Document omJRjKKZqJJ40eLnOdrVx6Q8R
*S.V-
C.v*^Wf)903
*CG 32
CODE RT-880-D PKG ___
OCT 28 1982
L2H76
(''DATE"')
7l o t ~n u mb e r >'
e s t . w t , 1 * LBS .
74> PREP AR#TOT NOTES:
D. V, 902,904
PROCESSES ( )RT-880-D <G)
TYPED BY= JHH STANDARD HRS. 9.3
APPROVED BY EWK 12-31-81
TINE JL2*j\
EQUIP MENT
| NAME: 14AT CHUNG RED B
! USE I LBS
I NOTE: BATCH MUST BE PRESSED PROMPTLY TO
j
I CONTROL COLOR, DO NOT START IF PRESS WILL |
i NOT BE AVAILABLE WITHIN 3 HRS AFTER MAKING.]
j RECORD;
I
i PRESS WILL BE READY.____M.___ _________PR SUF'V j
| START MAKINGM_;____ /________ MAKING SUPV]
N-CODE ACCT LBS
--i
| NOTE; NOTIFY PRESS ROOM BEFORE- ROPING OFF
! AREA UNDER V-922
I
if | NOTE: RUN 15* WATER INTO V-904. PUMP WATER !
I FROM V-904 THRU DISTRIBUTOR. IF WATER DOES i
| NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH |
] FULL FORCE, NOTIFY SUPERVISOR
]
l"
l
| RECORD-:___ ^BATCHES SINCE SPARKLER LAST
i
I CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
i
] SPARKLER & PRE-COAT WITH 15* DICALITE,
i.
L*FfCtER AID
i
Hifi OBTAIN.FOR S112-CHL0R0-4-AMINOTOLUENE-5- 1
I SULFONIC ACID
1
I 3 Jr OBTAIN FOR S27 3-HY DROXY-2-NAPHTH01C ACID. I
Jr\ INSTALL DV i CV RECORDER & CONTROLLER CHART I
777-A 740-C
921/ 931
r>
1/STI RUN 12* (S2GG) WATER INTO V-&L._& ADJ TO
I U50-100 DEG F ADD IN 2-3 MIN DRESINATE XX
j 7 i STIR 5 MIN & RECORD PH__________(9.5-10,5) I 8 | STIR 20 MIN OR LONGER TO DISSOLVE FOR S36
t 11:
99-A
115
RUN 37" <762G> WATER INTO V-922
]1
WEIGH IN SODIUM HYDROXIDE IN V-926 & RUN INI
I
M__/ 2s*.---, J5&JJ&--Z
j TURN ON AGITATOR & STEAM & DUMP IN FROM S2 I
2-.CHL0R0
LOT -2&1____
-tlOCX
'
I ,I
. __gO<?_ L3JLtl
4-AMINO
__rJi___ ___
TOLUENE __l'_______ ___
l 5-SULFONIC __afca____ ___ A*:& -- -f! Jfc* v i
ACID
_____ _
i -v ?40-C
226 1157
EQUIP HE NT
PAGE 2 OF 4
DATE PRINTED: 1/i3/62
| USE
CG 32 CODE RT-830-D CG)
LBS
-------
ACCT LBS
DUMP IN ACTIVATED CARBON
DUMP IN FILTER AID
HEAT TO 212-214 DEG F WATCH FOAM!!
RECORD:
MUST BE + , ADJ IF NECESSARY
SODIUM HYDROXIDE
ASSUME 50%
STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF
STEAM WATCH FOAM! NOTE: RECORD SPARKLER
PRESSURE
___ PSI* IF NOT ZERO NOTIFY
SUPERVISOR,
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOL1N IS CLEAR, MAINTAIN AT. 190-195
G F FOR S24* RECORD: START,,
TOTAL MIN__J/ __ CLARITY______<T
RECORD-: HTF 6 REC___ M-- F
25 I 1 13--Bt 10 I 777-A
902 6
cAJUs.
