Document oe0NdN3YB2Ya1VYzZvZ2be867
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DATE PRINTED: 1 /i2/82
S-V.
C.V. 105, 106
D.V
317, 322, 323
C& 46 CODE YT-820-D PKG -----
Jiii^2_|9_82..
. (> YT-820-D <D)
()
<)
7 DATE )
<L0,T NUMBER)
i) ( ) TYPED BY-i JMH
itsT. WT- 2563# LBS, '
STANDARD HRS. 8,8
jfyJ&1' "
PREPARATION NOTES:
j L-__E.X1
APPROVED BY EWK 10/21/81
TIME ___ M
EQUIP " MENT 1
DV 2
.1 E: DALAjf^R^YELLOWR \
iTAiN 3-NITR0^4-n INOANISOLE FOR S6 BTAI%ACETOACET ORTHO ANISIDIDE FOR S22 CLEAN ,fDRESS, CLOSE ^4* CLARIF PRESS 15 FRAMES %
1 USE 5 LBS
I
b l e e d in g -
I N-CQDE 1 ACCT I | LBS
396--C } 46--C I 1
IjN 17* (595^0 WATER/ INTO V_
UET-GH IN HYDROCHLORIC . ACj.D FROM V-324 ______ ,WJe5J--_X
| DUMP IN FROM Si 3-NXTRO- VAMINOANISOLE
LOT
100%, a
%
iS7o_ i
i JJJZ&L
!.
-_S
2^D I 559 396--C I 1190
4**$*
w
I 'r
><-_ Mgr i%Wtv;.
--i
.1 1
STIR 10 !P OR LONGER TO WET
"ADJ TO 33F (1155G) AT 28-32* F (ICE)
@21X330 i - 57-A |
1
[PHON IN SODIUM NITRITE IN 12-15 MIN
^_
M ,_43t3A___________ x
fI \iSL2_ i 725-a j
I,
STIRO^MIN AT 28-32 DEG F MAINTAINING
I
I
.........
+ CR, + KI FOR S 12 j RECORD* TIME, STARTJLj&jhM CR
<+),
KI -b~ ( + )
.1 JUL 4619.82
NOTE:
.
i
(1) IF CR-, KI-, ADD 20* "AS IS* INCREMENTS!
I
HYDROCHLORIC ACID
ASSUME 32%
RECORD:- CR_____< + > KI____< + )
1
I 28-D |____
i\
(2) IF CR+, KI-, ADD 20* AS IS' INCREMENTS!
I
i
SODIUM NITRITE
ASSUME 33% I________ I 725-A !_
RECORD; CR______:'< + ) KIC + )
|I
N32606
DUP050463750
EQUIP KENT
GE 2 OF 3
I ,USE CG 46 CODE YT-820-D <D) I LBS
N-CODE
] SLURRY IN 40 GAL WATER IN DRUM 6 PRECOAT ! CLARIF PRESS WITH DICALITE, FILTER AID
777-A
10 STIR COMPLETE,
IN DICALITE, FILTER AID
10
STIR 30 MIN AT 28-32 DEG F MAINTAINING
i
*- CR, +-KT FOR S 20
'
l__
RECORD: TIME START
CR,,Vt3+> ,
KI_^T__( + >
NOTE:
'
(1 ) IF CR-, KI-, ADD 20*. `-AS IS*- INCREMENTS
HYDROCHLORIC ACID
ASSUME 32%
RECORD: CR< + ) i `KI< + >
(2) IF CR+, KI-, ADD 20* *AS IS" INCREMENTSl
SODIUM NITRITE
ASSUME 33%
RECORD: CR_____< + ) KI.
.< + )
RUN 10- <970 G) WATER INTO V /&> 6
|
INSTALL TEMP CHART
-i- ' 1 /
DUR IN SODIUM HYDROXIDE M_IZL__^,T3i.SIX I Zf^inSL
ADJ TO 40" <3880 G) AT 66-70 DEG F .
1.3X330
LOSE STACK DAMPER
"
| ' *'
STIR FOR S 22
'I
28-D 725-A
7-D 57-A
ACCT LBS
10
569
WHEN S 14 STIR COMPLETE, TEST- DV & RECORD I
CR__4^r_( + >, KI 4~ ( + ) TEMP:_SjL_<28-32 F) i:______
NOTE:
'-
'
'
(1) IF CR-, KI-, ADD 20* 'AS IS' INCREMENTS
HYDROCHLORIC ACID
ASSUME 32%
RECORD: CR_____< + ) , KI____i<+)
<2) IF CR+, KI--, ADD 20* AS IS* INCREMENTS
SODIUM NITRITE-
ASSUME-33% '
RECORD : CR_'<+)
, KI____ ._<+X
TURN ON \~SlSl AGITATOR* CHOP & ADD ICE
N TURN OFF AGITATOR*
1^X330
PJJW'-'SV THRU CLARIF' PRESS INTO DV
MAINTAINING' TEMP AT 28-32 DEG- F
, .<
RECORD:' 'TIME_STARTTOTAL MIN.jyjL.
