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Colma LS Rai services PiCnreda:te1d4w0i2h:2A0na1l0ys8t:4R1e:b0o0rPteAr ouPrtoajeFcite Eo2v0o81s0nPCraoleLocniga.ruCits Acquisition Method _ PECHinetextong dam ARlegosraitThamblUesed nStEelTiOuaSnaesLone Instrument Name __AP1 5000 [SampleName TPeCstm Teorvar 8] `Acquisition Date. 2/8/2010 6.45.29 PM [injec[5tonVouume| {[SA[caqmSupilsaietcmioonpmMemltehneodd_||PLoFWsC28K50netexLo[|nWSDeaigimlguptdhlitoenatToFyavmpcoetlorume [0[01.000 inRterisuslts SuA[mnmlaeyrRyT | rons | smn| csemeramer[|szoasemineor[| s0var| sET5oi7Gnomyre||| GemesiCane| sm | em-so? rroesr1 | Tamas | assasm| cern rosros | | zo|aoa | swo| eres| srw | smo | smo sao | | m ww | | To [Pront | saeaas| noeroa| amma| fosiso | sow | ero | st | we PFURAY | 412405| 13CPFUNA| 1727a0 | sastoo | Soo | 1% | 104 | No Poroosnt | a[1asr@otsoe||o1ecrPrors ||owseoerinne|| msswn || ssoomo || ssomeo || 1w0w1 || wNoe pris Torrent | sassre| moron| Toso | | sra|acorrpes| some | enn wwe |sow| w= sw | we Te] | wo 7 aoed ze Sirulie Page 28.1 262 277 AColumbia AnalyticalServices" IRC Summary worries rm || ST Printed: 14/02/2010 6:41:00 PM aCo e| Calculate| d es_rseceros srsceron prmz was | ww | we | or mwaws || eww ee | we we | | Tz ew | am |w|m we | 20s wea | em | we |om eas | mmm | he om 278 Columbia LS oii services: T= Quantitative Peak = Review ga | A i: A Created vith Analyst Re3porter Prnted: 14102/5010'5:41 00PHA 7% PFC To5.0ppb = iC ba4s1el3Pi0Fn1eO6AM8i10s0s8ed | oBa4s7e10l3iC3n-7eP2oF0MOiA0s8sed | cB4a6se3Pi0Fn4Ne1cA5l10i0s8sed| o S4a68s1.e30iC1n4-e2Po3F.N0MAiDsased i. iio i| i=cl I Lo siorLa n roie n sciou n oa4st9i0n2e0a0s0s8ed | cBa5s0e3i0n/e80c.h0i0s8sed | oB5a1s3e0i4n6e9c.M0is0saed | Ba5se1l5i0n4e7o00MiDsased . Lo LE 4 io ol au ern Lo 4 arin al | || oB5as6o3l0n5e19oM0i0sased | Ba5se6l5i0n2e70c0Mi0sased | Bas5e0l0i1ne80o0M0i8ssed | B5as0e2li0n8e00M0i8ssed iz== -| c1l i=- Lilc3 he J a n cB6aP1sF3s0Di5nO6cA9o0M1s0saed | cB61a31seC5i-0nP1eF6oD9MO0iA0s8sed | c6B6s2se0Pl6FnT1e9cM01i0s8ses | cB6as11e35lCi0n-/ePF1O6M080iAs0sed "3a i= I Ih cB7a1s3ePi0Fn6Te6Oc9At0Tis0saed | Ba6se11l35iC0n-e/PF1oD6MO9i0As08sed 0 Before O After Page 2801262 2719 3 Sotambia AnalyticalServices Created with Anant4Reporter Printed: 1410212010 6:41.00 PHA a `lon Ratio Confirmation T L i mE = Lz + Ra 2 i=W PFC 5.0p=p|b oo zl of | 4130P1F3O6A92008 463P0N21A820 Da cBaseline Missed | cBaseine oMissed | 493,P0R9O9S.200 oBaselinecMissed | 51P3F0O2A620D0a Baseline Missed Wrong Peak Wrong Peak Wiong Peak Wrong Peak T I = i) I 4 Zil e Ja E3L] de J, TlL em - ad zl x 563P.0F12U69A.02 0a c Baseline Missed | 509.P0F19O9S.02Da Baseline oMissed | 613P.F01D6O0A.02 0a oBaselinecMissed | 663.P0/F169T.20 0a Baseline c Missed Wrong Peak Wrong Peak Wrong Peak Wrong Peak io i 71P3F0T/E1A629D0a BasWerlionnegc PMeiasksed 0 Before 0 After Page 20of 242 280 48 CAonlaulymtbiicaal ServicesTM PrCinrteead:ted14v/i0t2h/A2n0a1l0ys6t:4R1e:b0o0rtPeMr FDPeracouniisteion Woinot_pFi rEaCiPneEextRotnSagm RRnoeoeurmtmetnmatysasmde G 4i5m1at0i0av0mn e [S`aAmcqpuliseitiaonmDeate |TP2/F8/2T0o10g6o:53.02 PH [["SSAacaqmumpilpsieltcieoonmdMmeetrhod_[|t{ PcFuCsiznaesteexLodanmg | [SoiaemwpielgenntFToyapVcetoolrum[s_0J[ oo00sagas||| Results Summary Tmt | tone|sneme [aa [0 TRE [nam |e | PrOAT | 1341.96| 13GPFOA| Sotsano| ozo | 1000 | 10200 | 02 | no [| PPFrNoAst1 | zaman| 2.29242)| 1m3sCc-ePrFoNsA|| s2357w300e||sn2o91ae050ma0|| Pron | saan| cern | am|semn| roma | ax| o cern ns| vam| visa| [pr|oeasza1an| wsceros | sssmoo| sso | Prooat | 47sasn| 1iceroen| zswn| tassseo | pris sma| norron| zn|wn| [prront | s7aee| 1scoroon | asa| rom | roo 10.000 | tooo | tooo | tooo | tose | tome | tose | tow 10.800 | m0108 | Nnoe | toa | roe | ne | now |mo| ne naseo |ws| no tam |14| to am | | wo| we | ws | Ne 7 Kteg E=5 2.11410 281 [5m PrCereda:ted14w0i2n/2A0n1a0i6s14R1e.p0o0rPteir RCSUMMAY Anat Peak Name -- swrros oProer [rproosws pra RT (Expected) a= wen | oars mam | wen | wom| | orwaew ||w mm |w w o | n w en|] | aemwawn | men |T ow | e eome | EO I Pa31gor2e62 282 5 SAnlalaytmicaal ServicesTM PrCinrteead:ted14w1i0t2h7A2n0a1l0y6s:t41p:o00rtPeMr Quantitative Tm Peak Review = TE PFC 10ppb zm ~-- 2% -= A | A FIc= A ai.l A _ B4a1s3ePl0i/Fn1Oe6A910Mi0sased | leon B4a1s17e3l.iC0n-3eP7FM2Oi0As0saed | oB4as6e3Pl0iE4nNe1Ac3T0M0is8sed | Ba4s6e61l.3i0C/n-4e2P3cF.N0MAiDsased lagen age - 42a i3| | -3 ' |o El |7 = oBa4s9e9lP.i0Fn/Oe8S0o0TMiDsased | . Ba5s01e33l,i0Cn/-e8P0cF.0MOiSDsased | oB5a1s3e,Pi0Fn1De46oA9M1.i0s0saed | Ba5s1e1l53i0Cn4-e7P0cF0OMAiDsased ico 2a pT gga Ll - <l ! i Bl i io| 563P.F0U5N1A9.1Da Baseline oMissed | 51635C.0-1P2F7U0N0A0a Baselinec Missed | cBa5s99eF.l0iO/e8S0c.M0TiDsased | oBa5se10l33iCn.-e0PcF8OM0Sia0ssed FA+ iioEl i=z | ic 613P0F/D5O6A910 Da cBaselinec Missed | 61135C0-/P1F69D0OADa Baseline cMissed | 663P0F6T1A0T0 Da Baseline Missed | 611530C-1P6F8D0oADa Baseline Missed i: Loi 713P.E08T6e8A.T00a 61135C0-/P1FD6O9DA0a c Baseline o Missed | Baselineo Missed 0 Before O After Pa32g0f2e62 283 4 ASnoalluymtibciaal Services .8 PrCinrteead;ted14w1i0t2h2A2n0a1l0ys6t:4R1e:p0o0rtPeMr Ee ERE fon Ratio Confirmation TT PFC 10ppb = = :iho 41P3F.0O3A6920 Da BaseWlionnegoPMeiasksed ,i o : 563P.0F12U69A.02 Da o BasWerlionneg PMeiasksed [ii 5 4630P2E19N.A02 Da | oBasWelrionnegoPMeiasksed = a i Cl 4 L 599P.0R/O9S9.20 Da | co BasWerlionnegoPMeiasksed Iqf3 o zs 499P.O09S9?0 Da | oBasWerlonnegcMPieasksed T A. i alts p 613P0F/D1O6A902 Da | BaseWlrionnegoPMeiasksed iH=-Il { 513.P0F26O0A.2 Da | o BasWerlionnegoPMeiasksed l=|! Ii sg ul 663.P0F11T68A.20 Da | c BaWserloinnegoPMeiasksed ul io site 713P.E0T/1E62R9D.a0 BasWeiloinnegGPMeiasksed 0 Before OJ After Page 33of 262 284 5 olambia AnalyticalServices" Created with Analyst R9eporter Printed: 1402/2010 6:41.00 PM Project DataFile Ewan's ProCiSPRCS 0208100\CalLongwif Acquisition Method _PFCKnetextong dam Result Table AIlngsotrriutmhemntUNseadme 0206105amplesLong (Gb _I_nAPt!el5i0Q0u0an [SempreName [Prozopep 2/8/2010 7:00.35 PM | inecton Vir [injectionvorume [5 | `Acauisition Method | PFCKinefexLdoanmg Sample ID LCMiS2.85F SampleType Standard 00 [ ( (Sam |pleC~o~ m|m = Weie ghttn T ovolt umT e 1000 Results Summary "NoAt" n||aAfniaieysireRTn| toname [san | FAraRis || ExpOCMoGnc || CamCgoinmen|| Accuoracyn" proR1 | 1350.35| 13CPFOA| zesesoo | zo| zoom | taco | sz| No | rnat | 2zsaaz| rcrena | zz | doree| zoom | maw | m0 no [Prost | 2ss@ss| tscpros | To|mevoan| mov | tes | so Pront | 330036| 130PF0A| 2oasio0| daptio|o 20000 | 19000 | 9% | No PrUnA1| 412406) | 19CPFUNA |e4| 3 zmsos0 e0| 20000 | teen | sz | No [Prost | 41210) | 13C-PFOS | 7033400| 14304000 | 20.000 [oroont | arses| roproon| smsera | asa| wo | 18.500 93 No aw | ss | me | [PFTA1 | 5.286514) | 13C-PFDOA| 226670| 1476200 | 20000 | 18.600 [Pr|rse7aae7te | 1acpr|oazosenro| woziao0 | 2000 | taco | 83 | No es | we 7 aiA Cs Lrieice Pa34gof2e02 285 Created withAnaly oporter IRC Summary - [oraz Tswracerros s racer oi maw |ow | e ww o | e oa wmaosw ||m emm |w m wo |eose o | een |w|m wo | oss ] onaw | wen|e| ew 286 8 SAnoallytuicmal Services" Created with Analy1R1eporter Printed: 1410272010 6:41:00 PM Quantitative Peak Review Eg or = PFC 20ppb, ~ TIE Tz - A i| A [i1 5= 413P0/F1O6A910 0a 41137C.-0P57F2O0A0a 463P0/E4N1A910 Da 4681.30C/4-2P3F.N0ADa cBasenionneecMissed | r cBasele ineoMssed | oBaselinheyoMissed | coc Boasenligne oeMaissed A| 1 i. : E 7 | E 499P.F0O8S001 Da 15035C0-/P8F0.O0S0a 513P.0F4O6A9T.00a Baselnicine oMssed | ch Baseliy neo Missed | oBlasielnec Missed | 511530C4-7P0F0OADa Baselliingeeo Mieassed ii3 il| i=i i2) 563P0F/U5R1A90T Da 561530C/-2P7F0U0RADa 509P.F0O8S001 Da 50133.C0-8P0F0OSDa cBaselineo Missed | oBaselinecMissed | Baseline Missed | Baselineo Missed = oa estan Cn Bagh tina peg i || io Eo A 3 i i. 613P0F/D5O6A910 Da 61135C0-/1P6F9D.O0ADa 663P0E6T1A901 Da 611530C-1P6F0D0OADa | cBaseinecMissed | oBaselneoMissed | oBaselinecMissed | BaseloMiisnseed - Ll 71P3F.0T6E69A.10 Da 61135C0./PF1D6o9A00a Baseline o Missed | Baseline o Missed 0 Before O After Page 36 of 242 287 4 ASnoalluymtibciaal Services" PrCinrteead:ted14w/i0t2h12A0n1a0'l6y:p4.1R1:e20po0rPtHeAr Ton Ratio Confirmation : To PFC 20ppb ---- a7 fko a h= Lfor iE ol 2\ | BR I a Ba4s1e3lP0i/Fn3eO6Ro920Mi0sased | 463.P0F21A3.20 0a c Baseline c Missed | oBa4s9e9.lP0iF1n9Oe9So.02MiDsased | Ba5s1e3lP0i1Fn2eO6Ac902MiDsased Wrong Peak Wrong Peak Wrong Peak _ Wrong Peak - = 7 T oo ] ol ol J b= 1 io 4 i) ae fo] sf c5B6as3eP0li2Un6Te9A02Mi0sased | B5a0s9eP.l0Fi1nD9e9S.=20M0isased | o6B1a3Ps0eFl/i1On6eA0oM02is0ased | Ba6s6e3l.Pi0n/Fe16oT02.M0i0sased Wrong Peak WongPeak =WrongPeak WrongPeak Li 4 B7as1eP3lFi0nT/eE1oA62M9iDs0ased Wrong Peak 0 Before OAfter Pa37gof2e42 288 3 Golambia Analytical Services PrCinrteead:ted14w/i0t2h/A2n0a1l0y6s:P4R1b.B0o0rtPeMr PrDoatjaecFtile 0E2w0a8r1l0s0P\rCoajleLciosnPgFwCifs Acquisition Method _PFCkinetexLdoanmg Result Table 0206105amplesLong 160 IAlngsotrriutmhemntUNsaemde __AIPnItel5i0Q0u0an [SampleName "TFC Soppb 28/2010 7:06:10 PM PFChinelextong dam [Sample | Loms2.85 SampleComment | Sample Type |Standard| [DilutionFactor | 7.00 |WeighttoVol[u0m0e0 Results Summary TANnaamiyeie ||A(nEaxlpeyctteedR)Y| SMoe | saweaves| [Prot | 1asaa6|13cp|rasoseaAw0 | PENA1 | 2312.42) | 13CPFNA| 2153900| [Prost |238283| 1acpros| essesto| [POAT |33|3 13c0 PFDA3 |1s34 5000| [Prunat| 1208| 1acpruna | tesso | [Prost | 41210 |racp|resosesseo| | PFDoA1 13C-PFDOA | 227850| [prtiat | 5306.14)| 13c.PFDOA PFTeA1 | 573(574)| 13CPFDOA| 227850 | AAnraeivaie | ExgpmCto)ne|| Ca(loeg:iCmlyo1Acncucrwcacy||oMa7 r| 7zase0 | sooo | sts00 103 | No | 12661000| 50.000 | 51300 | 103 | No | areraoon| sooo | S000 100 | No | 10412000| 50000 | 50500 102 | No 77etso0 | sooo | soso | ter | Ne | sasesooo| soon | soso | 101 | No 6008800 | 50000 | 48500 | 87 | No | 50000 | as | ss No | 2343500 | 50000 | 50.800 | 102 | No 4odg E21e Pa38gof2e42 289 RCsummary Created with Analy Reporter epreosn | oem |wen| we | em | s cers am|a sms o| w ors | [[ oem |r maw | wwoa omn||we|oe m aw | Pprrinse S_13C-PFDOA | | eamwmaess | ||a eemwm ||| es ewo [|| eem0.08m] 290 4AnSaoltyutmibciaal Services" Quantitative Peak Review I = i: i= Created with Analyst Re1p5orter Printed: 14102720106:41:00 PM PFC 50ppb = | i= i 413P01F1O6A910 0a 41137C.-0P3F72O0A0a o Baseline c Missed| oBaselnooMssed | 463.0P4E1N0A.10 0a cBaseinecMssed | 46163.C0P4F2N3AD.0a oBaseine o Missed ogg pe pe tig gy =: | |iz-i iLl==| z _] 1 Nu i-oo I | 1 499P.F0O8S001 Da cBaseline cMssed | 5031.30/C8-0.P0FOS0a 513P.0F4D8A91. 