Document or2GoE234wmwM2Lq1kYgrDOR

CODE YE-698-D ( DATE ) L2H14 5527* LBS. < LOT ) ' ( EST WT ) PROCESSES ) YE-698-D <T) APPROVED' BYT FUP 10/15/82 COMTYP JOB NAME: 01YE698DMT BLENDED BACK : \G 01, PQ ( LOT r EQUIP MENT PREP 1 %* II 1I NAME: MOLYBDATE ORANGE 'y C ^OBTAIN SODIUM SULFATE FOR S-13 \x CALCULATE 6 SET ON BADGER METER (NITRIC ACID WEAK) . OBTAIN SODIUM CHLORIDE FOR S-33 OBTAIN. SODA ASH FOR S-37 OBTAIN SODIUM SILICATE FOR S-39 | OBTAIN SODA ASH FOR S-43 I OBTAIN ANTIMONY TRIOXIDE FOR S-46 S-1 6 L.% 351 WEIGH SODIUM CHROMATE INTO V-351. n o p t r 2U mg&Z OPTR MK USE 1 LBS ! N-CODE 84 I| 108-A J* I 33-D 734 1 4~A 146 1 3-A 237 1 32-D 350 1 3-A 70 1 711-B j M 10--D 1 ACCT LBS 84 60 734 146 237 350 70 1885 WEIGH IN SODIUM MOLYBDATE SOLUTION OPTR. %Gl- > MK 621, T-36Q j.-.OPTR , MK____ , T-_____ , f 423-D 1 303 UN 10' (500 G) WATER INTO V-358 'UN V-359 INTO V-351 6 PUMP IN V-351 ADJ TO 55* <2600 G) SIFT IN N-108-A FROM S 1 flR 5 MIN 6, RECORD : PH (9^'0r 1 0.0) ADJ TO PH 9.8-9.9 6 RECORD: PHJ&jL (CAUSTIC SODA SOLUTION) ASSUME 50% ASSUME 667. DD N-33-D FROM S 2 USING BADGER METER ADJ TO 66" (3121 G> AT 67~69*F Re c o r d : v o l ^^x." - __6pX_f STIR 5 MIN & RECORD: PH^^l (7.4-7.6) 6 G/ML Jj l 031-< 1 - 080-1 .083) ! NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK LIST 6 ATTACH. TAKE 1 QT SAMPLE NOV 3 1982 7-D 3 3-D 4- RUN 20" (996 G) WATER INTO V-_________ REpQRD N-41-D STORAGE TANK TO PUMP FROM. CIRCLE ONE: 402 41 411 42 424 425 CHECK WITH CU SUPV: *STORAGE TANK MUST CONTAIN AT LEAST 2376 GAI : 402=49" . 410=25* , 411=48", 420=25* , (524=25*1) 425=31 " *sfCRACE TANK MUST HAVE STIRRED AT LEAST 2 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL `LIMPING, FOR THIS BATCH IS COMPLETE SET METER FOR 300 G 6 PUMP TO SV JS>1 LOT.; EQUIP MENT | | | CQMTYP JOB NAME: 01YE698DN7 PAGE 02 - DATE PRINTED , i 5/32 I USE f N- iACCT LBS CODE LBS SV 5 GONT 231 I 24 AT APPROX 100 G WHILE CONTINUING TO PUMP. CHECK PH 6 DENSITY. RECORD BELOW. IP NOT IN RANGE, STOP PUMPING & SEE SUPV. * PH:_______ (2.2-3.7) * DENSITY: _________ G/ML (1.270-1.328) IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD DENSITY______ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING. USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21. CIRCLE DENSITY t, SETTING IN TABLE BELOW. >*** t a b l e *** G/ML 1.270 1 .271 i 07'? *A 1 1 .273 1 .274 1.275 1.276 1 .277 1 .278 1 .279 1 .280 1 .281 1.282 1 .283 1 .284 1 .285 1 .286 1 .286 1 .287 1 .288 1 .289 1.290 SETTING 1 G/ML SETTING 1 G/ML 1673 1670 I 1.291 1 1 ooo 1 1 A Am 7 AL 1534 1527 1 1.312 l 1.313 1663 1 1.293 1521 1 1.314 1656 1 1.294 1515 I 1.315 1649 1 1.295 1509 1 1.316 1641 1 1.296 1503 I 1.317 1634 1 1.297 1497 1 1.318 1627 1 1.298 1490 1 1.319 1620 I 1.299 . 