Document pMgk2xoOEaa6pnZ87BQ6N87X

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Jb . 1941 < i .Vi !*: L . > L ' i - tir J Hr. Frederick Laist, Vice-President International Smelting and Hefining Co 25 Broadway (Room 1720) New York, N. Y. 'll Dear Sir: Re: Johnson et al. Application, Serial No. 178,352, Filed December 6, 1937, For: Method of Producing Tfhite Lead Enclosed herewith are two copies of a Supplemental amendment which we have just forwarded to the Patent Office for filing to supplement the amendments made in our amend ment dated December 31, 1940. Very truly yours, iinc. C oy of Lett e r vi t h e r. closure & t r.t x. r . c use 1 /1 ?. / -1 s. PNYTOOOC841 IK THE VKITED STATES PATENT OFFICE !i In re application of i I GUNNARD ?- JOHNSON, REGINALD G. BOWMAN and A1..LIAM J. KNOX, JR., i Serial No. 178,352 | Filed Deoecber 6, 1937 Div. 56 - Room 4725 ; : S : METHOD OF FH0Du\,j.u WHITE LEAD J : New York, N.Y., January 9, 1941. Honorable Commissioner of Patents Washington, D.C. SUPPLEMENTAL AMENDMENT Sirs Supplementing the amendment dated December 31, 1940, jfiled in the above-identified applloetion, pleaae amend the application aa followsl Claim 2, line 11, after "bicarbonate" insert --ion-- j Claim 4, line 11, after "bioarbonate" insert -- ion--; Claim 5, line 5, after "bioarbonate" Insert -ion--; and j i line 8, after "bioarbonate" insert --ion--} i Claim 11, line 15, after "bioarbonate" insert --ion--} line 16, after "subjecting" insert --a portion of--5 j line 17, after "and" Insert --by--; end line 17, after "anolyte" insert --the remaining portion of--. PNYC00008417 N11214.01 H S IL A R K 3 Reconsideration of this application in its amended fora is respectfully requested. Applicants' solicitor wishes to acknowledge an interview courteously granted by the Examiner in charge of this application. During the interview the claims were con sidered in the light of the affidavit or Willie* *. Zu-__, filed concurrently with the amendment dated December 31, 1940 It appeared during the above-noted interview that the invention would be more accurately defined in claim E, 4, 5 and 11 if it were brought out that the improvement of this invention relates to adjusting the bicarbonate Ion con centration in tha anolyte. Accordingly, these olaims have been amended to insert the word "ion" in appropriate plaoea in the olaims. Claim 11 has also been amended in order more fully to define the speaiflc procedure recited therein. Thus, the claim in its present form calls for subjecting "a portion of" the oatholyta to excess carbonation and adding to tha anolyte "the remaining portion of" unoarbonated oatholyta. This procedure is neither described nor suggested in the patenlf to Johnson at al or by any of the other references of record. It ia submitted that the claims in their present form clearly and patentably define over the references of record and are allowable. Kach of the claims defines a control method which ia not described in the Johnson et al patent or in any of tha other references of record. Tha abov^ mentioned affidavit of William J. Knox, Jr. states aa a matter of fact that with the methods of oontrol represented PNVC0000341S ipy procedures (2) and (4) of the Johnson et al patent the jacetate ions and the sodium ions, respectively, in order to [effect control of the bioarbonate ion concentration, must be ^dded at a rate substantially in excess of the rate at which these added ions are lost during normal operation of the Jsleotrolytic cell. The fast that such v -7 of ions :1s not encountered in the control method of the present lu ll . Invention is also set forth in the affidavit. As a possible [explanation, but not as any limitation to the Invention, It is submitted that the feat that the white lead composition control is more sensitive to the addition of a small quantity cf added hydroxide than it la to the addition of reletlvely large quantities of sold or .bicarbonate may reside In the function of the added substance within the electrolyte. In It he case of added acid or bioarbonate, the edded subatance serves the purpose of changing reaction equilibrium by the change In the concentration of the acid or bioarbonate. In [the control method of the present invention the hydroxyl ions Lhich are added stabilize the ratio of bicarbonate to hydroxyl ions which would otherwise increase during normal operation until finally only lead carbonate would be produced (see page 4 of the specification, last paragraph). Thus, in applicants' control method the added ions which oontrol the resulting product composition are lone which enter into the final product ae it is produced. favorable reconsideration and early allowance are respectfully requested. Respectfully submitted, Attorneys "for Applicants 3. PNVC000C8419