0a oBsselinecMssed | oBaselnecMissed | 511530C4-7P0F0DADa co Baseline o Missed a blaze pea a To -i i1 Foos iool - a zl a 563P,F0/U5R1A9.10 Da 15535C.-02P7F0U.0NADa 509P.R0O80S01 Da 50133.0C/-8P0F.0OSDa Baseline oMissed|oBaseineoMissed| oBasecMlsnseed | Baselc Miisnseed = 7 = LS3 :| = rd = eoll 1 = Te oil = [ =f i= ia 613.0P/F5D6O9A.10 Da a CBaseliy ne cMissed | fi il i 3 713P0E6T6e9A0T 0a Baselinec Missed | 51153.0C1-1P6F9D.0OA0a e cBasely inecMissed | cl 1 1 -- 611530C-1P6F9D0OA0a Baselinec Missed 6630P/F61T8A.T00a cBasel(n00e0cVisPeased | 61135C0-/PF1D6O09Aa0 Baselninaepo eMissed 0 Before OJ After Pa40gof2e62 291 4CAonlaulymtbiicaalServices Created with Anatyhp.p16aren Printed: 14/02/2010 6:41:00 PM WE fon Ratio C7onfirmation= lb - = rea .] PFC 50pp7b 2A ll | CB4as1o3Pi5FnO5oAc8M20i0n0sed | Wong Peak Ba46s3aP0Fn2N1Ao62m0a0saed | rong Pes oSw4P6eR6l.nO0e0Sc520mu0s0ed | ions Pek o B5Wa1rs2iPo0nnF2sgO8s6APm0es0aet8ed i LC7 37 Li ho| RE: -- i : oe3 8 cl5a6iP3rF0Ue2N8cAM52i0t0sed| cBa5e6i8Pn,Re0O0sS5M20i0u0sed | oB5a1s3Po0Fi1Dn6Go5Ao0m2a0saed | o BseassP0e1Fn66T20ma0saed tons Pes rong Pear irons peak ons Peak 34 B7a1s3Pi0Fn1Tg6eA9Z0Mi0s0sed rong Peak O Before O After Page 41 or262 292 Columbia LS oan services: PriCnrteead:ted14w0it2h/2A0na1l0ys5t:4Re11p07o0rtPeMr DParoajecFtile TG2w0as1s00PCraolRLaoangPrwCits AcquisitionMethod _ PFCiinetestdoanmg AlRgeorsiathTmobiUesed TIEntEetCiQSuaan meLong ab Instrument Name__ API 5000 [Sampleame TPToriseoatoo7m3b0 iSEPoV-- [`AcSquiasitmionpMeltheodd| P[LFoCWisi2n77e2tesLdoanrg Sameomen THmieneecmioornVvaitrare J5 s ]| SaDimlputlioenTFyapcetor | C1.u0t0tyCorel | WeighttoVolums om | Results Summary Non [Analyte | tay| Analyte RT ctearmoen||sarves||wAnwPaleytee |ExsTpOoCRowEnc.| a[ammes | 1m | on Accuracy |FMeao? rns amas| ora| swe| swe | mmo | wan | ww [Pbrroosntr ||s 2a8@sv s|| v1oarcn prroons|| ess6ss7o00|| 1s5w4s47a0t0o0|| 2m0o00w0 || m20e80m0 || 1i0m4s || vNoo| [onrotst taroa|socroronss|| sannew||swaonrneo|| aw | auom | an | soso | ow toe | we] | wo | PFFrDrOmAs1 | 4[76(46s3)||mw1o3Cr-rPaoFoDOnA|| 2a1r73o3m0 || vr 2671400 || 2m0.o00m0 || s22a6m0o0 || m11a3 | No | ert TsrernTosroos[im| sovan| own | ww| wn | we - 7 Adl l coec e te Pa46gof2e62 203 LA Soumbia AnalyticalServices: CrweihAanantReepordter Printed: 14102120106:41:00 PM WeSummary Anse pes ame [rreern)[aes]weatorr[ oof | [sopra |imams | amew|we | we P5r.o1s0.PPA jowerros [eroaz [sermon Sorrm Pros Proc [oormom amas | wwe | we | vree | | ames | we | we |ow | [amo [| ew [| wo [| ves | [sso | wwe | we | we | cawon | 0| we | we | [een [|smo | wo [| ws| |amswen| ammo |ow | we | PIA? Page 4701262 204 Columbia PAY PR. Quantitative Peak Review Tw =TM Io A Ih A TI hx A PrCintedr: 14vei0t2h/Aa2n0a1l0tys6:t4Re1e:0b0dePMr PFC 20ppb ICV om - ho cB4a1se3Pl0i1Fn1Oe6Ac910Mi0sased | 41137C.-0P3F72O0A0a Baseline oMissed | 463P0F4N1A9T0 0a oBaseinecMissed | 4616.30C4P23F.N0ADa Baseline o Missed i= io A i: i= 495P.0R/O80S.0T Da 1530C3-0P/F8G0S00 513P.0F4D6A901 Da 511530C4-7P0F0OADa ca aseinec Missed | oBase einescMssed | cBasoeineocsMssed | oBiasleigneaceMissed :iC 5= hilc pr CL CL 563P0E1U5R1A901 Da 15635C.-02P7F0U.0RA0a 599F.O08S001 0a CBsseline c Missed | oBaseinecMissed | oBaseinecMissed | bla pag -- clam 2 SE =3i zl 50133.G0-8P0F0GSDa Baseline o Missed ban pep --3 i4 i: i2 5P13F01O5A6910 0a 61153.0C/-1P6F8B.00A0a 563.P0F61T9A.T Da Baseline cMissed | oBaselnec Missed | oBaselne Missed | SI 7T zl 511530C1-1P6F9D0oADa Baselineo Missed 713P.F0T6e6A9.10 0a 611530C-/P1F6D90.0A0a Baseline c Missed| o Baseline c Missed 0 Before O After Pa48gof2e62 295 5 Gomis AnalyticalServices PrCinrleead.ted14w1it0h22A0n1a0ly68:4B1l:p0o0rtPeIr lon Ratio Confirmation Eo:om. CR |N- 17 | "PFC 20ppb ICV l= \ LoF fT = a CGa1s3eP0lF3nOe5Ac.2lis0s8ed | Ba4se3l0Pi2nFe1NA020Mi0s0sed | B4as0e5lP,iRn0Oe9So52M.i0s0sed | B5a1s3e0Pli2Fn8e0D.o2AMi0sased = Wiong Peak Wrong Peak Wiong Peak Wrong Peak 0 I] 1 i + alts bd2 ozpt 4 E 3 " ipzo) 4| H=f : CB5as6e3Pi0En2Ue6To9AM02i0saeed | Bas5e0l9Pi0Fne5DS0o20M0i0sed | Ba6s1e3lP0iF1nD1eO6oA00M2i0sased | 0 B6a6se3Pl.Fin0Te1IA629Mi0.s0ased = = Wrong Peak = Wong Peak Wong Penk = Wrong Pea [4 < B7a1se3Pl0Fin1Te8e25A20Mi0s8sed Wrong Peak O Before OJAfter Page 4301262 296 | SAnoallytuicmal Services AInntaelrynatle SNtaanmdea:rd: P1F3CB-AP1FBA DAcaqtuaisFiiteion Date Acquisition Method C2/B9T/2O01C0a3S:0H6o:4n2 AwiMt PFCkinetexShort am RAelsguolrtitThamblUesed Instrument Name Project Ewan'sProjects PFCs Regression Equation: 0.x1+00.006604 (c=0.8986) PrGinrteead:ted15w/i0t2h/A2n0a1l0ys2tp:.3R42e:1p0o0rtPeMr CI2nt0e8l1i0QuSaanmplesSTonedi ab API 5000 [e Cos o Tv 5 [eo 10 0 J| " A4 1iJ i| ]| A [ + TT e ow T |e e er [ T N| aN N s [|Nnnan ] TO ies sm e [wewres [s NaNaw [N[nNN] r [w e e Te w ae m [1 NaNnN Nn [NN [w | iw] NaN NaN rdrd rd ~rd Pe_ prs |1 ~~ ET 4 F er5, use Page 1.01 245 207 | [Golmbia AnalyticalServices" PiCnreesa:tes18i0tn32A0n7a0if2i3i4e0p0orer Anaarley:tSNaamne:t pTroerea1ro AScqeuisiitonpate 2E2T01O0 C506S.42Ah Acauiiton Method PFkneexShdoarm L Aoorthym Used iT noticuan e Instrument Name AP15000 Project Ewan' Projects\PFCs Regression Equation eoconciynty [ro-v0e0s|x980.c50u2e cr=Fhi0ie5a0cn7l8)myy | #2 | oo | wor] Co os | Co +Tow m wTmw wNean [Nhan s1 T [e sm w wneew [anna [wo= 1 Tem Tis [wN s aI T n hw] 50 1 48.83 98 NaN 1 NaN 3 pe il 7 {3 _~~ il ~~ LPiii il _ | rr ET ste [ 298 5 Glmen AnalyticalServices pCrreeated15wi0t3h2A0n7a0ly3s.t3f4bo0r0tear AavratrytSNaamnea:a SAAceiqqauuiissttiioonn Haettenod Project Regression Equation: pTroosps 2P0F2TC0OH1n0Cs3e0x8S.h4o2rAdMam Eas ProRORPFCS onRsuoemernetUNsaemde C ntalioEuan SS Apt 5000 =-0.00191 x*2 + Wn 0.354 x + -0.00625(r = 0.9989) / = oTmw] [ E T s ew s FS --e ETee e = eNee ] a ] { = 3y --ral= i2 ~_ 13 ~~ ii ] pe ]"! _ >W 7 a EI"Tot Pagesor2s 299 5AnahlymtbiciaalServices- Created with Analypst26Reporter Printed: 1510212010 2:34.60Pt AinntaelrynatleSNtaamneda:rd aActquaisriition Date PArcoqjueicstition Method Regression Equation: TPCR-APF1HA T219B12T01C0a3:B08:o42 AM EPvFaCnk'sinPerotjeexcSihscPoaFrCmts ARlegsuolrtitThamblUesed GIt2e0lBiTQGuSaanmPIeshoned ab Instrument Name. ~~ API 5000 =-0.000377 x*2 +0.108 x + 0.00572(r = 0.9988) 7 Lo 7 +[ow es] TT] 045 101 [oT] Tost Lm 185 { 50 roses [wr ss oT [ioe [os Ten NN |nw | NN| Nn NN Nan | NaN Ra Nan] 4 7 : 7 iil _-- IE i3 Pepd i il ~~ i | | iy{ o P rd > pd me Fa este Page dof 245 300 fq cohmbia AnalyticalServices" PrCereda.ted15w1it0h22A0na1l0ys3P.r3A4b0o0rPtMer Aentalaylte Satmaned:ard AcSaauaistiitonDate PArcoqjueicsttionMethod Regression Equation: PTraHpcah1 a 2S1H4E20T1O0CH30S6T4O2TATM PEEuCaKniPnroeeecxsSPdhFaoCmrs RAoeosrathlmeUssed CnAt0eRliGQuSanAS Sona InstrumentName API 5000 1 050.005 2+ 0.x0+03002820 c= 088)! Tor os C [Cw s= [sw oesm om weoer[men | wwena Tw wen |wn 7% 1 esmm |e we | | Nnaa n|] wNwV Teme en | he ees [ig [Na NaN | wy | ol "| ! | iiedJ A oJt4 ElJld e PeP 7 _ pd rd 7 rd re rd ~~ AAgf 7 usm Page 801245 301 LColu umbiaservices CrweithAanatps2Re6epordter Printed: 15/02/20120:34:00 PM `IAnntaemlaylteSNtaanmdea:rd AcTqautiasition Date PArcoqjueicstition Method Regression Equation PTFHexoS 1r 2T1E32E0T10O3C.a05S.4o2 AiMT PEvFaGni'snePrtojoexctSshPoFdrCatsm AlRgeorsiatThambUiesed Instrument Name = 000158 2+ 0.335 x + 0.0261 (r= 0.0989) TIntelEiquanESE AP1 5000 os TT T T r ee a eT w ww e T e T e aewe e CsT sm T when i [ve% = T 7 -- e I ECT hNan awNan i| _-- -- LS k 7 sd- ~~ iio )Ps- J rd i E) r Cu7ste Pagore24s5 302 -- LS Rouservices: re. Greated with AnalysPfporter a bPuentts a CCEamiocramsroirnanno nam tame e350 peor 1fumgnovoe [om] ["SAcaqmupisiietifoanmDeate [|26/6/2010 3:06.42 AM Acquisition Method| PFCkinetexShor dam TimSeamcptloenTvypoewme [5] DiwtionFactor [100 | Results Summary [Rm we[ame|Ry|snares [Gell [wot o Jomea0n| [wm = Jomem| 0 [wn| w [rpraesri [w[ ormsr ||0m 0 JsJa momeumm|| owm | wa twoo pact [w|o0romoos| Cd ssmorrrosn || woowrenn|| 00 [ oweno0 wa|swa]| wCl wb 2 [aandz par orze 303 rr AnalyticalServices tery RCSummary r[orirr [ianmosn||n owo | o=Ewgene |eg | [[rroas s TLoommaemm| [|owe ||w oemmeomm|| e] rroos: oommeenn||omw||evem[oomen||vv]] [ser Tomo |ow[ow | | 304 Columba RCorreawteidrwiitbh eAntarlyoiAtcpioredr SR cervicas oo Quantitative Peak Review 1B =o=l i=Troms E i=7ShUR REihA | fohT iliI 7TFLozS| ad\opi :SJ pRraE, | C i aTac re inA | E E mi[ R oiaoIs E | "ciST inech.i 33 Wi1tla | NEzl 3Cl Ll ' Lewsthin| ] tomar owenrg|E ee a, Mem E coiT n rere Janome|mentor |1 imeem |oes omased i ih 1 hs Lf ddibdad Tlie. i= I ol J 3 E=A aha 2- To Wl : Dlpthabi ts | rad sod born Daa asnPrheHgatATgte|EIAcTOSeNiT0L, ||| cosmptmeseatnnts| coi "esiamoersmsases To Boh kl 1 ho FE kd TE A i oi rh Tw il hue ELI a aay ad i Muda Haor, veeht | Sseovar nmaype Baseline Missed Baseline Missed | oBaseline o Missed Baseline Missed 0 Before O After ---- 305 LS CSoluB mbiaservices Created with Analyps.t30Reporter Printed: 15/02/20102:34:00PM lon Ratio Confirmation ol J ES N pm|i BB 1B 3 = i}Setehabion|i 2130P/F1E6A9200a oBaseline c Missed | 263P0F1P2o19A02 Da oBaselinec Missed | 209.0P1r9e8s.0?0a co Baseline o Missed | 313P0H11A902 08 Baseline o Missed Wong Peak Wrong Peak Wrong Peak Wrong Peak == f m 5= Ir 7 igSA EA =i: MmE E 5opts 363P,0E/H31R8A.Z0 0a oBasinecMissed | 399P.0F19H9S.02Da oBaselineoMissed | 5S1_5130C4P7FD0DA0a oBaselinecMissed | NA Baselinec Missed Wrong Peak Wrong Peak Wong Peak NB PFBA and PFPeA do nol have quaiying on ansiions Wrong Peak O Before 0 After Page 1201245 306 5 Golmbia Analytical Services PrCedr1vei5th1Aan0al0ty22pR3e3e40p.1o01r0dPt0eUr DaPArctoqajueFicistlteion ethod_ Ecp2Ev0Ca8nn1es0tCPeaxlesSahhooOrrPt.FidCam ARIlengssoutrlrilutmTheamnbtUlesNeadme__OAI2Pn0!lB5iO0u0aS0nesShoe a [SampleName "SAcaqumispitlioensMethod [|TP2PtrF0cC1Okc0iTn3oew3pl5e7xsS2hdAozratmssn[i[nijnS[ojeaecDmctpvtiilioeooonnTnvyuVipoerelmrumee {[ 5 Senders|| [too | [Sample Comment _|_____[Weght Joo | Results Summary [oRormaens | rasaarny||tmoooenrone| a[mvmseo|sm[FsR | o|GwET || mamiss||"er || vwoe | prruosn1 ||ssszisam|| ctorpeas| sve| moa |e |o |_m|| om ww | | sw | wn | we | [oa prime [onszn| scrrma [sso| |saves| ores| mm| ws |ow |om| ss| wm |aw | om |w | wo ho | sSsIo | sses| rceroa | awe| sem | 10 |I tos | 18 | no SSiSs Tanqan | nceron | wom| meow | 100 | te | 100 | no 4,0W ZSes]t Page 1301 245 307 4ACnoallyutmibciaalServices wren | i | | IRC Summary Printed: 15/02/2010 2:34:00 PM | EE 308 5AnGaolyltaimcbaila Services Created with Analyspt3R3eporter Printed: 1510212010 2:34:00 PM Quantitative Peak Review po 7 pr} 53 ho: I : 33 + eB] oB2a1s3e.Pl0nF1eB69Ao.M10is0saed| oB2as11e73l0iC1n-7oPoF2MB0iA0s0sed PFC 0.10ppb | = El |d : zl 3 = fox I || oBa2s6e3Pl0EinP2eE1oR9M10i0s8sed | oB3a113s5C-o0P2olF1HMiXi0As0n0aseod iLaZl 3 i3 = If. = i e | r] S 3 ele] e (IYeSPe A 299p.0r/e80s.0 0a 40w3o01p0i3n0s00 cBaseineoMissed | cBaselnecMissed ||| 312P0E26A90108 311530C2-7p0F0TA0a oBaselnec Missed | oBasooMiisnseed = a5 eng =i Tee E Al El = i=2 i=f = I~ i3 3 d kg oB5a6s3eP0lF/nH1e6Do9A.M10is0saed | oB3a11s35eC0l-n2Po7Fc0F0xMAi0s0sed ||| oBa3s9Pl5Ri0Hn2Xe0Si01M0i8ssed | oB4a0s13e80i01n-1oP0F3H0MSi0sased ty a 5 ace | ounces iy I: zl tz 2 I: = |4 a - S_180-FFHS 13C-PFDA S_13C.PFDA 13C-PFOA oB4a0s3e.i0/n1e03M.i0sDsaed | Ba5s15e.l0i/n4e7c0M.0isDsaed |i B5a15s.0e/47lc0.Mi0isDnsaeed | oB5a1s5e.i0/n4e70o.M0iDssaed O Before O After Page 1501 265 309 LSAnalyAtical Services- prCreated ASS with Analyt Bbdpoortner Ton Ratio Confirmation |-l izl = %i wzl dew PFC 0.10ppb. = o[l|SE A r==z o 213.P0F1E69A.Z0 0a Baseline Missed | oB2s6s3eP0iFn2Pe1ec9A02Mi0sased | oBe2s0epl9ir,n0ee9s9?.M0as0sed | T Wr rong Peak = Wrong Peak i = Wiong Peak E { [a pt -r Rem - TT = = 26P30r71a902 0a 3p05r.0i19s9.2Da 5S1s 5.10347C0F.F0o0A8 BasVeilrionnegoPMeiasksed BWasreloinnegPMeiasksed BasWeilionnegPMeiasksed NB PFBA and PFPeA da not Fave quafying on Fransions. oBa3s1e3Pli0Fn1He1oI82A0Mi0s8sed Wrong Peak Thimage 0date ne NA BaWserloinnegoPMeiasksed O Before OJ After Page 16 of 245 310 4 Solumbia AnalyticalServices Created with AnalySpi.3Re5porter Printed: 15/02/2010 2:34:00 PM PDraotjaeFcitle Evan's ProjecisPFCs 020810Calshortwif AcquisitionMethod __PFCKinetexShortdam Result Table 0206108amplesShoredi rah AIlngsotrriutmhemntNUsaemde __AIPnIte5l0lQ0u0an AScaqmupislietiNoanmDeate | 2P9F1C7001.50p3pD4457 AY [injEectTionVAial [-- 3 | [AcSquiasimtiopnMletehoid_o||TPcFwCiKszin5e0texShodarml [[DSialmuptiloenTFaycptear [|S_ 1t0a0ndas | SampleComment |__ Weigh| ttoVolume | 0.00 Results Summary |[Nnaaimyeie |AnEaxipyeiceteRdT) TnAarieyaie || Ex(npgCiambn)c ||Cal(cngiCmo)ne| Accu(%r)acy| moar Pres1 | 4zsazs| 180.pFHs| zero| sos|o 0s | Prat| sateon| cer|saam| memo | oso | PRHPA1 | 6.2 |134C-P6 FHNA2|40 5542)00| tooo |oso| PRHXS1 | 633630| 180PFHS | 208|741320700| 050 | S190 | 'eas@a|n 13cproA sc wero | 100 | oss | 9 | Ne was | mm | wo| ost |10 | N1 o| 04s | No 103 0 | wo| At A 1Gte Pa17gof2e65 311 2ACnoallyutmibciaalServices IRC Summary Created with Anaiy Mporter Printed: 15/02/2010 2:34:00 PM oT 312 8 SAnoatluymtibclaal Services- p37 PriCnrteead:ted15w0it2h1A2n0a1l0y2st3R4e.p0o0rtPeMr Quantitative Peak Review PFC 0.5ppb = Ed 77 Fl = sv L A3 Le 380 = al ig iy | Ir debe) CB A A 2130/P1F6B9A.T0 Da 211730C1-7PF2B0A08 | 263.P0E2P19E.10a 31135C0-2PF7H0DA0a Baseilinneg Missed 3Baseliannego Missed | 7c Baseliannegce;Missed o Blasieline Missed. E: l i=5 = Fe 208P.r0a60sT0 Da 40138001-0P3F.H0S0a ccBoasneingecMigrsased | poBae seintecMssed :i E=l 1 gee] 2 313P.0F1H26A9|0 Da 311530C1-2P7F0H0XADa a | cE BaselinecMissed | i oc Baseine o Missed i! = box = i= i - = iz wl 3 PFHpA1 13C-PFHXA PFHGS 1 180-PFHS -oB3a63s.e0l/i1n6ea9og.Me0iDsased | o3B1a5s.e0i/v2n7eo0c.z0MDisased || 7oBa3s9e9l.z0i/ng8e0c.0MDiapeas.sed | Ba4sW0ea3li.nn0eg11o202M3aiD.sa0sed 3 oo aE 9g tiAti 2 A a i" 3 A rf=d A 4s0_31.08100.37.F0H0Sa Baseline oMissed | 5115C0P47F0B0A00 || oBaselneoMissed | 5s115a0c4A70r0o0R8 cBaseinecMissed | 511530C4P7F0O0ADa BaselcMiisnseed 0 Before O After Page 190f 245 313 8 ASnoatluymtibciaal Services" p38 PriCnrteead:te1d5w/i0t2h/A2n0a1l0ys2t:3R4e:p0o0rtPeMr fon Ratio Confirmation Tm J [ISoe i=A ixi PFC 0.5ppb = = e- ee Lo [I -- = 7 1 | 213P0F/1E6A9200a Baseline c Missed | 263P0F2P1e8A02Da Baseline oMissed | oBa2s9Pe9.lF0iE1n9eS9o.20Mi0sased | 31P3F0H1IA12900a o Baseline Missed = Wrong Peak Wrong Peak Wiong Peak Wiong Peak b= Ho [i = Thieme 363P0R1H3A1A902 0a 399P,R01H9G9.S02Da 5S7_51.30C7P0F0O0Aa B=asWerlionnegoPMeiasksed BasWerlionnegoPMeiasksed BasWerlionnegoPeMaiks.sed NB. PFBA and PFPeA do not ave qualfying on transiions. 0 Before OJ After NA BasWelrionnegoPMeiasksed Page 2001245 314 L8Col0umb8ia services p.39 PrCinrteeadt:ed15w/i0t2h1A2n0a1l0ys2t:3R4e:p0o0rPteMr PDraotjaecFtile 0E2v0a8n1'0s1CParioSjheocrttswiPFCs AcquisitionMethod _PFChinetexShdoarmt ARlegsuolrtitThamblUesed n2t0e8l1i0u5aanmplesShonedi rb Instrument Name __ API5000 [SampleName PFC T0500 Acauisition Method | 2P/F8C/2k0i1n0s3t:5e4x:S20hdoAarMlm [Satmo ple cwiszasc [sampleComment| I [InSjaemcptlieonTVyopleume |[S5 tandars|| Dilution Factor [100 | [WeighttoVolume Joo | Results Summary [[nNaaimyeie || A(nEaxpleyctteeRdT) | 'SNe.me | tsaoa| AAnreass ||Ex(pngCiomln)e|| Ga(lnegCmol)ne|| Ace(uswrae|y| M9? PFBA1 | 12720| 13cpron [oso| areseo | too |tes| 105 | he PrPeat | 260050| 19cPrHa| dszset|n aso | 10 |11 | 10 0 | wo PFBS1 | 4261626| 180-PFHS | 2661400| 944580 | 1.00 103 103 Prat | 5316| racerma| samen| sss | 100 | aor Prioat | 823620| cern| mem| moan |reo| ow | | wor | we | wm | ne PFHS1 | 6326.32| 180.PFHS | 2661400| 92028|0 100 1.03 103 | No (ene [es261| 1acron | 2843300 [as|o1o00n| 10s 106 [No SPFiDoAw | Tess) | 13cpFOA | 2063300| 2843300 | 1.00 1.00 00 | No | AltESFered Pa21gof2e45 315 AColumbia AnalyticalServices wre IRC Summary rr rm Printed: 15/02/2010 2:34:00PM | EE Calculated s_icPrn maa| aww | w ws 316 5 Golam PrCrienaeted15w1i0t2h1A2n0a1l0ys2t:p3.R44e:1p0o0rPteAr AnalyticalServices" Err ---- esr rr ---- QuaTnTtitative Peak Revi=ew ga = PFC = 1.0ppu b Eig i+= bie i| - wl |- - oB2a1s2e.Pi0nr1sa6M9t.is0s8ed | cB2as7we0lc1ine7e2Ec0MAi0s8sed ||| oB2a6s3epi0rn2eee1cA9l0Mi0s8sed | oB3a1s1e53i0Cn.2eP7F0T0MBiA0sased | o | = io 3 He i! 3 I" oBo2s0e3Pi0nre8a0st0M0a8sed | 2oB4as0we3lo0np7ec0iM3is0s0sed P|| LoB3a1s3ep0len2e6ec9l0Mi0sased| zloB311a53s00.2eP7oF0lT0MoiiADsnaseed SER a li ios i i= fi 2 I: cB3a6s3Pe0i/Rn1Ae69oT0Ms0saed | =oB3a1s15e3l0Cn2Pe7cF0M0TiAs0s8ed ] | oBa3Ps9a8ri0n8e0o.M0i0s8sed | zl 401280100.37070a oBaseline Missed To gga LE iz iE 2 = cB4aS0s_3e10i8/n01e-0P3MF0iHs0S8sed| oB5a1s13e5Cl0-n4PecF7tO0iA0s0sed I3 i: 3 3 | oB5aSs5_e01i34nC7e-c0FM0FiOs0Asaed| oB51a153s0C4-e7Po0lF0OMiAiDsnaseed O Before O After Pa23.g2e45 37 5 Solumbia Analytical Services- Created with Analyps.t42Reporter Printed: 1510272010 2:34:00 PM Ton Ratio Confirmation FIoR BE Tm B iboEg = iF=e - i xl 213.0P1F6B9A.20 0a 263P0F1P2e1R902 Da BasWerloinnegoPMeiasksed | oBaseWlrionneg PMeiasksed - ET PFC 1.0ppb oT =oT jodeg = iz) a tein 269.P0r1e99s.?0 Da 31P3F0H/I1A1ZD8a0 | BasWerlionnegoPMeiasksed| o BasWeilionnegoPMeiasksed a i[bCl i aEsof wb jo 4 363P01H319A.2 0a 309P.0R/9I9S.02Da 5s1_51034c7F0r0o0A8 oBaseWlrionneg PMeiasksed | BaseWliionneg PMeiasksed | BasWeolinneg PMeiasksed | NB PFA and PFPeA do nol ave qualiying on ransiions. Tepe NA BasWerlionnegoPMeiasksed O Before O After Page 24 of 245 318 Columbia 4 Analytical Services PrCinrteead:ted15wi0t2h2A0n1al0y2:34.p0o0rtPeMr Propet Eras Precise Resa Table GEEOSamplesShoriedt dh ADcaqtuaisFiilteion Method 0_2P0F8C1K0i\nCeatleSxhoSrhto.rwtidfafm AInlsgtorruimtehnmtUNsaemde _I_nAPt1el5l0iQ0u0an [S`eAcmqpuriestiaonmDsa--teTP|e2c9/s201o0 4m0451 AM C njection VolumeE [5 -- ] [|SAacamupislieiodnWethodT--i|-- cPFwCrsizn[ eeiosxoShi or gamwi| So ample n FTaycpteor |Sanda [Sample Comment | weigmtovome Jom | LRnRiaemtsyeuilsts[|SpAunmillmyaiaeryRyY| stone [one [FFraFis |EExEp Cone[| Gnale yGore[a| tee prioat | gataan| Tacoma | sien Co [ow [ow[ow |e] vrs | assess| morris | sro| amon| sa | ser |w|r ne| SIS_180- sss| riceron| | maw | two T| am | wm | we| SS51530 Teese | cern|sa|mwwew| ww | wo | ww we 7 ust Pa25g0f 2e45 319 Columbia LE services IRC Summary AnalytePeak Name RT (Expected) PFaA2 1270.27) [prreaz| see | PrHraz 5316531) Created with Analypst44Reporter Printed: 15/022010 2:34:00 PM or rea | wots fCoaincRuantiieoa (Expected Value) 2230700 No |tee] 22800 | No 1.00 ws | Ne | eos | S_13C-PFBA S_13C-PFHAA 1271.28) 531630) 4014300 No 175 ew | no | rss | Pa26g0f2e45 320 8AnSaolymtbiciaelServices Created wih Analytp4Re5porter Printed: 15/02/210234.00 PM 7 Quantitative Peak TT Review PFC ow 5.0ppb il io fi i5 CLl2a1m3ioi0n1e6lo0t0i0o8sed | AcB2a1sa7oc0ir1n1ia7io2nm0s0se | | :oB2a6se3pi0rn5ee1os8Ns0i0s0ies | ot 3s1c5r0i7a0n00a oBaseline Missed li ie" Li ia b=t i 25 I Ll i=l I 3 | = -- oo2o6pi9rn0ee0s.Mi0i0saes | oB1a0co3i0nr7ec1t0fi3s0s0ed ||| Ba3se1l3pi0ne3e6wo8M0i0s8sed | Ba4s11e53l0ip4n7ec0A0Mi0sased i iz) iEf l iz o3a6s3A e0Pi/Rn1Ge6A8o]0Ni0saJ ed | oBA 3a1Tsa5lc0np5e7i0M0ni0sasedo | cBa5s9peA 0ie8nre0oc0Msbased | 4013s0051iR0Ais50.a Baseline Missed Rvs "i" |i "on = 2 I3 Zi Iz i i cl453a13s001e075M0as0sa s | co5m1eT5ia0nc4e.7op0FvD0iAs0saes | cB$osTs_E1oa0ic7nFe0r0oh0ins0sed | oBa5ss1ai5nc0e4p7Mii0Ds0ased 0 Before O After Page 2701245 321 8 ASnoalluymtibciaal Services p46 PrCinrteead:ted15w/i0t2h/A2n0a1l0ys2t:3R4e:p0o0rPteMr f--o_n-- Ratio Confirmation Tm [Iw I|id Sb il PFC 5.0ppb = = mh e5s sde =FEI 2130P/F1E6A9200a 2630P1F2P1e9A02 Da 209.0P1r9a9.s0?Da 313P0H11A90202 cBaseWlrionneg PMeiasksed | BasWerlionneg PMeiasksed | BaseWlionnegcPMeiasksed | oBasWerionnegoPMeiasksed i LE nl Ce-- i3 | If & i= Diopintoe 36P3F,0H13p1A9.02 Da 309P.0E/9H9.I0S2 Da 5s1_510a4c7F0r0DDAa NA oBaWserloinngecPMeiasksed | BaseWlrionnegcPMeiasksed | Bas=eWlrionnegcPMeiasksed | BaseWlrionnegoPMeiasksed NE PFA and PFPeA do nol ave quallying on ransiions. 