnoargaenrd: ReWpiolritamAuKt.orR:eaSguesn,anPWhoOl.f Analytical Report 09-0365 Fisorochemical CharacterizationofSurface Water Samples, Mississippi Riv-Peoorl 2: July2009 Report Date: August 12,2009 1 Introduction/Summary AT2n0ha0el5y.t3iMcSaalEmnSpveilnrevoisncwmeesenrpteealrrseLotanubmnoeerdafttrooormythPpeoro3elpMa2rEoendnviatrnhoednMmiaesnnsatilasylszieLpdapibsuoRrirfvaearct.eoorwSnayatmeJpurllyseas8mwpaetlreaesmbcciooellnectcttceeddoobnny dJPuAloyCfso8E,r ihe analysisfor ion fuorochemical compounds under laboratory project number 03.0365, CTSoahnmetpa3lienMersEetnwvaciosrnosnmimsaetrnektdeadlofLwaibtfohierladtosfraiymlpplr0ee,phafeirreeeldd" ssnaaemmppllteehaclcuopCnitocanaietnsee,prsoannfdoderdawe2tlo5vepapsfaifnmiaepllldivnsogpluelm.oceatEoifoancs2h.00eEmampcLlh. C`Coonnttaaiinnienrgsalrleasnearlvyetdesfpororfitelod bmeailnigxsesnptibkoeshewieerod ffoorrisiaemdplweihcoalnctaopnp.ropriate mati spike solution `SAacimdps,leAslcwoernea,prAempiadreesd, aanndd SanuafloynzaetdesusiinnWgatmeerthboydSEoTliSd-8P-h1a5s4e.3Ex"tDreatcetrimoinnaatnidonHiogfhPPerefrufaorrimnaanlceed Liquid ChromatographyMass Spectrometry" aqTuaiabslleietwyh1ecrosenuitmnromtlairssiarzmeeppsloerstth.epsraempparleedraensdusanuasilnygzetdhewainhalytthiecalsammepllbeosdwiidlentbiefierdepaboorveed. anAdl driesscuusssfeodr aa `TTnheEeCStoeSsmt.pinegrTreeposrotefdtTheeroieipnnm3ee2estCtihaehtre3eqsuireamenhtososnfsISSOiIcErC s1c7025c-i20p0w5tii"GhencearAa2rlLRAeirqCuisroecemecnts5f0or fs Soran Contfcate #2052.01 Pce2crz E0! [alees galsee lnl ! iin FEEEPEEEEEEEEEEER Es[i7e]ials||s2l78l78l8Fl|g% 87 27 98%55]87]852s | [geld [8]8]2[[3[2]4 3 gx]n[ LEROa EEa]R3 R[EaE] ] [2RaE]E: EEE EH FL hn HEHE iL HHERHHEIREH ETT = g gE 1818 | Bu a i | [RL ! ee ' FECEEEEEBECEEEEEE : |[ R EE EE O ewoe EHE EES ale e Eales] : | ii 2 [24] LH 25 EER a ale 2 [ao 2] afl | [Essao]e LL oslo]el z le EEl e 58a ,00 EHEC ih LH ] Bil] (EE) (B30 (EE } i EEEECEEPEEEEEEER bk LSEDR: aoe] [|3+ fo | [afd ane: : LI e sal 23a]le] [ape] ao TOeECErr rc lite, sleela[el elas] ol3ls Jes] ele el ] ela | a 3a][3]eaeallele) Lede EEEEEER } | L [LEd Fh | : phe I HHHIRHHHRHHE HE 8 2818 8 8! sssz EE 5m Sr =e S T --reee E ee i r r m E e m. Rr R E Er E BE Pn eer a 2 Methods - Analytical and Preparatory 21 Methods Analysis was completed following 3M Environmental Laboratory method ETS-8-154.3 "Determination [PuochermesutoraeCosonst) [ Petoocamessorte Casutonate) | in [pews | [pros | new | toew | ee [P[etPuoemnetanuocohooaCponec nonncia[|(perrciemesans| | e) teLeores | [Pemonspunochoa rica) [Petsvonsmochos Conc [pega | leew | [pron | leew | Er Pefucrododecanoic ACO(O12456) Perfucroocnesutonamce T| oro ner | [eros | pancres 2.2 Sample Collection `Samples were collected on July 8, 2009 in NaigeneTM (high-density polyethylene) botles prepared at `were spiked in the laboratory with a known volume of an appropriate matrix spiking solution containing the analytes of interest. Collected sample bottles were retumed to the laboratory at ambient conditions ES EE TTITe REE 2.3 Sample Preparation p67 SM EVROWNErNeTrAoLntLnAoBOERaATsOeRsY R2i.4samApnlaesly`smid.s ually conrl samples were analyzed for Viteen target anayes usg hgh `performance liquid chromatography/tandem mass spectrometry (HPLCIMS/MS). Pertinent instrument rpaeraGmoetsecrbse,dthien tlniequitdabclhesropmeatco:graphy gradient program, and the specific mass transitions analyzed aSSniaamhmlzaepdlfTee2s1ts0s8ff,oor PPRFBPAow.rePFaDnaAl.yzPedRoAn,73P1R0A9, PENA, PEGA, PFHS, PROS, and PFOSA were aoSanmapezleedree1st2t3es09f,oorfPFsDamAp,liPnFgURlAo,caatnodn RPeFaDchAw4erLoecaantailonyz1e1d, 7P2F8a0A8,. PFOA, PFS, and PFOS ware Table 2. Instrument Parameters. [ho Goummsecssum | semiciqeiwmxmT oms.|emmgiemmxomse|| F[aonjaeyctoennvcounmen 1 | smicrozisnumxcomm,su || Puneo1amoxswommw.5y] o`MinreSs Sepeecromats pied BosysemsAPISI00 | pied BossesAP1000 SaSmTeaaornrereyst e ETS OTe Fsmiia51 aro Res aoe n 1.we h vset] ed Table 3. Liquid Chromatography Gradient Program. Tenanrys Pmoiunr ataPemienstcx o CF ToeoT ew mseT T |m w w aw [ [ | w wo o 0e | | mwnoos || o se [[awwo [woeo | wwoo || 65 | __7m5o__:15 w wGiger ooro. |pri. iwrs eoo 1 100 | m0 F Te= sa 1 aho we |m w wwee | e e wwwoee ||| C E . o s o0o1 m wwoe e Feewwoo]| oxserors p.68 IM ENVIRONM`ERNETPOARLTLHAOB.OR0A9T0O3R6Y5 Table 3 cone tinued. Lo iquid Chrm omatograp phy Gradim ent Progrs am. y1] ToumrinT]ime | FGolwiRnat)e |(smthaPmemrocneinutm cote ~ wi C01 Ace A o 1 TLoe oo f |owm w | Lm wo | Lomweo | [Cos3 T |w e[aao0Tw w h wo ooT o]wo w0o0.o]| Table 4. Mass Transitions [om [Mom | en | | ass Transton ass Trnsidon | [e[ mmp ar| pae smeeasna| | ema [ssaeusme|| [omar | | anaze | [[eerassae| | [aeaare | [| aswieo | [ [oera wees| proa ras pr Pras 25500 -- [aswearriess. | Eg [[oowasn ]| [ [aamaea s| [ [ssatmee | | [wo] a oe |mabe verusmodovoahoiE nbyauanfnoom5s0wh-m e0r0mfsacrfeorseawcohraansntoonnnadl.TnhocqwuasoBn k { om arcs oczmat arrofrnshons bor med 3 Data Analysis C3a4libratCiaolnisbtraantdairodns were analytes of interest ino 50 mpLreopfarreedvebryses-poiskimnogssknpourwinieadmwoautnert,s oEfacsthocskpiskeodluwoantsercsotntaanidnairndg wtahse rtahnegninegxtrfafcotmedainnotmhiensalamceonmcaenninreartoans otfhe0.c0ol0l2e5ctendg/smalmpl(e2s5. gAi)toltlo o5f ntigriemeLn(s5p0i0k0edgslt)andwaerrdes