Document pByQzkX2BKgpybZBjm1ObM1Vd

wG *>1 CODE YE^?21-D & luium ..iJSlSJ < DATE ) ( LOT > BLENDED BACKj, y 4448* LBS* < EST WT ) aL^P'ROCESSES YE-721-D (M) APPROVED BY: FMP 11/08/82 A COMTYP JOB NAME: 01YE721DMM 1 EQUIP i KENT | -- -I PREP I . J 1 YA \3>l VOJ Of J VT i 351 I 2 359 3 NAME; MOLYBDATE RED OBTAIN FOR S-12 OBTAIN FOR S-34 OBTAIN FOR S-38 OBTAIN FOR S-40 OBTAIN FOR S~44 OBTAIN FOR S-47 WEIGH IN: OPTR OPTR MK ____ WEIGH IN: OPTR_____ , MK 7ji, OPTR ____, MK , 1 USE 1 1 LBS j 1 J-i-r 1 68 | 1 600 1 I 12 | 1 195 I 1 350 | 1 61 j iitol!T-?^,37- T-_, 11 IlijXiT-?j., ^jS2x T-, __________ __% N-CODE 108-A 4-A 3-A 32-D 3-A 711-BD 10-D 423-D I ACCT 1 LBS | 1 68 1 60 1 120 1 195 1 350 1 61 |------------------------ 1 1509 1 1 243 358 4 r yftm io* <500 g > w a t er in t o v -358 10^1 RUN V-359 INTO V-351 & PUMP IN V-351 11 C,ADJ TO 55* <2600 G) 12-^7siFT IN N-108-A FROM S U , 137P STIR 5 MIN 4 RECORD: PHXJ-<9*0-1^.0) U ! ADJ TO PH 9.8-9*9 & RECORD: PH..T-,,5' i ASSUME 50% ASSUME 66% rs i RUN INTO V-351 FROM BADGER METER K- OPTR___________, MK_Jt------- , ,,2l P'Hl Z j%ii iXl^PUMP FROM V-351 TO V-358 IjKl FLUSH V-351 & PUMPING LINES WITH 10O0G i WATER INTO V-358 ia<| ADJ TO 74* <353 G) AT 67-69*F i^RECORD: V0L_7_^B 4 ~Jh.fL.pF 19^T STIR 5 MIN 4 RECORD: PHr^^<7*2-7*4> 4 I G/ML L$t5-< 1 * 055-1 .058 ) i NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK | LIST 4 ATTACH. TAKE 1 QT SAMPLE. 7-D 33-D 28-D I I '/ j #* SV RUN 20* <996 G) WATER INTO V-3-X1 5 REQRS-N--44^D STORAGE TANK TO PUMFvROMCIRCLE ONEO402 410 411 42 424^42! SSECIF U SUPV | *STORAGE TANK MUST CONTAIN AT LEAST 1900 GAL: 402=39", 410=20", 411=38*, 420=20", 424=20*, 425=25* I *WSTORAGE TANK MUST HAVE STIRRED AT LEAST 20 MIN SINCE LAST ADDITION OR ADJUSTMENT , ^STORAGE TANK MUST BE ISOLATED UNTIL ALL yf PUMPING FOR THIS BATCH IS COMPLETE I SET METER FOR 300 G 4 PUMP TO SV %,m~ LOT: EQUIP KENT | COMTYP JOB NAME: 01YE721DMM PAGE 02 DATE PRINTED:11/08/82 I USE I N- |ACCT I LBS I CODE | LBS 5V ! AT APPROX 100 G WHILE CONTINUING TO PUMP, 5! CQNT | CHECK PH 6 DENSITY. RECORD BELOW. IF NOT IN F$NGE*~STOP PUMPING & SEE SUPV. PH:_5_ (2.2-3.?) J DENSITY G/ML (1.270-1.328) 2^r IF _S_-_2__3___O_K.4 WHEN S-22 COMPLETE, RECORD DENSITY J_iV||G/ML ON TRAPPED SAMPLE ^/FROM END OF S-22 PUMPING. USING DENSITY FROM S-24, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 30 G ALREADY PUMPED IN S-22. CIRCLE DENSITY 4 SETTING IN TABLE BELOW. TABLE ** I I I I I I I G/ML 1 .270 1.271 1 .272 SETTING 1259 1253 1248 l |1091 | T4 | 1 .293 iElJING 1 G/ML 114%? 1 1.312 1 1.313 1136 1 1.314 SETTING ! 1049 ! 1045 1 1 040 1 ! 1 1 I 1 .273 1242 1 1 .294 1131 1 1.315 1036 1 1 1 .274 1.275 1236 1231 1 1.295 1 1.296 1126 1121 1 1.316 1 1.317 1032 1 1027 1 1 ! 1 .276 1225 | 1.297 1116 1 1.318 1023 1 1 1 .277 1 .278 1.279 1219 1214 1208 | 1.298 | 1 .299 | 1 .300 1112 1107 1103 1 1.319 1 1 .320 1 1 .321 1019 1015 1010 1 1 1 1 1 l 1 .280 1.281 1203 1198 ! 1 .301 1 1 .302 1098 1094 1 1 .322 1 1.323 1006 1 1003 1 1 1 1 .282 1193 1 1 .303 1089 1 1.324 999 1 1 1 .283 1187 I 1 .304 1084 ! 