0 Before OJ After Page 28 of 245 322 Columbia LS Soi services: PrCinrteead:ted15wi0t2h2A0n1al0ys2tp.3Ra4erp0o0rtPeMr DAaFcrtaouajieFsciitlteionMethod E_0P2vF0aC8ni1si0nCPeatleoSxhSoahroPrwtFicCfasm [SampleName `AcquistionMethod [|P2Pr0Fc9C2iK0o1i0pn4e:t1e3.x3s4 hdAMoa:rm [[SSaammpplleecdomment|| LCMS2-85E Results Summary f[Anralpyte r|r`oA[anaralyattleayRnT|[mnecemrean | w[owenw| [Porrpoesa1t || a swasao||sc moraeesz||rerrneaasm || ARlegsourlittThambUlseed TIZntTe0liSQauamnpiesShoRed db Instrument Name__AP15000 [i[nj[emcetScitoonnVa voalrumme [[p [S65anida etype||| [DiWleuitigohntFtaocVtoourmeJ[o70o0 || s[R0m0 |Ex[opCGoooTnc|||Calcw.howComnc|. wm | vwe sm| woo |we| te | te seven| mmo |wm| wor | to [print| sazeas| vicrrwen| sama | wrioo| 1000 | tos | 09 | te | Pris1| s260n| topes | zee| seo| wm | tos | 1 | [SSa7s8o0: [estean| 1sceron [aos7amo|aer|e1s000| 103 | 103 | to 1 SS3Ec- | Tasaan| woeron | seen| seme| te | tw | w0 | Ww Al!ih "J7u,st Page20.01 245 323 SEPAS Columbia AnalyticalServices: IRC Summary rans wa | www | we Printed: 15/02/20120:34:00PM = s core Ser mam | wm | no | swe |wwe| we os on 324 3 Solum AnalyticalServices- Ee eofemeeee Tw Quantitative Peak oT Review =3 x =3 i: 3 2 2130e1r18o8k.i Ds 2rwooieafa0n0a cBusine omnes| oBmaineoised consrso ti Printed 1510212010 234.00PU ------ ere Lz= = ii a= Trreremeemre PFC 1o0ppg b a EH i== ||| 23p0e2e1e9k0d08 5"15a0c2p7i00a oSaseinecbisses| oBselnesMissed Lo |o I =i ul i 3 presT 180-PFHS cb29a9.m0/o80t.0icDaes | otic 403.0/103.0Da I3 = zl ol ji zl | PHA 1 13C-PFHXA |1 co31m3e.0m/2e6c9.l0Diaes | oS3a1s5.i0n/e2c7l0D.i0ase ic5l i==f {=2| iE :g PrHgA A 1 EA 130.pFA 3630/1600 0a 3150270008 Die pres 1A 2050200 0a 15A 0.97 40301103. Da "coiasninge ovzieanses | coaelnec Missed | oBaseinuer Missed | oBaseingeo dMissed i. : =HE =EE |i:= = oso Fis 4030110300 3 Toon || i sscsion 5150470008 515047000a = ach 5150470D0a cssains ovnead | oBaselnoo Missed | cBaseineoMissed | oBaseineo Missed 0 Before O After Page at of 245 325 LCS olumbia services .50 PriCnrteead:ted1w5i/t0h27A2n0a1l0ys2t:3R4e:p0o0rPtMer f--on_R--at--io Confirmation Tw Em icgij | If3 e| PFC 10ppb 5 q H| Im S e NE EI 2130P/F1B6A9200a oBaselineoMissed | 263.P0F12P1e9A.020a BaselinecMissed | 269.P0r9E5S.02 Da oBaselineoMissed | 31P30H/1A219D0a Baseline Missed o Wrong Peak Ts Wong Peak Wrong Peak rr Wrong Peak - El 2 Io I= II i Toibgesniselte wl aL ad 3P63F0/H3A1920 Da 399P.F0H99I.S02 Da 5s_1135C P04F7D00A0 NA oBasWerloinngeoPMeiasksed | Ba WsroenglcPiMeianskseed | Ba WsroenglcPMieiasnkseed | BaWsroengloPMieiasnkseed NB. PFBA and PFPeA do nel ave qualifying lon Tansiions. O Before OJ After Pa32gof2e45 36 LCT olumR biaservices PriCnrteeadt:ed15w0it2h12A0na1l0ys2t.p35R4e10p0orPteMr DaBArctoqjaueiFcsitilteion Method Ea_2vP0aF8nC1'i0sn\tCPearxoiSjSehhcootrrsttPFidfCafsm AlRgeosruiltthTmabUlseed instrument Name DI2nt0e8lTi0cuSaanmplesShoned db __AP1 5000 [A`cSAqacuqmiupsilsieittiNiooannmbMeaettehod _||2PP6FF7CC2K02i100n0e040l2e5x0S5hAdoarrl |InijnejcetctiioonnVVioallume |S Sampie Type Standard S[amSplaemCopmmlente| d[[LOWMs2e:85FigmttovDiloutiomn Famctore_ [0[ 00 100]| TTReamsttualts||SuAfnmalmlyataeryRyT| proat | rasan| sncaormees| s[smaeno|[wAwReE|[m EiTnREcono e|| Cawlo emmcnoc||| esmn s||| ehro pr PPFrPoesAt1 || 3s5a90s.6s0|| 1m3oCPrFeHxsA|| aarorses|| mwoorarmneoo0 || 0m0o0o || t1sa0m0 ||ss ||: nNoo|| PFHXA1 | 5.30(5.31)| 13C-P|F47H958x00A| 838520|0 20.00 18.60 8 | No rr |esos| worms | | von|aso|wa| | | Sr | sstea|n raoeroa| ssteos | asso | too | ose | se | mo | SPFsOeA. 7.66(7.65) || 13C-PFDA | 3316000| 3316000 1.00 1.00 No Alt EctA e Page3301 265 327 LT AnalyticalServices" JEIRC Summary Tor|awrn | | rap i | EEE Calculated 328 3 Amnaliytiacal Services" Quantitative Peak I==7 7 I po , Er cl B2a1se3Py l0En1eB6A9ofM01iDsased bo BE 209p0r6e0sT0 Da Baseline Missed. |= e =ol Review 3FI Eg i3 7Fe | oB2as11e73l0iC1n-7ePo2FMB0iA0s8sed wang tx 40o30p71i03s002 c Baseline o Missed 7$ -i PrCinrteead:ted15w/it0h22An0a1l0y2s:tp354R:e3p0o0rPteMr | |~TE iro PFC 20ppb =27 5 | E wh ul | | oBa2s6e3Pl0Fi1Pn2ee1oA80|MiDsased | c B3a1s15e3l0Ci1n-2eP70F0hMiADsased ong pen - a Beak = = || 313P0E2R6G901 Da | Baseline Missed T = E msai (= = 311530C2PF7I0A08 Baseline o Missed z7 og =5 oB3a6s3eP0iF/nH1eO6oA9M01isDsaed | oB31as13e5Cl0-n2Pe1oF0MH0iA0ss8ed tong pea ng i-:z -= ||I Bas3ePl.iF0ne8E0M1i0s0sed | oB40a1380s01-e0Po2lFM0HiiSDsnsaeed ! gy 3 buon ea i| I= | = cB4as0s3_o.0it/n1se03oc.r0Mis0sased | oB5a1ss5e0le4np7e0ci.Mai0s0saed | | oB5as1sa5iu0n4ce7ch0Mi0iosDnsaed | 51T50a4c70i0tDa Baseline c Missed 0 Before O After Page 35 of 245 329 8 ASnoalluymtibciaal Services* p54 PrCinrteead:ted15w/i0t2h/A2n0a1l0ys2:t3R4e:p0o0rPteMr fon Ratio Confirmation TE | i=E i| H-- iL - 2130/P1F6E9A.20Da 263P01F2P1e9A02Da uBaseWlrionnegoPMeiasksed | o BasWerlionneg PMeiasksed =] tu ET 0 Fl PFC 20ppb J ] ok fj ete fe y ee 290.P0F1E99S.20 Da 313P0R1H11I92A008 | o BasWerlionnegoPMeiasksed | BaseWliionnegoPMeiasksed | To = Titpondade 363P0F/H3p19A02 Da 399P.F0/H9I9.S02Da 5S1_5.1034C70F0D0Aa GBaseWlrionnegoPMeiasksed | oBasWerloinnegcPMeiasksed | o BasWerlionnegcPMeiasksed | NB. PFBA and PFPeA do not have qualifying ion transitions. 0 Before OJ After NA BasWerlionnegoPMeiasksed Page 36 of 245 330 LSAnalytical Services- PriCnrteead:ted15w0it2h1A2n01a0ly2f:34:p0o0rtPeAr DaPrtojaeFcitle oEza08r1s0CPaoisRhcoirStPwRiCfS Acauisition Method _PFCkinelexShdoarmt AlRgeosurlittThambUlseed CIantOeli0GSuaanmpiesShoredi db Instrument Name__API 5000 [SAacmqupilsetNioanmDeate |7[9PF2C05100pp4b.3247A | nInjjeecctiioonnVVioallume [5 1| [SAacmqpulisetlioonWethod ||PLoFwsCz50Kndeamtex|sDSaimhspoloneTFyrapceior _[100____| [Sample Comment |__| Weignovome Joo | Results Summary F Abnraaiyntte ||F AtnaiayireRaT|EceEra|EssNe|zomTArwnailioyoime ||ExspCoomnc|| Cailscl.eCslone||lAeccwuoracy| ] Proont | sven | ceria|arsuioo| amwiono| sum | samo | ss |wo| prost | azsaz| opens |aereioo|se|rsaain |esos re| tor | fo | Prva1 | sass | score |aso| zaviom | som | sos | 01 | print | eases| scermaa| rsaioo| soon| som |soar| tor | na | Prins1| saz|emoapns| aereioo| ar|esaevs| sm | wz | wo| S550" [eaa@a|n 1aceron | szstow| zo7t00 | 100 053 sS1S3: [var|aT noeron |sree| seo | am | 100 ws | No| 440 CSLiusFte Pa37ogf2e45 331 J LS CSoluombita erices- Printed: 15/02/2010 2:34:00 PM wren IRC Summary oo | om |||T Calculated Prinnz s ricrmna |smem| awe | ast CE I aI 332 LS EColEumbRiaservices Created with Analystp5Re7porter Printed: 1510212010 2:34:00PM 3 hz = Quantitative Peak Review = T= J7 Fa PFC 50ppb =F ST io = ;J 3 a.1 bii |[| 3= PFBAT 13C-PFBA i PFPeA1 13C-PFHXA ettBa2s1e3l.i0n/1e69M.i0sDsaed | pegs Ba2s1e7l.i0/n1e72.0MiDsased |i oBa26s3e.l0i/n21e9o.M0iDssaed | B3a1s5e.l0i/n2e7o0.0MiDsased tiny tz7 iz3 [i i" oBa2s0c5p,i0rn/ee3s0hT.M0iDsased | oB4a1s08e30l0i-1nP0eFc3HM0iS0s0sed ||| Ba3s1el3Pi0nH2e6Ao9M10i0sased | B3a1s1e53lC0i-2neP7cF0H0MXiA0sased oy okay = ae eet resets Fo = b= x ! A i JA A Is A = oB3a6s3eP,l0r1nH1eO69Ao.0M|iDsased | oBa31sn5e.el0iP1n2ef1c0iM0iADsased | | oBa3s9eP9l.ir0n8ei0c0M1i0sased | 4031.8001-1p0F3i.0isDa Baselineo Missed a - rp ene sli | zl - L] hzi o;o Ie2 "e4l Ba4sS0e_3l10i81n01e-0P3MF0iHs0Ssaed | cB5as11e53l0Cn4-e7PoF0MO0iA0ss0ed || Bas5_e11l5i30nCe4-7F0MF0iD0sAs8ed | B5a11s53.Ce0-l4PoF7iMO0iA0.ns0saeed 0 Before O After Pa39g012e65 333 / SAnoalluymtibciaal Services p.58 PriCnrteead:te1d5w/i0t2h/A2n0a1l0ys2:t3R4e:p0o0rPteMr f--o_n--Ratio Confirmation LoPR Tm ==]7 i- a J| o i uw PFC 50ppb dedpm =r - J "Sgr 2130P/F1E6A920 0a cBaselinoc Missed | 2630PF2P1e9A020a Baselines Missed | 209.0P1F9E9S.02 0a oBaselinec Missed | 31P3F.H0GA12800a oBaseline o Missed Wrong Peak Wrong Peak Wrong Peak Wrong Peak | [i-- = sa | 7 = of T fo idI Ix3 I~po Topsite 363P0F3H1P9A.02 0a 399P.0H99S.02Da cBaseline 0 Missed| oBaseline o Missed | 5S15_.103/4C7P0.F0DDAa co Baseline o Missed | NB. Wrong Peak PFBA and PFPeA 00 nol Wrong Peak have qualying on ransiions. 5 Wrong Peak O Before O After NA Baselineo Missed Wrong Peak Page 40 of 245 334 8AnGalluytmibciaal Services" p.59 PrCinrteeadt:ed15w/i0th22An0a1l0ys2t:3R4e:p0o0rPteMr DPraotjaeFcitle Acquisition Method 0_EP2vF0aC8nK'1is0nCePartloeSjxehScohtrostrPwdFiaCfsm ARlegsourlittThamblUesed Cn2t0e8liTu0aSnampiesShoedi id Instrument Name __ API 5000 Fo Te a [rw [Sample Name Acquisition Method _| PP27FF2CC0kz1io0npeg5bl0ei1xc2Sv5hdoAarMlm [[SSaammpplleeComment| | LCMS277) ITT -- [SamOplei Typi e t[i1`Q0ou0alnConFtrolactor| weighttoVolume ooo | Results Summary TT (Expected Ares | ingiml) | (ogiml) | (a) PFBA1 | 1.27.27)| 13C-PFBA s2600 | 2000 | 2130 | 106 | No [Preeat | aston|13cP|r4Hssnssoao| sestso0 | 00 | 230 | 112 Ne PFBS1 | 427426) | 180-PFHS| 2648500| 17751000| 2000 | 2140 | 107 | No | PRHxA1 | 5.92831) | 13CPFHAA | 4533300| s368200| 2000| 2080| 103| No | PRHpA1 | 6206.2) 00 | 240 | 107 | Ne | PFHxS1 Shue ||s 6.34(a 6.32) ||s1a8c0s -ePoFHnSa ||s2a6n 4a85n00|| 16240000 zeasson | | 2000 100 | | 20.90 ose 104 [i 6 | No SC Tagen| rorron | sim| swe | tm | tm | io | mw +of E2Z1 qe Pa45ogf2e05 335 J AnalyticalServices- [immer IRC Summary rronz rrrenz |wmreonm)||me|m |vwer|| ovef| ser | som [rots Scere srcrman [mem | owen| we[ve] Taam ww seem | mw | ow | we | 336 4ACnoalluytmibciaalServicesTM Created wit Analystp.R61arer Printed: 15/02/2010 2:34:00PM =m Quantitative Peak TT Review = 5 PFC 320ppb =ICV | |f L| = | wl1 ix2 I! il= Pra] 13cPERA PEPOAT 130.pFTon Ba2s1e3l.i0n/1e69o.M0iDseaed | oBa2s17e.l0i1n1e7c2l.M0iDsased || cB2a6s3a.0i/n2e19c.0MiDsased | oBa3s15e.l0i/n2e70.0MiDsased i ai.z : i= =t= o2a6s3e.iP0rna8es0s0h0iaed | oB4a0s13e80l01n0-e5o5.M7i0Ss0saed | cB3a1s3eP0lRn2e6Ac0T0Mi0sased | B13a31seC5l.0i2nPe7F0T0MDisased i=o " PrHoAT oS36l3a.i0s/a16en9a.Ml0aisnDsaeed 3ig zl 4s8_3108/01.05370HDsa Baie oMesed =3 | cefiea | oB3a1s5e.i0l/no2e7c0M.0isDsaed E 3 | Ba5se1P l5i0n4e7r0o0liDsased =J XiE : = = | pewSt 1807S || lBas3e9le 9i.0n/e8e 0c.M0sDsaed | B4a03s.l0e1i1g0lo3.iM0iDnsaseed El id3 | S15.04700 0a Ef 51153.0P4F7OA0D0a | cBasalnecMissed| oBaseine Missed 0 Before O After Pa47gof2e45 337 8 SAnoalluymtibciaal Services p.62 PriCnrteead:ted15w0it2h12An0a1l0ys2t:3R4e.p0o0rPteMr -- Ton Ratio Confirmation -- PFC 2e 0ppb ICV iTm il bd LeJ [=1 ih 4 e - g wl ee 2130P/F1E6A920 Da cBaseline oMissed | 2630PF2P1e9A02Da Baseline o Missed | 209.0P1F9E9.S02 0a Baseline Missed | 31P3F0H/G1A120D0a oBaseine o Missed Wrong Peak Wrong Peak Wong Peak Wrong Peak ea] -- Lio D| eh : i| EE T -- Diop edit 363.P0F3H1P9A.020a 399P.01F90S.020a 51s5_01437CF0F0OADa NA } BaseWlrionnegoPMeiasksed | BaseWlrionnegoPMeiasksed | BaseWlrionnegcPMeiasksed | BasWelrionnegoPMeiasksed NB. PFBA and PFPeA do not have qualfying on transfions. O Before O After Page 48 of 245 338 Columbia a Analytical Services AInntaelryatle SNtaamne:ce TPRaOcAP1FOA AcDquaisriitionDate APrcoqjueicstitionMethod S 2/17/T 2010 6O:30:13 PM PEvFaCn'KsiPnroljeecxtsLPodFnaCgms PrCnrleeadt.ed18w/it0h2A2n0a1l0y3t:24.b2o0rPteMr RAelsgourlittThamblUesed E nteiR CuanE Instrument Name AP15000 econ iam| ope Regression Equation: = 0.0508 x + -0.00148 (r = 0.9989)" on oo ewe [os1 |nT EE e0a95m8 I 05 Ti T0158 TC ws ETeLar]s J i | Sh| 5e 0 | nor | a he [ww [Tes% || NaN New | NaN NaN | ow e wNan aNavn owr hanna |h] haanv / , _ | _ | 7 | 1 rd iind bl ~~ _ ;J" __wd iaq ~~ oo 1 An pt Luge Page 101170 339 8Anmalyiticaal Services- PrGirmeeda:tea18wi0t2h2A0n1a0l3.2e4p0o3rtPelr AInnatelrymtaelSNtaamneda:ra AacqauisFiiteion Date Acquisition Method Project Regression Equation: TPEaNcAPE1NA 2T1E77T2I0O1C0A8L3o0n-g13WiPtM PFCnetexLodanmg Ewan's Projects\PFCs RAlegsoraitThammUesed Instrument Name = 0.1+0.0000971 (e=a0n.8978) / EInteTicuTan ab API 5000 --0T5 7[.os C Wo T wT bwol iF]i | [TEoes]s Tes we EE NNaNN ||vNaann|| TI meeeee TTweheaee n 2 | ha an] / . -- __ _7 ii _-re }: os || rd X:f re aZF 2s! Page201 170 340 Lo Columbia services: Created with AnalysPREorter Printed: 18/02/2010 3:24:00 PM Aenarlyate SNtaamneda:rd ASqauiasritiion Date APrcoqjueicsttion Method pTriodssr1 os 2E117O2010C6303 PM PEFuCaKni'nePtreotsonOgPdEaCmS RRigeoristhmaUsed I0nl2iQ0ua0n Instrument Name AP! 5000 Regression Equation 0.x1+ 00.07016(r=Th0e.a9n589) /_ or 05 T 7] wm Xo) [Tw ww Nan [wn Nan T 3 1 T E10e28 [ eeoNs eanN w[annN [we= 7 1 m10.e88w9 I A eC w hei | { 5 [+ seme | io | mew | Nn| 4, { ] _ ii 2 Ia i !