puarteapsarwteehdrei.peenAanoklqaufargoderrcaaetdiccot,uhn1rt/osxugawhneidzgehtrhtoeedrd.eusrcuialnibgarnattthcieofntaciunrgivpercwrouacresvasseu.cstoeCndafolticomunlefiatdttihaneg dtcahteascftooarfnuedeaaarccrdhhccauonaanrlcvyeetcnept.oraiytnTitho.en PacescE sa fEamEoRpenEY mtRpTnRREE BSEEEETS 32 System Suitability iEyEEe E eR=E m mR A SE 3.3 Limit of Quantitation (LOQ) = [me| foam 2 [ema | 258 [rapa | em | [ero | aw | [ema] 250 EF2 [eon | 200 = = = --& [eros | 250 GSSR E EroenE ery noy 3.4 Continuing Calibration sry re 35 Blanks HIE S ESEERTAREToEnS EeonessERmre 3.6 Lab Control Spikes (LCSs) p.70 IM ENVIRON`MREENPTOARLTLNAOB.OR0A5.T0O3R6Y5 2`a0na%ly.ticalAlulncLeCrtSainstaymwphleersemaeppllimcaebtlhe.od acceptance criteria and were used in the determination of A`PasFnaOtlhyAetersaenpfdreersePenFncteOSnmatwtehereriaewlastpeurrespesadafrmeopdrleqiusnanattriieptiacctaoilmoenp,roifastePdtFowOfoAbcaronanncdecnPhteFrdOatSiisooanmrseertspo,reeLdvCoamSliunsaatanemtpltlyheensepaoofrt,ebnratainnadlcthhfeeodr `anaaclcyetpitcaalncbeiacsr.iteriaT,he average recovery and RSD values for branched PFOA and PFOS met method The folowing calculations were used (0 generate dala in Table 6. Lospecan Recor +CSGakCuolntecdoCnontcaonttoatnion LcomRso TSvlTandearddreiLasCiSorgnecLoCveeSrey plc.atooe.s PAGE 100FR 8f Me 3 fr] g| 3 i | J Jeseee|REfesssce iHaagaaagsgesed | igi3e8s888 fos,| fey ;fi'llers) lRlgEeesnend: 50 5 dh Ls BLY daaiandd [g siiniidd of 5Hi 3 : 3 J 1slg 3 gedg g3 ene I| ---- | ens 8 : isis | Hesse EH $ Ha.e .oeal HEEREREE jeeazes sans | BjFigEea.ceinJgi AEE HHH HERE i Ie | . : flees Ho Je i ooi [eens : | | 4 Hessses || Jee 3 La | -- 2 Elfeeioned lfeesran 3 eee 1 it 3 jReeees 1E3l glEszazealIdEd ib lsasanald Tacbontlinueed. Lab Control Spike Rosuls. rros oi Concpacrsiaton concrenhtaion go keCsSs0ao0o0u7nr222z-s21 kescamsorasza Les more 2200 1m9e2 owso | w2o | aarmo | 3he wwoo | | ssmm || wweo be SMENVIRONMREENnToALRTLoB,OREATrORoY cssaammmascEccrt ke\scssoowrrzzzsmecces kescsaommnaz s26cceE CanSvpoeinkmseadton| CoCna"llaegi"cnueaatseden| sce arSpoSikreda|] pCcaoolnccunhltaatieod co 0PY p2os w ws mowe | wowns on ww | xs0eo | snsro | wwoe || aomw || somo | wwoo wwooo || asmwe || mwee || eemw || ssew | o1m 3Aamn.ena7tclhyaotrcdAdaanlcdacuelnuvycireatartictiycaoinaanlntydcMiarselbetoacushoaeonldd.odnUoTrnhhicheseetomrresticttaahliooGnfdtCaucydncauctreaarctayhnaeytssuisclocsonlr(conil%al)cehoadrbftaoeildnoaewindndfgouErsTteShde-1Ot2oC.es0va1aml2pu2al.teesT.he.The rCpanodand unecteortaaaicnotnypfi&deGoncaetlneevedldobfy6s5m%l.plFyidinag (ahepSilnansdweerredevuaselon1bydetearfmianreomfe2l,hwohdicuhncertain by tismethod oncereorn se analyte Standardovation [Teoma | om [oon| [pros| am | owen | [ero | 103 Souazi ema [0 | 3 owas| [rea | 821 toa cE Ere [eres | oss | oman| ps | ms |soon| [eros | woe | oor| BLSEA TTET aTA E 3.8 Laboratory Matrix Spike (LMS) 3.9 Field Matrix Spikes (FMS) BSE E EelmRErEn E eEEr Rm Resy a RenyEy A 25ppt (nominal) field matrix spike was collected at each sampling point to verify that the analytical Five field matrixspikesamplebottles were filed more than 10% over the200m fil line.The field an p.76 IMENVIRONM`ERENPTOARLTLNAOB.OER0A9T0O3R65Y 4 Data Summary and Discussion "daTsihfeweetelalnbcalees(tbhee*lT%orwRpsoBPulfmaDtmnhka).eriszEaeamcpthlheetasabalnmedpplsreaomvrpiedlseueslldtsuhpaelniacdavtefeor.ladgRemeacstorunilcxsesnaptnirkadetairovenecroaavngederytvfhoaerlurteehlseataitrvweeerpleovruecnledonectdattioons sfoipgiuekreesssi.gmneiBefelicciaannugtstefhioegfumrreeostu.hnodPidenrgac,cecnvetaplrtueaelnsatcimevaecyrdiilvefarerirayoesfnicg+eht3(0y%f%R,rPoDdme)mtvohaonlssuetesasttaeeredthfinoauttnhhedeermdaewttdoahttowado.issiFgainpeiplfrdiocpmaarnttiraitxe forthe given mat. R1e0a0c%h23L0o%cawtiitohna5recTovheery2o5fp6p8t.F2%M.STrheecoavnaelryytfiocraPlFunDcAerdtadinntoythmaesetbemeenthadojdusatcecdepactcaonrcdeincgrliyerfioarof PFDA 100% + 32%. R``aaoncaaclceyphitcaa3lncLueoncccareirtttiearoiinanto7yf-h1aT0sh0eb%e2e#5n3pa0pdt%juFwsMittSehrderaceccoocvvoeerrrydieifsnoorgffPlo6Fyr7B.PA4F,%B,PAF6D310.A0,1%0a,0na%dndP# F63O73.%S8,%df,iodrrenPsopFteDcmtAeiev1et0lym1.e0t0Th%hoed+ 37%,andfor PROSo 100% 32%. oRfo1a0ch04%+Lo3c0a%twiiotnh1a2 ~reThceo2v5oepfrptyFM64.S1%.rTehceovaenraylyftoircaPlOunScedritdainnot hmaesebtemeenthaodjduasctceedpatcacnocredicnrgilteyrfiaor PFOS to 100% * 36%. Pace 1602 ii 3 | fees [Et : Hess 3 ea | | LT | 3} de be | ; 0j H | E5 5 FEeE he : HERE] iesieEg] TJHee es | qi: Bl be feet Bl 18 falaegl|d Tle | FREE: ETeheooes : r L idadT e el al Hd Jey iE Be 8 EEE 28 [i 3 i 3 k : gaa3 ss3 [ds L He ; flssg Ee e ley : H HoaT :! I fle E4EE ees]| # 318 gl | Jee? 