H SODIUM NITRITE IN PT-i FOR S45 M... ______ ,
rGH SODIUM NITRITE INi DRRUl M FOR S51 m_J.______23^&r.
H SODUM NITRITE IN DRUM FOR S52
m_s _____
MEASURE Jkkl/^UNITS IN V-928 FOR S42
HYDROCHLORIC ACID
M__q I____ , J3lL<J0L_%
RUN 1* <______G> WATER INTO V-_?<?/___
J
NOTE USE CV IF MTY, IF CV NOT MTY USE V-904|
WHEN SI 8 IS COMPLETE', PUMP IN V-922 THRU i
SPARKLER, MAINTAIN V-922 AT 190-195 DEG F,- 1
RECORD: START_________ TOTAL MIN__<#______
[
RUN 63* <16480 WATER INTO V-902
WEIGH SODUM HYDROXIDE IN V-926 & RUN IN
M /2- , SO, (fa '/.
DUMP IN FROM S3
J-OT
3-HYDROXY .
____
APHTHOIC.ACID
ADJ TO 70-90 DEG F i/STIR TO T>lsffiUp.t fr
r
llMZi //a i i
I WHEN S24 COMPLETE, SHUT OFF PUMP 6 INSERT
-922 FOOT-PLUG 1 RUN IN ,10* <209G) WATER 6 HEAT TO' 190-195 F j CIRCULATE 15 MIN THRU SPARKLER* I CIRCULATE 15 MIN THRU SPARKLER,
?
7-D 82-C '"
1
i i 1
i !
473 10SS
/-c j
904/CV 8- " .
922 9
j --LU.M,, *904/CV
>|
PUMP V-922 tHRU SPARKLER INTO V-904/CV
I RUN IN 5" <104G) WATER & HEAT TO 190-195 F i
| CIRCULATE 15 MIN THRU SPARKLER*
I
,, PUMP V-922 THRU SPARKLER INTO V-904/CV l WHEN MTY BLOW OUT SPARKLER INTO V-904/CV
DUP050060751
DATE PRINTED: 1/43/82
^i5SfFT'""` ,,r1ENT | 1 PAGE 3 OF 4
I USEI N-CODE ! ACCT
CG 32 CODE RT-880-D (G) l LBS |
| LBS
904/CV1' 10
CONT I
1 DISSOLVE ALKANOL XC IN 20G WATER AT 135-145!
i F WATER FROM HOT WATER MIXER IN DRUM & POUR!
] HEAT V-904/CV TO 165-170 F FOR S41
1 1
i 32 |
J |
| 133-B j
! |
32
l WHEN S28 COMPLETE,/ MEASURE TRISULPHOIL SOAP I 105 I
CALIBRATED CONTAINER,- SLURRY WITH 46G I
|
ATER IN DRUM & POUR INTO V-902
II
ft EJECT IN V-921/931 FROM S8
II
39-A | ] |
.1
105
FT-2 \yt>KRUN SODIUM HYDROXIDE INTO PT M_/2__, 12- TO 20" <72G) l^ri. STIR 5 MIN OR LONGER FOR S57
I I I
7-D { 132 1
! 1 NOTE: IF N-740-C SOLUTION WAS PUMPED
|
DIRECTLY FROM SPARKLER TO CV AT
1
S' S- 23 & 24, OMIT S*S 40,1. 41
|
iV 4^URUN 1" <95G) WATER INTO V-J3JLj L_
I I
IF V-904 IS USED, PUMP V-904 AT 165-170 F |
THRU UNDERSURFACE DISTRIBUTOR INTO CV AFAP 1
<12-15 MIN) MAINTAIN165-170 DEG F
}
L RECORD: STARTTOTAL MINJ I "T RUN IN N-28-D HYDROCHLORIC ACID FROM S22 l
Jr>lM 12-15 MIN*
I
>-STIR 5 MIN
I
ADJ TO
(4252G) AT 32-38 DEG F
147X330
I :REC0DTTEMP_e2fiL__F` STICK *
I
IN N-725-A SODIUM NITRITE FROM SI9 AFAPI
15-10 MIN),& RINSE IN ,