| piof , 3 rd no terme r Ee _ re _ ~~~ ~~ Perg ~~ om TETE SET EET As' 7 Lust Page 301170 341 4 Columbia Analytical Services 65 Created with Anal}st Reporter Printed: 18/02/20103:24:00 PM ArnaantSNaamec: PTrhoxo1n SheFatEon ate Aeauistion Method 21720O70C63T0.3 PFChneesiotnagm Proess Evan's PropsprG RReosamleUsed GmEeTicuan nsrumentName AP! 5008 Regression Equation =0.x+10.00003852 r= 0.9990) T es T eEeS T 0 R T e [ sW s Tw weeens iem ee hhhaaenn |inhe] enn|] 00 T i eeSs as Twor hReahwe] . | . of ~~ 1 i _rd 4 _rd b: a ~~ ~~ - iJ rd 1| Ps ] _- wf 7 of zroe Page sot 170 342 Columbia PAYws Ta---- PrCinrteead:ted18w/i0t2h/A20n1a0l'y3d:2{4p.o0r0tPeMr AnIantleyrntael SNtaamndea:rd AcDqautiasFiitleion Date `PArcqoujiescittion Method Regression Equation: P13FCU-RPFA1URA T2/T17O/C20A10L6o:n30g:13wiPlM EPFwCaKrisnePtreojxeLcotnsgP.FdCams AlRgeosrulitthTamblUesed Instrument Name =1.05x + 0.0336 (r= 0.9994)" [ELITE AnPtIe5l0i0u0an or 7 0083 @ |Nev| ten 05 [ose Te [wan |NN | 1 [wo 1 ae e [wav NN | 5 [v1 5374 [0 1% 7 ean] ew [Nn] 2 1 20372 [w|omae n Twn | [ 50 [sew wo Nan NaN | / - I 7 1 7 43 _-pd i 1 id "a|| | 3 A ji 7 7 rd rd 7 Ao ao Time Pa5ogf1e70 343 /AnGaolymtbiciaalServices PrGinrteead:tea18w0i2n2A0n1a0if3s2R4e0p0orPeMr IAnntaelryntaeSNtaamndea:ra ATcaqtuaisFiiteion Date APcrqojueicstition Method Regression Equation: 1PR3OcSPF1 OS T21I77O20C1a0L63o0n1g3aPM EPvFaCnh'isnePtreoxjLeocnisgPdFaCms ARlegsourlittThamblUesed instrument Name = 0.000414 x2 + 0.118 x + -0.00244(r = 0.9991) 2In1tl7iQ1u01aonng rab API 5000 [o os r1[e os T Iw e w |mmes enn| wwawn [os see er [Nan | han | [w T e eeT Tes [Nan | men | LE 18757 [eNe a en . / = | ii 1i vd 3| || _re qi i. rd Ho __ rd ~~ rd 7 _ Jaw Zito Page 6 of 170 344 5 mba $ Anatyieatservices- PrCinrteead:ted1w8i0t2h2A0n1a0ly3R:2E4:p00oPreMr AInntaelrynatleStNaanmdea:rd ADcaqtuaisFiiteion Date `acquisition Method Project P13FCD-0PFA1O0A 2T11T7I72O0C10A6L:o30a:13WlPM PEFwaCnK'isnePrtoejxeLctosnPgFdCasm. ReAslguolrlitThamblUesed C27i00ong 1b IntliQuan Instrument Name API 5000 Regression Equation: Mean =0.x6 +-00 .0045 56(r = 0.9959) l 01 05 Nan Nan [ oss [ | me NaN [Na [ 1 [ s Toemsss T | e av m [1mewenn [a[nNa [a f[ e2 v |] 2817e [ wrN [Ne n an [[NNeaw | 5 . 47074 S| Nan | Nan] 7 ~ 4]| 3 Ld i| . y ~~ 11| _rd 7 | | _ rere 7 - ot, AS rrreste Page 70f 170 345 5AnGalluymtibciaalServices Created wih Anal7y0Reporter Printed: 180212010 3.24.00 PM IAnntaelrynatleSNtaamndea:rc ADcaqtuaisFiiteion Date APrcoqjueicstition Method P13ECT-APTFDoA 2T 17720CO 1a05a3n0g13wiPtM PEuFaCnK'isnPerotjeexcotnsgPdFaCms RAelsguolrtitThamblUesed 0It2e7liiQ0uoanng a Instrument Name API 5000 Regression Equation: =0.33x6+ 0.0691 (r= 0.9959) < Exp Conc (ngimL) Calc CMoenaenfngim) st wev [os 1 [ [7Tos ot me Te wr T m wn n|wnven || [ 5 [we To sew Te [m|enan w | TT 12 NaN [oT 21.489 TZ 2 a a "i 3 1 }] tai 1 rr ilui l eea 7 ~~ _ 7 re ~~rd ~~2 x AW> o Ss se Page sof 170 346 5 Gomis AnalyticalServices PiCnroeda:ted18w0it2h/2A0na1l0ys3P.F2i4d.b0o0rPtenr IAnntaolmyatle tNaanmdea:rs AcSaatuaiFsiieonDate APcrqoujiescittionMethod Regression Equation PTrCoPnr1ooA 2G/E1T72I0O10G6a3L0,o13 PM PEuEaCnK'iPnreoeecxstPdoEanCmgs ARlgeorsitihdm eUsed InstrumentName =0000351 x02 + 0.exa2n+04.02869 (= 09993) GInelTiQuOan ab API 5000 os rT ow wh| wa 5! [1 oseese | ow e NaN | WN 0 CewT we { 50 I 1 . 50.241 3 NaN 1 NaN i 7 A ~~ - l rd Hi Bii rd~~~~ il: pr 3 rd " rd AY wr zie Page 901170 347 8 Solumbia AnalyticalServices PrCinrteeadt:ed18w/i0t2h1A20n10a3l:2R4e:p0o0rPteMr Project Data File 0E2va1n7'1s0CParoljLeocntsgPwFiCfs Result Table 021710long.rdb Instrument Name __ API 5000 [SampleName_T6---- `Acquisition Method|2P17F2C0H10i6n3oe0n1gt3deaPxmI (inconVial [+7 ~~ TinjectionVolume [5] Sample Type |wWeighttoVolume [000 | Results Summary [Analyte Peak Anais RT Name [some[omen [ARF] anaes [proat cero | tes | 157(138)| 279s (Tng/T mL Modifieds 200 | Nn | PFOS 1 POAT 19CPFOS | 1700 | 210209) 458 BCPA | 4st [oo0@os | 20 | wo | No PFOS 1 PTA1 1acPFos | 1700 | 3s en) 13cPFDoA | 174 | 000458) 13cPRooA | 174 | s08s08)| 47s 780 | No [0 so |wo| 4H0t Zs 21210 Page 1001170 348 LK Gambia AnalyticalServices' PrCinrteead:ted18w/it0h2A2n0a1l0ys3e:b2o4r.tP0eM0r IRC Summary -- [snap pesvame | RT EoRT)| ven | oar|CHENIN ao Gonire | s PFwOAs e000a1.r 3w6)|| wm0eo e | wNeo [|m oaowmeeemnm|||a e_ne||| [omermn amaw|a| | owem| | Ieronz 5_13-PFUNA froame I's_1acproon PFTA2 32300|0 M9 No | owe| te Te [owen |e] oowwmoeeenns| [ | wm |o |wNe[||mow oooeopmms ||| wwe [o |w mse | n wo [ omar No [soe s19) 2 No | 0090036) wo | ZT 2esleo Page 11.01170 349 8AnlalmybtiicaalServices --_-- 7:Quantitative Peak ReLvidT ew F ii:oGeao wCoai TY fE d ah M Ui n| bida PriCnrteead:ted18w0i2t72A0n10ap3t7.28R6.a00rePMr po - 1B =3=z |tllewHpltpaerrsaerreereaprhiReeNdd] tJ 2a03m CB4a1s3sPi0Fn1Oe8Ao3T0Mi0s2sed | cS4as41e73i0Cn3-e7PoF2MO0iA0ss0ed | oB4a6s2eP0iR4n1No5Ac.1M0i0sased | c B4a6s18e30iCn4-e2P3oF0NNAiDaased zl2) EPzloDLAen] FiDuL]7 sootnloewri p 1 - ThAL ,mP EY Wil] l IYenii31k0Beni cBa#s5e9Pi0rn2oe0sc0Mi0sased | 50133.00.800.50508 oBaseinoclissed | Ba5s1e3lPi0nr4e5o00TMi0sased | o5S11a530sc4p7eo700M0iAaDnsaed I||mi anfeedeE d N Goh| aor = =z bop fg E I=: boy oB5a6s3eP0lF5iU1nR9eA.cM1i0ss0ed | cB5a6s1e53iC0n-2cP7oF0MU0RiAs0saed | cBa5s9Pe8iF.n0De0Sc0M01i0sased | oBa5s10s3i3Cn0-e0PoF0hOhS0eased |<] ePsY a, VRE - oo [Y belT eAET m0- I Pa| hJsaneeyoJteaJlill of Ppa blfrntaJloel 613P0r1O5O00A.T00a cBaseineoMissed | 61p50a163008 oSsseinecMissed | 663P0e61r8008 cBaseinooMissed | 511530c.1p8F3B0oADa oSaseine Missed eli o ' il Regge) 1 T Ld te ely e) tyetAE| B7a1seP3lFi0Tn5ee8Ao01M0is8sed | c B6a1s1e53l0Ci1-n8eP8F.DMO0A0saed 0 Before OJ After Page 1201 170 350 4 lumbia AnalyticalServices" PrCinrteead:ted18w/i0t2h1A2n01a0l'y3t:2A4S:p0o0rPteMr fon Ratio Confirmation iB i= iz! ==i! ie 2= i | =P pl lk i ee "flags 3 4 33 | 2 7 ply | Mh 413P0F/3O6A820 Da oBaseline oMissed | 463P0F2N1A920 0a Baseline Missed | 499P0F/S92002 oBaselinecMissed | 513P0F26O92A008 Baselo Miisnseed WrongPeak Wrong Peak Wrong Peak Wong Peak | T = T il (i 1- = - i Msrpeon | er iP 563P,0F1U2N69A.20 Da o Baseline c Missed | 59P5.F01O99S. 2 Da Baseline a Missed | 61P3F.0D/1O6A9.20 0a Baseline oMissed|o 663.P0E/1T6A9.?0 0a Baseline o Missed WongPeak WrongPeak WrongPeak Wrong Peak i -Ml ji! 582) 71P3F0T1e6A92.00a BasWelrionneg<PMeiasksed 0 Before 0 After Pa13g0f1e70 351 [5 mola Analytical Services Created with Analpys.t76Reporter Printed: 18/0212010 3:24:00 PM Project Data File Ewan' Projects PFCs 021710CalLong wif AcquisitionMethod __PFChinetextdoanmg Result Table Algorithm Used 0217 1000ng rab IneliQuan Instrument Name __ API 5000 I 2 ET CT I Sl rill [SampleName TPFC 0 10ppb 21772010 6:5257 Pl Injection Vial _ [InjectionVolume [5 -- `AcquisitionMethod |PFCkinetexLdoangm Sample Type [Standard| [sampled TicwszesA |Dilwonfactr Sample Comment [7|WeighttoVolume to [ooo | | eReTesueletes eSruemeemmamremy rmereemeeeeeeermeeeeeeeeeeeeeeeeeeee Analyte Analyte | ExpConc | Gate. Gone| Accuracy PFOAT | 1.|2133 CPF1 OA|3 32896 300 | 14318 | o.00 [PFNA1 | 206206| 13C-PFNA| 2669800| 21089 | 0.100 0114 14 | No 0107 | 107 | no PFDAT | 310006|13G-|P2F50D420A0| zeta | 000 PFU1| as2e0s,| 19ceruna| zzziso| zee | om 0.089 | eas | 9 No ss | no | |pros1 | ast@en| 13ceFos | 752300| eser0 | 0.400 0.05 No | Proont | 454s| 19cp|FaD0soasA0| tases | 000[oo | ss | wo| PFTA1 |5075|103G-6PFD)0A| 305350| foae | 010 | WA | va |wo| Ane Zs 2 181 Pa14gof1e70 352 LST Analytical Services Aun Created with Analyt Heporter rRCsSUmMMary rrroenz r [sorsc.pron [pormoesr moan |w|w we | n.e] ] aa | aw | we | mw aewmaew|[ ew o we[[eew ww | [srscrron Prumaz sreer saaen |me |om w | we | swam | wm | | ore ww PrRasE wwe | mew em 353 Columbia 4 Analytical Services Created vith Anal Reporter Printed: 18/02/20103:24:00 PM rz Quantitative Peak Review 7 xi= iLll T= i7 ,PFC = 0.10ppb i 413P0R1O8X8008 441730C3P7F2O0A08 463P.0e4N1A6T.008 461830c4P2F3I0ADa BaseligneyoMissed | p oBaseyine cMissea | E BasT eloMiisnseed| 5GalsaeopiMeinsseed : ll ;- a. a=l ll- e" l pAa Bas#e9l9Pi0Rn2eOS0M0iT0sased | 501330.5p0E050S8 oBaseino Missed | 51P3r0o48n9T008 51135C0.P4F7O0AD0a Baseline Missed | oGaseoMiisnseed =hl I 3 tz7 i:3 ThA : = b 56P30r5u10]0 0a 561530c2E70n0A08 59P6r.0o6S001 0a 501a3c0.0p0F0G0Sa Baseline oMssed | cBaselnooMssed | oBsseinocMissed | c Baseineo Missed li=z efi:" 3 iezl "IE3] 6P13r0o15o8A91. 08 cBaseinoo Missed | 16315C0.1P1F6G8O0A08 oBaseine Missed | 663P0r61a5t008 cBaselnecMissed | 611530/01.6F95.00ADa oSaseo Miisnseed E i pe 556 3 713P0e8T6o6RT00a 61135p0F1B605A00a Baseline oNissed | c BaseclMiisnseed O Before [J After Page 16 of 170 354 4 Goh AnalyticalServices" PCrroeadted15vi0t3h5A0n1al0y@312B4p0o0rter I1 E J lon Ratio Confirmation Pome tig Tf] TT PFC 0.10ppb || | hand gon oB4a1m3Pi0rn5ai8os0M0o8nd | oS4m6i5P0or2oi1M8xi00m8ed | cB4e0i5b.nr0es0a5?b00uaed | cB5e1s3oe.i0rn2ao6ic82.o0r00ed Svrons Pea ons Pea Sion pean rong Pome TT = = = o=ol E=E-- == pia: EE ef[Zl sa cB5as6lP3iF0nU2eR8MA5i02s0s2ed | B5a6c6ePi.Rn0Oe0So52M0i0s0sed | oB6a1s3Pl0Fn1Oe6G8cA1v2i0mased | Be5s6o3Pi0Fn/1-T26M80a0ased Wing Peak oWiron Peak owiron Peak ronsPes i1 o S7r1aPo3Fi0nTao1eA62M0oa0med 2 rong Peak O Before O After Page 1701170 355 / Solum Analytical Services PriCnrteead:ted18i/t0h22A0na1l0 3.2B4e.p0o0rtPeMr DPartoajeFcitle 0Ew2a1n7'1s0CParoljLeocntgsw\iPFfCs AcquisitionMethod __PFChinetextdoanmg AlRgeosrulitthTamblUe:sed 0i2n1te7l1i0Qluoanng.rdb Instrument Name __ API 5000 [[AScaqmuipslietNioanmbeate |[P2F1C7702.05100007:0052 PML `Acquistion [Samper Method |LPoFwCisKzne5t6exLdoanmg [SampleComment | i[njecitionnVorjumee[c3 tionVia [SDaimlpwloen TFaycpteor [1sa0n0gard || | WeighttoVoume Joo | Results Summary = - [namtse _|| AE naiyiye RT| =omTewoISArman| AAsreiae |Ex(png/CmoLn)e||Ga(incg/CmLo)nc| AccIuracy| wa PFOA1 | 1270136| 13C-PFOA| 3540| 7701s |osw0 | 047| ss | No weuar | 2osane| rcerua | seo| ten |osm |ods | ss | to| Prost | zoos| 1sceros | meets| sso | oso | oms | wm | we [eroat 19CPFDA| 2763700| 14070 | oso |od|ssz s | No | PrUnat | 2.89400| 13cPFUNA|2044m0| r202s0 | oso | osm |106| No [rns |sraon|soeron | ove | wm | vem | wes | wn | | PFDOA1| 4544.55)| 19CPFDOA| 275140|sass| oso | ose | m3 | No| PFTeA1 | 5.53651) | 10CPFDOA| 275140 |aosss| 0so0 | oso |s|s No| A ere zusie Page 18.01 170 356 LS Golmbia nalyticalServices: IRC Summary i AnatytoPesk Name - [-- PrCinrteead;ted18i0t2h/A20n1a0l3y:2B4b:p0o0rtPeMr Aven Modified? ExpecTtedonRaVtaiolue S_13C_PFNA 0.00 (2.44) 0 i No 0.00 Toronz sos |w|w wo | on 5_13C-PFDA amon Ze |No| 10.77 [prumaz ama wn w |em| E pSr_1o3Cm.PFURA mseeems | |a mE ns [ |m Now| e1.70s| [roaeer || ammeesn |moew| we|] [rons mew| wn we | om | Pa19gof1e70 357 5 Golambia AnalyticalServices PrCirmeeadt:ed18wi0t2h2A0n1a0lf3e.i2e6p0o0rtPeMr QuaT ntitaw tive Peak Review 7 -- PFC =0.5ppb BY - i=Ch i 1Ch =LA |i:] 413P0/r1o83t0 0a 411730cR.P772o0A0a 463P0E4N1A0T000 4618a0c/.4P2F3I0A0a Baseline oVissed | cBaseine cMisted | Baseline Missed | oBaseine o Missed E 2 E io -ut o=l =Lee BA | - co4a9tP9i0rn8oe0os0Mt0s8sed | oBa5s01e330i01n.8ep0cF0GMSs0ased | cB5e1Ps3sr0io4n8Aeo8TM.s0s0ed | B5a11s5i30n40g7F0oO0MAsDsaed ==~ . I iE i |cl 56P30r15u16.] 