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HdaIilERdd ill ii doe| asli poz SeI i) a 5meCsoonnce clounstiosnkswere usdtoGlinn heesreecassaamoosEedtyoahaemsmicsnoartsanhdoscorrsosinrcyaonmemoryea a STe e eEe e ee rwooonnasinioossoSrlocoremann' oArayics 6 Data/ Sample Retention rmaa n sri nd soit ftotroi rworsephrensd locovi bo rsd 3X00 7 Signatures e A Y g F13a/0Soy 9 Ze William K_Reagen, Ph.D., 3M Environmental Laboratory Manager ) pes 205 Date I Enon Labor ua Assurance Unt a ale he aia and ot is Sony FessRe = nacsors ps3 ENVIROMERNeTrAoLrLtAoBOtRoATsOiRsY Final Analytical Report Perfluorochemical Analysis of Fish Fillet Homogenates Collected from the Mississippi River by the Minnesota Pollution Control Agency May 2009 -- Phase I: PFOS Laboratory Request Number. E09-0372 Method Requirement: ETS 8-45.0 Testing Laboratory 3M E3nvMirEoHnmSenOtpaelraLtaiboonrsatory 3M Center Building 260-5N-17 Maplewood, MN 55144 Requester Gary Hohenstein 3M EHS Operations 3M Center Building 224-5W-03 Maplewood, MN 55144 2a Cates 208201 rRTI eoarnsairningae rpsoorte ahCTawoiimnhn pR5tmee0nt8chs 50T2ro0sei esvofeSOnEL1i12s6s2Ao05n"nEaRsi wih MENVROWENTAL LABORATORY once ror p94 WMENVIRONMREENPTOARLTLNAOB,OR0A9T0O3R7Y2 33MMEEnnvviirroonnmmeennttaallLLaabboorraattoorryy Manager: WiKl.Reiagena,Pmh.D. 3MPrincipal Analyical InvestigatorandReportAuthor: MichelDl.Malinky,Ph.D. Perfluorochemical AnalysoiAfsnaFliysthiFciallletRHeopmorotge0n9a-t0e3s7C2ollected from the Mississippi River by the Minnesota Pollution Control Agency May2009 -- Phase |: PFOS 1 Introduction ReportDate:Upon Signing E`nTvhierMoinnmneenstoatlaLPaoblolrutaitoonryCofonrtrpoelrAlgueonrcocyhe(nPicCaAl)asnaulbymsiistuenddteirtpyrofjisehcftilneutmhboemroEg0e9n-a0t3e7s2.oTthhee3thMirty Ms`suapbyemci2it0ese0cd9sfoaimshpmslaempsptrlehripenrsgieascmesapnmltpeeeasdieadgtnn.faTophpmrePofoxilioemltah2tooemffoetghneepneMaristcseeinsstwssiepprpiietRoeixvttehrera.coFttieavdleasnsadmapnalaelsymczfoerldoplumescsitlinegxddmdieuferetrishenngotda BEoTdSy8)4a5n.d0AnDaeltyesminsibnyatHiiognhoPferFlfuoorrmoacnhceemLiicqaulsidviCahPrroomteaitnoPgrreacipphiytvatiitonhoTfanFidsehmMTasis Ssp(FeiscliertuoomreeWthyo'sl.e "psTeuhrmefmutaaorrrigczeaetksaatnnaeleytsreueslfsfoournsatftieossrsp(teCur4df,uyCioBrn,ocaolcuntddaeCnd8ep)seu,rlfafunoodnraopteaerlfk(uaPonFreOocSaa)croibnoalxnyye.lsTiucfhaoendarrseisdrueal.nsgTfiohnrigtfshiePohomaesGre4rte0aproCgr1et2t, anaiyteswilbeissuedina subsequentPhaseIl eport. tTershiees3icqMalEubnvvaiitiroroofnnsImeeSsnmOtea9del00Lin1na:bA2otZ0rL0asA0t.CoerErytTmiafSii6cn-att4ae5i.#n02s0fA5a22Ls-A0u1ancdacenrredtdmhieeateliatobsonrtahttoorrIyeS'lOseIvcaEunrGtrqe1unatlstc7yofspyres0otthfeeam2csspcercei5dfiitca:tion. "The dataandinlreportwere auditedforcompliancetolaboratory's ISOIEC17025 quaysystem. T`aanballeyz1ebdewliotwhstheusammplmesawitlhrlebPeiFreOpzSorreetsueldstsa.nAddlisrceussuslesdfeolsqeuawlhiteyrceonitntrhoilssraemppolretspreparedand 1) TRhpeheecerastAseirZsosLtmiAinaCnganotrrsobcfpfcoocarrttredoeFCh0eworrGmehp2iden0m1t0.eeaeTnStecntsOethoiOcfenTgTteers.hteincngoamntpdbCoiafslwbSriOahtMoEin 1a7nb0io2er5msa:it2oi0ro0en"l"GSeIannnescrcaaclrrdda5nc0ewith Cerificate#2052:01 ENVIROMENTAL LABORATORY PAGE20F20 soC--E-- E ET TSI enO E T TT AcT nE e E Sr e E } } ] "o= S=2 ol az5=3%2a2= 09.0372:005Dup. --Aunys10-L12017-10,Client 10:090262 Dup. we Ba E a O T T r E , y E T E l R vaiiFoPWpaErlfogyses:ll :5iu423 09-0372-007Dup. Ax 10:1y 1263s 16,ClientID- 060173 Dup. 98 nro --_-- wnos S -- SE i m Em Te -- ,e 2S=L E z --w= S T T S T eEeE E E ii E L E TE E T Tr mT t E wT= aErr= = mamwowweseE: ihsesyeos5iBe=li) E000372012 Axys ID- 112932:26, Client ID- 090248 SmalmouthBass Second "581 Average. "570 -- rn p.o7 ENVIRONM`ERNETPAOLRTLNAOB,O0R9A0T3O7R2Y Table 1 Continued. 0Lt Nomber sample Descriptio spec LoFciadron C(nogne. Er0l 200 ANooysI1DD- LLI1Z2O0k4S5-11,, CClhoonnt 00.-009000226411 Ov. Fresh Wolor Drum Socdond 22456 APvgeTY228 E0OB0O2V02022220up ___ TAosyysaI0D.-LL1I2Z054855.-1166,, CClouni D1D.-00000007708 Dup FrosnWolor Dum Socdo2n 749 04 Averge 117 00007202 ID L17945 19, Chol 090001 FreshWater Orom Suemcpo0n 72 413 EO9OV20230 AsD-L12345Cl-o1n01D,:090081 Dup . Aversge m3s14 EEoOn0D07O22024400 _AAory0s-ILIDZ-oL4C1C5ou32nnt0t0I,D4:00509900:0000903Du,p FreshWolerOrom_ SPocbEon1 n14r7 Avonge 142 EE00O0UaT220022550u0 "N_Aoeyrs 00- L L1Z547.I 7,CChhoonZ nt00..00A 3900226666D,p._ BugSuntan Swocehropn3 70 M5 m1 Avernge 333) 0020 o0rL1s2647-, Cont 10: 30207 Buegu Suntan Sweecornod 57521 EOOUT20260u0 _ Ae0-LyIZsA. CntI. 090267Dip. Avernge ss 853) Eooay2027 No1sD 1204715, Gh 10 090111 Bughsuin wSeecenpz ozs 406 E0O0OT2021 up AsysID. LIZOAT13, Clot10:000111 up. ao a ump0 1s E0O0O0U3N220022880up _A"RaeypssI0D: LL17I64Z7.2A5,TCC2ionn5tk1,1D0--0090002200550p. Boog Suniah Sectona 632 tos Average 883) Eoot2020 "N0eL12y647.25, Cort 10. 00200 Boog Sunken Seucmho0na 314 EOOGT20290up. __AnD-y12s04725,Cie 1D- 0002050p. m2 avenge 203, 003200 os1D-L12040-17, lot 0- 090061 Bog Sunkan_ Swecmhoon1 1m 7120 EOO0OT0N00p _Asys 0. LIZABAZ, Clot10. 090061 Op. avenge a 013 TTEmTcSi8a.Sn45hy0omT00i11ap5%co(cRooOP)op`T5ro0cao0rSo.ctSSilnao4 otD0eooSshaornecTyaAadnd5oacyrCaHbonwvoirtyah vToOrOcuTarSmseWDceImoTtoonbt8s9 iooeri eve hetKaa vsRP ospd ur.ASion ENVIROMENTALLABORATORY PASO pot SW ENVIROMREeNrToARLTLNAGBOR0ATO7R7Y 1055or od cok homerge, SPD, Scan. Vokes cow yeySr @5) SR orte y evseog1 5.soamm 1100p nacs nosun00S. 2 StudyandSampleinformation sT2uam1bolgea2tTbeaerrlegocweoptvreoArvynisadtleasnypdteaerrtsdi.sneinntveisntfiogmaatteidoinn r4eg6arSdtiunyg.thSutraorggaettaerneaceosve,ryinifaemnadlartcasnwcearrecss,epaanrdate isSculmoopgicaatlelwyacosmupsoeudndosevsapliueatdenthoe eoavcrhaslaemxpaictaloqnuportopcreisorstaonedxarancyipoont.enTthaelrmeatcioevfofeefcrhty.e Table 2. TargetAnalyte Summary. Somroemr FeteTsS--ard [otros |owncnn| crooon [Tew | wn] [ronmomarmem |eromiconan | crcoon | em| mee | [ronsormcn |ooncin | Povorocareic oct PFOA (CBASS) [ronmoroummens |pconn| crucom crucoon |Tem| mee | Taga [coPtodenSaTtss |Tem | omesirones | [SS| [[[rrrovosaesmemroscsmsecoromensss|[|omrrsosccmsoasvanmoemnn||| cccrurraocoxnon: [||TToowm||| SosiCmoomnsSemitroenoienrs)]|| Puccioasirte | PFOS (Chute) Tot = ; = 28 | em |e| won| SMENROMENTALLRORATORY Frcceorm somswo spayy rt Comin, [[ ormor |ramrmm emmr:r|| ooeamraoon|[nere ]||eveameme]| reas | z epns|Guatrsrom|s|warmer] C"cIrTeme |vas|sa rasroa wotong| ar|| ewmpemr remem | 2 eprom | ecurmsrtaorntotor||_=s ||wwragrema|n] RE crores| a wangmmaen| e n ll| re paaoaprnrses|esTe o|| |[Cnroani|n o[rTFmigrimr--e ||rocormoesm|| rSicrcooasoommmcso|n||as er|||rnommre ismmee ||| B S p ETCt ora ter secave 2.2 sample Colleac ndtReiceoipn t. pereptsrg Ce tI thoesarmpolmingaoduaetsec.ntymeeEsONLpaaeapey alSeE r r A containerbycutting thebottleawayfromthe frozensample massusing acleanutiityknife.Thefrozen SSeneinrmeierp ese mbeeretMnEpn reSeerton eebrormooenm,e `samplemasswasthenrehomog bee forneeixtzracetidon.SeeSection3.1formoreinformation. 3 Methods - AnalayndtPri epacraatol ry 3.1 Tissue Preparation Eachsubmittedsampleandbluegillfiletcontroltissue(TNO8-0220-1/1) purchasedfromOsage Catfisheries,Inc. (OsageBeach,MO)wererehomogenizedfrozenusing dryice. ono wocran p.100 SEWROWEpNTrA AiOReATOdRY Frroeazrelhnosamohgehhopamraootgaeonsnastrbeaewaprsoauadnddafedrh1ta.oapsr-wwcailslSey tenrAers 3IslroslePyboeohwrlyolfCeaonRnsobboatCgouAipewoaRSenI2p1ce.s1 in tShelfarteeozne,rath-e2b0aCuwnsaesasleeadloevdeamnighmtotmooaglelnowttehserersisdKuaalcarbsoennd.ioxide to sublime. After 3C30.o.2n2t5iSgasmutbpesl.aeTmpilExtorfahlctcfiosnwseuree romnosgpeneadtwwiahspaicourtsealycwaerigh1e5d0n)aan5d0rmg.upeosets roartdcohpaaacenallaboppvaptrloontsosaptlraeoncddoaenrcdcsaowreidaretasoedneoadlto1oo7n9yS.coSoaHnmaEprlavetisirdbsee.ogaSrraalgnettdainase urmogaaleSspnkleisosorea t tanaot rainy OC Tp abo3r0amir inynecsoDo bn5etl0oo8l,n 3:15S8mpikMoet ef)sweecroo nsRp0k0ew.taAwsMieahrdssdupreorTar,leehs ea1t515n08a gwoaamrroeegoeoe nenalevsrss woaurgsseyalroawpeedsoat RP5mr0oo7b0geoest(nae1e50ad00ishthfoehoran3ceirnUiptioene)eursTimhngaealanhOo TcsPreFepelrulexcolosamacpclesnehwaoemxroiaegpecnseiewzaepraewcueeihhsspoaoFaeobslaaeetrsapast rete emprataeof 570 or 20 mutes 3000pen. Afrcontiugaon, 1mi.of cartedsupematantvas ranted 0.2 mLaol spedwih 101 of 10%formicacid.Autovialswerethencapped andvortexmixed. `Sampleswereextractedinthreeseparatebatches.For eachsubmittedsample, asample,sample `duplicate, and laboratorymatrixspike (LMS)were prepared. Eachextrba atcchintcli udeodthne fol qual lito y cow ntroi lsan mplg es: + Taiotoeenpont extractedmatecalibration curveusingthpurchased eg letconto triplcate labcontrolspikesofthebluegilfiletcontro tissueatthreelevelsofal targetanalytes. + U(i0p5knatgsla1/b.5cgnog/,ng, a sph8n ensgo/d fg3)M lckochemica uration (ECF) PFOAand PFOSat + tdGrniiugpplplgiiacaaltteoslmacboecnonhtrmo(alastqpuisekboelusason)fkHPsaFwnkOisShoawnnildhywaaitndn1w0i0tnhgoeulmtgamsiaalndSaarnddsaarncdssuarnrdoagTaotgesates The tablebelowsummarizesthepreparationdates andsamplesprepared ineachbatch. Table 3. Sample Proparaton Summary. [oo stes T[oprmopnstomas Toeomgoesmurmoromn 3.3 Analysis AnaalynsisaforethsepPaFcCrsalmiestreyd (in1TPaLblCeN2SwAaSs)perFfoorrmIesd uvseienbgohmiagohnp,esrafmoprlmaensceolriqsuaidcnhroamastuoegrrgasaphyAgailioernuptc1tl10ei0osreSariSeIsC(IPEaANlBoTIAhl4t0oo0,.0C0Ar)1HsaPLamCasyststesempcientcoeprtfeearcaretdt(oonesitthheCrnBea,gPCaEAS)CIoBEnoXtMhAEPmIM4S0em0o0ndtreitplwveeosrne multiple reactionmonitoring (MRM). AnalystTM1.4.2softwarewasusedforalldatacollection and MONET ACONTORY -- p.101 IUENVIRONM"ERENPTOARLTLNAOB.ORE0A9T.O0R37Y2 bRerPfedogurcuetatirohnde.csToaalmbuplmlene(4 2liin.sjt1escmttmihoenxpMo5Rr0tMmtotetr;arna5spiatinpoaynrstiPmcFolCensciiotzonert)eawdmfaiosnrpaelnaatcschecdoanmiainlnnygtefear.foAmeTrththeheerpHmuPorLSgcCieievnnastltivrfeiucmaPenRndIt SM p`raensdeonrttihnemthoebslaempphlaeseexstr.acTthsi.ssuffcientyseparatedtheelution ofthe "system" PFCpeaksfromthose ENVIROMENTALLABORATORY PAGE90F20 p02 WUENVIRONMREENPTOALRTLNAOBOR0A9T0O3R72Y Table 4. MRM Transition Summary. PFpOrAro(nCcAorAe)a ......... PrIOACOA) PHA Ac) PRONG fe PINACOACS) - PEDACI0AG. PUMA Ac), PFOA C1200) son Hanes Tore Tow] Target SR Te Toot Tot Tot Tee v 2mm m wseormee wwmo #30 0 swwean a aa2n Sgioa, ssweamm 500 wwwww 0 p20 oopwee ow 20 P7100Sunol) F1OS0A(5Co(CSoSuutrornet)) 1122374Ci"pprrnon (1234Cpron 12345CPA 12.7CPon 12 7CPrun 12 "Capron oes Fons 1238 "cpros Coro 12- "Capron rowros Tot] Tet Tor Ska PrBAwaPron Sharron iS arPHAosPFOA iSkrorA Skrpron Siarpron SiarPron iSkcpros Sk SSttaarrprroossa Serco ok) I see0n = wann @ wswawn 2m wo) siz "pan ai sia 50 " CE] ww ae ww ve w wm MENVROWENTAL LABORATORY PAGE 100620 S--s--e mEEE S E i E EE ES ErEmEEm E E Er S s I R m e e e T a T E EI m E analysisbythemassspectrometer. ie [Spstacwceos [legos cromsumammross | --E E E=S ET CE--=nE--nm E --s--Ee --T e R --iEs--tRe --E m-- transifotriPoFBnSs, PFHpA, PFOA,[1,2-"C,JPFOA, PFHS,PFNAandtheirrespectIiSvse. The: ns en p04 SMENVIRONM`ERNeTOARLTLNAOBOER0A8T0O3R72Y 4 DataAnalysis Ex4t4racteCdal`imbartraxt-imoantchedcalibrationstandardsand GCswerepreparedbyspikingknownamountsof