I
i STIR 20 MIN- AT'32-38 F MAINTAINING*CR,
I_______
+KI FOR' S$4 RECORD
ME START_A?._,, I
I CR_-T_r___< + ) KI XL_< + > NOTE,:
1
1) IF CR-, KI -, ADD 20* "AS IS" INCREMENTS 1
RECORD: CR_, < + ) KI____ < + )
I
HYDROCHLORIC ACID
ASSUME 32% I____ _
?) IF CR+, KI-, ADD 20* "AS IS* INCREMENTS |
"RECORD: CR __< + > KI____ < + )'
I
SODIUM NITRITE
ASSUME 33% i_______
fp IN CALCIUM CHLORIDE "Tc
l H66
DUME^fN. STRONTIUM NITRATE r ,r
I 255
57-A
57-A
28pD 725-A |
20-A | 1 1 66 246-B,EI 255
\5J^1 ADD FOR MAINTAINING AT 32-38 DEG F DURING
1 . J-'tOUPLING |>T I POUR. IN N-725-A SODIUM NITRITE FROM S20
137X330
57-A 112**}
902
POUR N-725-A SODIUM NITRITE FROM S21 INTO I
I
V-902 ,,-
If
14
! DiAMF^IN AMMONIUM CHLORIDE 6 STIR 2-3 MIN | 228 1 165- A
228
CV I54M IMMEDIATELY COUPLE 902 THRU UNDERSUFACE I
15 I 1 DISTRIBUTOR INTO CV IN 18-22 MIN, MAINTAIN I
| Qi^*T**32-38 DEG,,F* RECORD: START*,3;~r--. I
TOATL MIN.JjB___ _
I
15S | INSJAfctr' 5/16" ORIFICE IN UNDERSURFACE
I
| J^tf&ITlON LINE
-I
IXTI WHEN S54 COMPLETE, STIR 30 MIN & RECORD 1
1 I BASE_^,,( + ) DIAZO__,!frrn:) PH.#X.<5,6-6,0) I
! i I i I i I I
DUP050060752
eq u ip/ MENT
CV 15 CONT
DATE PRINTED: 1/13/82
OF 4 CG 32 CODE RT-880-D <G>
~USE I n -c o d e ~"Ta c c t
LBS I
/ i LBS
-D FROM S39THRU 5/16* ORIFICE
RINSE IN RECORD : j5SL,__MIN <40-50 JfTN)
STIR 2$ MIN & RECORD; PHtM(-g?^CZ<0-8.5)
BELOW 7*0 ADJ TO PH 7^8.5 WITH
-D ONLY. RECORD PH____ ASSUME 50%
WEIH"SO0IUM HYDROXIDE IN V-926 & RUN IN
ASSUME 50%
STjtft^S MIN & RECORD
+) .
A20__*!L-_(-) PH__Km--__< 90-9.8 >
I IF PH BELOW 9.0 ADJ TO PH 9.0-9.8 WITH
H>D ONLY. RECORD-PH
?ODIUM HYDROXIDE
. ASSUME 50%
MEASURE I OCTANOL IN CALIBRATED.CONTAINER
POUR IN
HEAT^TQ ,19^95 DEG F IN 75-80 MIN. RECORD
l CORD : HT^fei^lDEG F h REC_tf^-DEG F
" JLjAT 193-195 DEG F. RECORD:
MIN S66 STIR
RECORD:
/ ' PH_ML__< 8.8-9.3)
1 IF PH BELOW 8.8, ADJ TO EH.8.8-9.3 WITH
| N;>M? ONLY. RECORD PH_
JDIUM HYDROXIDE
ASSUME 50%
1 WHQKS66 COMPLETE, FLOOD TO 180-190*
L>K7-18,000G)
STOP AGITATOR
WHEN INSTRUCTED BY PROCESSING AREA HALFWAY
THRU PRESSING
?
<1) DUMP IN I OCTANOL
<2) STIR 5 MIN
<3> ADVISE PROCESSING TO RESUME PRESSING
10 | 588-A | 10
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DUP050060753
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