Document pLjMdeyZ23wDxn1Na1Jp1v57

Mr Mq 37 9 P/}L/$3~ - i mtE 3 < tot > 0 LBS. ( EST WT ) < > RT-898-D (0) EWK 03/22/82 COMTYP JOB NAME: 32RT698DM0 STANDARD HRS.___________ TIME PREPARATION NOTES:____ ___ __ __________ ________ ______ _ EQUIP MENT NON-BLEEDING NAME: WATCHUNG RED B I USE 1 ] ACCT I LBS I N-CODE I LBS RECORD:_____ BATCHES SINCE SPARKLER LAST I CLEANED. AFTER 4 BATCHES, CLEAN, DRESS I SPARKLER E PRECOAT WITH 15 DICALITE .J FILTER AID I OBTAIN FOR Si 1 2-CHLORO-4-AMINOTOLUENE-5- ! SULFONIC ACID I BTAIN FOR S4 3-HYDR0XY-2-NAPHTH0IC ACID i INSTALL DV J. CV RECORDER E CONTROLLER CHART] NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF 'I | AREA UNDER V-922 I 1 NOTE: RUN 15* WATER INTO V-904. PUMP WATER I | FROM V-904 THRU.DISTRIBUTOR. IF WATER DOES I i NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH I ] FULL FORCE, NOTIFY SUPERVISOR T I 777-A /\S* I 74-C 1 82-C | RUN 24* (494G) WATER INTO V-932 E HEAT TO ] 80-100 DEG F I ADD IN 8-9 MIN DRESINATE X 1 488 I 53-A 1 488 STIR 5 MIN E RECORD: PH_________(9.5-10.5) | STIR 2 MIN OR LONGER TO DISSOLVE FOR S5 I RUN 35* <721G) WATER INTO V-922 1| WEIGH SODIUM HYDROXIDE IN V-926 E RUN IN1 ,/-a | m.__l l ,__ _, ii TURN ON AGITATOR & STEAM E DUMP IN FROM S2 i i 2-CHL0R0 LOT 4-a min o t o l u e n e _X.2V.___ 4100% % I ,, ,, _ I 5-SULFONIC ACID__________ ____ . _________ l_______ .] ' 7- D I 21^ 74- CT 1 8^ DUMP IN ACTIVATED~CARBON I "5"'" I- DUMP IN FILTER AID HEAT ,T0 212-214 DEG F WATCH FOAM! i i ! i 10 J IJ .RECORD: BY__lfr__< + > IF NECESSARY ADJ TO ) "| <BY ASSUME SOX l__m_l STIR 3 MIN AT 212-214 DEG F, THEN SHUTOFF] | STEAM. WATCH FOAM. RECORD: SPARKLER PRES- 1 | SURE ___ PSI IF NOT ZERO NOTIFY SUPVR. | PUNCHED CIRCULATE 15 MIN OR LONGER THRU SPARKLER 1 UNTIL SOL'N IS CLEAR. MAINTAIN AT 190-195 F] FOR SI 9. RECORD: STARTiP Jt* TOTAL MIN_iirT CLARITY.fife__-BT__/.4__ F E REC_8&1_ F ] Sfp MENT*' PAGE 2 OF 3 /(Sj '/ , USE | CG 32 CODE RT-698-D i (0) 1 LBS cqde ACGTj ! L.B.SVI RUN 2' (58G) WATER INTO V-9044B* WHEN SI7 COMPLETE, PUMP IN V-922 THRU SPARKLER- MAINTAIN V-922 AT 190-195 DEG F Re c o r d ; s t a r t *.&sC_.jLT-OTa l min ^,,4CT RUN 65* C1696G) WATER INTO V-902 1' I DUMP IN CALCIUM HYDROXIDE & STIR TO SMOOTH 1 255 | 542-D SLURRY FOR S43 . '1 I MEASURE___ IjC- UNITS IN V-928 FOR S35 | , r? i HYDROCHLORIC ACID M___ J2-__________l A4_Z.il WEIGH SODIUM NITRITE IN PT FOR S38 , M___ _3-3^3A.X 1//Jr_5| WEIGH SODIUM NITRITE IN DRUM FOR S43 I M_____2_____I 28-D >-;/ i r I 725-A 725-A WHEN Si9 COMPLETE, STOP- PUMP G INSERT V-9221 FOOT PLUG -| RUN IN iO* -<200G) WATER & HEAT.TO 190-195 F| CIRCULATE 15 MIN- THRU- SPARKLER 1 PUMP V-922 THRU SPARKLER INTO V-904^l Oa$M' ** /l I j | I 1 ,I 255 394 388 32- 922 10. T WEIGH SODIUM HYDROXIDE IN PT ' m___ 4i--> ,, DILUTE TO MAXIMUM VOLUME +/-1O0G FOR S47 |^ | \ <l 1L i 1j RUN IN 5* (SOGh WATER & HEAT TO 190-195 F I & CIRCULATE 15 MIN THRU SPARKLER 7-D J 194 904/Jp*iiM<J 11' . #Jpr!