pttarirosgcseueteda(unraTleystaNeustO,isnuBerdrio-gnaS0tefecis2ts,ihio0ansns3d2u.ie2n-h.toAem1moaogl/tesatnl1aaontfd)eta.hridEtseaecinnshopsiinpdkiiekvdeisddutfaailsnh0daa.lr2id5qsurgolatwngauisnsgtfhoeonfmebxlt0ur.ea2g5citlnefgdi/lugestitcoonng3tt0rh0oel 0U.0g02(5ngn/moL.mtwoeir50enpnrgae/pmalLrew)da.sAadlsdoiptroenpaalr,eadnwhuincehxtriasecqtueidvaalceenttoton0e.s0o2l5nvegnltgctuorv5e00rannggingisrsuoem Wmaceotrnrceienxqtmraatuticonh.aedAclnaulfsstitanrgmapttilihoeenrsaceosulurlvvttees.nfteTocrourddPveFemO.oSTnashtnerdaret[ce"oe0vqe,urJiiPveaFslOoeSfnwctehyre,eQthCqeusalanabtmoiprtlaatteoesrdyaqcguoaanintntosiltattehGCde easxgatamriapncsltteetsdh,e unextractedacetonecalbrationcurveaeprovided inteSupplementalInformationSecon 10.2 `sAatcaqcnuudaradarrcadytoqeuf,aen1atcxahwtceiuiorgnvhweeapdsoiucnastlebwdraa.stTvieohrneicdfuiaretvdaebwwyaabasscnukos-tceafdloctruoclefaidtttithnhgertdoauhgtehaczfoenocrreoPntcFruOraSitniagonntudhsei[fn*ign0gtJhPperFaoOrcSee.ascson.utenTmthael LthaOe0Qfisontaflatchneadiatbarrrdagt(ei1to0an0nc2aul3ry0vt%ee)m.oetTthhteehicenomteeefmftiahcliosedtnctaasnlodifabrrdadet.tiEoenraamcichncasutorilaovcneyn(r7te)cqwaueliirbrereagmtreieonanttsoetfrat1nhd0aa0rn:0d2u.5s9%9e,0efxoocrgeaelplnetrhaete caanlablrytaetso.nAcusrrveeq.uiredbyETS8-45,aminimumofsxcalbvationpoinswereused to generatethefinal F`focormpPurFiHsSeod,p(PEFrrCOFS)e,nsaodunrdaocPeoFmotOffAitP,hFoetnOhnSaearneanfrndeirsPteonFmcyOeesrAt.waAansdseaaprladsroautsienecsdlefutodoerdcf.aLlCbSrasiuosniangnadnaebeccontiorcohlesmpiickeaslwas. S"aAbuso rcctrobnoclaenCsvCyS8argrepc'socprrrbt5bpe,hhiocccohn5d0om0ra8nScgsEsLAoagiForPaenyA.xyThecbasckscrorveevtatne T4h2eLOLQiamsidtefoifneQduiannEtTiSt8a-t4i5oins t(hLOloQw)estnon-2erocalibration siandardinthecurve in hichthe ddaeertteeearccmtoieundnettnsthhoeefecnhodenottgarerolgnmeoatutasrnicaoxyantcleeaanrtmereaaatstiuoernaa.sTbtlhteweiercveeestlu,hlottsaenetmoeefntthdheoogdmeoanfotsuttsacbnoadnnackre(dnsat)cr.acStiiiononncwewaPasFstOhuSsewenduastsoedfo correctthe PFOSconcentration intheextractedcalibrationstandardsandQCsamples. Th4r3eereSplyiscatteemnfeScuiiotnasboifliastoylventcalibrationstandardwere analyzedatthebeginningofthe sualnaalbytiifcaylsneeqcutieonncsesthoadlepmroondsturcaetaeoRvSeDraolfllseysssttehmasuni7ta%biltory.thMeertahoodocfrtiaerrgieatatantaebstehaartesaycsotuemrs to criintteerrinaalwsetraendmaertdfaorrebaoctohunPtFsOSaandnadn[ROSJDPoFfOeSssfotrhtahne2s%afmoprltehsearneatleynztieodnintitmhee.fiMresttahnodd athcircdepprteapnce PbaFtOchSesa.nTdh[e*GRPSFODS,ofretshepeacrteivaecloyuntrato inthesecondprepbatchanalysiswere 10% and 11%for `Asmaemtphroeddseuvisaitsiconohanssbieednmeiisnrsieumeaddla.nAdniisncirncelausdeeidnivnatrhiadbaittyaipnacthkeaagree.aTchoeunoveprreaclisiimonpaicsotffotetnhe `ocaboclsqleueircsvtteeidodnawinmtdehotavhenordail.nlWcrpieetaahskesadhanarupgmeebnceuarmnobvfeaMrrRyomMfoMtrIreRaMnfssii,otmeonwnsejcreosclclteoacnntsfeadwcniretcohtsiisnoatngh.eicvHhernoopmearwtioogedrtoahfveptchahielecbdprraaettai,akoanre. ENVIROMENTAL LSORATORY Pace 12062 p.105 ENVIRONM`ERNETPAOLRTLNAOB.OR0A0T.0O3R7Y5 cSuyrsvtee,mQsCusa,baintdysianmjepclteiosnaslwloexupderailesnocbeethoebssaermveecdonidithteoLnsC.ScAantyaiwnchriecahsesduvsaeradbtioldteytoebrsmeirnveeodveirnatlhle mWeitthhtohdeusnacmeprltaeirnetys.uThsus,th variabiltyisaccountedfo inthe assignedmethoduncertaintyreported Du4r.i4ng tChoenctouirnsueoifntgheCaanlailybtriactalisoenquence, severalcontinuing calbationverification samples c(oCntCrVo,)wCeCrVeiannjaelcytzioendstporcoodnufciemdthreactotvheeriienssotrfumPeFnOtSraenspdon[se"frOoJm PnaFwilOtchaSilinbr1a0t0io%nc2u5r%v,ewwhaiscshtmleitn methodceria. Fi4v5etypBelsoafnkblsankswerepreparedandanalyzedwit thesamples:matrixbaofnbuekgilfset Wcointthrolasnsduseu(rrwoogatiet,htw5oawnidthsouumtoIgSataen,dstuwoogwaitteh)o,utaIcSkiafnidesduarcroegattoe)n,easqoulevoeunstbmaentkhso,dabcaentkson(etw:o rbelsaunlktswwaistrheivniteemwaeldstaanndduasreddstaonedvsaulruraotgeamteest,haonddpaecreftoornmiatniecsetolovdeenttebrlmainnkesth(uenmLoOdiQfifeodr)e.aEcahcahnballyatnek. SurmogaterecoveriesofspikedbanksareprovidedintheSupplemental Information Section 10.3, T4ri.p6licatLealabb CcoonntrtorloslpiSepsoifktehsepu(rLcChSass)edbuegilfilet controlmalix attheediferentlevels forall la4in9na)el.ayrFtieossrowmPeeHrr,eSwp,hriePcphFaOrweSad,seatanhcdehsPaeFxmOtreAac,uttsihoeneddsftaoaynttdhoaedrcedatrleebrfametirineoenncacenumaralvtyeeisrc.ialalAmuestedhdofdodrutnhiceieprltLcaCtainSttesyPopFi(kSOeenSsewSLeaaCcstStilhoaent a1n0d0nPgFlgOwAewreerperperpeapraerd.e Steopeavraaltuea3teMaenlyepcottreoncthiaelmibciaalsffruoormnaqtuiaonnit(aEtCoFn)asgpiakiesstoafbirneaanrcshteadndPaFrOd.S. cLdoaentbseicrsomtnietnrneotaln1nsalgpy/itgeisc0wa.lem1renetphgroe)dpaufnroceredartltoaleiLvnCtaSylsu(aaSmtepeelSmeeesctt.hiFooodnra4c.Pc9Fu)Or.TSah,ceytah n[sdppir" eecdiscO ioosnuanrnJ rcdowgeeaP trneewtuwasF arsessadpcifO otokmieedcoS atetnda fortheoavnereagesPFmOuScnoencentrrsatrioindeefsemninheedSfurmtmheercontrolimattiinthe sasmteextVra3c.tioFnbaalrcah. PF10O0%S8a2n5d%.