Document oEypqZRD4J00bewEK31JZ5m8

CG 59 CODE YT-714-D PKG____ SEP 2 4 1902 ,,o? a : 7~DATi >" 7L0T"NUHBiR)~ cZtlS EST. WT * 2gum* LBS. ,PREPARATION NOTES : PROCESSES, -APPROVED BY: <- )YT-714-D (G) EWK 12/23/81 .... .. j .:/ . COMTYP JOB. NAME: 50YT714DHG- STANDARD HRS* TIME _______ ;M ' NAME; GREEN GOLD I OBTAIN FOR S4 2,4-DIHYDROXY QUINOLINE 2 i OBTAIN FOR S9 P-CHLOROANILINE NON-BLEEDING- USE LBS N-CODE ACCT LBS 44-C | 613-HC- }' RUN 39* < 2037G) WATER INTO V-283 & HEAT TO 85-90 DEG F I | DUMP & RINSE IN FROM SI LOT ! 2,4-DIHYDROXY - ^L6Lt&- QUINCLINE W. Wfl\ _........ .......... _/_5l ZL2__ 44-C 1078 -- - DV 3 --j. sv 4 JST I ^AITJ TO 54* (2836G) AT-85-90 DEG F I &SY DUMP IN & STIR TO SOL`N FOR SI 2 SODIUM ! | CARBONATE - . i 369 1 11 SON 17* (595G) WATER iI-NTO^V-j2A5_._ - ! RUN IN FROM V-324 HYDROCHLORIC ACID I ; . j jrf HEAT TO 68-72 F & DUMP IN FRM S2 X. LOT, I l NOTE: THE RESOURCE CONSERVATION ( | RECOVERY BILL HAS CLASSIFIED PARA-___________ I, i | CHLORANILINE . <N-613-0 A HAZARDOUS____1. I | WASTE MATERIAL* THIS REQUIRES EMPTY N613C | l j CONTAINERS TO BE GIVEN 3 WATER RINSES WITH | | I 135f-145F WATER FROM HOT WATER MIXER INTO } { | DV BEFORE DISPOSING* NOTE <2) N-613C IS - | I ^EXTREMELY TOXIC DESTROY DRUMS PER STD PRAC ! \J>A STIR 30 MIN OR^LONGER TO DISSOLVE FOR SI 3 I RECORD: STARTl^l^Z^f' I 3-A I I I I 28-D 613-C 369.... 560 796 RUN'5* <4890 WATER .INTO V- & INSTALL 1 MP CHART I WHEN S6 STIR COMPLTE, RUN IN DV THRU SCREEN| MAKING INSTRUCTIONS:BATCH UNIT EQUIP MENT PAGE 2 OF 3 V CG 50 CODE YT-714-D (G> II^Hw HEN S10 STIR COMPLETE* ADJ TO 61 C2100G) I USE 1 LBS I i 16X330 J N-CODE I ACCT-1,LBS ' 57-A ]/ $&. V j --AT 56-60 DEG F* ICE I............. I IJA^i SIPHON IN IN 10-12 MIN * SODIUM - NITRATE^ J. '! -..jxr . '- M ....cj _35.*6Lr ZMj.fl..I t i-rS^STIR 5 MIN & RECORD: KI^___^ :MUST-BE. + Li^T | STIR 30-45 MIN At 60-72 DEG F MAINTAINING -1. L | +CR* +KI; FOR S20 - RECORD: TlMEiSTARf^Qi^^M : - -| r : T.CR - ^ (+) . KIl _^___(+) ; . f I NOTE : (.1 ) IF CR-KI-, ADD 204- 'AS- IS* ....... I- ' - I L I INCREMENTS HYDROCHLORIC. AOID.- ASSUME 32JL: -1 __1 ! f RECORD: CR______;_< + > KI_____ _____ ( + > I - I- \ i <2> IF CR+KI- ADD 204 * AS IS* INCREMENTS \ *#- \ I I SODIUM NITRITE ASSUME 33%' - i________! I RECORD: CR;______ (+> KI__________(+> }. : - ; I - I -,. | . .r 725-A T~~437^. -725-A I 57-A- I - ^ , 1. ' -28-D: i ^ - - }^ . 725-A 1 v .. 283 6 T RUN 15.' ( 7600 WATER INTO V-2S3 AND : HEAT - .p-^- _ |--... - L f J?''Tb'66-"80 DEG F ,-v;- .. , : :J |' -| .Ti " IN 6 STIR TO DISSOLVE NICKEL' SULFATE- - I - i^939 --J - 707-B^L -939:; . Ij^O-SIPHON IN IN 10-12 MIN -& STIR FOR S30- - = - } v-:.5l0 |,.. ;~-122-B?