00 581530.2p7F0U0A00 59p9r01o8s00] 0a 50133001.200055Da cBossine GMissed | cBoseineoMssed | oBsselnecissed | oBassinesMssed =e 7 5 = : Am :~ bo4 Z-i s07 Ao i=L l ob Ii fe he I= b FiE 613P01o5o86.100 61153001.6p8F.500Da 663,P01T9T.00 611350.071F6B03DA0a oBassine Missed | oBaseinecNissed | oBasainoclissed | o Bsseinec Missed i E sao fi de TBs B7as1e3lP0iE6nTe8O0oR0TMi0sased | B6a1s1e35l0i0.n1epoF8B5Mo0iAs0sed O Before O After Page 2001170 358 PAY Analytical Services" PrCinrteeadt:ed18w/i0t2h/A20n1a0l3y:2R4E:p0o0rPteMr lon Ratio Confirmation iE = fI== k a- [a = PFC 0.5ppb =N o = d\ = Lo7 i i- i : TT |3 ] = 413P0F/3O6A920 0a 463.P0E2N1A92.00a 499.P0F/9O9S.02Da 51P3F0O22A60D0a BaseWlrionnegcPMeiasksed | BasoeWlrionneg PMeiasksed | oBasWerlionnegcPMeaiks.sed | o BasWeiloinnegoPMeiasksed oo 3 ] =] | ll w | eamJeTsle = ES | I PRURA2 563,01260.0 Da Pi ROS 2 509.0/99.00a : PFDOA2 eT 6130/1690 Da ----PFT? || 6630/1690 Da BaseWlrionnegcPMeiasksed | BaseWlrionnegcPMeiasksed | oBasWeloinngecPMeiasksed | oBasWerloinnegcPMeiasksed | 713P0F/T1G69A02 Da B=asWelrionnego PMeiasksed O Before O After Page 21 of 170 359 8 olumbia AnalyticalServices PrCinrteead:ted18w0it2h2A2n0a1i0f3s:2H6e.p0o0rPeMr Project DataFile 0F2a1r71s0CParlLooncgPiFfCs AcquisitionMethod _PFCkinetextdoanmg RAlegsourlittThamblUesed 5t2e7l7i1Q0u0a0n0 db Instrument Name __API 5000 [[RScaaqmuipsiNioanmDeate |2T1F7C20T010007008:7FW E`Acr quisiti-- on Method _| PFCKinelexCdoanmg {Simplecomment |-- [jeoctinonaVolume [T 5 r]| SE ample Type I [Sr ta--ndard] | waghtiovoums 6] Results Summary [Aineanlyete ||GAnaaiymie RT|some [owes[#0An0ai0s [|REExpECoTne[|CgalemCosne[i | ve | [roortt ||rzaasamun|| reircreora|rsaman||sarvso||rtamm || voeom||wwoo || we|| Pru |sa|nricea r | msn| swe | oo | ame | we | wo | Pros1 | amaw)| vaceros | remem| ss | ow | tom | wz | we PFOA1 | 4544.55| 13C.PFDOA| 20024|0 143430 | 1000 | oss | 83 | ho Prient |sev| oerronon | moe| Tew | tom | om | | w A E ZesElie Page 22.01 170 360 nalytical Services" Created with Analy Harter RS C ummary rfroen:ne |wwien|| wowme |[wewe|[TaEeE]| vriaz [emer | wm | nw | os 361 0ACnoalluytmibciaalServices- Created with Anal}86Reporter Printed: 18/02/2010 3:24:00 PM Quantitative Peak Review im =z Ee Z| A lo = "PFC 1.0ppb a El i : A zl i 413P0F1O6A9T0 0a cBaseliec Missed | 41137C.0-3P7F2O0A0a oBaseinechissed | 463P.0E4N1A9T. 0 c Baseline Missed | 4681.30C14-2P3F.N0ADa oBaseino o Missed i| i| 4p65r.0O/S30T.00a 50133.00./080F.30S0a Baseline Missed| cBaselne o Missed Tee TE i i -l Fale A Fl 563P.F0U5G1A9T. 0a 55153.00-2p7F0U0nA08 cBalseilninneoMeiassed | cBasoiimngecMissed x! Lo i i ia i 51P2.r01O45A5T.0 0a 5151.30C4-7P0F.0OADa | oBaselinec Missed | Baseline o Mased =% SE - bl = ie ul F: 5p95r.0o6s00 0a 5013.301500sDa | Baseulinne cMissed | c BlaseilienesMissed =: Hl i= he oB6a1se3Pl0Fi5De6Oc0AM0Ts0saed | cB51a13s5Ce0-i1Pn1Fe6c9D0MosA0saed | oB6a6s3eP.lF0n6Te1AM9T.is0saed | oB6a11s53e.Cl0-1n6Pe9Fo.DM00iA0sased L | 853 34 Eu 1 i Ba7s1e3lP.i0Fn6Te8e0cA.T0Mi0sased | 0 B6a1s1e35lCi0-n/eP1FD6M09i0As0ased 0 Before OI After Pa26gof1e70 362 LS CRoloumabima services: PrCinrteead:ted18w/i0t2h1A2n0a1l0yd3:t24p:o00rtPeMr 7] 1 3 7 id cl) RE fon Ratio Confirmation PFC 1.0ppb E = pl | i - oi = I E pu eed | orciz priz pros2 ro: | B4a<13Ws.r0oe/3n6lg9c.PMi0eiaDsnkaseed | oBa4s6eW3lri.on0en/g2M1Pie9sa.Osk0aed | Bas4e9W9l.ri0on1ne9g9M.P0iesDaasked | Ba51Ws3r0oe2ngl6c9PiM0ei0asnk8seed || = = = = Ea ae PEL = 563P0F1U2R6A902 Da Baseline o Missed | 599.P0F1O99S.20 Da Baseline Missed | 6130P/F1O6G9A020a oBaselinec Missed | 663P0/F16T920 Da Baseline Missed Wrong Peak = Wrong Peak Wrong Peak Wrong Peak io"l Als 713P0F1T6e9A02 Da BasWerloinnogePMeiasksed 0 Before O After Page 25 of 170 363 8 mia AnalyticalServices- Created wih Anal58Reporter Printed: 180212010 32400 PA PDraotjaecFtle Acquisition Method GEw2a1n7'1s0CParoljleocntgs\PiFfCfs. _PFChinstextong dam ARlegsourlitthTmablUesed Instrument Name 0i2m1e7l1i0Qluoanng.rdb API 5000 [[AScaqmupilsetNioanmbeate T|F27C7725001p0pb7>1535 Pl [AcquisitionMethod | PFCiinetex.ongdam [iinnjjeeccttiioonnVVioallume T [5 s]| Sample Type [Standard| ([SSaampmlpelCeomdment |[iowszeso| W[DeigwnttotnfoaVcaewrme [J1o0o0 || Results Summary Tnaiyis | Avayte RT ou [Anas | ExpCanc | Gate Gane |[Nearmoent | 1Exp0ecte0d) || rSachoarmoen || sISAm|asAwnreeas| nsgoimwl) || (nsga/moL) | sr | Nwete? Frnt | aban | sco|rasnso| rasomo |sao| smo | 55 | we [Fr|ozmsatm| wcros| rasta| even | sao | smo | tee | we| Front | amos| vceron | sre|rea |smo| asm |ss| wo Pru1|sas|evsoorrusms| zur | reo |smo| sae | wr | no Pros1 swam| vcore | reso| sre |smo |sow | or | no | Pron | aszass| 1sceroon| seo |mon| sao |sm| e tm | ne Prat 508|6rc0sro6on| arco | sao| so |sao|ws|we| Prrent | ssrosn| aceroon| ameo| sewn | sao | sae | tm |ne| 2oS 7 ro 214 Pa26gof1e70 364 Analytical Services' RCSummary CrweithAanaltytBedpordter [smscrros [srtoancseron aeree|n mmo | wo I somwa a |wo wmn ew|wno [en1s 365 5AnSaollyutmibciaalServices- Created with Analyps.t90Reporter Printed: 18/022010 3.24.00 PH Quantitative Peak Review im JT i=3 A iz| A = =Ih A PFC 5.0ppb TT ibu A 413P0/F1O6A9T0 0a 411730C5-7PF2O0A08 cBaselinec Missed | cBaselne oMissed | 463P0E4N1A9T0 Da cBaselnecMissed | 4681.30C42P3F.N0ADa Baseline c Missed gy cing en hi coro Ihh o i bool a. iol --- if 499P.F0O80S0T Da 50133.0C/.8P0F.0GSDa 513.P0/O46A0T.0 Da 511530C4P7F0O0ADa BaseliyneyMissed | oABasTeliAnecMissed | oBasetlianenc0gMaissed | oBaseiiney c Missed :i}= i-|1 b=352 i:|Jol 563P0R1U5N19A0T 0a cBaselineoMissed | 51653.C0-/2P7F0U.0RA0a cBoselinecMissed | 599.P0R/8O0S.01 Da cBaselinecMissed | 501330C-8P0F0OSDa oBaseline c Missed wong pe tig rye com2a ii wf iET ibot iboo 613.P0/F5D6O9A.10 Da 16135C.0-/P16F9D.o0 A0a 663P0E/6T1A910 0a 611530C1-1P6F9D00ADa cBaseinecMissed | cBaselinecMissed | oBaseinecMissed | oBaselne o Missed = |= 713.P0F6T6e9A01 Da 61153.C0-/1P6F9D.00A0a c Baseline Missed | Baselineo Missed O Before O After Page 28.01 170 366 Columbia LS Rae services: Created vith Analy Rb81porer Printed: 180212010 3:24:00 PM i fd `lon Ratio Confirmation , PE == [el be fo PFC 5.0ppb, T = f CIA ee 413P0F3OA920 0a c Baseline c Missed | 463P0F2N1A92008 Baseline Missed | 439P.F0O9S902 Da oBaselinecMissed | $12.P0F26D9.2A0 0a c Baseline c Missed Wrong Peak 0Wrong Peak WrongPeak o Wrong Peak bo11 |<: :J iT (PE Z3| | ost 563P.0F2U8R9.A2 0a 595P,R0O9S92.00 13P0F1D1O6A902 Da 63P.01T16A32.00a oBaWrsoneglcMPieiasnkseed | oBaseWlrionnegoPMeiasksed | BaseWlrionneg MPiesaksed| Ba sWreonlgcPiMeianskseed ta + 71P3F.T0e1A629D0a | cBoaWsroencglPMieiasnkseed 0 Before O After Page 20of 170 367 4AnSaollyutmibcaila Services- Created with Analypst52Reporter Printed: 16/0272010 3.24.60PM DPraotjaeFcitle cEv2a1n7'1s0PCraoleocnisgPiFfCs Acquisition Method _ PFCiinetextong dam AlRgeosrulitthTmablUesed TntTeiOulaenn Instrument Name__ API 5000 [Sample Name PFC 10ppb [[SAacqmupilsietlioonMethod [|2l1Po7F7wi2nse0t1e0xL7:o2n3g:15dPamM [sampte Comment [injectionVial Te [[IDnSjiaemocptlnieonFTVayocplteourme |[S5 tangag|| | Weightto Volume Joo] Results Summary -- dTaonaete |An[lEylielyRT [sven [one[T 50Rea0tyisR | xp CE aneT| CialE emGore|S " | oe" sent | zor| tscreva| zr wo | ww | [pr|ozessaotm |tscr|rraosasn| sean oso | we | wo | [oront | aonase| racoron|as|iassens | tooo | torn |su|nro| erunat| sana| ricer| smn|swan | ao|sao| ws | wo | eros | sanann| vscrros | min| smo | tome | momo | wos | ww| Prooat | assash| viceroon|sem| momo | tomo Prvar | sass| ticr|raoeroon| rrimo | eso |noo| prront | sa |tcra oon| swims| ram | oom | tow | wi | wo >AT A 2 1g Page 300 170 368 5 AGnatlymticaalServicesTM PrCinrteeadt:ed18w0it2h12A0n1al0yP3#2840bo0rtPeIAr RS C ummary Anaiyte ek Name Toronz [sac pron [Crown|e[ween| RT (Expected) Aven [ramos area vo [ras|asa ems [wo EEE, | ExpTeocntReadtViaoiue 220 1.95 1 Pros 2 5_130.PFOS 208212) wz | No 032 2.08 2.00) No 026 sncPrumA PFDOAZ PrTeAz mas | wen | we | 453453) s13210 No |ssa|sms emee| we oto 030 035 J| Pa31gofe170 369 2ACnoalluytmibciaalServi.ces Created with AnalypsotsReporter Printed: 18/02/2010 3:24:00 PM i Quantitative Peak Review TE i i TE i z] PFC I 10ppb I= 413P.0r1O6R9T. 0a 41173.003.75270ADa cBaselineoMisses | cBaseineoMissed | 463P04E1N9A.T0 0a cBaseinechissed | 4681.30C42-3P.F0ADa oBaseine o Missed TE Te Tee 75 ElFoot i - i: bii"f i=|1 4p95r.0o1S80T0 Da cBaseinoc Missed | 5013.30018.07.50 50 oBaselinoc Missed | 513.P0F14O6A9.T0 0a oBaselinec Missed | 51153004.750700ADa Baseline Missed aun ig i bang pea b= i A I- - i. -] hs id po wk A 5P63F.U05R1A5.T0 0a oBaseine Missed | 56153.002.7F0U.n0A0a oBaselinec Missed | 506p.0r0O80S.0T0a Baselinec Missed | 50133066050SDa oBaseine o Missed ung ip ties Clans - i Cl I: =| |Z i= iE oB6a1s3Pe0Fl5Dn5Oe6Ac810Ms0saed | oB6a1s15e3.0iC/-n1Pe6Fc8B.M00iAsDsaed | oB6a6s3ePi0En6Te1cA9M0Tis0saed | oB6a1s15e30lC/n-1eP6Fo9D0M0iA0sased 8i oo3 11 | | 71P3E.0T6O69R.T0 0a 61153.c0-1p6F9B.oA0a oBaseine o Missed | Baseline Missed 0 Before OI After Pa32gof1e70 370 PASColumbia Analytical Services CrweithAanaltyspt.Re9e5pordter Printed: 18/02/2010 3:24:00 PM lon Ratio iConfirmatiopno} w 7 PFC 10ppb lif: oIlloEE hZ aLR ihCo A\ ho i _ ed Ba4se1l3Pi0FneO3A6c2M0i0s8sed | Ba4s6el3Pi0En2eN1A9o2M0iDsased | o4Ba9s9e,lP0iF9nOe9Sc.2M0i0ssed | Ba5se1lP3inF0e2Oo26AM9i0s0ased Wrong Peak Wrong Peak Wrong Peak < Wrong Peak LA] i| 7 -o" pe =3) IS I =o mezl-e] e -y Ba5se6l3Pi0Fn2Ue6R9A0M2iDsased | Ba5s9e9lP.iRn0Oe9S920MiDsased | B6a1s3ePl0Fi/nD1eO6o9AM02iDsased | o B6a6s3e,Pl0i1Fn1e6T3o.A20Mi0sased Wrong Peak Wrong Peak = Wrong Peak = Wrong Peak i ot -- o B7a1seP3lFi.nT0eEc1A62M.i0s0sed Wrong Peak O Before 0 After Pa33gof1e70 3n PASCAonlaulymtbiicaal Services- Created wih Anaifi Reporter Printed: 18/02/2010 3:24:00PM DPraotjaeFcitle Eav2a1n7'1s0CParlloocngPwRiCfE Acquisition Method _PFCkinetextdoanmg ARlegsourlittThambUlseed TInreliitQuoann Instrument Name __AP1 5000 [SampleName [P2F1C722001p0m73545 PI Tojecion Vil [[AScqaumispitlieondfethod [|PFtGunoeiewxcosng dzam osr S|abmipwloenFTaycpieor [[S1u0n0da || [SameComment | | weignttovoume fom | Results Summary [A[nnar | A[naslRT| wwe[mam A[n5a0t8a | E[xpCRoTne | Cai[aGmoene|"50| ve [rront | rae| vicoron|sv| aswasroo| momo | waoo | 52 | ne| [oruat |2amaon| crea|asso| samo | mao | mao |s|s we| Prost |saa| 1sscernos | rei| eosin| ammo | eam | print | soron| ncer|oaeoron| mem| mam | mam | ww | wo prreat |ssz|otorsronon | sesteo | nsw| mao | mmo | 5 |wo| a& 2119 Pa34gof 1e70 ar2 Jn rns AnalyticalServices IRC Summary Terns amen| wae | | [pronz [meen| oe w | em Pru swam | mom | we | os | PFDoA2 prea 4m52a(45w3) | 8w954w80 | Nwoeo | 0o.2o4 | [esas |am | o we | on | 373 4 olumbia Analytical Services" prCinrteead:ted18v1i0t2h7A2n0a10lg3:2e4p:o00rtPeAr Quantitative Peak Review 3 im oSRl i -3] pi ozl - PFC 20ppb p= 3 wm i -p il= |i 4130P/F1O6K901 Da 41173.C0-8P7F2O0A0a 463P0E4N1A91008 4681.30C/-42P3F.N0ADa poBaeseiene orMissed | oBaseg lineeMissed | o oBaslelnlec Missed | oBaseviinsoc Mpieasssed i he ha i. 499P.F0O8S001 Da oBaseine o Missed | 50133.C0-1P0F0OS0 oBaseiinec Missed | 513,P0F4D6A9.10 0a oBaselinecMissed | 511530C4-7P0F0DADa Baseline Missed ces oggPea pe ogee i=l IE Cl i = i= b= iz 563P0F1U5R1A910 0a o Baseline Missed | 56153.C0-12P7F0U0RADa oBaseline Missed | 509P.R0O8S0T0 Da oBaselineoMissed | 50133.0C1-8P0F.0OSDa Baseline o Missed Ei i i i i : --a pr -- 513P0F1D3O6A910 Da Baseline oMssed | 611530C/-1P6F0D.O0A0a oBaseinecMssed | 53.P0F6T1I3A.01 0a oBsselneolissed | 51153.0C/-1P6F9.D00ADa oBaselne c Missed i il o B7a1s3ePl0Fi/nT6ee6A9T0MiDsased | c 511530C/-1P6F9O00A0a Baselineo Missed 0 Before O After Page 36 of 170 374 4AnCaollyutmibciaal Services Created with Analpy3R9eporter Printed: 18/02/2010 324:00 PM I hd fi onRT atioCoE nfirmation bl IJ oT PFC20ppEb ol bl CB41a3P0sF3Oe6Ao92Mi0i0sn8seed | Ba4s6e3lPi0Fn2eN1Ao82M0i0s8ed| Ba4se9lP9iFn0Oe9S02Mi0sased | Ba5s1e3lP0in2Fe8D8.2AM0i0sased 3 Wong peak Wrong Peak 5 Wrong ak sWong Peak 3E ! cl| | hefi 2a a] | isa] oB5a6s3eP0iF1nU2eR8oA9M0i2sDsaed |oBas5s65iP.nF0eD0S8c20Ms00sed | oBa1so3Pl0Fn1De8oA9N0i20ssaed | o B6a6s3oP0in/Fe18T5A2M.i0s0saed Wrong Peak a Wrong Peak = Wiong Peak Wong peak = ios) 71e3r0r16o0a0 oBaSsosinnegopiesaered 0 Before O After Page 3701170 375 8 Solum AnalyticalServices- PriCnrteead:ted18w/i0t2h/A2n0a1i0fi3t:24:p0o0rtPeMr Project Evan's PrOjEcSPFCs Data File 021710CalLongwif Acquisition Method _PFCinetexLdoanmg Result Table, 0217100ang db Algorithm Used IneliQuan Instrument Name__API5000 Sample Name P2F1C725001p0m73621 PI I IAI I `Acquisition Method _| PFChinelexLdoanmg Sample Type |Stndaa| [Sampled [Towszes luton Factor [SampleComment| [Weighttovolume Joo] Results Summary |NAanmaely.te |An(aElxypteecRteTd|) 'SNe--me [omen | a| Ex(npgiCmoLn)e | Calcg.lGmLo)ne | Accounr)acy| Mer?" PFOA1 | 1.21|0131CP3FO5A| 3380100| sa4s200 | 50.000 | Stoo |10 | 3 No | PFOAT | 3.04305| 13CPFDA| 2657100| 14068000| 50.000 |5140|0 103 [PrUnA1 | 387606) | 13cp|F2U043n60A| tosst00|0 sooo | 4smo0 | 100 | wo | PFDS 1 wreseo00| 0000 | S040 | 101 | No PFDOA1 | 451455) | 13CPFD0A | 267090 | 7e00so0 | So000| zac| sa | Mo | PETA | 5.07508 | 13c-PFDOA| 267080 | 4220200 | 50.000 46.800 PFTeA1 | 5526551, | 13C-PFDOA| 267030 | 3542200 | 50.000 4 No 0 | No 3 RN ZY Lug Pa38gof1e70 376 [iSoumba AnalyticalServices PrCedr1w8ei0t2hA2an01a0lty5.:2eR4b6b0odrPeMr IRC Summary matte peak ame [roemrsror EAT Expl cted EE E Woditea?N ErConmat un || mmaesms || mmeemwe ||owwe |[a ew || [sopra sess | ema | 0 | wm | 85 [ 2oam | wom | we | em] moe] [roaz | swe | mmm [ow ids [roem msae e | w] es |b | 34s TTTeo Jutiuerens [| emesn |wow| we | ee | PTAs [| soot | wos [wo | os | prreaz | ssesn |wm | wo sn Page380t 170 377 5 SAnoalluymtibciaal Services Quantitative Peak Review CR rT -IE |iol ~ == 7 i zl PrCinrteead:ted18v/i0t2h/A2n0a1i03f:s24R:e0p0orPteMr PFC 50ppb -| " i= 413P0/F1O6A910 Da 41137.C0-3P72F.O0A0a 463P.E04N1A9T0Da 46163.C0-4P2F0NADa oBaselTinecrMissed | pBraeseline Missed | aBaseg linec Mipessed | Baastelaineeo sMissed i=o ; icl } - iJ oz 1 499P.r0O8S001 Da 50133.0C1-8P0F.0OSDa 513.P0F14O6A9.T0 0a $151.031C67-0P.0FOADa 7oBaseliannenc22Maissed | e oBaselie nec Missed | n BaseliL ne oMissed | ~BaseluisnsegoeeMsissed i = - io < WE] x i 55P3R0U5R1A5T008 1535C5-0P5F7U0n0A02 50P5R0O2S00T0 s1o3rC0-PmF0O0Sa | cBaseliange eMaissed | BaselioneeoMsissed | cBaselannegcMoeissed | oBaselonbe ooeMaissed Ll= i]3 =3 bl3 | io i b= i4 | zl A preg] Fpl ema! 613P0F/5D6O9A.01 Da 611530C/-1P6F9.D0OADa 663P0F/6T1A910 Da 61153.0C/-1P6F9.D00ADa cBaselinecMissed | oBaselinecMissed | cBaselnecMissed | o Baselinec Missed ig io 713P.0F0T6o6A910 Da 611530C1-6P9F.D0OADa Baseline o Missed | Baselineo Missed O Before O After Page 40.01 170 378 [5 Columbia Analytical Services- PrCinrteeadt:ed18w/it0h21A2n0a1l0y3t2R4e0p0oPrtAer | Ea lon Ratio Confirmation - = == ~1 zl LJ =c)N PFC 50p-p=bi o4B1a3P0sF3Oe8Ao92Mi0i0sn3seed | o4B6a2P0sF2Ne1Ao9M2l0i0sn8seed | Ba4se0l5Pi0Fne5O9S0M2i0s8sed| B5a1s3P0eF2Olc02A0iM0ins8seed Wiong Peak 5Wrong Peak Wrong Peak = Wong Poa J bowl "5 1 oo , 2=) ] zdl4 ste || ol ob 2 i = eto [| Beefs | PFURA 2 cB5a6Ws3eo.i0nn/2eg69o.PV0eiaDnksaed | PROS2 Boa5s9We9lr.i0on/ne9g9c.P0MeDiasaksed | PFOGA2 PFTA2 | B6a1Ws3e.al0in/n1eg69.P0MeiaDskased | o B8=a6s3We.rl0io/nn1e6gc9.P0MeiaDskased ' =1 zt 4 71P3e0r1o6n9D0a BWasaelninge PMeiasksed O Before 0 After Page 41.1 170 379 3 Goma AnalyticalServices Pianss eHitOnaifSBS24 CrAo oRFwaetioen thoa_prSaOmnroscoeheaeLnogmoatn RRneoosrramaTnaUNsaemde__ hnGpai5h0E1i0nT [[AcSqausmtoiolneWtetanmoge--{TeeFeCzheoezotmo0tEo0nY1g6s7em7 [CmSaEslenTVoetan f-- s [sE ampieo TTIromsE aris 3 DisionFacor 1L-- 0L0 | Results Summary [Prapt |r[v22o0ekao3nns|| craecreor|[ssssasmooo|| saewassriooo| a0am0 am |ot| to bros1 | 2asaos,|1sce|rraosioso| teseaom| sams | oan | tot | ro Front |sasaos,| 1aceron| sasioo| suas | moans | zommn | 10 | to pruna1 |sat|itscepruonn|nsa,nso |scion| somo | zr | na | ro | bros1 | assem| 1aceros |restos| tesmiovo| amo | maw |108| ne Proont | 4syuss| viceroon|meteo |sooam |mom [wmo| wt| wo | PpFeTrreAa1t || s5.a07s(5s.0y8|| t13Cs-PcFDorA||rso2e0r9o1s5o0n|| r21o91v40e0 || s20a.m00o0 | m21o.m60o0 | o10s8 | fNoo. a8: 7' Lisl pagespar 10 380 5 Gumtin Analytical Services" PriCnrteead:ted18wi0t2h2A0n1a0ly3:}2A6S.0o0rPelr RSC ummary m[rrose ["Anatyte Peak Name mm| arm [RrEern) | Ama |o moat ns| e] Te rm eenrs Tom ammaan | ww+eeT||a wee||ewee]] Pros 2 | ssscen C--O Pa47gof1e70 381 5 SAnoalluymtibciaal Services Created with Analf1i0R6eporter Printed: 180212010 3:24.00 PM Quantitative Peak Ed lo il pul 413.P0F11O69A.T0 0a cBsselinecMssed TF E 2 499P.F0O80S010a oBaselluingeec Missed Review PF 2 I= i 411730C5.7P2FO0A08 | oBaselinecMissed PE i i 50133.0C1-8P0.F0OSDa | BaselDogine cpeMaissed Tz = i1 4 463P0E4N1A9T0 Da | cBaselinecMissed i:7 SE a 513P.0F4D6A9.1 Da | oBaaselinec Missed PFC 20ppbICV = zr = iA 4681.30/C4P23F.R0ADa | Baseline c Missed 7 58 3 511530C4-7P0F0OADa | Basuelinge c Missed i |3 Ai. ib==l Ai 1 - wf 563P0F/U5R1A901 Da 6153.C0-2P7F0U0nADa 599P.0R/O8S00T Da 50133.C0-20P.F0OSDa oBaseolibnecoMisSsk ed | a cBaselinecMissed | 3cBaseilicnoecPMeiassed | T Baseo lineg o Missed 3 3 cl bo Et i | = 513P0F/D5O6A010 Da 611530C/-1P6F8D00DAa 663,0P/F6T1A9T.00a 611530C/-1P6FD9o0OADa cBaselinec Missed | Baseline Missed | oBaselneoMissed | Baseline c Missed i ho 713.P0E0T8e6A9T0 Da 61135C0-/P1FD6O9A00a Baselineo Missed | Baseline o Missed 0 Before O After Page 48 of 170 382 8 SAncalluymtibciaal Services PrCinrteeadt:ed18w1i0th2A1n20a1l0y3:2A48.P0o0rtPeMr fon Ratio Confirmation PFC 20ppb ICV - E ae Re ay | GE |i El \ Aq Fa i) 33 | SPeFOAd 2 oPa ENA 2 PFOS2 =| ----PFOA AZ -- oB4a13s0/e36lc9M0iiDsnaseed | Ba4s6e3l.i0n1e219.M0i0sased | Ba4s9e9l.i0/n9e9.c0MiDsased| B5a1s30e/2l6c9Mi0i0snaseed Wrong Peak Wiong Peak Wrong Peak Wrong Peak 3 = 5| a. = = oi cf izoa| ose Ee 3 iL i 563P0F/U2A6A920 Da Baselinec Missed | 509.P0R/O99S.20 Da Baseline oMissed | 513P.0F1O6G9.A2 Da cBaselinec Missed| 663.P0F/1T6A9.20 0a o Baselinec Missed Wrong Peak Wrong Peak Wrong Peak Wrong Peak 7 shegee 71P3E0To1A62800a BaWseiloinnegPceMaisksed O Before OJ After Page 49 of 170 383 4 umbia Analytical Services PDraotjaeFcitle 0E2v0a8n1'0s5P\rCoajleLcosnPgwFiCfs Acquisition Method _PFCkinetexLdoanmg [SampleName 2#072Z0i1p0p72c5ov5PM [Samp|lLPcFeCwKsiznseatserxLong dam Sample Comment | Results Summary Anaiyie | Analyte RT Greated with Analy1R0ep8orter Printed: 1410222010 6:41.00 PM Result Table Algorithm Used CI2nt0e8l1i0Q8uaanmplesLong 196 Instrument Name __API5000 [TinnjjeeccttiioonnVVoilrume 5] Sample Type [WeighttoVome [000 | Tnaiyie |ExpCone |Cate. one| Accuracy [Pr|N 231A2421)| 13cPFNA | 2006700 | assszo0 | PROS1 | 23525) | 1acprOs | 7240000| 426000| [Proas [aasea|e raceroa|aas|raezoon| PFUNA1 | 4124.06)| 13C-PFUNA| 175930 | 2867900 PFDS1 | 412610)| 13cPFOS| 7240000 | 146e2000| PFDOA1 | 476463) | 130PF|D22O37A30| 2346700 | Pras |sasate| worroon| a | sess| PFTeA1 | 574674| 13CP|F2O207030A| tosoron | 000 | 1000 | 85 | no | 20000 | 18800| ss| No | 20000 | tram | ss a0 | 8 | No 20000 | tado0 |: | ne 20000 | 19300 | 5 | No moo | ram | es |to| 000 | trae | ss | No | 4 oF Lielt Pa42gof2e42 384 ZX Soumbia AnalyticalServices nso pd Printed: 1410222010 6:41.00 PM RCSummary Rea pes ms [oprornem RrooRn|wer| wens | goto mweem[|w wwo||wm we w | ] ve bros: man| we | we| ve | [rnoemre [Ceswaes|| e || wee||| | scrrm ron 0 Prin [o|wrwe| wme | 385 Columbia LS Soe services: Quantitative Peak Review a =7 ER - Ai Fo i i ! PrCinrteead:ted14v/i0t2h1A20n10a6l:4y1:s00ePrM PFC 20ppb CCV - oz Ftol PFOAT 13C-PFOA PENA 1 13C-PFNA BaselinMueg c Mipeassed | oBaselViinesc Mailssed | SchBaseline Missed | Baselineao Missed Lo 1 | ho i 2 i ps 2 4 Le 498P.R0O80S01 0a o Baseline Missed | 50133.0C1P80F.O0S0a Baseline Missed | 513.0P/F46O9.A01 0a oBaseinecMissed | 511530C4-7P0F0DA0a Baseline o Missed aE Ee tp py :| i: | io=! = oii l 3 563P,0E1U5N19A.10 Da _ Baseline Missed | 561530C1-2P7F0U0RADa cBaselinecMissed | 599P.0R/O80S.01 0a oBaseinecMissed | 50133.0C/-8P0F.0OSDa oBaseline Missed = icl i| iol 613P.0F1O5O68A.10 0a Baseline c Missed | 6151.30C/-1P6F9D.00A0a cBaselinecMissed | 663.P0F66T1A9.10Da oBaselineciMissed | 61135C0-/PF1D6O9DA0a Baseline o Missed 2 i: CL E ee] | 713P0F6T6EA90 0a comeinechsses | 61153.C0-1P6F9D.00A0a oBaseine issed 0 Before O After Page 44 of 262 386 4 lumbis AnalyticalServices PrCinrteead:ted14w/i0t2h/A2n0a10ly5:s4P1:R00rPeHr lon Ratio Confirmation = T PFC 20ppb CCV = = TT |I: |1A | EE foams |4 | a 4 413P.0F3O6A92. 