Document p2gyGJGB5O0y7Rp93rJg90Vxa

AXY5 YE'"400 MU431 R."01 CLIENT ID: Lab Nan,.: AXYS *NALYTNX. SERVICES 4t91 WATER 25Nw2004 02.Dee-2uo4 OMec-2W4 ,,me: 20:37:58 samy. coli,ctiM: Pmj.d Name: Lab San@* ID: 5amph slza: ln*ia, C~libraGon Dam: 6lslNmMt10: Lc Column ID: SampI. Dataflk: S,.nk Oab FIIbnamc cd. VW. Data FII.rUIM: 22.Nw2@3412:20 NIA L7411-1 (A) 600 mL 0%Dac-m LC-MSIMS Dimcry Cl6 PFS,G-II0523 PFS4G-llOS20 PFSdG~ilOSlJ COMPOUND PFPeA PFHXA PFHpA PFOA PFNA PFDA PF""A PFDol PFTA PFBS PFHxS PFOS LABELED COMPOVND CKWFDA LAB FLAG' " u " " " u " CONC FWND' 0.433 0.207 0.011 0.036 0.013 D"WXlON o.ooS5 0.0026 0.0017 0.0016 O.wO3 o.ccQ5 O.wOl o.ow2 O.GlO2 0.0116 0.0061 &Da05 RETENTION TIME 3.32 4.32 6.20 7.32 6.16 LAB FLAG ' SPIKE CONC. bwl 50.0 CONC. FOUND OXI) 47.0 R(S) RETENTION TIME W.0 8.77 PERFLUORHATED ,a.,, Nmn.: AWS ANALyTlCAL SERWCES 414, WATER 26-NOQOO4 02.Des2Giu 03.Dec-2001 FOIl-il1AL4 SURFACTANT ANALYM8 REPORT smp* conuson: P,o)act mm: Lab smpl. ID: sunph Sk Inis., C*Nb",lon D.lW bl*humnt ID: The: 2o:f!i:,6 LC Column ID: 2 10.0 S!ank Data Filename: WA WmL COMPOUND LAS FLAG' COW FOUND = DETECTION UMlT PFhA PF".XA PFHpA PFOA PFNA PFDA PFUnA PFbA PFTA PFSS PFHxS PFOS 0.369 0.210 0.01 I 0.036 0.018 0.0107 0.w30 0.0016 0.0014 o.Mw)z 0.0007 O.MK12 O.CCC? O.MMl 0.0131 O.OW7 OS403 CLIENT ID: 22-No"-2004 12:20 NIA WGI4411-104 469 rnL 03-Oec-2W4 LCMSlMS Discwery cm PFS4G-110522 PFS4G-4 1OS20 PFS4G-lloS13 RETWTKNl TIME 3.32 4.32 6.20 7.32 5.13 LASELED COMPOUND Ct3-PPDA LAE FUG ' SPIKE CONC. ml) 64x0 CONC. FOUND kwl 47.8 RoL)* RETENTION TIME 66.6 6.77 AXYS YNlNoD PFOS_s1~02 YlA-03~ Rw 01 PERFLUORINNED Form lu2 suRFAclANl MLYSIS REPORT WENT ID: 22.No".20(Y 13:26 MIA L,,,,-2 600 rnL 03-0S&004 LGMYMS Dbc.wery Cl6 PFs*G-I,OG2. PFG4G_11OS20 PFs4G~llO.313 PFPbA PFHXA PFHpA PFDA PFN* PFDI PFUnA PFDOA PFTA PFGS PFHXS PFOS LABELED COMPOUND Cl,-PFDA UB FLAG ' CONC FOUND " " U " " 0.020 U U DETECTION Lllln 001 to 0.0923 o.oo20 O.M)18 D.tnO2 O.OW4 0.0001 0.0001 o.Oca2 0.0124 0.0066 O.CQO6 RRENTIDN TINE 3.32 4.32 6.20 7.32 6.16 IAn SPlKE wnc. FLAG' CONC. (W) 50.0 R(W)* RRENTIDN TIME 95.2 6.77 AXYS METHOD WA.031 PFoJ_SI$2 R.v 01 PERFLUORINATED Lab Nm,.: UYS ANALyTlCAL SERWCES 4191 WATER 2s~~-rn OZ-ES-2004 034%C-2OM 2 10.0 N/A nghL