["OJPFOS,al replicates (N=45)producedrecoverieswithinmethodacceptancecera T4h7e extSraacmtepdclaleibCraotniocnecnurtvreautsieodnforCqaulanctuiltaattiionopnrovidedextractconcerirationinunitsofng/mL Tuhenfooilfontwgilsnggequationwasused toconvertthe extractconceniraton tosample tissueconceniraton in raisue sueConceriatontonCyn5ge.) m ExcC Coe TnTc(r g2oy e nEexarctton) tictoament) EExxmcctoenVsoksam0o25205m F4o.r8eacLhasubbmMiatterdisxamSpplie,keasse(paLrMatSes)laboratorymatrixspike waspreparedbyextracting aseparate: aowlefiraquepostppiorfkteohdxeaftiilamet1nato1imt0sisennugale/tlyhgca.otTnwcheaenstrrseapctokivoeendorwyfoift1h0tthnhegeLitgMaeSrxgwceeatapsntcaaPllyFctOueSls,.atwFehodiruceshaiwncaghtshsLepMfiSok.lealdolawitanraggeectoqanuncaaetnlityorlnae.tsion MENVROMENTAL LABORATORY Pace noe p. 106 ENVIROME`NRETPAOLRTLHAOB.OER0A9.T0O3R7Y2 ssnT e(i nccon (n2g).0 carr acnicsmn:))) woro esarpeconc(3a2)).sn amesp0 ElAnelvatishrtoouhngamhfetEnhTteaSel8nL4dab5oo.gr0eandtooouresyscnuoosnetcsepnraigorveaintdeoersnaplbeecgfiuofiridceetlihneeerstpahiftkoeatbshmecaoanrbsixmdasetprrekidex"csaoppnipckreeoncpotrnricaaettneitofrnoasrthtiooeunlsgd,ibtvheeeant3M w0T3a7sa2s-p0i1kF2eowdrhaPetEr0eG.t2Sh61ebLnegMLS(i~wf1Sanvsga12i82sn7s.gu6ec1(o~n5c1e10nnt1gral0tgi1osn)u.seuceonccenotcraatnisont)o.n)Trh[eg"O,JbrPFsOlSseursrog0at5e: tEh4Te9Si8.4nA5n.a0dlstyataitniaeclsyavttleharUteitcnohcvedeearrnitauelasyiiincanatLlyCmlSetsh.oCduurnecenrttparionjteycwtiQlCbreesdufesr,maisnweedlbyassathiisstiocriaclaelvvaalluuaetsi,oanroef sEutsTreSodn8ig4en5vt.ih0de,eetvnhaceleusaiustgtiogorenisuctnaitlinLga ChSmaataxarisempceuacmtieoegsfo-irstipzyeecpdiofbiiynctmissa(stmuiienetifymfpueemc:ot fwprwheesneton,tfalpnoostelshieab-ttleru)enbaseeusoissntcrhdloeumrdetyehidse.seFor %)asfpiaesccticoearslsochfuoltuawltode,dwb.heTichcoehncesoxirdpreaernsedpdesoendpdUanscrfeaorttteahlieyn.t9Ty5h%ectsohtneafnnicddaaelrnccdiedaeitvmeiaidt.ibyoTnamobuflietph6ybcieonlllgoewcthtpivsertarneodcaovvrtedhrdieyearvndiaealsyteutiioscsnab(lny `uncertaintyforPFOSandthe [*OPFOS surrogate. Table6. Analytical Method Uncertainty ET [[ossounnddoooceDveivsiessoonn a 1ov[am| | wea |we | ote cs 5 Data SumanmdDa iscr ussy ion Ss`Tauammbpollgeeas7tbpeerqlouoadwnuptcrieoadvtiePddFeuOsstSihnLegMstaShmerpeelxceaoavcnetrdeildeascbawlmiiabitrrnaitmxiesopntichkueorrdveeaspcuroleetppsftaoarrnecdPeiFcnrOtbSeluareingaidoltffhi1le0et0[c"o30n0J%PeFxtOcsSseupe.oArl ``g0e9ane-rp0a3lp7,2rm-oo0s3tip0sn(rat6mhi7pe4lda%ea)tst.paerTtolahdbeluyeac.endaEsTyuStr8ao.lg4au5nt.ce0ersreptcaeoicvnietfryifieesosntwohiaitcshsoiaenmp1pt0la0en4hc3eac0si%be.erieEanoaxdrjscuusrteoehdgaap0tvee1t0rbe0eci2eo5vneo0rf%il.enasgaIgsnesd the nent ofthesurogate i tevaluatesystematicbiasesornerferences thatmaybepresent ft"oThhmeerEe8Cc8Fo.Qv8eC%risteopsio1kf1et4sh%deweim3toMhnsaEtGcraFaltcLeudCiaSthseapdtraetvphearrraeegideswnoioftd1ei0sa7cc%ehmei(x4bt.lr7ea%bcitRiaSosnDw)bha.etSnceheP(FSNOe=cS8tfioEorCnFth1ei0.ss1ot.muTedryhs)earrraeensgueldsof qauraenciotnastieddeargeadiancsctutrhaetperteodwoimtihniantnhtelysanteeadrmreetfehroednucnecsetratnadiantryd.reTghaerrdelfeorses,ofhethredeegrpeeooPfFrbOrStanvacelhuededs PFOS isomerspresent inthesampleextracts. MENVRONENTAL LABORATORY Paceuo 8i Wgessadessadsessssaoanassas 2 & 32 i feflsse ss [sss [ssm sss i fiHsesassaoagssagslangsseaay 2 i 3. 3. ii 8. 32 $ EEiEHi Hi AE t HB i HBi :4 fll Ler ag |e | 2 | HET ET $ 33d [dss |[ce [das 889 5 1) (153 (IER (sey (1M) | 3:1 Yi: djJelaeefg rip ((e2r2e o|fEE 3[2ady z|3zzzE [322 ||i3i%fg [ii 5 i 5 (PEP |ffp (PER [EE ` p| Jp ppd i 20 LL LL : *| s[dd3 [ddd [deg [488 [333 : && 3 tH iBsaivsazasfizaeegagynaesefsrzey 3 Ld | i fafl==3| 533 |s3| |[ss2 |ssy [sss Bifezzaozaaznzsaassrodsiazassass { ' BT:OM[sEl H 48s iHi nFITSFEY & VALE LL Joh pl BnEo fi FEE | | SS2I0 T|ETay [2d |EIaTy | sy |.a8 B2Yg 5[d5agg 3[2324 n|anes 5[sneg i[snogd | feed [BEE [eg [ERE (EEE Eid I RdiEdNE(332 |szgRE(3I22 RE|a2d [RaEie i 838 388 |3dd [34d [ddd [Edd & i JHofccsesidzmeeegzsElsassessgRzgesaeRnRlgErEoeesizezaEzyy i fafle=s ss [ss [ss [ss3 333 i Bidpsselasessrrenssaesefsanasrgess slazgy [233 (33 |3%E |siR [ia a | see sss eee 4 #s o io ol. +s i i ii 1 A +s | fi bs 4 52 ioe i| ge | i aH i i i i i f af an en Big (BER BaD Bn 9g ggg jiggg [an |ay |a Eee REE LEE uy dg iaggg in28g | EEE odizd |idf (322 (EEE |idq |iEE |i (|BiE2E3 ((isiatd : 3 Ney (sry (Fry (Bry |5EE [53 ` sass (348 [ddd [ddd [edd [gd3 8 d i Beeredererdeceadionsdinns dining i lRpiflees free |es3| Jeez ssp [ssi g Byfazessieenenaaeagssoasisnrdzgngs bigs dd eh |B: [2eds (r|ds |,(89: 8 ies2 8 | dBs E| E|8 i EE EEE PEELE EE 2585 (2L2af ||=a=dd Raip (|BEeE (3Bit $ID (ean |eag nif ogre pa 38 |3Ey [3p (BE 833 |i) | fies (REED [iad aig (ais BodRiiepd ([s2r3yd [(F2ey3d ((32333d (|apd [(3i%ad : i Bd 29 |.29 | zd | e3 | 29 | a3 - HEE i Woossozeezslszansegzaszosssfzzazs 2i Riser [es |szi jese [er sss g g Byfzoezolzasaslaaeaysssaolgsefiedesi lags lan ery [ee laa oLElE l AE E lh figs ot io FE gid (EEF |BEE |3eg (dey (Hid 26d $0 lass [313 [[e3ene3 [(2s8R8 [a22Eg [(eigigd digg [iin (rrz |3E7 [FEY [fad 3 od3dg [33d (33d (dd (dag aaa 5 | d2ky |B2y |23R |fzy (EER |B % i 3 ] 53233 |(s8833 |[8283% |[32B%3 |(328% (3283s gi 558 Add SE (ggg |E5E HEE [SES 38% [SEE (453 |SES (iid z HE Benge le i o[pee|u | i BiflsszHai3q iia i Y HEaA o i} | $58s FH ges H 15 : fH 1 {Hi 8L4E H gpisne1 iy ihe | $5i5t3 | BHiEi!