1484 I 1.320 1614 1 1.300 1478 1 1.321 1607 l 1 .301 1473 1 1.322 1600 1 1.302 1467 1 1.323 1593 1 1.303 1461 1 1.324 1586 1 1.304 1455 I 1 .325 1 580 I 1.305 1449 I 1.326 1573 I 1.306 1444 1 1.327 1566 1 1.307 1438 } 1.328 1566 I 1.307 1438 1 1.328 1559 1 1.308 1432 l 1.329 1 553 1 1.309 1427 1 1.33 1546 f 1.310 1421 1 1.331 1540 1 1.311 1415 1 1.332 SETTING 1410 1404 1399 1 394 1388 1383 1378 1372 1 367 1362 135? 1351 1346 1341 1 336 1331 1326 1326 1543 1537 1532 1526 25| SET METER 4, PUMP________G (RECORD FROM TABLE) FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS 261 ADJ LEAD NITRATE TO 76* (3625 G) AT 67-69*F. RECORD __________ *F 271 STIR 5 MIN 6 RECORD PH: ______ (2.2-3.7) 28| IF NECESSARY ADJ TO PH 3.0-3.1 ASSUME 66% 6 RECORD PH: ______ ASSUME 50% NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING 291 RECORD: _____G/ML (1.143-1.144) IF OUT OF SPEC FILL OUT CHECK LIST 6 ATTACH. 30| STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE. 41-D | 5110 57-A I______ 33-D 7-D I s / 1 DUP050059959 COMTYP JOB NAME: 01YE698DMT PAGE 02 AT APPROX 100. G WHILE CONTINUING TO PUMP, CHECK PH 4. DENSITY. RECORD BELOW * IF NOT IN RANGE, STOP PUMPING & SEE SUPV. * P.H 2/-t2>*.- <2*2-3.7 ) * DENSITY: lZ.99-- G/ML- <1*270-1*328) IF S-22 OK i, .WHEN S-21 COMPLETE, RECORD DENSITY ^229-, G/ML ON TRAPPED SAMPLE fm END OF S-21 PUMPING* USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW* NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21. CIRCLE DENSITY & SETTING IN TABLE BELOW* **#* TABLE **** LBS | CODE LBS I_____________ _ G/ML 1 * 270 1*271 1 * 272 i . 273 1 * 274 1 * 275 1 *276 1 *27? 1 .278 1 .279 i . 280 1 *281 1 *282 1 * 283 1 *284 1 - 285 1.286 1.287 i . 288 1 *289 1 * 290 SETTING 1 G/ML SETTING 1 G/ML 1 644 1 1.291 1504 i 1*312 1637. 1 1*292 1487 1 1*313 1630 I 1*293 1491 1 1.314 1623 i 1.294 1 485 1 1*315 1616 I 1*295 1 479 1 1*316 1609 1 1*296 1473 1 1*317 1602 ! 1*297 1467 ! 1.318 1595 I 1-298 1461, 1 1.319 1 588 i /rr._299 "T455*) j 1.320 1582 1575 1 -r.-3Do ~~T433 j 1.301 1444 1 1*321 j -j 322 1568 ! 1.302 1438 ! 1*323 1 562 I 1-303 1 432 1 1.324 1555 i 1.304 1 426 ! 1*325 1549 I 1*35 142 i 1.326 1542 1 1*306 1416 1 1*327 1535 I 1-307 1410 1 1.328 1528 I 1-308 1 404 1 1*329 1522 j 1*309 1399 1 1.33 1 515 I 1*310 1 393 I 1*331 1510 ! 1*311 1387 I 1 * 332 SETTING 1382 1376 1371 1367 1361 1356 1351 1345 1340 1335 i 33 1324 1319 1315 1310 1305 1 300 1295 1 290 1285 1280 l^BT.SET METER & PUMP /^3J_G (RECORD FROM TABLE) | I | FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY | ! j 3O-SEC0NDS j ADJ LEAD NITRATE TO 3625 G <76' -242/245 6 74*5" | S I 247) AT 6?