FOml aI2 SURFACVNT ANALYMS REPORT SmphcauKtlon: sanlple Dhfo~: B,,". D.b Fo.nanm: Cd. VW. Dala Flknmn.: CDMPOUND LAB FLAG ' CONC FOUND' DETECTION LIMIT PFPeA PFHXA PFHpA PFOA PFNA PFDA PFUn* PFDOA FFTA PFBS PFHXS PFOS " 0.005 u " " " " " u U " " 0.0003 0.0300 O.OOW O.WOO OX03 O.WC4 0.0002 0.0401 O.wOl 0.0045 0.0023 O.OlJO2 CLIENT ID: 22*-m ,430 NIA L7411-3 500 ml 03-Deu2004 LC-MS/MS oinmry Cl0 PFS4G~,lOS25 FFs`lG~HOS20 PFS4Gv110S13 RETENTKIN TIME 4.32 LABELED COMPOUND ClJPFM LAB FLAG * CONC. FOUND fnol 55.0 RETENTION TIME 0.77 AXYS YETNOD MIA431 R=OS~.S.!Z Rev 01 PEWL"ORlNATED I.& Mama: AWS ANALYITCAL SERWCES 4181 WATER 25Nov-m 02.Dec.2004 --m 2 10.0 NIA WlKlL Fonn m-2 SURFACTANT ANALYSIS REPORT Samph C~UacUom ProJ~wM: nmm 21:34:10 l.m CONC FLAG' DETECTION LIMIT PFP& PPHXA PFNpA PFOA PFNA PFCM P!=U"A PFDoA PITA PFSS PFNXS PFOS 0.36s 0.158 0.036 0.021 " " " " " u " u O.OW7 0.0034 0.0009 0.0010 o.wo1 o.w.5 0.0002 o.cvO2 o.ocQ2 CUENT ID: P-No"-*oo4 rJ:w WA L7411.4 Ml rnL 030~2004 LCMSNS DLSCZNry Cl8 PFS4G~llOS26 PF.s4G~110s20 PFS4G-1lOS13 RETENTION TIME 3.32 4.28 &XI 7.32 LASELED COMPOUND CWPFDA LAB FLAG' FOUND M9J 46.2 RW RETENTION TME 92.4 8.77 AKYS YETHOD WA431 PFas_srp Rev 01 PERFL"ORINA~ED La,, "a,,,.: AKYS ANALYTICM SERVICES Form 1112 SURFACTANT BNALYSIS REPORT SamphcolMlon: Pm,Kt Name: CLIENT ID: 22-Nwt20041555 N/A L7411-5 503 mL 03-Dec-2oM LC-M.?iMS Dbco"ery Cl8 PFS&~,XW7 PFS4G-11OS20 PFS4GmllOSl3 COMPO"ND PFP.A PFHXA PP"pA PFOA PFNA PFDA PF""A PFDOA PFTA PFBS PFHXS PFOS LASELED COMPOUND CIS-PFOA LAS FIAG' COW FOUND ' 0.079 0.035 0.001 o.Oo4 DETECTION LIMIT o.OoS7 0.0020 O.owB 0.0012 0.0002 O.COO8 o.owJ2 0.5XJl 0.0031 0.0075 0.0038 0.0002 RETENllON TIME 3.26 4.32 6.20 7.36 IAS FLAG' SPIKE WNC. (WI 50.0 CONC. FOUND w 48.2 R(K)' 96.4 RETEWION TME .sn .- Axe3 hmHOD PFOU,-D2 YL&ml Rev 01 PERFLUORINATED Fom IN2 SURFACTANT ANALYSIS R- sample c- Lab Nan,.: u(yS ANALYOCAL SERVICES PmbctNme: 4191 Lmb amp* ID: WATER smnpk shw 2sNov-2ow InNhI C,llb"Non Date 02.DBC-2004 lnstrurmnl ID: 05C8C-2wl mm.: 22:,,:M LC Wumn ID: 2 SamIlk htali~ 10.0 Blank DN F0m.m: N/A Cal. VW. L9.l. FS.nam.: CUENT tDt 22.No"-20441115 Nm L74H-S 453 rnL OMesmo4 LC-MS/MS Diacovely Cl8 PFS.G-HOSZS PFS4G~l1OS20 PFS4GeHOS13 COMPOUND PFPeA PFHti PF"p* PFW