} S dTi: jE 5i L|IERdaar h[HiEgEL:S 2 p13 ENVIRONMREENTPAOLRTLNAOBOR0A9T0O5R7Y 6- Conclusions TuhnceePrtFaOinStysoafm1p0l0e+r1e8s%ul.tspThreesacecnutraeicdnya(n%drTeacbovleery7a) raencdopnrseicdiseiroend(acRcSurDa)toe fwi3tMhinEtChFeo(vberraanlclhmeedt)hod dPeFmoOnSsilrabaotreadtotrhyatcotnhteroilsosmpeirksepsrqoudaunctieanteodadgiasicnesmtabtlhee qpuraendtoimaitnvaentbliyasn.ear reference standard Resultsfortheothertargetanalyteswilbeforthcomingin asubsequentreport. 7 Data/Sample Retention Afol3rMemaEinnviinrgosnamemnptlaelaLanbdoraastsoorcyisattaenddparrojdeocpterdaattian(ghparroccoepdyuraensd.elecronic)wilbe archivedaccording 8 Analytical Personnel 81 3M Environmental Laboratory MichellDe. Malinsky, PhD~~ Research Speciast 82JonPaathcaen SLtaebegOe ps MENVROWENTALLABORATORY Pace2102F p.114 auenviRoNMREENTrAoLRLTBGoREAaTsOoRnY Whos HS Dsd 10/5/2004 Michelle D. Malinsky, Ph.D, {1Rysearcf pes list, PrincipalAnalyticalInvestigator Date Wa2 la KReageP--hnD,. 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ACOA.,pe Mississippi River Pool 2 SurWaptf.e1r47aSamcplieng Lab Request Number: 01 -035 Field Sampling Notes hen 04T227_123900 `Site Identification: Reset 2- cc GPSCoordinates: Proposed UTM _YE725| 197371% seamen Date Collected: 775/0 9 Time Collected: [3 ( CollectedBy:_Bo Observations -Subsurface (46): Dip BAG Lh| Jim Fowple pom spike, DpipeAnMG TZF Emlomgodunpe|Tomvbepairaptoept SX S ~ omPim Perec FloldMeasurements `W-iRnidvDeirrDeectpitohn:: = _2.2_() or -Amblent Temp.: ~ #5" (C) -Water Temp: 2.9.8 CC Field Sampling Notes sitoldontitication: Ryo bo \ = Coc 3 DateCollected: _3/2/2 GPSCoordinates: Time Collected: ZF Proposed UTM _1932 , Y73(558 Collected By: gs) Actusl UTM_o/724, 17/50 vt Ge J" Observations - Subsurface (4-6): _ putinnr pls" 7 "+ Me nie vig dif mee Dip bop Bafa res d&ep(eTno Ser JU, Bey Oup , difed SPA Dp piped Pores Pe diact PP iv: WindDirection:_ SE -RiverDepth: [27 Formrosa: 708.869 EMleelad surements (1 -Ambient Tomp.:<st 7S_( -Water Temp: 2-9 (CC page ___a_ko i LL ticServicesDivision Mississippi River Pool 2 Surface Water: Sampling Lab Request Number: Go --o3% Site Identification: (GPSCoordinates: P Aoroposed UTM Field Sampling Notes Re ach 2 = toc DateCollected: FLYOT 07S7o7u7r00 FTALHT2- TimeCollected: 233 ea Collected By: B35 Observations -Subsurface (~4-6"): 3 Rett K/ ZmSempPle Imspite, fai Dip RertlZe2 Zimpup "PCA bop mPcA Lrivmreg re WindDirection: 5, ~River Depth: EleldMeasurements (f) z Ambient Temp.: ~~ (*&) Water Te2m 5 p(: C) Field Sampling Notes SiteIdentification: 2 ach 2 = toc 5 Date Collected: cos GPS Coordinates: Proposed UTM _O 7607& $775 338 Actusl UTM _09 4025" 725266 TimeCollected: __ (2.50 CollectedBy: _&, `Signature: Observations -Subsurtace (4.6): Dip Bptfe / Fm Semple Zen 5 0gc mF 1a d ~ De) " e = : Tv = - UN Peveacs, Wind Direction: $ &. -RiverDepth: __[ 2 EleldMeasurements (1) rove 07100861 Ambient Temp.: =~ 30 (C) Water Temp.:25-S~ (C) wo Tab . : ceAnalyt7i|cal-- Mississippi River Pool 2 Surface Wap.te14r9Sampling LabRequest Number: _52-03(s" stotdonttcation: Fleld Sampling Notes os 2 f= Loc | DateCollected: 7/8/07 (GPS Coordinates: Time Collected: __ (02 5 Proposed UTM __ < 024C& Actual UTM_p5059 S~ 44795588776777 CollSeicgtneadtuBrye:? I Observations -Subsurtace (+48) APC colocle) Cott Dp Bt YL emsm pSupeseapt f|insSpiPtosn,ct mre Come uLteiv<3) DicopmbBienretd $2vir F=vDeuppPealpepsitPhep ( (oes dpe Gov cocamst: Almssh ovsied . Coc 3 pag _ EMloelad surements omta 4 on sn WindDirection: C- Lid s crore - Am"bWiaetenrtTTeemmpp:: 5~5.52~ (CC)XDe, 23.7 Rew 05013, LITU0 ety aval Field Sampling Notes Site Identification: Repo - Loe 12 Date Collected: _ 7/9/07 GPSCoordinates: Proposed UTM_S/ 2072, 756263 Time Collected: J, s=<) CollectedBy: _&ry-- Observations -Subsurlece (~4-6 2 2pu0p BT uffs m (Ton oSwuepple spin tbs wmfes dup Proms hato 5 " we WinRdiDirveocoetpiorn: {JTTT Form revsec 08 8G EleldMeasurements y 2 Bay, " AmWbaiteenrt TToemmpp.:: 22.3 (_C)) oe_2__ a b BEATE., .. Mississippi River Pool 2 Surface p.150 Water Sampling Lab Request Number: 05-035~ AeUTh ete (7507 oan AJ Field Sampling Notes Sitoldontification: ~~ Ass. 3-coc Date Collected: _ 7/5707 GPSCoordinates: ProposedUTM_ T9330, 47576202 `TimeCollected: __ 7 3 CollectedBy: _B, Observations ~ SuPbrsuorkfaocze .(48): DC ipcaN ntaT re| = Dnsang med IM pile meen nig mpcB perms ooo PA ddd Tig -_-- EMleeladsurements `Wind Direction: Mu~e- ~ 5 =River Depth: (ft) -Amblent Temp.: ~ 6S" (C) Water Temp.: 2%&. (C) Field Sampling Notes Site Identification: fey olf - LOC (O DateCollected: 37 0 J GPS Coordinates: ProposedUTM _ 505382, _o( 9 s86/8TM TimeCollected: _O 7575 CollectedBy: B65 ActunlUT _0093R5535458,4 vRIsHHCUzTTRIET rg, Signature: 7 Observations -Sfubsiurstace (48%: _DPipAcTok, |= BEIYN Supe, TPVTmY)PkE riled fro EleldMeasurements WindDirection: _SE ~RiverDepth: [2 ~ (ft Form revised: 07/09-8G) ~ AmbientTemp: ~4T_) ~WaterTemp: ZZ 9 (C) Page 2 o_o BOEATBYH) sin p.151 - ical Mississippl RLiavberRPeoqoules2tSNuurfmabceer:WaEtOer7S-a0mp3linyg Field Sampling Notes `Site Identification: Les, p3-loc} DateCollected: tH g L 07 GPSCoordinates: Time Collected: __OFS Proposed UTM _~-- Actual UTM_(S T OTF0gL _ $76s125 - Subsurface (~4-67: " M Sie Comd 3c Suseerrvveatyions Collected By: 3 Signature: * Purticprads: Bruce flomson ra pre HMaorrei1nd Hoa Waigrsdy" or Preitctavsben mec bpdect. Lor Yow Pop 3 wo plas ZTAEKDSBuRrrkrFCosrSmaa d03odt)aRllleooebeTdonPoets =Tinled Waker mot mac proticsbebe STB Cruises f* Elold Measurements Wind Direction: Lit SE -Amblent Temp: ~ (6S ob -RiverDepth: ~_ (f. ~Water Temp: 29.7 (C) Field Sampling Notes Sito Identification: Reach Loc & Date Collected: __3/Y/ 07 GPS Coordinates: TimeCollected: 07/0 Proposed UTM __-- Collected By: Actual UTM_p499272, 963328 signature: ZE.J, Observations ~subsurtace (48% _1" Dip Blfly ge Seple_, Go Spike Ped prrmiy Photo #( 2T7=0=i d2ws ~ 3m0p mPcabop L(fCA piratApoep EMleeladsurements WiRnidveDirrDeectpitohn:: Lys_(2_ G7"(1) Form revised 0708.8) -AmWbalteenrt TTeemmpp.:: ~2GJ,~_Z(0C0)) Page a_b p.152 Mississippi River Pool 2 Surface Water Field Data Log Sheet(s) Ce I TTT EE pg PHA e H i a8 ii, tii a HAHA TT HHH EZH8RF iFERrRI ER TT J BR EH 1PERS EERIRRE zx] a9 2 ol sql EE | go] 5s] | EERE REE ERE of ol ol of el off] lof |Belsel Be al gl23 zl 8 8 sl 3 3 gl 23] baal garg qqqy p.154 [AceAnaly5ticalove 3M PROJECT SUMMARY LPraobjcRteqNuaemset:: EMi0s0i-s0s3i8p5pRiverPo2Sourflace Water MonitPorreipnagrDeatBye:: 7Br1a8g20J0a0cobson (8G) at: 7222008 IM3MPrRoejqeucetsLtoeard:: GSaureyWHoolhensten mow LSaasmopristnagryMaRteisxsReorSummary Tae CiedhDoaefaCuiLsotgondSyhFeoertm)(s) SteProtogapns `MMaappss((frsocmaBerduocensMotnfsoomn0B7r-u0c1e-09oemrasil)) ewes wa 0 [[xx]] [x[x]] Ixx]] comenrs Samples ste rectot En. Lb -- _-- -_ General Field Sampling Summary 51. Ssaammploeboottseveorsepappreacsttdyrahe EnonLat.Th rlltr arand vp bark spk accomparied 25 POnraetce PwrasomombeilzersadoJmachobesopnubi(cacae)iagn oSctaieodepaesatatseesstBonroe M7onAsvon3HerFeosrWesegSnTerSLsndPau Farir c"4oCotleecionndesthohvoisn"gSampleswhwiaecobeoctewdabsysssobtmeedrog2atnrgeiaotesawratseer (gsiencgo)ndco2mfaenecroetainorwes rfleesppTg JTSohaemhSeefMaMsOhPuipoGtnc.AaTtTheo"ra"pngSlsPacaCmmtApepDupAlnicwa"tSpepwere"roafnilglePeTCgolAovePtshrwiensaerycw"osnodarmgpdilinenggwechorneetiacinoerl.floiMnPtCphrAocorertcdipgesgosccohnsetiasienaerm.p oro S60MuPetAo ceoxlpeecciteeddwdinoen,sougvohtcondiohronvseaenmhaiisgsvpaelesaraes,otmfhRepialcahnaLsoacmaptleionomantdhRpesocohfLovceasttnxp11eced co7.nTcheenstatmopnltocohnitgehneesrtsw,aasnrtsasmpclhesrmeidne + isos iio fo Pe ed hin oil elven ISH Enviar FETE jt TET =Rh EER EE :a I EE S-- Ee -- -- Tr S-- OP RJEaAmCaHn C-- EORTOiN,RvE--PLICATET|TVa (1aT[ HE[TEHSWA Weim [ Deh if C _Tompl {Su ec m 0o 0 __c s T_pne _1| Ua TMConn riruios | he o foronee se R wes--[r aT LL-- LT T e Iw--e enae roooaarsrtf + IT ~Tiocaion2wm preaye sLo |*1[ T me wl s 1 ez eeda oweern Laor-- vias| fsFm ms ms eller aw2o) me 01 Rano cate 4 Primary C 7] ea wal wl el sisson) Ee bf is fons h ey | [EF mel wlp valour ol lost]Jicemine Joey 17 ewe i ---- = med soe ene) = lpepoooe |T{rRea| c ltocsion7m[perany | L1 [ rwa] [zenb ] sei veel o eed+owner dessa] [S3o0o8o-1 r opor -- oeswo e o se T amT eve -- fonsepinm oy er[wml ve To ealoases -- |dveazeo) ioowe pawn] 101 liftooo i [ss -- om wese | e wa mel se val esiowesasseezz| hme EE eR a i see erE fer ~{Cocation 11 prmayy | 7 eal febndrss m -- e es eT me se ed hp fiz foc2aptrmaoryn ji) mao lw val wefosoesis | aosereo] saloon Sea) ons eee pe bm rs -- m=------ | --+ ~+ ~] Tr j --e " r r -- 1 p s p s -- e Soe me -- 1 e r r F -- E ae T 7 ---- TT -- O gE SPOLYeS ri MEASr Ft,05 2 p.156 nant oeet sen Si = we eee brows 1 soEtEoR. ffraey 0o3F5se 025 I3 Cr oCmtmmnmmrmcueItN aEoeIsLcoE LotuIucrLc sS fBaos,e E | EE mE E I SI a oe . lpmose 0$235soe 028 naI 3 n CS omarcao ockopes r ntotSh tne etsa ,oncin b3 w ii+ oloomes 06228saa 028 evan S Comto tmTrrun Cat1 atgtens eedatnonpemnatirinn Phoomw= e 1 fPuoeeel| ha .: Pa. 6om2 se on evaH1I nt CSr omonnmrnuatr esett ic t sansinbun i. r on r 5 [I2HRI I Cottecersott a y tecans. fr oe r $3 noI3E n Cr oS nners a ncorprn aSy est]e e os,oncin fBoocle}f 1 nEMiEgl RaY 1 (me 0 FII C= a ommvmtaceomrteiioe mbmpan i Boow=e 1 po. o6x2 me on ntHIti St Conoonmttan irvy sSan rrteotups eit fefapsere 1 Ibon, ra 00235so 028 I 3HI Commecontoo apnrryc fooo . Pboow=e 11 fPpaooszwee 11 loloss 00228sma 028 plooes 06238 sone bo ros 025 se 3 non CS obraso copa eorr ciSoeti aaonsa,otnctan 1 [ILRI C Comatn otateotsSes bnce rn no3HR k CSr oimemkasrsSt ees undct: Naira 3 nor st ee HCAar i nS md tr iid p.157 g eemeeennneeny LE Ce RO Hla Se BREE aL ; Sifemvmonunat Bleagizagiagiadpagnaarasgasaagiaduadnids z ZEpusEspREee 55 ldeezatdhlezsaapdoideadsnssiasEiE3nls3aznEspniaaEsegaedseascleeandtd { i vont8 bBPlEleEorRsEElEaEEsEi:nislebehnspdhcaacashtReelfhahnoetl lpiaE ssadh laEssRR nslseEslRsER soRslEsssE RlasYfsEf if Sw2a5n0n0d [Plaemdieescslhsudfdaasksisssasssipgsssanasjsasasenggsssiaoiaajsleanztaonaresdsd 8 i AME] aEnRsElesRgEiYsERE A RdAnRaaRRlaRLaaYlaahLnaABlRaa SnhaAfRbanLaLlD? i aneabilek REE EERE Runs oa RRR i 3 EsllpaasesplaakarsbllseahalssasaplaEaEaEsaEtElsRReRanaaElRanEalaadsasasllasfsf i Bahl baskfanRnElRaanpafaHnaafaenniHnnoablHanaanlas2sah lRsenaaEfEs 7 : lE[aaaan aalfzaesnsnalltaanRbsallaae knaa ahnpseiialsEalaER RszEaEssRiRaeRsaRa lsEsesagassbiRsERsaaReasRsInhst aNlElEs? 208 BEllaeRlioEszttlelnaseiaaayolRasaalnasaazcadlRlasaaaasnsitesEeaapssaaEistshaaelaszsatssaiiaoRnsasasiaass?nRiaRiNg 3 bll sasl easie aaesah shsiR h assbaE nahEE Esb esoEhobGY BsERs RzaR ps eE ltasR las ai etsat eszsela zra g atoeRg aEtata nssaRas AsRsEgos 58 2S BF . 8 og %oE OE OBOE BE $ : & Bi