~|69F | ! I RECORD: ic*F & ICE CONSUMED <330*/BL0CK> 1330X !J>f^rfIR 5 MIN G RECORD PH: <2*2-3*7) | ] | jfciHrtr USE TTTRIMETER TO ADJUST N-41-D PH #*## | 128TIF NECESSARY ADJ TO PH 3.0-3.1 ASSUME 66%| 1 1 & RECORD PH : SQ.^ ASSUME 50% I I jliOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING! |>PT RECORD: G/ML <1*143-1*144) IF OUT OF SPEC] ! | ^-PILL OUT CHECK LIST h ATTACH* I STIR AT 67--69*F FOR S-31 TAKE 1 QT SAMPLE* 1 41-D I 5110 1I 1 57-A i I 1 33-D ! 7-D OIZ iJ 11 i .! i DUP050059960 wUMTYP JOB NAME: 1YE698DMT PAGE 03 OBTAIN 1 QT SAMPLES OF S-18 6 S-30 SOLUTIONS 6 TITRATE TWICE NOTIFY SUPV IF ML N-1 HD IS NOT IN RANGE 7*1-7*4 OR IF THE TWO TITRATIONS DIFFER BY DATE PRINTED:1 415/82 USE N- I ACC? LBS CODE I LBS ,1_____ I I MORE. THAN 0.10 ML N-10-D <IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS). DO NOT PROCEED IF N-1-D TITRATION IS OUT OF RANGE ADJUST V-358 FOR A TITRATION PH OF 2. (flr"TP* 3.30 FROM FINAL IN-LINE TITRATION, RECORD LOWEST PH6 ML N-1 O-D j 33-D 7-D WHEN S-31 TITRATION OK , STRIKE V-358 THRU BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN 6 I I 16-18 MIN ^ I RECORD: START TOTAL MIN_,,Zt___ i NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS BUBBLES APPEAR IN SIGHT GLASSES IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER OR 15 MINUTES 34^1 DURING S 33, WASH IN V-358. 55^TSTIR 2 MIN 6 RECORD PH^0_|/__<1 .8-2.5) I ^WBXS, <MUST BE + ) STIR TOTAL OF 15 MIN^FROM S-33 6 RECORD: TEMP^ieZ__F <67-73F> DUMP N-3-A FROM S-4 TIR 3 MIN ] POUR IN N-32-D FROM S-5 TIR 2 MIN RUN IN LIQUID ALUM USING BADGER METER IR 3 MIN 6 FLUSH ALUM LINE WITH WATER 734 115-D 367 3"TJDUMP IN N-3 FROM S-6 44''TSTIR 4 MIN FOR S-48 RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW CONTROL PANEL MK _2L_, MK___ _________ % DUBWG S-44 SIFT N-711-B FROM S-7 INTO V-39 WITH AGITATOR ON IN 1-2 MIN STIR 1-2 MIN TO MILKY SOLUTION - 28-D 28-D 1 5 SV 8 I WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B SOLUTION GRADUALLY OVER 5.MIN PERIOD INTO SV j WATCH FOAM!.'! IF FOAMING IS EXCESSIVE, STOP | L^UNTIL FOAM SUBSIDES. LIMP IN BLANC FIXE N ^WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON || TOP'OF PAGE 1 > I 1^.- RECORD : CODE__________, LOT_____ ____ , _________ * L^rn^-STIR 2 MIN. - STvr~*r r,rrC0RI) . PH_4.l CL.. < 5...8~6.0 ) IF NECESSARY, ADJ TO PH 5.8-6. ASSUME 5% 6 RECORD: PH-____________ ASSUME 66% FLOOD TO 153' <7298 G} 6 STOP AGITATOR 33^^ 12 i 28-A 33 7-D 33-D START j TSBPJSL iF-iIKNIiSirHi\ /t uOPr TifRt . ___ _________________ DUP050059961