DUMP ACETOACET ORTHO ANISIDIDE INTO CV
FROM S2
.LOT
*100%
%
. x //%&- --Mgzl _
_____
57-A 28-D 725-A 57-A
46-C
~1547^ ' -^-^1
;
k23Q^STSR, 10 MIN TO DISSOLVE
OPEN STACK DAMPER
" '
w*-..-. 4
.....
RUN-IN ACETIC ACID UNDERSURFACE; IN^^g -
nriR 5
& r e c o r d : PH.^S3I<sla~6.3>" * 1
IF NECESSfAfeY, ADJ TO PH 5*8-6*3 &'RECORD.;. I
PH--------- <5.8-6.35 SODIUM HYDROXIDE ASSUME50%I.
ACETIC ACID v ASSUME70%I.
7-D 30--D
87T *
DUP050463751
L*'U1P WENT
...
~ DATE PRINTED: i/I2/82
MAKING INSTRUCTIONS:BATCH UNIT
OF 3 CG 46
YT-820
-CODE 1-ACCT I LBS
WHEN S 21 CLARIF COMPLETE, WASH DV <S 4). I LINES, PUMP & PRESS FOR 20 MIN OR ~TCkA -CR J TEST ON A SAMPLE OF TOTAL*PRESS EFFLUENT,1 WHICHEVER COMES FIRSI* COLLECT WASHINGS
DV <S 215 STIR 5 MIN 6 RECORD: TEMPjg.,,(28r-32*F5 & IF NECESSARY, ADJ TO 2B-32*F*. RECORDj;_____ *FI
___________ __ ...
_ MIN & RECORD: IF NECESSARY, ADJ TO fKI
mmSimmm
D RECORD KX~_X--<HH>
RECORD: VOL
'
MISC ?
CV
TO
1
T. yt"-; *v
i34 I WEIGH SODIUM HYDROXIDE IN DRUMS FOR S41 '
!i
135 I DISSOLVE IGEPAL CO-630 IN 2 GAL WATER IN
| 1 DRUMS FOR S43.
i!
I *T I ^'
7-d I 337 979-D
h&ri WHEN S 33 COMPLETE, ADJ
" -"130-84 "DEG F .
VL
TO 43* 14197 G5 |
I
CHECK ACCURACY: HT_JLj___ DE
RECORDER
DEG F
.: I
IMMEDIATELY RUN IN DV TH DISTRIBUTOR IN 60-65 MIN
NDERSURFACE MAINTAIN CV
I
AT 8-84*F.
'
h
RECORD: TIME START_,,_jJfy' TOTAL MIHj?L
STIR 10 MIN, DISCONNECT.TRANSFER LINE AT
IMMEDIATELY
'.
' -.
. RECORD^ DIAZO__rrL_L<^)^ASE^_il__^{+) ,
I PH_ifl_<4*3-4175 NOTE: <i> IF DIAZO +,
{ BASE -, & PH BELOW 4.3:> '-: - - .
<A5 ADJ TO PH 4*3-4*7 SODUIM HYDROXIDE
I-'--'--*
" ' ASSUME 50X1 _______
I <B.) RECORD:
-- 1 ,
I <21 IF DIAZO +,BASE - & PH ABOVE 4*3 ADD 8*[
I 100% N-7-D SODIUM HYDROXIDE ASSUME 50%|
I TO A 55G DRUM* ADJ WITH WATER TO +/-25GI
I ADD 20S 100% N-46-C.AND STIR TO
i_______
DISSOLVE, POUR IN CV AND STIR 10 MIN. I
<3) REPEAT ABOVE AS NECESSARY TO - DIAZO, ]
+ BASE .
_
I
POUR IN N-7-D SODIUM HYDROXIDE FROM S34 & I
I L-STXR 5 MIN^ r
.
I
L4Sf| II
RECORD PH_^1<7.1-9.0) & IF NECESSARY ADJ1 I PH 7.* 1--9.0 ^ ^SODIUM HYDROXIDE ASSUME 50%|.
l
4
I J-^RECORD : PH_L,, -HYDROCHLORIC ACID ASSUME 32%t,,
IN N-979-D FROM $35
1
TO 200-204 DEG F/lN 58-62 MIN
_ STIR 30 MIN AT 200~2f4j KEG^F
i URECBRD: TIME START W VO. .__
I-4t5rT FLOOD TO 94* <9174 G). AND STOP AGITATOR
I I I
'"I
.
7-D -T_,2_ 7-D 46-C
7-D 28-D -
II
START
FIN
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DUP050463752
N32606.01
DUP050463753