\ PUMP WHEN POUR HEAT V-922 THRU SPARKLER INTO V-904 MTY BLOW OUT SPARKLER INTO V-904 IN IGEPAL CO-630 . TO 165-170 DEG F FOR S34 979-D j' 68 1 ffifTEi IF N-740-C SOL'N WAS PUMPED DIRECTLY FROM SPARKLER TO CV OMIT STEPS 37 & 33 RUN IN 1* {95G) WATER INTO WHEN S32 COMPLETE, PUMP V-904 AT -165-170 F THRU UNDERSURFACE DISTRIBUTOR INTO CV AFAP <12-15 MIN)- MAINTAIN 165-170 DEG F IN CV RECORD:; START_JIi>J3._T0TAL MIN___J2-___ RUN IN N-28-D FROM S22 IN 12-15 MIN STIR 15 MIN AT 165-170 DEG F. c ADJ TO 46* (4347.G) AT 32-38 DEG F .4X330 RECORD: TEMP__iV.iL.DEG F, V0mME,,_^L__" RUN IN N-725-A FROM S23 AFAP (5-10 MIN) & RINSE IN- PT' STIR 30 MIN AT 32-38 DEG F MAINTAINING +CR, +KI FOR S40- RECORD TIME STARTl^-fJZ- K CR___ jfc____< + ), KI___ic___<+) " NOTE; N-23-D HYDROCHLORIC ACID X'S IS LOU FOR THIS PROCESS- BE VERY CAREFUL WHEN CHECKING CR-K IF YOU LOSE +CR, YIELD WILL BE LOW- * 57-A VZ2J& DUP050102163 .... ................................................. ......... COMTYP JOB NAME = 32^T698DM0 PAGE 03 PAGE 3 OF 3 .. CG 32 \ . t. ' EODE RT-698-D (0) DATE PRINTED: 8/1 0/82 I USE i N-CODE | LBS | ACCT LBS NOTE i) IF CR-,KI- ADD 20* 'AS IS* INCRHTS | h y b r o c h l g r iCa c id - I- | I RCRD: CR#^___< + ) KI____ _< + > ASSUME 32% . I_____ 2) IF CR+ ,-KI-- ADD 20**AS IS*INCREMENTS. | 1 SODIUM NITRITE '.I ! RCRD : CR___ __ < + ) KI_______( + ) ASSUME 33% i I DUMP IN FROM S3 G STIR 10 MIN LOT * . | I 3-HYDR0XY-2--NAPHTHOIC ACID ____X4MJL ij-OLr_l ^076. j | ` H?* ,,__I'Z5lC2 DUMP IN CALCIUM CHLORIDE 1 448 I ADD FOR MAINTAINING 32-38 DEG F THRU S46 130X3301 28--D 725-A 82-C 20-A 57-A 994 . UR N25A SODIUM NITRITE FR S24 INTO V-902I DUMP IN AMMONIUM CHLORIDE I 245 | 165-A 245 IMMEDIATELY AFTER S44 COMPLETE, WITH V^?2 j AGITATOR ON PUMP V-902 THRU UNDERSURFACE | i DISTRIBUTOR INTO CV IN 18-22 MIN. MAINTAIN | ___ ___ I 32-38 DEG F IN CV. RECORD; START_i.JL | L MIN___ /_$___ I STIRJ3 MIN 6 RECORD : PH_ (51 0-6.0) j _S_7___DEG F (32-38 DEG F> I RUN IN. PT SODIUM HYDROXIDE FR S28 THRU UN- j ____SURFACE LINE, RINSE IN PT"G STIR 15 MIN.] RECORD PH_&u 2l <9.0-9.8>, IF PH IS BELOW 9.0| ADJ TO PH 9.0-9.8 SODIUM HYDROXIDE *i a ^-- ASSUME 50% | AND RECORD: PH__Z'_L?__ DIAZO___m_<-> i i < +) HYDROCHLORIC ACID ASSUME 32% iM EJECT V--932 FROM S8 INTO C^' . IN I OCTANOL HEAT TO 173-1 75 2>EG F IN 55-65 M2fTAND . RECORD: HT_^^XDEG F 6 REC_/li>._DEG F wmmmmm 57-A 7-D ]_ I. 28--D W____ ' 588-A 32 902 DURG S5i2 HEATG, RUN 10 * <2680 UTR INTO V902] 15 TURN ON AGITATOR 6 STEAM 6 DUMP IN BARIUM | 110 CHLORIDE | T6 I HEtff"TO 155-160 DEG F 6 STIR . TO DISSOLVE I 16-B l 110 CV 16 * \gn i WHEN S52 COMPLETE, STRIKE V-902 AT 155-160F i I JWRtJ UNDERSURFACE DISTRIBUTOR INTO CV IN 1 MIN. RECORD: START^/^L_TOTAL MIN_jL__ | HEAT CV TO 193-195 DEG F IN 10-15 MIN 159 | STIR 60 MIN AT 193-195 F. RECORD SJART^^^ ^*6--| AFTR 2 MIN S59 STIR RECORD PH_^l8.8-9.3) I | IF NECESSARY, ADJ TO PH 8.8-9.3 ASSUME 50% I | AisIS-RECDRD: PH__7v/__ ASSUME 32% . j 6j^TAFTR S59 STIR FLOOD TO 180-190* (+/-18000G) i r I AND STOP AGITATOR i ] I WHEN INSTRUCTED BY PROCESSING AREA HALF WAY I J THRU PRESSING, .DUMP IN I OCTANOL, STIR 5 i | MIN 6 STOP AGITATOR. RESUME* PRESSING. START J&t-s zj z.JL'z. FIN /(_:&* Ay '~%~7sy OPTR I 10 7-D U-iPfeS 28-D 588-A 10 DUP050102164 DUP050102165 # (ywi/^jg Vqo ^ .a ). X'to 3ioi<^ife-- jW 1/lA^ Av)t- Ht.-rfiiaa..'&Vfno*l U^tjA> AiU,\M ^f--V.. (-i^J... /6 ^ -Soj^bj) syd^rgr- ikn=&- --- % ( vuyJL^AAJo --&-yUSAJ^M- r1 l. f\\Auu^ r ------------------,--------------------- DUP050102166