PFNA PFDA PF"nA PFDD* PFTA PFBS PFHxS PFOS IASELED COYPouND LAB FLAG ' cow FOUND a DETECTION ulm 0.024 0.013 o.cm 0.0049 0.0011 o.oom o.ow7 o.m* 0.0003 0.0001 o.oom 0.0002 o.cms O.Oillfi 0.m RETENTNIN TIME 3.32 4.32 7.36 IAB FIAG' SPIKE CONC. CONC. FWND RW' REIEN'DON nue CUENT ID: tab NW".: AKYS ANALYTCAL SEWtCES Contract No.: 4101 Mdrhr: WATER Sample Receipt Dab: 25Now2004 Extra*" Dab: 02.Dee-2004 AMtysb Da,.: 03-oec-2004 Extract "cd"rn. ,mL,: 2 kljecson "otumn (PL): 10.0 Dt,vtn" Fa.dOC WA Cmeent"oon unns : nm*: 22:303~ amp* cotbcilon: Pro,ed Nmn.: Lab Sampb ID: smpb slu: bkbl CattbmNc." Dak h.INM"l ID: LC totunln ID: smp* DabSNc Blank Data Flbenw".: Cd. VW. Dab Ftbtum.: LA0 FLAG' CONC FOUND' DETWTtON t.tNlT PFWA PFHaA :: PwA u PFOA u PFNA u PFDA u PFUnA U PFDOA U PFTA U PFBS " PFHxS u PFOS U 24-Nov.- 14:0!3 NIA L74(1-7 502 ml 030802004 LC-MSIMS DtscwelyCls PFS4G~llOS20 PFS4G-11 OS20 PFS4Ge11DS13 NETENTtON TIME LABELED COMPOUND CWPFDA LA0 FLAG' SPIKE CDNC. b-a) 50.0 CONC. FOUND b-0) 51.4 NW) 103 RETENTION TtME ST7 AXYS YErHOD HlAal PFo6_slJn Rev 01 PERFLUORINWEO L.b Nm: AXYS ANKYTICAL SERWCES Form ml2 SURFACYANY ANALYSIS REPORT Sampb Cdbcllm: Prq.ol Nam.: &mph Dldaflb: Sbnk D.t. FS.n.m.: Cal. VW. ht. Flbrum.: CLIENT'R: 24Nov-2cQ4 1450 NIA L7411-0 5ca ml 05DEQ2004 LC-MSMS OiSmVeryClB PFS4G~110530 PFs4G~l,OS2u PFS4G~ilCS13 COMPOUND PFPeA PFHXA PFHpA PFOA PFNA PFDA PFUnA PFDotl PFm PFSS PFHrS PFOS LABELED COYW"ND CIIPFDA LAS FUG' u " " " " u " u " " " " CONC FOUND ' DETECTION LlNlT 0.000% o.m* 0.0002 o.cwJ4 0.0002 0.0000 0.0001 o.wo2 O.wQl O.CW7 0.0018 o.occ9 RETENTION TIME LAS FIAG' SPIKE CONC. 1W) 50.0 CDNC. FOUND IW) 50.4 RW)' 101 REENTION TlME 0.77 AXYS METHOD MLAQJt PFos~WD2 Ft." 01 PERFLUORINATED Fmln iuz SURFACWNT ANALYSIS REWRT Lab Nan,.: AXYS AHALYTCM SERVICES Pm,.d NW".: Y&k SampI. RDcdp* Dmtw Exlmc"o" CM.: Analya Date Exlx.ct "d"rn. (IIlL): I",nclk.m "Ol"rn IpL): lx,""ct" F*ctor: C-b.atlon Units : COMPOUND PFPd PF"XA WHpr PFOA PFNA PFDI\ PFUnA PFDOA PFTA PFSS PFHXS PFOS LAS FLAG ' CONC FOVND = DETECTION LlwT " 0.0162 " o.ooo9 " 0.0005 " 0.0004 " o-o033 " 0.0006 o.ooo1 0.0002 0.0002 0.0320 0.0013 0.0007 RETENTION TGAE cu"PFD* Lpg FLAG ' SPINE CONC. ewl 50.0 CONC. FOUND (W) 55.t R&l RETENTtON TIME 110 8.77