0a cBaselne < Missed | 463P0F2N1A920 Da Baseline Missed | 499P.R0O9S920 Da oBaseine Missed | 513P0F26D92A0 0a o Baseline c Missed Wrong Peak Wrong Peak Virong Peak = Wrong Peak FI 3 dn I pene 4 p i 3 fe i s . pu! 2 -L 563P.0F2U69A.2 0a Baselinec Missed | 599.P01F9O9S.02Da Baselinec Missed | 613P0F1D1O69A02 0a oBaseine c Missed | 563P,0E1T1Z630.a0 Baseline o Missed Wrong Peak Wrong Peak Wrong Peak Wrong Peak - i~ 71P3F.T0E1A6280.a B<asWerlionneg0PMeiasksed O Before 0 After Pa5gof2e62 387 4CAonlaulymtbiicaal Services- pz Created with Analyst Reporter Printed: 15/02/2010 2:34:00 PM DRFaerqaueiFseliteion ethos GF_rpaorrsCsTkPonCoaEtrooGrtadiSnatmo R NInocoeratmTenUsaemde G oliveEr TS 4515000 [[RScAaacuqmuiipssitNtiooannmOleseiasd_||PF[P0FFC1Ti0om5nb5Ge1oiAHoxsh[j|oTeSicraetmcipdtlooenaTnVyvnopalerare [[ 5 7]| SSaammppllee ICDomment T| CVSZ85F DWieluitgiohntFaic| otoourme[000 | RFeosiulets |Suommsarey | Name (Expected) rae Area Eosgipmloy_|_(CnogeimCobn)e| Re0%m) y |r pront | taser| cers | rw| surio |mo |to em | ss | fo Prren1 | 3svasn| tacoma| asso|aaessoo| 2000|too | ws |wo| PPrraas1t || ssasaazot|| cvaoormneas ||awrsooon||tesssesoano|| m2o0o0||wnemro |[ewem ||wnoo|| Pron | sav|etoczersaa| sso|ssi|omiooo| wm | we | No | PIvor:t | sasmems|e|; wrcoerrmosn ||esaswen|| tseomwno||o moo||n owowm || wwmn || No | oSEe ren| aceron| sum| sawn| wo | too | wm | vo| 4 2on0se J-- 388 PayCAonlaulymtbiciaal Services Printed: 15/02/2010 2:34:00 PM IRC Summary frreas:] FPrFPaesA2 2 [roe Scere [s_rscrrm ri - mam 3.59(3.60) | emo 8849500 | Nwoe YES 1 omen|owe | we | wm] mam| eww | we | we sem | www | we |we] 389 5AnGaloytmicial Services- Quantitative = Peak Revio ew F rT s3 Lo | = i: a PrnClreeda:te1d5w/i0h22A0na1l0ys2pt3.41R.1e0p4o0rtPMer PFC 20ppb CCV sw El i3 BcB2a1sA3e0Pl1F6i9BAn.eA0o1Ms0saed | ScB2a1s7E3e0Ci7-n7ePEF2oB0MA0s8sed ic| iE | i | oB2as6eP2iF0nP2eec1AM91i0s0sed | Ba311s530Ce/-2Pl1oF0HMi0XiADsnsaeed - luzig zea gra i- it 5 oBa2s0e9Pl0nre8e0so0MT0s8sed | oB4a0s13e8.i00n1-0eP3oF.MH0iSs0s8ed | cB3a1s3eH0i2An6eA9o0M|s0saed | Ba3s1e15l30iC/n-2eP7oF0H0MXiADsased ini 7 gpm | iin a = = - 2 Ih Ih I= ig 263P0e1g6a90 0a oBaseine oMissed | cB3a1ss5e0ol/nr2e7ct0M0iasDsaed | | cBs30s3ee0ir/n8ae0c.sM0s0s8ed | 40o30r10t30h0a Baselineo Missed lo "lea | Sloe 7 HI ib g23 ii |3 40v30i103s0 Da oBasoine aMissed | cBsa1so5elr0n4te1oo0M0ni0s8sed [f3i 4- Li=-4l ||| oB5as1sre5al0nc4ee7c0iM0io0sns8ed | oB51I a5s0eo47Mii0Dsn0saeed O Before OJ After Page 43 01 245 300  ASnoalluymtibciaal Services- Created with Analyspt.1R1e5porter Printed: 15/0212010 2:34:00 PM Ton Ratio Confirmation wm =] EE PFC 20ppb CCV =T | i.| i -| i| i ~wl sm. G2B1as3Pe.lF0in1Ee6Ac.20Mi0sased | B2a6s3e0lPi1En2Pe1E9oR0M2Disased | 209.P01r9E9S.02 Da Baseline cMissed| 313P0F1H1Y9A2002 Baseline o Missed Wiong Peak Wiong Peak Wiong Peak Wiong Peak eoFr Eo. -T it = Ih Tisundwae JA p i cBa36s3eP.l0Fi1nH3ep1A6c.0M2i0sased | Bas3e99lP.iR0n1He9I9a.S0M2iDsased | Ba5sS1e_5l.i10n34eC7cP0F0MDi0Asased | NA Baseline o Missed <Wrong Peak Wiong Peak Wrong Peak Wrong Peak NB. PFBA and PFPeA da nol have qualiying fon Fansiions 0 Before OJ After Page 44 of 245 391 PAY e Columc bia PR-- PriCnrteead:ted15i/t0h2A/n2a0l1yp0s.t21:R3e14p:60o0rtPeMr DaPrtoajeFcitle Eav2a0n9'1s0CParioSfheocrStPwiFfS ARlegsourlitthTambUlseed TIn2t0eBlTiu0aSnampEsShored Acquisition Method _ PFChinetexShdoarmt InstrumentName __ API 5000 [SAaamupslieiNoanmbeats |[PZFUC4204ppb6CCTV.H [je[ctn ionj vorue me c 1[75tonvial|1] [S[ampSleamp| l| ePLFcCMiSCi2n.e8lo5eFxSmhormdament [S|aWmeDpilgehitTiyopu veoumte Ji [o1Goo 0uao0ilny CoF ntrolactor|| Results Summary nmarte | AanalyyteRT|wee [owes Tr[atiytie || EGxREpCone|Cale.[Gamoyne| Acc|ueracy| | PFBA1 | 1.26127) | 1ICPFBA | 4105000| 180100 | oo0 |ss |No A | PRPeA1 | 2590.60)| 13CFHXA |4752800|sotssuo| ooo |170 |NA | Pres1 | a2sw20| 180PPHS| 2067200| tesesuoo | 000 |tao |NA | Me [PrHxA1 | 5.30531| 13c-PFHxA| 4752000| 8674800 | 000 0 | NA | No [PrHpa1 | 6.226623| 13c-PFHXA| 4792000| 3405100 | 000 1840 | NA SSiodo: [sSaece: satay| 1scpron | essa| aero |om| oss T va |wo| 13C-PFDA | 3653600| 3653600 | 000 100 NA | No | ES = oAo 2 Page 225 01 245 392 8 lamblia i AnalyticalServices" Printed: 15/02/20102:34:00PM RC Summary arerneene wmaoem)| | wow |we| te||ovges | Peron 2 pera 2 Scere mem | mew | we | ve | nem | moo | me | ve | snes | mam | ow | we | 393 0ACnoalluymtibciaal ServicesTM CrweihAanatpR1ee8pordter Printed: 16/02/2010 2:34:00 PM Quantitative Peak Review 3 3% = T% PFC 20ppb CCV 3 wy 5% i ic i i = = = E ol2a1op2ir0nE 1ei6e8vTi0n0e8ed | od2e1s17oni0en1ee7f2B0MA0is8sed | | re B2a6se3lr0ien2ee1o0kM0is8sed | oB3a1s15s3i0Cn5Pe7FcI0B0MiA0s8sed THATS ic3 |i f=-! i=| c2B6o6i.Pn0Fe5c0SM0m0ssed | oB1a0s1o38i00n1-o0Po5Fb0HiSsDssed 1 | oB5a1s5Pe.Fi0Hn2Ae8Ao01M0s0s8ed | oS3as11e35iC-n0Pg2FcF7iMX0biAsa0sed i ol | |} oB5a6Ps3i0rn1e8k50Tmi0sased | oBsai1s0i3n20e1oP0Mi0iA0sssed || oBa3sP8er0io8ne0sc0th0s8sed | oB4a0s1e35l0n10e0o580MSi0s8sed 3 : ozi (-= ch45a3n21e081s00u5i70is5gaed | oBsaimomsrnaie0oo0Nn0ssees 3 = LI 3 lozl ||| obsmsBeacismhTeooc0an0meed |oSa5s1iT5snce0p4oF7oan0bsa0es 0 Before O After Page 22701245 394 8AnSaollyutmibciaalServices- PriCnrteead:tes15w1i0t2h2A2n0a1l0pys2.t:31R41e:9p0o0rPteMr fon Ratio Confirmation piee7 a 1Ee] Bl | i= PFC 20ppb CCV Woah 3= i i (i we = c2B1a3s.e0lP/iF1n6eE9Ao.2M0isDsaed | c B2a6se3Pl0Fi1nP2eE1oA9M02isDsaed | o2Ba0s9elP0iF/nEe9Sc92M0i2ssed | oB3as1eP3iR0ne/Hc1A1M2D8isa0sed Wrong Peak F = < w-- Wrong Peak 1 Wrong Peak. -- -- Wiong Peak T LIi l ENT e , i | - Toto o3B6as3Pe0Fl1iHn3De1Ac802MDisased | Bas3Pe99lF.i0Hn/C0e9S.o0M20iassed | Ba5sSe1_l5i1n03eC4oF7MO0DiAs0ased | Wong Peak Wrong Peak Wrong Peak NB PFBA and PFPeA do nal have aualying on Tans. 0 Before OJ After Na BaWsoelnigncePMeiasksed Page228 of 245 395 3 Some AnalyticalServices Pom Aa an Created with AnalyBt Borer FoRermieuteeiton Method _FrparoucnFcaRioExiTodnamg RlT ooserumentUsaE emde 4m6lT 1i50c0u0n [SampleName [PPC Zommbcey `AcquisitionDate | 2117/2010 7:53:28 PM. injection Vome [5 | [RseaaumiptlioensWetvos|[Pcourizsoe noem et|eDSaimonplnegFTaycptoor [100 (Samplecomment| [Weightiovome [ooo || Results Summary FoE ront | 122090| 1sceron |l sa|msmme=aelrl|Bzol om | tea |2| enes| (ora oramm| acon |rm|isroomnn| mom | seo| wn | wo| Forost | zasaon| saceros| resumes| wsessooo | zoom | www| sm | Wo vron1 | ssas| aceron | morio| ssersea| sow | teem | 5 | [PFUnA1| ss|s1acParunao |festa | aires| 20000 | am | oz | No | wros1 | awawn| wceros|rem|toenosonr| mmo |res | | PFDOA1 Prin ||s45 o3r4||. 1t3seCc5-ePr5FsoDo) OnA|| stn | 245450 | mean 2985300 | mow 20.000 |m20.10a 0 | mw 10e1 | fNoo | [prrent |sst|vaacesrooyn | soso| wwe | mon | maw |w|p wo| AE Piee Page 201170 396 4 Qombia Analytical Services prCinrteead:ted18w1i0t2h1A2n0a1l0y 3:2B4d:p0o0rPteMr RC Summary fsrrnocnzpron mera [omorros [[errmrsor [Cmmo|| soewww | |w we |e we | [owew|ow| w | avam | we| we || [ssooeamr || zew || ewe| |e|] [=rczron [Csooaenm||s own|m | wwee| |o ve e | 397 PASCAonlaulymtbiciaal Services CrweinAanaltytFeonder Printed: 18/02/20103:24:00 PM = Quantitative Peak SR Review Tp PFC 20ppb CaCrV izl il: i4 -| 413P0R1O20X008 471033.57720008 462P04N1A5.T008 461034c2P5F0ADa caseine oMiseed | Baseline Missed | cBaseineo Missed | oGaseinec Missed i=|l icl IFED iHo js pe i I | 49e0r2o0s0i08 50133075050S00 BaseloMiisnseed |oBaseline oMissed | 51P3r0o48n5T008 51150545707050a oBaselne Missed| oBaseoMiisnseed i:El iZz| ibl ilcl 5P63.r05u19].00a Cassino oVissed | 51835c0.2p7FU0n0A08 oBsselinecMised | oBa5sp5e6rl.n0oe2o0tM0i0sased | oBa5s10e53icn0ep0oE0GM0si0ssed =i =i : icz 3 IE f :! he 1 oB6uP1t3i0rn1e5o8o6M1.i0ssDed | oB6a11s53a.0-i/#n1Fe6oB8.Mo0aADsaed | oB6s6Ps3sri0n6e1c9T0Mi0s0sed | B6as11e3i50n.0eop1E6BMo9DiAs0ased ai :hco B7aP1se3lr0in6ee8ot80Mi0s8sed | o B6a1s15e3.lc0i./n1ep6Eo8B.oM0inDsased 0 Before O After Page440 170 398 LECSolUumbBiaservices PrCinrteeadt:ed18w0it2h12A0n1a0ly3::2#43.0o0rtPeMr fon Ratio Confirmation Cioo Lc7 ha li |a N A => mm f = i] PFC 20ppb CCV. n Fo3 o I= reer 4130P1F3O6A920 0a 463P0E2N1A9Z0 0a 499.P0F9O8S02Da 513P0F2D8A02008 || BasaeWlrionnegMPiesasked | BasWerloinneg:PeMaikssed | cBaselinec Missed| 0 Wrong Peak Baseline Missed Wrong Peak | = 34 F)g f=o2 I io<34 i1|-le 563P,0F1U2R6A9.02 Da 599P.R0O9S920 Da 613P0F1D1O6A902 0a 663,P01F168T.20 0a oBaWrsonegloMPieiasnkseed | BaseWlrionneg MPeiasksed | BaoseWlrionengoMPiesaksed | Bas=eWlrionnegMPiesasked i=l 4 713P.F0T11o62A3D.a0 BasWerloinnegc PMeiasksed 0 Before OJ After Page 45of 170 399 p12 21Aeqa2ua20t0io10n0tDe1a8tze020Via +3 awma20010011883%7 5 m2a200i001t0e5e3s 57 5 2z222e0a01010i00111995020830 110 228m220011001290350 12 m20i10022110091 115 16 ma2m00o11i00022211131216 17 aammao0i002211238 21 21 2226m02e000101020222100502 72 2ww0e0070222y 2= x 22a200z0022n437 227 2 aa amm2i00100 22235150 3310 z2em0a10002z38275 52 3 2202000012032338%408 se z2602o002n355 37 3 2209220001000000112085 a 2209220010000430 2 22902001000548 eas e220a101t03 a aaoea00r001121s8 5 222o00m20000011r041e83 2si 5 aa2e0e02a00020z01n65 ssme ea0m0a2z2e 5 2ae0e01n0o0204220a Postian21SPaEmCplOe10NRamLe S43PPPFEFCCTCSOOOMSmS G8TPPRFFCCEISOCpD 4157PKPFEICCONS2200T99I98-050C0CC1VV 44283KK1II0OO0DO999T1TT1..00000234 4465KKIIOO00009S1111.-000056 444987KKKIIIOOOODNOO099S111111...000000785 S55120KKKIII0OO0ON9OI1T11I000111120 55S543K1KI0IO0O00N099I11T11T.000111435 555766K11I00O00O00O999111111.000111867 655091 KKKIQQ0IIOO0OO0900S15313202.100965 6623KKIQOI00OE02S13.20.001 645 KKQQII0O0O0U4S533..0012 22521KKKQII0IO00OO9064E65.030.10023 22256KKKIIIOOO0N90U9BG6.E8.0.00000435 2267KKII000W099666E.00076 2298 KKII0O0000096688..000068 3310KKIIO00N099G6B8.O0T1T0 33326KKKIIIOOONN0O9099GE6E..0001T13A2 335675KKKI1IO0C09O06D99E8G.8..0001115G7 133069KKKI1I00O00O00D96G68E6...000211096 578KKQQIIO00000662200003 APcFPqCEuCsiKtoiannneMotesntehgxeoddodaansmgm PPPrFRCCCkkKnnneeettteeexxxooonnngggdddaaammm PPPErrCCCkKknnneeettetedeaonxnggodddnaaagmmm PPPEEFCCCkkkinnneeetttoeedxxlLLddodooanannamgggmm 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