-.L^.5i0sfe4 I -[ AMMONIUM HYDROXIDE .-.v... r...; } L.>.... w- | r DV \$f \ WHEN Si 6 STIR COMPLETE, TEST :BV:icRECORDI --L-: : 7i ...... t-*TLcNOTE: (1> IF CR-, KI- ADD 204 -"AS-IS^ -- L -V ;v,. -plL^r^INCREMENTS HYDROCHLORIC ACID ASSUME^325C-r.:..: fL.LLi.LL I -2S-A- t -.asTM ^tf^fcSRECORD:- CR__ v | - r (2) IF. CR+, KI--ADD 204 *AS IS*. INCREMENTS- \ I ; 1' - f. - SODIUM NITRITE - - - - , ASSUME - 33%-- -I { --725-A ^ - I -^RECORD : CR_. ,< + >- KI^L*.- ( + > ~ > ...|... ...... . ... | - 124^1 SETTLE -15-30 MIN FOR S24 6 -RECORD- --- --I-..............: . -I< I .^M^__',DV, START^iSC^-- * !_------ -- ! i 122 f SLURRY WITH +/- 30 GALLONS WATER IN DRUM | - 113 1 892-D | I I FOR S32 SURFACTANT G3300- ^ .} - - \ - --* ADJ V TO 78-82 DEG F 39* (3787G) 6-RECORD |2X330 J > DEG F ~ St REC 0/ DEG F I WHEN S21 SETTLING COMPLETE, COUPLE-DV v I ~ - - UNDERSURfACE IN 60-7 MIN RECORD:- . . ... . ^RT /lOiQSfy- TOTAL MIN -(*$0' - L Ar--'- I. AIN IN DV 5 MIN & WASH-IN LINE ONLY - -! WHEN S24 COMPLETE, STIR 30 MIN 6 DISCONNECT - I. RANSFER LINE AT CV IMMEDIATELY- ,- - RECORD: DIAZO_JrC__< --> , BASE-.^fl^H-) , . i- t-;-- I- PH,,^_ (8 * 0--9.0) . - J.-/' vtrfVi- *. NOTE: (1 ) IF DIAZO +,. BASE & PH'-'BELOW 8.0 . ..... j -.i-'L (AT ADJ TO PH -8*0-9*0. SODIUM*CARBONATE (B) RECORD PH,,___ _L_. T . ( 2 ) -1F DIAZO HiBASE^c^T &- P^ STO'-- OR. ABOVE (A) ADD 104 i100Z N-44-C: 2,4-DIHYDROXY?' > ......(. i- .QUINOLINE : - 'T-.; Vi CB> ADJ -WITH WATER:?TO -+/-- 25G <--L (Cl STIR' TO' DISSOLVE t L"-' (D) POUR INTO CV -: -j` w -: V ~-S- I ----~ <E) STIR 10 MIN ' . ... ..s I .., (3) REPEAT (1) 6 (2> ABOVE AS NECESSARY-TO ' - DIAZO, 4. BASE - ' v- 57-A - - 1 - -~-i Tt3-::' ' V. DUP050103912 Ae g s u s p . ` NEN cv r CONT MAKING INSTRUCTIONS:BATCH UNIT- . PAGE 3 OF 3 CG 50 CODE YT-714-D <G> -1 LBS ,,*_AT TO DEG F IN .14-18 MIN , .} STIR -20-25 MIN AT 04H3<EDEG F* DURING ! TIR - WASH DV TO SEWER* -r^y I RUN IN-V283 IN ,28-25 - .MIN MAINTAIN l&f'rjOJB] IR 5 MIN:-^ RECORD :-PH_Fk|L<7*8-8i8. .. I DUMP IN -N--892-B -SLURRY FROM -S22 L- } STIR 9< DEG F RECORD: f STARTs 'FLOOD TO "TOP AGITATOR' 1 TAKE 1 QT SAMPLE - |. S35 V-100 V-105 V--1 06 V-182 | 81 ` '94* 94' 84 * | GAL* (805OG) <9174G) <9174G) <8300G)1 I START W) FIN,, OPTR *} : I I '. 1 SUPERVISOR NOTE: /- ..........> ......................... I f <1> IF DIAZO + AFTER INITIAL COUPLING <S27> | i ADVISE PROCESSING TO: . | |<A> LOAD IN DRUMS @ 3254 NET AS PRESSCAKE I | DO NOT DRY* TAKE 1 GJT. SAMPLE I KB) HIGH PRESSURE HOSE PRESS AND BOX AFTER | i DROPPING BEFORE FILLING NEXT BATCH I I SUPVR:__ ;______ _____ _ DATE:________________ ' i-~- v.v - :\ -LBS-.....X 1 !- - i- ! -I -I 1-v I - DUP050103913 DUP050103914 DUP050103915