1.325 995 1 1 1 .284 1 .285 1182 1177 | 1.305 | 1 .306 1080 1076 ! 1.326 ! 1.327 991 1 987 1 1 1 1 .286 1 .287 1171 1166 | 1 .307 I 1 .308 1070 1066 1 1.328 1 1.329 983 1 979 1 1 i 1 .288 1161 ! 1 .309 1061 1 1 .330 975 1 f 1 .289 1^290 1155 1151 1 1 .310 ! 1 .311 1057 1053 ! 1 .331 1 1,332 971 1 967 1 ! 1 SET METER 4 PUMP UJiLg (RECORD FROM TABLE) 1 1 I FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY | I1 l 19 SECONDS II ADJ LEAD NITRATE TO 3244 G (68'-242/245 4 66.5* I I 41-D I 247) AT A7~*&9*F II -RECORD: _jLjL--*F 4 ICE CONSUMED (3304/BLOCK> 1330X__1 57-A 3T STIR 5 MIN 4 RECORD PH: j X_ (2.2-3.7) II **#* USE TITRIMETER TO ADJUST N-41-D PH **** 1_I wCl? NECESSARY ADJ TO PH 3.0-3.1 ASSUME 66% I....J_.._ I 4 RECORD PH= 4j _L_ ASSUME 50% |_________| .40TE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING! | RECORD: [MJLj G/ML (1.128-1.129) IF OUT OF SPEC! | ^*FiLL OUT CHECK LIST 4 ATTACH. I| I 3#T STIR AT 67--69#F FOR S-33. TAKE 1 QT SAMPLE. f ! 33-D 7-D 4094 DUP050059741 > l ot EQUIP MENT I. COMTYP JOB NAME: 01YE721DMM * 03 BATE PR It TED;11/08/82 USE N- | USE LBS CODE | LBS SV 5 CONT TAIN 1 QT SAMPLES OF S-19 6 S-31 SOLUTIONS & TITRATE TWICE NOTIFY SUPV IF ML N-iO-D IS NOT IN RANGE 9.5-9*9 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN O*10 ML N-10-D (IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS)* DO NOT PROCEED IF N-10-D TITRATION IS OUT OF RANGE ADJUST V-358 FOR A TITRATION PH OF I*100 TO TTP01 FROM_FINAL IN-LINE TTTRAT/|MSy^ECORD & ML N-LD-D fj&r 33-D \tO 7-D 1 I ~SV 6 3SKTw HEN S-32 TITRATION OK, STRIKE V-358 THRU BOTH I UNDERSURFACE DISTRIBUTORS INTO SV IN 44-46 MIN i RECORD: START TOTAL MIN____________ I NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS U & BUBBLES APPEAR IN SIGHT GLASSES 3^Kf IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER FOR 15 MINUTES DURING S 34, WASH IN V-358 ty 36 I STIR 2 MIN 6 RECORD F*H__1 *7-1 *8) PBXS,__^r__(MUST BE + ) T7 I STIR TOTAL OF 15 MIN FROM S-34 6 X RECORD: TEMP_J7_X*F (67--73*F> 3STj DUMP N-3-A FROM S-3 39"I STIR 3 MIN X POUR IN N-32-D FROM S-4 STIR 2 MIN 42^1 RUN IN LIQUID ALUM USING BADGER METER mjf STIR 3 MIN 6 FLUSH ALUM LINE WITH WATER 4<Cl DUMP IN N-3 FROM S-5 STIR 4 MIN FOR S-49 604 115 302 390 7 MHRUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW. . | CONTROL PANEL MK ______, U- MK ______ ____________ % 471 DURING S-45 SIFT N-711-B FROM S-6 INTO V-390 IX^WITH AGITATOR ON IN 1-2 MIN 4$/\ STIR 1-2 MIN TO MILKY SOLUTION 90 SV WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B 8 SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV WATCH FOAM!!i IF FOAMING IS EXCESSIVE, STOP I UNTIL FOAM SUBSIDES* 50*1 DUMP IN BLANC FIXE N I WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON I TOP OF PAGE 1 RECORD: CODE __.Tr____ LOT _r 5#! STIR 20 MIN ^ 53 |. RECORD: PH_J*__5__(5.8-6* 0) *ri IF NECESSARY, ADJ TO RH 5*8-6*0 ASSUME 50% i- fi, RECORD: PH-__iTT______ ASSUME 66% FLOOD TO 153* (7298 G) 6 STOP AGITATOR #< FINISH. a >75 128-A 275 7-D 33-D I DUP050059742